CN108254401A - A kind of rock NMR instrument sample carries bed and its application method - Google Patents

A kind of rock NMR instrument sample carries bed and its application method Download PDF

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Publication number
CN108254401A
CN108254401A CN201810036971.XA CN201810036971A CN108254401A CN 108254401 A CN108254401 A CN 108254401A CN 201810036971 A CN201810036971 A CN 201810036971A CN 108254401 A CN108254401 A CN 108254401A
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China
Prior art keywords
arc groove
strip arc
rock
bed
nmr instrument
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CN201810036971.XA
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Chinese (zh)
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CN108254401B (en
Inventor
李杰林
周科平
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Central South University
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Central South University
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N24/00Investigating or analyzing materials by the use of nuclear magnetic resonance, electron paramagnetic resonance or other spin effects
    • G01N24/08Investigating or analyzing materials by the use of nuclear magnetic resonance, electron paramagnetic resonance or other spin effects by using nuclear magnetic resonance
    • G01N24/081Making measurements of geologic samples, e.g. measurements of moisture, pH, porosity, permeability, tortuosity or viscosity

Abstract

The invention discloses a kind of rock NMR instrument samples to carry bed, including carrying bed ontology, the load bed ontology is equipped with strip arc groove, it is identified with scale and scale number in the strip arc groove at one side edge in an axial direction, it is equipped in the graduated side of mark in the strip arc groove and can slide item in axial sliding along strip arc groove, the sliding bottom end face extends to strip arc groove bottom center, and overlapped with the vertical plane where strip arc groove bottom centerline, diameter spirit bubble is equipped at strip arc groove one end bottom center.The invention also discloses a kind of application methods for the rock NMR instrument that bed is carried comprising the sample.The present invention is especially suitable for test analysis of the same rock sample under the conditions of different testing procedures is carried out using rock NMR instrument, have the characteristics that easy to operate, quick, data result comparability is strong.

