CN108246227A - A kind of material reaction unit - Google Patents
A kind of material reaction unit Download PDFInfo
- Publication number
- CN108246227A CN108246227A CN201810187110.1A CN201810187110A CN108246227A CN 108246227 A CN108246227 A CN 108246227A CN 201810187110 A CN201810187110 A CN 201810187110A CN 108246227 A CN108246227 A CN 108246227A
- Authority
- CN
- China
- Prior art keywords
- autoclave body
- water
- inner cover
- cooling tube
- rabbling mechanism
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/0013—Controlling the temperature of the process
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
- B01J2219/0009—Coils
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Accessories For Mixers (AREA)
Abstract
The invention discloses a kind of material reaction units, and including autoclave body, cooling tube, inner cover, outer cover, rabbling mechanism, stirring motor, the top of the autoclave body is provided with feed hopper, lower part is provided with discharge port；The cooling tube helical arrangement is connected with Water-cooling circulating mechanism on inner wall of kettle between the water inlet and water outlet of cooling tube；The inner cover is set to the outside of autoclave body, and thermal conductive cavity is formed between the outer wall of autoclave body；The outer cover is set to the outside of inner cover, and the top of the outer cover is thermal insulation board, lower part is provided with heating chamber, and heating rod is provided in the heating chamber；The rabbling mechanism is set in autoclave body, and the stirring motor drives rabbling mechanism mixing high molecular material.The configuration of the present invention is simple uniformly cools down, and cold mixed effect is good, and working efficiency is high, and can exclude residual gas can simultaneously prevent from luming；Meanwhile there is cooling water self-loopa, reduce energy consumption and labor intensity.
Description
Technical field
The present invention relates to new material technology field more particularly to a kind of material reaction units.
Background technology
New material product is being added man-hour requirement by high molecular material hybrid reaction by present new material industry, during mixing
The general interior heat that carries out of reaction kettle of first putting into is mixed, and heat sneaks out the chemical process that journey is not only physical process and complexity, macromolecule
Material such as carries out high speed impact, sheds, rubs at the movements in a kettle, it is made to reach defined terminal by the temperature requirement of setting
Temperature, and complete the requirements such as homogenization, macromolecular simultaneously during this period, due to easily there is residual gas after heat is mixed, make
Secure satisfactory grades sub- material clumps, so as to influence to react, the further performance for influencing product.Existing cold mixing device is typically anti-
Answer and cooling water be passed through between the outer wall of kettle and inner wall, into trip temperature transmit cool down, when cooling water after a period of use, cooling effect
Fruit is deteriorated, and lengthens incorporation time and so that the energy consumption of reaction kettle is big, also needs manually to replace cooling water so that cooling water keeps certain
Temperature increases labor intensity.
Invention content
In view of the deficienciess of the prior art, the purpose of the present invention, which is that, provides a kind of material reaction unit, structure
Simply, stirring is incorporated into one with refrigerating function, high molecular material of the heat after mixed is carried out cold mixing makes it uniformly cool down, cold
Mixed effect is good, and working efficiency is high, and can exclude residual gas can simultaneously prevent from luming；Meanwhile there is cooling water self-loopa, subtract
Energy consumption and labor intensity are lacked.
To achieve these goals, the technical solution adopted by the present invention is such：A kind of material reaction unit, including kettle
Body, cooling tube, inner cover, outer cover, rabbling mechanism, stirring motor, the top of the autoclave body is provided with feed hopper, lower part is provided with out
Material mouth；For the cooling tube helical arrangement on inner wall of kettle, the water inlet of cooling tube is set to the top of autoclave body, water outlet setting
Water-cooling circulating mechanism is connected in the lower part of autoclave body, and between water inlet and water outlet；The inner cover is set to the outside of autoclave body,
And thermal conductive cavity is formed between the outer wall of autoclave body；Be provided with conduction oil in the thermal conductive cavity, the oil inlet of thermal conductive cavity with it is fuel-displaced
Mouth is symmetrically disposed on the top of inner cover, and heat-conducting oil furnace is connected between oil inlet and oil outlet；The outer cover is set to inner cover
Outside, the top of the outer cover is thermal insulation board, lower part is provided with heating chamber, and heating rod is provided in the heating chamber；The stirring
Mechanism is set in autoclave body, and the stirring motor drives rabbling mechanism mixing high molecular material；Wherein Water-cooling circulating mechanism includes
Water pump, one-way cock, brine tank, the water outlet are connected to brine tank bottom with water pump, one-way cock successively by outlet pipeline
Portion, water inlet are connected to the top of brine tank by inlet pipeline；Spout is provided at the top of the brine tank, the spout is with doing
Ice sprayer is connected；The thermal insulation board include upper decoration plate, cellular board, lower decorative panel, the upper surface of the cellular board with it is upper
The lower surface of decorative panel is connected, the lower surface of cellular board is connected with the upper surface of lower decorative panel；It is equipped in the cellular board
Honeycomb slot, the honeycomb slot is interior to be filled with foamed material；The rabbling mechanism includes agitating shaft, stirring turntable, and the agitating shaft is set
It is placed in autoclave body, top is connected with stirring motor；The stirring turntable, which helically rises, to be fastened in the table of agitating shaft
Face.
