CN108284699A - The PVD silk-screens pierced process and a kind of glass panel product of a kind of glass panel - Google Patents
The PVD silk-screens pierced process and a kind of glass panel product of a kind of glass panel Download PDFInfo
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- CN108284699A CN108284699A CN201710014989.5A CN201710014989A CN108284699A CN 108284699 A CN108284699 A CN 108284699A CN 201710014989 A CN201710014989 A CN 201710014989A CN 108284699 A CN108284699 A CN 108284699A
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- silk
- screen
- pvd
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- glass panel
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B44—DECORATIVE ARTS
- B44C—PRODUCING DECORATIVE EFFECTS; MOSAICS; TARSIA WORK; PAPERHANGING
- B44C5/00—Processes for producing special ornamental bodies
- B44C5/04—Ornamental plaques, e.g. decorative panels, decorative veneers
- B44C5/0407—Ornamental plaques, e.g. decorative panels, decorative veneers containing glass elements
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B44—DECORATIVE ARTS
- B44C—PRODUCING DECORATIVE EFFECTS; MOSAICS; TARSIA WORK; PAPERHANGING
- B44C5/00—Processes for producing special ornamental bodies
- B44C5/04—Ornamental plaques, e.g. decorative panels, decorative veneers
- B44C5/0446—Ornamental plaques, e.g. decorative panels, decorative veneers bearing graphical information
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- Application Of Or Painting With Fluid Materials (AREA)
Abstract
The present invention provides a kind of PVD silk-screen pierced process of glass panel, the step of technique includes carrying out halftone silk-screen to glass panel using protection oil, and PVD, subsequent strip protection oil are carried out after drying, and cleaning obtains finished product.The present invention also provides the glass panel products for using the technique to prepare.
Description
Technical field
The present invention relates to Material Fields, in particular to a kind of PVD silk-screen pierced process of glass panel.
Background technology
With the development of science and technology, the requirement of client and consumer to product is higher and higher, adds in glass panel Logo
Mostly it is that ink for screen printing, the mode of last strip, the core of this conventional method are to move back again using elder generation PVD in the conventional method of work
PVD layer is plated, but PVD layer, because of color requirement difference, corresponding membrane system (target) is also different, corresponding strip mode, strip material
Also different, and ink layer is unable to strip, admittedly leaving ink station component level, influences bonding process below, complex process, operating difficulties.
It is then strip protection ink that the present invention, which uses Logo hollow out screen printing methods, core, and no matter how PVD membrane systems (target) change, all
It can be can be realized using unified strip method, compare traditional handicraft, withdrawal plating is simple, uniformly, and effective solution passes
System technique PVD Logo lead to difficult strip, complex process and ink station component level problem because of different membrane systems (target).
In view of this, special propose the present invention.
Invention content
The first object of the present invention is to provide a kind of PVD silk-screen pierced process of glass panel, the technique use guarantor
Shield oil first carries out halftone silk-screen to glass panel, then PVD is carried out on protection oil again, therefore, during strip, it is only necessary to
Oil reservoir strip will be protected, you can take away the PVD materials on oil reservoir surface, and retain the PVD materials for being deposited directly to glass surface.
The second object of the present invention is to provide a kind of glass panel product prepared using the technique, the panel production
Product have beautiful hollow out logo.
In order to realize that the above-mentioned purpose of the present invention, spy use following technical scheme：
The step of one aspect of the present invention is related to a kind of PVD silk-screen pierced process of glass panel, the technique include,
Halftone silk-screen is carried out to glass panel using protection oil, PVD, subsequent strip protection oil are carried out after drying, cleaning obtains finished product.
The method of the present invention changes elder generation PVD ink for screen printing again in the prior art, the process of last strip, but elder generation is in face
Oil is protected on plate surface silk-screen, then carries out PVD deposition, so that PVD material parts are deposited on protection oil reservoir, in strip
When, it is only necessary to by oil reservoir strip, you can take away the PVD materials on oil reservoir, and retain the PVD materials being deposited directly on glass material
Material, to achieve the effect that silk-screen hollow out logo.