Description

A kind of rock NMR instrument sample carries bed and its application method
Technical field
The invention belongs to petrophysical parameter test and analysis technology field more particularly to a kind of rock NMR instrument samples Carry bed and its application method.
Background technology
In recent years, nuclear magnetic resonance technique due to detection speed is fast, to sample nondestructive, result is accurate the advantages that become interior The conventional means of petrophysical parameter test, especially in blowhole measures analysis, Magnetic resonance imaging test increasingly Favored.When being tested using rock NMR instrument, need rock sample being placed on strip arc groove first It carries on bed, then will carry bed and sample is put into coil box together, coil box connects circuit and is placed in magnetic field, and then completes Nuclear magnetic resonance is tested.Due to generally requiring that multiple testing procedure is carried out to same sample in experimentation, to obtain difference Condition, the nuclear magnetic resonance image test result of different time, then compare and analyze.And existing sample carries bed and test side Often there are errors for method, are mainly manifested in:Load bed is strip arc groove, and rock sample is cylinder, and the diameter for usually carrying bed is bigger In the diameter of rock sample, therefore rock sample is placed on and carries on bed, easy to roll, it is impossible to ensure that sample is placed on load bed axis during test every time Same position on direction.Therefore, because sample is placed on the spatial position difference carried on bed, after leading to different testing procedures The nuclear magnetic resonance image result of acquisition is variant, is unfavorable for intuitively being compared, affects the analysis of nuclear magnetic resonance test result.
Invention content
The technical problems to be solved by the invention be to provide it is a kind of it is easy to operate, quick, data result comparability is strong Rock NMR instrument sample carry bed and its application method.
In order to solve the above technical problems, rock NMR instrument sample provided by the invention carries bed, including carrying bed ontology, institute It states and carries bed ontology and be equipped with strip arc groove, scale and number of division are identified in an axial direction at one side edge in the strip arc groove Word, the strip arc groove is interior to be equipped in the graduated side of mark and can slide item in axial sliding along strip arc groove, institute It states a sliding bottom end face and extends to strip arc groove bottom center, and the vertical plane where with strip arc groove bottom centerline It overlaps, diameter spirit bubble is equipped at strip arc groove one end bottom center.
Further, be equipped with axially extending guide groove in the strip arc groove, the sliding item be equipped with it is described The guide pad that guide groove matches.
Further, the sliding item is arc-shaped and is close to the strip arc groove, the top of the sliding item and institute It is concordant to state strip arc groove top end face.
Correspondingly, the application method that bed is carried the invention also discloses a kind of rock NMR instrument sample (utilizes and includes this Carry the method that the Nuclear Magnetic Resonance of bed tests rock), setting-out marks one on the end face of cylinder rock sample one end first Diameter line;Cylinder rock sample is placed in strip arc groove, slides sliding item against cylinder rock sample, and ensure to mark The rock diameter line of note is located at the bottom end face institute of sliding item planar, and records number of division;The load bed of rock sample will be mounted with Ontology is put into the coil box in Nuclear Magnetic Resonance, is tested, and ensures that the bubble in diameter spirit bubble is placed in the middle during test.
The present invention is suitable for carrying out the test of cylinder rock sample using rock NMR instrument, realize it is easy to operate, Fast, the purpose of data result comparability is strong.
The invention has the advantages that when being tested using rock NMR instrument, by scale, slider bar by rock sample Fixed placement records specific number of division on bed is carried;By diameter spirit bubble come ensure carry bed be to lie in a horizontal plane in coil In box, it is identical for can ensure that spatial position of the same sample in different measuring process, so as to the nuclear magnetic resonance figures to acquisition As comparing and analyzing.
In conclusion the present invention is a kind of to carry out same cylinder rock sample in different test steps using rock NMR instrument There is easy to operate, quick and strong data result comparability rock NMR instrument sample to carry bed and test side under the conditions of rapid Method.
Description of the drawings
Fig. 1 carries bed and coil box cooperation schematic diagram for rock NMR instrument sample of the present invention;
Fig. 2 is the vertical view that rock NMR instrument sample of the present invention carries bed;
Fig. 3 is the half sectional view that rock NMR instrument sample of the present invention carries bed.
Specific embodiment
Below in conjunction with the drawings and specific embodiments, the present invention is further illustrated.
Referring to Fig. 1-Fig. 3, a kind of rock NMR instrument sample carries bed, including carrying bed ontology 1, carries bed ontology 1 and is equipped with Strip arc groove 2, is identified with scale 3 and scale number 4 in strip arc groove 2 in an axial direction at one side edge, in strip arc groove 2 Item 5 can be slid in axial sliding along strip arc groove 2 by being equipped in the side for being identified with scale 3, the 5 bottom end face extension of sliding item It is overlapped to 2 bottom center of strip arc groove, and with the vertical plane where 2 bottom centerline of strip arc groove 6, strip arc groove 2 Diameter spirit bubble 7 is equipped at the bottom center of one end.By diameter spirit bubble 7, to observe load bed ontology 1, whether level is put into coil In box 8, when test, needs to ensure the horizontal center in diameter spirit bubble 7.
In the present embodiment, axially extending guide groove 9 is equipped in strip arc groove 2, sliding item 5 is equipped with and guide groove 9 The guide pad to match.
In the present embodiment, sliding item 5 is arc-shaped and is close to strip arc groove 2, slides the top of item 5 and strip arc groove 2 top end faces are concordant.
A kind of rock NMR instrument sample carries the application method of bed, during test, first at 10 one end end of cylinder rock sample Setting-out marks a diameter line on face;Cylinder rock sample 10 is placed in strip arc groove 2, sliding sliding item 5 makes it tight By simultaneously stationary cylinder rock sample 10, and ensure that the rock diameter line marked is located at the bottom end face institute of sliding item 5 planar, remember Record number of division;The load bed ontology 1 for being mounted with rock sample is put into coil box 8, is tested, ensures that diameter is horizontal during test Bubble in bubble 7 is placed in the middle.
Above-described embodiment is only to clearly demonstrate example of the present invention rather than the restriction to embodiment.For For those of ordinary skill in the art, other various forms of variations or change can also be made on the basis of the above description It is dynamic.Here without can not be also exhaustive to all embodiments.And the obvious variation or change thus amplified out It is dynamic to be still in the protection scope of this invention.