As a preferred embodiment, it is provided with exhaust outlet at the top of the autoclave body.
As a preferred embodiment, the upper decoration plate and lower decorative panel are aluminium-plastic panel.
As a preferred embodiment, the foamed material is polystyrene foam.
As a preferred embodiment, the polystyrene foam is bonded in by polyvinyl acetate adhesive layer in honeycomb slot
Portion.
Compared with prior art, beneficial effects of the present invention：Stirring is incorporated by the configuration of the present invention is simple with refrigerating function
One, high molecular material of the heat after mixed is carried out cold mixing makes it uniformly cool down, and cold mixed effect is good, and working efficiency is high, Neng Goupai
Except residual gas can simultaneously prevent from luming；Meanwhile there is cooling water self-loopa, reduce energy consumption and labor intensity.
Description of the drawings
Fig. 1 is the structure diagram of the present invention；
Fig. 2 is the structure diagram of thermal insulation board in the present invention.
Specific embodiment
With reference to specific embodiment, the invention will be further described.Following embodiment is only used for clearly illustrating
Technical scheme of the present invention, and be not intended to limit the protection scope of the present invention and limit the scope of the invention.
Embodiment：
As shown in Fig. 1~2, a kind of material reaction unit, including autoclave body 1, cooling tube 2, inner cover 3, outer cover 4, rabbling mechanism
5th, stirring motor 6, the top of the autoclave body 1 is provided with feed hopper 7, lower part is provided with discharge port 8；2 spiral of the cooling tube row
It being distributed on 1 inner wall of autoclave body, the water inlet 21 of cooling tube 2 is set to the top of autoclave body 1, water outlet 22 is set to the lower part of autoclave body 1,
And Water-cooling circulating mechanism 9 is connected between water inlet 21 and water outlet 22；The inner cover 3 is set to the outside of autoclave body 1, and and kettle
Thermal conductive cavity 31 is formed between the outer wall of body 1；Conduction oil is provided in the thermal conductive cavity 31, the oil inlet 32 of thermal conductive cavity 31 is with going out
Hydraulic fluid port 33 is symmetrically disposed on the top of inner cover 3, and heat-conducting oil furnace 34 is connected between oil inlet 32 and oil outlet 33；The outer cover
4 are set to the outside of inner cover 3, and the top of the outer cover 4 is thermal insulation board 41, lower part is provided with heating chamber 42, is set in the heating chamber 42
It is equipped with heating rod 43；The rabbling mechanism 5 is set in autoclave body 1, and the stirring motor 6 drives rabbling mechanism 5 to mix macromolecule
Material；Wherein Water-cooling circulating mechanism 9 includes water pump 91, one-way cock 92, brine tank 93, and the water outlet 22 passes through outlet pipeline
94 are connected to 93 bottom of brine tank with water pump 91, one-way cock 92 successively, and water inlet 21 is connected to brine by inlet pipeline 95
The top of case 93；The top of the brine tank 93 is provided with spout 96, which is connected with dry ice sprayer 97；The guarantor
Warm plate 41 includes upper decoration plate 411, cellular board 412, lower decorative panel 413, the upper surface of the cellular board 412 and upper decoration plate
411 lower surface is connected, the lower surface of cellular board 412 is connected with the upper surface of lower decorative panel 413；The cellular board 412
It is interior to be equipped with honeycomb slot 414, it is filled with foamed material in the honeycomb slot 414；The rabbling mechanism 5 includes agitating shaft 51, stirring turns
Disk 52, the agitating shaft 51 are set in autoclave body 1, and top is connected with stirring motor 6；It is described stirring turntable 52 helically on
It rises and is fastened in the surface of agitating shaft 51.
Preferably, the top of the autoclave body 1 is provided with exhaust outlet 10, for discharging the gas generated in autoclave body 1.
Preferably, the upper decoration plate 411 and lower decorative panel 413 are aluminium-plastic panel.