For the method for the present invention due to being to carry out strip for ink, withdrawal plating is more simple compared with the existing technology, unites
One, and can solve the problems, such as ink station component level in the prior art.
Preferably, the material for the PVD includes in titanium, copper, graphite, molybdenum, niobium oxide, silver, aluminium and alloy target material
It is one or more.
The material of PVD sprayings can carry out different selections according to the requirement of product.
Preferably, the PVD thicknesses of layers is 80-100nm.
Preferably, the protection oil is crude oil.
Preferably, it is measured with No. 7 20 turns of rotors, the viscosity of the protection oil is 30000-40000cps.
Preferably, the halftone mesh number that the halftone silk-screen uses is 180T~200T, preferably 200T.
Preferably, it is 5-7 μm that the thickness of oil is protected after the halftone silk-screen, it is preferable that the silk-screen speed of the halftone silk-screen
Degree is 250-350mm/s, and scraper angle is 60-75 °, and halftone height is 2-3mm, wherein the scraper angle is point value or model
It encloses.
Preferably, the temperature of the drying is 130-150 DEG C, it is preferable that the time of drying is 10-12min.
Preferably, the strip temperature is 60-80 DEG C, and the strip time is 2-3min.
Another aspect of the present invention relates to the glass panel products for using the technique to prepare.
Compared with prior art, beneficial effects of the present invention are：
(1) the PVD silk-screen pierced process of glass panel of the invention first carries out halftone silk using protection oil to glass panel
Print then carries out PVD, therefore, during strip on protection oil again, it is only necessary to will protect oil reservoir strip, you can band goes rancid
The PVD materials of layer surface, and retain the PVD materials for being deposited directly to glass surface；
(2) technique of the invention is no longer needed for the different strip method of different PVD material selections, but unified to oil
Layer carries out strip, and withdrawal plating is simply unified, and can improve the defect of ink station component level in traditional handicraft；
(3) technical maturity of the invention, the glass product that the method according to the invention obtains, the primary qualification of ink layer
The first-time qualification rate of rate and PVD film layers is high, yield height of product after the completion of strip.
Description of the drawings
In order to more clearly explain the embodiment of the invention or the technical proposal in the existing technology, to embodiment or will show below
There is attached drawing needed in technology description to be briefly described.
Fig. 1 is to coat the sectional view of protection oil reservoir on glass panel surface.
Fig. 2 is after having coated protection oil reservoir, further to carry out the sectional view of PVD.
Fig. 3 is the glass panel sectional view after strip oil reservoir.
Reference numeral
1- glass panels 2- protects 3-PVD layers of oil reservoir
Specific implementation mode
Embodiment of the present invention is described in detail below in conjunction with embodiment, but those skilled in the art will
Understand, the following example is merely to illustrate the present invention, and is not construed as limiting the scope of the invention.It is not specified in embodiment specific
Condition person carries out according to conventional conditions or manufacturer's recommended conditions.Reagents or instruments used without specified manufacturer is
The conventional products that can be obtained by commercially available purchase.
Embodiment 1
A kind of silk-screen pierced process of glass panel PVD Logo, includes the following steps：The first step, ink pour into halftone
In；Glass product is placed in silk-screen pedestal by second step；Third walks：Silk-screen is carried out to product according to the silk-screen parameter set
Hollow out Logo；4th step：The product of the good hollow out Logo of silk-screen is put into oven and is dried；5th step：The product of drying is carried out
Cleaning；6th step：The product cleaned up is subjected to PVD Logo；7th step：The product for completing PVD Logo is subjected to strip
Protection oil；8th step：Process is processed after the product that strip is completed is cleaned up and dries progress.