Claims (4)

1. a kind of rock NMR instrument sample carries bed, including carrying bed ontology, the load bed ontology is equipped with strip arc groove, It is characterized in that:It is identified with scale and scale number, the strip arc groove in the strip arc groove at one side edge in an axial direction The inherence graduated side of mark is equipped with can slide item in axial sliding along strip arc groove, and the sliding bottom end face prolongs Strip arc groove bottom center is extended to, and is overlapped with the vertical plane where strip arc groove bottom centerline, the strip arc Diameter spirit bubble is equipped at the bottom center of slot one end.
2. rock NMR instrument sample according to claim 1 carries bed, it is characterised in that:It is set in the strip arc groove There is axially extending guide groove, the sliding item is equipped with the guide pad to match with the guide groove.
3. rock NMR instrument sample according to claim 1 or 2 carries bed, it is characterised in that:The sliding item is in circle Arc and it is close to the strip arc groove, the top of the sliding item is concordant with the strip arc groove top end face.
4. a kind of rock NMR instrument sample carries the application method of bed, it is characterised in that:First at cylinder rock sample one end end Setting-out marks a diameter line on face;Cylinder rock sample is placed in strip arc groove, slides sliding item against circle Cylinder rock sample, and ensure that the rock diameter line marked is located at the bottom end face institute of sliding item planar, and records number of division;It will The load bed ontology for being mounted with rock sample is put into the coil box in Nuclear Magnetic Resonance, is tested, and ensures diameter spirit bubble during test In bubble it is placed in the middle.
CN201810036971.XA 2018-01-15 2018-01-15 Method for testing rock by using nuclear magnetic resonance spectrometer Active CN108254401B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810036971.XA CN108254401B (en) 2018-01-15 2018-01-15 Method for testing rock by using nuclear magnetic resonance spectrometer

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201810036971.XA CN108254401B (en) 2018-01-15 2018-01-15 Method for testing rock by using nuclear magnetic resonance spectrometer

Publications (2)

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CN108254401A true CN108254401A (en) 2018-07-06
CN108254401B CN108254401B (en) 2022-01-18

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Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1655617A2 (en) * 2004-10-29 2006-05-10 University of Brunswick Methods and apparatus for measuring capillary pressure in a sample
CN201965077U (en) * 2010-12-17 2011-09-07 中国石油天然气股份有限公司 Rock core computed tomography (CT) scanning fixing device
CN102338759A (en) * 2010-07-14 2012-02-01 中国石油天然气股份有限公司 Standard sample of whole diameter nuclear magnetic resonance rock sample analyzer
KR101171736B1 (en) * 2012-01-18 2012-08-07 한국지질자원연구원 A device for measuring core sample
US20150061669A1 (en) * 2013-09-05 2015-03-05 Saudi Arabian Oil Company Tri-Axial NMR Test Instrument
CN206020254U (en) * 2016-08-20 2017-03-15 青岛海洋地质研究所 The shallow rock drilling heart camera arrangement of Marine Geology
CN107037129A (en) * 2017-05-16 2017-08-11 长江大学 A kind of rock anisotropy measurement clamper and its measuring method

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1655617A2 (en) * 2004-10-29 2006-05-10 University of Brunswick Methods and apparatus for measuring capillary pressure in a sample
CN102338759A (en) * 2010-07-14 2012-02-01 中国石油天然气股份有限公司 Standard sample of whole diameter nuclear magnetic resonance rock sample analyzer
CN201965077U (en) * 2010-12-17 2011-09-07 中国石油天然气股份有限公司 Rock core computed tomography (CT) scanning fixing device
KR101171736B1 (en) * 2012-01-18 2012-08-07 한국지질자원연구원 A device for measuring core sample
US20150061669A1 (en) * 2013-09-05 2015-03-05 Saudi Arabian Oil Company Tri-Axial NMR Test Instrument
CN206020254U (en) * 2016-08-20 2017-03-15 青岛海洋地质研究所 The shallow rock drilling heart camera arrangement of Marine Geology
CN107037129A (en) * 2017-05-16 2017-08-11 长江大学 A kind of rock anisotropy measurement clamper and its measuring method

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