Preferably, the foamed material is polystyrene foam.
Preferably, the polystyrene foam is bonded in the inside of honeycomb slot 414 by polyvinyl acetate adhesive layer.
Specifically, raw material enters from feed hopper 7, the heating rod 43 heats conduction oil, and thermal insulation board 41 plays pair
The effect that autoclave body 1 is kept the temperature, stirring motor 6 drive rabbling mechanism 5 to carry out to raw material stirring hot mixing reaction, while terminate when heat is mixed
Afterwards, cooling water is passed through into cooling tube 2 by Water-cooling circulating mechanism 9 and is stirred cold mixing reaction, is gone out after the completion from discharge port 8
Material.
The above is only the preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art
For member, without departing from the technical principles of the invention, several improvement and deformation can also be made, these are improved and deformation
Also it should be regarded as protection scope of the present invention.
Claims (5)
1. a kind of material reaction unit, it is characterised in that：Including autoclave body, cooling tube, inner cover, outer cover, rabbling mechanism, stirring electricity
Machine, the top of the autoclave body is provided with feed hopper, lower part is provided with discharge port；The cooling tube helical arrangement is in inner wall of kettle
On, the water inlet of cooling tube is set to the top of autoclave body, water outlet is set to the lower part of autoclave body, and between water inlet and water outlet
It is connected with Water-cooling circulating mechanism；The inner cover is set to the outside of autoclave body, and thermal conductive cavity is formed between the outer wall of autoclave body；Institute
State and conduction oil be provided in thermal conductive cavity, the oil inlet of thermal conductive cavity is symmetrically disposed on the top of inner cover with oil outlet, and oil inlet with
Heat-conducting oil furnace is connected between oil outlet；The outer cover is set to the outside of inner cover, and the top of the outer cover is thermal insulation board, lower part
Heating chamber is provided with, heating rod is provided in the heating chamber；The rabbling mechanism is set in autoclave body, and the stirring motor driving is stirred
Mix mechanism mixing high molecular material；Wherein Water-cooling circulating mechanism includes water pump, one-way cock, brine tank, and the water outlet passes through
Outlet pipeline is connected to brine tank bottom with water pump, one-way cock successively, and water inlet is connected to brine tank by inlet pipeline
Top；Spout is provided at the top of the brine tank, which is connected with dry ice sprayer；The thermal insulation board includes upper decoration
Plate, cellular board, lower decorative panel, the upper surface of the cellular board is connected with the lower surface of upper decoration plate, the lower surface of cellular board
It is connected with the upper surface of lower decorative panel；Honeycomb slot is equipped in the cellular board, foamed material is filled in the honeycomb slot；It is described
Rabbling mechanism includes agitating shaft, stirring turntable, and the agitating shaft is set in autoclave body, and top is connected with stirring motor；Institute
Stirring turntable is stated helically to rise and be fastened in the surface of agitating shaft.
2. a kind of material reaction unit according to claim 1, it is characterised in that：Exhaust is provided at the top of the autoclave body
Mouthful.
3. a kind of material reaction unit according to claim 1, it is characterised in that：The upper decoration plate and lower decorative panel are equal
For aluminium-plastic panel.
4. a kind of material reaction unit according to claim 1, it is characterised in that：The foamed material is steeped for polystyrene
Foam.
5. a kind of material reaction unit according to claim 4, it is characterised in that：The polystyrene foam passes through poly-vinegar
Sour ethylene adhesive layer is bonded in the inside of honeycomb slot.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810187110.1A CN108246227A (en) | 2018-03-07 | 2018-03-07 | A kind of material reaction unit |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810187110.1A CN108246227A (en) | 2018-03-07 | 2018-03-07 | A kind of material reaction unit |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108246227A true CN108246227A (en) | 2018-07-06 |
Family
ID=62746038
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810187110.1A Withdrawn CN108246227A (en) | 2018-03-07 | 2018-03-07 | A kind of material reaction unit |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108246227A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113856599A (en) * | 2021-10-30 | 2021-12-31 | 安徽华塑股份有限公司 | Temperature control and medium circulating system of polyvinyl chloride polymerization kettle |
-
2018
- 2018-03-07 CN CN201810187110.1A patent/CN108246227A/en not_active Withdrawn
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113856599A (en) * | 2021-10-30 | 2021-12-31 | 安徽华塑股份有限公司 | Temperature control and medium circulating system of polyvinyl chloride polymerization kettle |
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|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WW01 | Invention patent application withdrawn after publication | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20180706 |