Further, during the ink formulation in the first step, the can opening viscosity of crude oil is that (No. 7 turn 30000cps
20 turns of son), viscosity of reaching the standard grade is 30000cps (No. 7 20 turns of rotors)；Ink is a kind of ink for screen printing that product is specified, and model is
WE-4500L, allotment ratio are the direct silk-screen of crude oil；Halftone is the indispensable part of silk-screen, the Logo sizes of halftone be by
According to the 1 of product Logo sizes：For 1 ratio come what is designed, mesh is 180T~200T, preferably 200T (500 mesh) steel wire halftone；
Further, during being packed into silk-screen pedestal, this silk-screen pedestal is used for placing production glass product in the second step
Product, play the role of fixed product, and specific size is：The appearance and size of pedestal cavity and glass product is according to 1:1 ratio
Example designs.
Further, for the third step during silk screen product hollow out Logo, silk-screen software is that screen printer is included
Software；Screen printer model is eastern remote CCD high-precision screen printer MATAGW-25PP, and silk-screen speed is 250mm/s；Scraper angle is
75°；Halftone height is 2mm；Ink thickness is 5um.
Further, for the 4th step in product baking process, oven is hot air circulation type tunnel oven, baking
Parameter is 140 DEG C, and baking time is 10min.
Further, the 5th step is in product cleaning process, and cleaning machine is 12 slot cleaning machines, wherein the first slot and the
Two slots are separately added into 001 alkaline cleaner of 1L and 2L capacity；Three, six, eight slots are pure water cleaning showers, time 30s；Four,
Five, seven, nine, ten, 11 slots are pure water ultrasonic cleaning, and ultrasonic frequency is 28KHZ, and electric current is 1.5A, and temperature is 60 DEG C, when
Between be 70s；12 slots are slow kerve, and temperature is 70 DEG C, and the time is 5s；Board is finally Drying tunnel, and temperature is 90 DEG C, drying
Time is 4min.
Further, during the 6th step product PVD Logo, the model of coating machine is friendly prestige continuous film plating machine,
Target is Al/Ti, and PVD thicknesses of layers is 80nm.
Further, during the 7th step product strip, the model of decoating liquid is 311L-2, and strip temperature is 70
DEG C, the strip time is 2min.
Further, after the completion of the 8th step strip cleaning, drying parameter with reference to above-mentioned 5th step.
Embodiment 2
A kind of silk-screen pierced process of glass panel PVD Logo, includes the following steps：The first step, ink pour into halftone
In；Glass product is placed in silk-screen pedestal by second step；Third walks：Silk-screen is carried out to product according to the silk-screen parameter set
Hollow out Logo；4th step：The product of the good hollow out Logo of silk-screen is put into oven and is dried；5th step：The product of drying is carried out
Cleaning；6th step：The product cleaned up is subjected to PVD Logo；7th step：The product for completing PVD Logo is subjected to strip
Protection oil；8th step：Process is processed after the product that strip is completed is cleaned up and dries progress.
Further, during the ink formulation in the first step, the can opening viscosity of crude oil is that (No. 7 turn 40000cps
20 turns of son), viscosity of reaching the standard grade is 40000cps (No. 7 20 turns of rotors)；Ink is a kind of ink for screen printing that product is specified, and model is
WE-4500L, allotment ratio are the direct silk-screen of crude oil；Halftone is the indispensable part of silk-screen, the Logo sizes of halftone be by
According to the 1 of product Logo sizes：For 1 ratio come what is designed, mesh is 180T~200T, preferably 200T (500 mesh) steel wire halftone；
Further, during being packed into silk-screen pedestal, this silk-screen pedestal is used for placing production glass product in the second step
Product, play the role of fixed product, and specific size is：The appearance and size of pedestal cavity and glass product is according to 1:1 ratio
Example designs.
Further, for the third step during silk screen product hollow out Logo, silk-screen software is that screen printer is included
Software；Screen printer model is eastern remote CCD high-precision screen printer MATAGW-25PP, and silk-screen speed is 350mm/s；Scraper angle is
60°；Halftone height is 2mm；Ink thickness is 7um.
Further, for the 4th step in product baking process, oven is hot air circulation type tunnel oven, baking
Parameter is 130 DEG C, and baking time is 10min.
Further, the 5th step is in product cleaning process, and cleaning machine is 12 slot cleaning machines, wherein the first slot and the
Two slots are separately added into 001 alkaline cleaner of 1L and 2L capacity；Three, six, eight slots are pure water cleaning showers, time 30S；Four,
Five, seven, nine, ten, 11 slots are pure water ultrasonic cleaning, and ultrasonic frequency is 28KHZ, and electric current is 1.5A, and temperature is 60~65
DEG C, the time is 70S；12 slots are slow kerve, and temperature is 70 DEG C, and the time is 5S；Board is finally Drying tunnel, temperature 100
DEG C, drying time 3min.
Further, during the 6th step product PVD Logo, the model of coating machine is friendly prestige continuous film plating machine,
Target is TI/NB/TI, and PVD thicknesses of layers is 100nm.
Further, during the 7th step product strip, the model of decoating liquid is 311L-2, and strip temperature is 60
DEG C, the strip time is 3min.
Further, after the completion of the 8th step strip cleaning, drying parameter with reference to above-mentioned 5th step.
Embodiment 3
A kind of silk-screen pierced process of glass panel PVD Logo, includes the following steps：The first step, ink pour into halftone
In；Glass product is placed in silk-screen pedestal by second step；Third walks：Silk-screen is carried out to product according to the silk-screen parameter set
Hollow out Logo；4th step：The product of the good hollow out Logo of silk-screen is put into oven and is dried；5th step：The product of drying is carried out
Cleaning；6th step：The product cleaned up is subjected to PVD Logo；7th step：The product for completing PVD Logo is subjected to strip
Protection oil；8th step：Process is processed after the product that strip is completed is cleaned up and dries progress.
Further, during the ink formulation in the first step, the can opening viscosity of crude oil is that (No. 7 turn 35000cps
20 turns of son), viscosity of reaching the standard grade is 35000cps (No. 7 20 turns of rotors)；Ink is a kind of ink for screen printing that product is specified, and model is
WE-4500L, allotment ratio are the direct silk-screen of crude oil；Halftone is the indispensable part of silk-screen, the Logo sizes of halftone be by
According to the 1 of product Logo sizes：For 1 ratio come what is designed, mesh is 180T~200T, preferably 200T (500 mesh) steel wire halftone；
Further, during being packed into silk-screen pedestal, this silk-screen pedestal is used for placing production glass product in the second step
Product, play the role of fixed product, and specific size is：The appearance and size of pedestal cavity and glass product is according to 1:1 ratio
Example designs.
Further, for the third step during silk screen product hollow out Logo, silk-screen software is that screen printer is included
Software；Screen printer model is eastern remote CCD high-precision screen printer MATAGW-25PP, and silk-screen speed is 300mm/S；Scraper angle is
75°；Halftone height is 3mm；Ink thickness is 7um.
Further, for the 4th step in product baking process, oven is hot air circulation type tunnel oven, baking
Parameter is 150 DEG C, and baking time is 10min.
Further, the 5th step is in product cleaning process, and cleaning machine is 12 slot cleaning machines, wherein the first slot and the
Two slots are separately added into 001 alkaline cleaner of 1L and 2L capacity；Three, six, eight slots are pure water cleaning showers, time 30S；Four,
Five, seven, nine, ten, 11 slots are pure water ultrasonic cleaning, and ultrasonic frequency is 28KHZ, and electric current is 1.5A, and temperature is 65 DEG C, when
Between be 70S；12 slots are slow kerve, and temperature is 70 DEG C, and the time is 5S；Board is finally Drying tunnel, and temperature is 100 DEG C, is dried
The dry time is 3min.
Further, during the 6th step product PVD Logo, the model of coating machine is friendly prestige continuous film plating machine,
Target is TI/AG/AL-MG/TI, and PVD thicknesses of layers is 100nm.
Further, during the 7th step product strip, the model of decoating liquid is 311L-2, and strip temperature is 80
DEG C, the strip time is 2min.
Further, after the completion of the 8th step strip cleaning, drying parameter with reference to above-mentioned 5th step.
Embodiment 4
A kind of silk-screen pierced process of glass panel PVD Logo, includes the following steps：The first step, ink pour into halftone
In；Glass product is placed in silk-screen pedestal by second step；Third walks：Silk-screen is carried out to product according to the silk-screen parameter set
Hollow out Logo；4th step：The product of the good hollow out Logo of silk-screen is put into oven and is dried；5th step：The product of drying is carried out
Cleaning；6th step：The product cleaned up is subjected to PVD Logo；7th step：The product for completing PVD Logo is subjected to strip
Protection oil；8th step：Process is processed after the product that strip is completed is cleaned up and dries progress.
Further, during the ink formulation in the first step, the can opening viscosity of crude oil is that (No. 7 turn 35000cps
20 turns of son), viscosity of reaching the standard grade is 35000cps (No. 7 20 turns of rotors)；Ink is a kind of ink for screen printing that product is specified, and model is
WE-4500L, allotment ratio are the direct silk-screen of crude oil；Halftone is the indispensable part of silk-screen, the Logo sizes of halftone be by
According to the 1 of product Logo sizes：For 1 ratio come what is designed, mesh is 180T~200T, preferably 200T (500 mesh) steel wire halftone；
Further, during being packed into silk-screen pedestal, this silk-screen pedestal is used for placing production glass product in the second step
Product, play the role of fixed product, and specific size is：The appearance and size of pedestal cavity and glass product is according to 1:1 ratio
Example designs.
Further, for the third step during silk screen product hollow out Logo, silk-screen software is that screen printer is included
Software；Screen printer model is eastern remote CCD high-precision screen printer MATAGW-25PP, and silk-screen speed is 300mm/S；Scraper angle is
75°；Halftone height is 2.5mm；Ink thickness is 6um.
Further, for the 4th step in product baking process, oven is hot air circulation type tunnel oven, baking
Parameter is 140 DEG C, and baking time is 11min.
Further, the 5th step is in product cleaning process, and cleaning machine is 12 slot cleaning machines, wherein the first slot and the
Two slots are separately added into 001 alkaline cleaner of 1L and 2L capacity；Three, six, eight slots are pure water cleaning showers, time 30s；Four,
Five, seven, nine, ten, 11 slots are pure water ultrasonic cleaning, and ultrasonic frequency is 28KHZ, and electric current is 1.5A, and temperature is 60 DEG C, when
Between be 70s；12 slots are slow kerve, and temperature is 70 DEG C, and the time is 5s；Board is finally Drying tunnel, and temperature is 100 DEG C, is dried
The dry time is 3min.
Further, during the 6th step product PVD Logo, the model of coating machine is friendly prestige continuous film plating machine,
Target is ALAG alloy membrane systems, and PVD thicknesses of layers is 100nm.
Further, during the 7th step product strip, the model of decoating liquid is 311L-2, and strip temperature is 80
DEG C, the strip time is 2min.
Further, after the completion of the 8th step strip cleaning, drying parameter with reference to above-mentioned 5th step.
Experimental example
Quality inspection is carried out to product among the technique in embodiment 1-4 and finished product, standard is as follows
1, criterion of acceptability of ink layer：Ink thickness (standard：+ 2.5, -0), sand holes (standard：No sand holes), tooth lack
(0.02mm)
2, criterion of acceptability of PVD layer：White point (0.01mm2≤ 5pcs), dirty (≤0.02mm2), scratch (≤0.02mm)
3, non-defective unit standard of the finished product after the completion of strip：White point (0.01mm2≤ 5pcs), dirty (≤0.02mm2), draw
Hinder (≤0.02mm)
The results are shown in table below：
| Group/project | Ink layer first-time qualification rate | PVD layer first-time qualification rate | Yield of finished product |
| Embodiment 1 | 93% | 96% | 92% |
| Embodiment 2 | 92% | 96% | 92% |
| Embodiment 3 | 94% | 97% | 94% |
| Embodiment 4 | 94% | 99% | 95% |
Ink layer first-time qualification rate is 95% or more, and the thick thin dimensional tolerance of glass product ink film is 0.002mm,
The first-time qualification rate of PVD film layers is 99% or more, and glass product PVD film layer thickness dimensional tolerances are 5nm, after the completion of strip
Yield of Logo 90% or more.
Although illustrate and describing the present invention with specific embodiment, it will be appreciated that without departing substantially from the present invention's
Many other change and modification can be made in the case of spirit and scope.It is, therefore, intended that in the following claims
Including belonging to all such changes and modifications in the scope of the invention.
Claims (10)
1. a kind of PVD silk-screen pierced process of glass panel, which is characterized in that the step of technique includes using protection oil
Halftone silk-screen is carried out to glass panel, PVD, subsequent strip protection oil are carried out after drying, cleaning obtains finished product.
2. technique according to claim 1, which is characterized in that the material for the PVD include titanium, copper, graphite, molybdenum,
It is one or more in niobium oxide, silver, aluminium and alloy target material.
3. technique according to claim 1, which is characterized in that the PVD thicknesses of layers is 80-100nm.
4. technique according to claim 1, which is characterized in that the protection oil is crude oil.
5. technique according to claim 4, which is characterized in that measured with No. 7 20 turns of rotors, the viscosity of the protection oil is
30000-40000cps。
6. technique according to claim 1, which is characterized in that the halftone mesh number that the halftone silk-screen uses be 180T~
200T, preferably 200T.
7. technique according to claim 1, which is characterized in that it is 5-7 μm to protect the thickness of oil after the halftone silk-screen, excellent
The silk-screen speed of selection of land, the halftone silk-screen is 250-350mm/s, and scraper angle is 60-75 °, and halftone height is 2-3mm,
Described in scraper angle be a value or range.
8. technique according to claim 1, which is characterized in that the temperature of the drying is 130-150 DEG C, it is preferable that is dried
The dry time is 10-12min.
9. technique according to claim 1, which is characterized in that the strip temperature is 60-80 DEG C, and the strip time is 2-
3min。
10. the glass panel product prepared using any one of the claim 1-9 techniques.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710014989.5A CN108284699B (en) | 2017-01-09 | 2017-01-09 | A kind of the PVD silk-screen pierced process and a kind of glass panel product of glass panel |
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| CN201710014989.5A CN108284699B (en) | 2017-01-09 | 2017-01-09 | A kind of the PVD silk-screen pierced process and a kind of glass panel product of glass panel |
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| CN108284699B CN108284699B (en) | 2019-12-03 |
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| CN110156342A (en) * | 2019-04-24 | 2019-08-23 | 北海市龙浩光电科技有限公司 | A kind of glass panel dizzy coating local transparent empty avoiding production method against sunshine |
| CN110304838A (en) * | 2019-07-17 | 2019-10-08 | 北海市龙浩光电科技有限公司 | A kind of large scale cambered surface dizzy, anti-fingerprint glass cover-plate preparation method against sunshine |
| CN110550127A (en) * | 2019-08-30 | 2019-12-10 | 福耀玻璃(苏州)有限公司 | Hollow line design method of automobile glass screen printing plate |
| CN114672317A (en) * | 2022-04-06 | 2022-06-28 | 长沙永安新材料有限公司 | PVD (physical vapor deposition) coating stripping liquid and process for sapphire |
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| Publication number | Publication date |
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| CN108284699B (en) | 2019-12-03 |
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