CN108225829A - A kind of remote instantaneous sample device and method of mixer-settler material liquid outlet - Google Patents
A kind of remote instantaneous sample device and method of mixer-settler material liquid outlet Download PDFInfo
- Publication number
- CN108225829A CN108225829A CN201611149979.4A CN201611149979A CN108225829A CN 108225829 A CN108225829 A CN 108225829A CN 201611149979 A CN201611149979 A CN 201611149979A CN 108225829 A CN108225829 A CN 108225829A
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- China
- Prior art keywords
- sampling
- sampling bottle
- mixer
- settler
- liquid outlet
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Classifications
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/02—Devices for withdrawing samples
- G01N1/10—Devices for withdrawing samples in the liquid or fluent state
- G01N1/14—Suction devices, e.g. pumps; Ejector devices
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/02—Devices for withdrawing samples
- G01N1/10—Devices for withdrawing samples in the liquid or fluent state
- G01N2001/1031—Sampling from special places
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/02—Devices for withdrawing samples
- G01N1/10—Devices for withdrawing samples in the liquid or fluent state
- G01N1/14—Suction devices, e.g. pumps; Ejector devices
- G01N2001/1418—Depression, aspiration
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- Life Sciences & Earth Sciences (AREA)
- Hydrology & Water Resources (AREA)
- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Sampling And Sample Adjustment (AREA)
Abstract
A kind of remote instantaneous sample device of mixer-settler material liquid outlet, including ball valve, sampling bottle channel, mixer-settler, sampling part, control cabinet, feed liquid receiving slit, expanding reach wherein on the right side of mixer-settler in connection sampling part, expanding reach is a groove structure, sampling part includes motor, stent, upper limit position switch, lower position switch, discharge nozzle, transmission shaft, sample bottle rack, sampling bottle, sampling probe, expanding reach, motor is installed above sampling part Hu stent, motor drives transmission shaft, and transmission shaft connection sampling bottle rack, sampling bottle rack can support sampling bottle, sampling bottle is inserted into sampling probe upper end, expanding reach is inserted into lower end.A kind of remote instantaneous sample method of mixer-settler material liquid outlet, includes the following steps:S1:Open ball valve;S2:Sampling stent is made to increase;S3:Sampling bottle is put into S4 on sampling bottle rack with manipulator:Feed liquid is being inhaled into sampling bottle;S5:Sampling bottle is removed with manipulator.
Description
Technical field
The technology belongs to sampler field, and in particular to a kind of remote instantaneous sample dress of mixer-settler material liquid outlet
It puts and method.
Background technology
The mixer-settler of certain radioactivity production line is placed in hot cell, these mixer-settler main functions are by feed liquid
In uranium recycled, remove the utilization and recycle of fission product and organic phase.To ensure the stable operation of mixer-settler, need to determine
When these mixer-settler material liquid outlets are sampled with analysis, operating personnel are according to operation of these data to mixer-settler
Situation is analyzed and determined that, because design initial stage does not design long distance sampler, mixer-settler operating condition can only pass through heat
Outdoor feed liquid receives storage tank and takes the data of aggregate sample to do rough judgement, and this rough judgement exists and yields poor results, judges standard
The defects of exactness is not high, operating personnel find mixer-settler occur unusual service condition at least lagged than actual conditions 8 hours with
On, it is impossible to meet the needs of technical process control.
This patent be directed to there are the problem of, devise remote instantaneous sample device in a kind of hot cell, directly mixing
Defecator material liquid outlet installs sampler additional, successfully solves mixer-settler material liquid outlet sampling analysis and judges that there are timeliness
Difference, the defects of accuracy of judgement degree is not high, avoid and cross contamination etc. is radiated and reduced in operating personnel's sampling process ask
Topic.
Invention content
It is an object of the invention to:There is provided a kind of mixer-settler material liquid outlet remote instantaneous sample device and method,
It solves mixer-settler material liquid outlet sampling analysis and judges there is the defects of yielding poor results, accuracy of judgement degree is not high, avoid operation
The problems such as being radiated in personnel's sampling process and reducing cross contamination.
Technical scheme is as follows:A kind of remote instantaneous sample device of mixer-settler material liquid outlet, including ball
Connection takes on the right side of valve, sampling bottle channel, mixer-settler, sampling part, control cabinet, feed liquid receiving slit, wherein mixer-settler
Expanding reach in sample part, sampling part include motor, stent, upper limit position switch, lower position switch, transmission shaft, sampling bottle branch
Frame, sampling bottle, sampling probe, expanding reach, install motor above sampling part Hu stent, and motor drives transmission shaft, and transmission shaft
Connection sampling bottle rack again, sampling bottle rack can support sampling bottle, and sampling bottle is inserted into sampling probe upper end, and lower end, which is inserted into, to be expanded
Section;There are upper limit position switch, lower position switch on stent respectively, the height available for limitation sampling bottle rack;Ball valve is located at sampling
Bottle upper part of channel, sampling bottle can enter sampling bottle channel from ball valve.
The sampling part connects feed liquid receiving slit by discharge nozzle.
The sampling part also connects control cabinet by conducting wire.
The expanding reach is a groove structure, available for keeping in material.
The control cabinet includes rising indicator light, declines indicator light, rising button, declines button.
A kind of remote instantaneous sample method of mixer-settler material liquid outlet, includes the following steps:
S1:Ball valve is opened, sampling bottle is sent into from sampling bottle channel in hot cell;
S2:By control cabinet rising button, rising indicator light is bright, and motor driving transmission shaft rises sampling stent;
S3:Sampling bottle is put on sampling bottle rack;
S4:By control cabinet declines button, motor driving transmission shaft declines sampling stent, touches lower position switch and stop automatically
Only decline, sampling probe is inserted into sampling bottle at this time, and feed liquid is inhaled into sampling bottle under vacuum;
S5:Control cabinet rising button, motor driving transmission shaft, rises sampling stent, runs into limit switch stopping, using machine
Tool hand removes sampling bottle.
In the S1, sampling bottle vacuum degree is 0.08Mpa.
In the S2, sampling stent runs into limit switch and is automatically stopped rising.
In the S5, after running into limit switch stopping, sampling bottle is removed with manipulator.
In the S3, sampling bottle is put on sampling bottle rack with manipulator.
The remarkable result of the present invention is:The device, can be suitable under the premise of keeping not interfering material liquid outlet flowing unobstructed
The remote instantaneous sample of the realization mixer-settler material liquid outlet of profit, solving mixer-settler material liquid outlet cannot be remote
The problem of sampling avoids the problems such as being radiated in operating personnel's sampling process and reducing cross contamination.
Description of the drawings
Fig. 1 is the remote instantaneous sample schematic device of mixer-settler material liquid outlet of the present invention
In figure:1 ball valve;2 sampling bottle channels;3 motors;4 stents;5 upper limit position switch;6 lower position switch;7 discharge nozzles;8
Transmission shaft;9 sampling bottle racks;10 sampling bottles;11 sampling probes;12 expanding reach;13 control cabinets;14 mixer-settlers;15 feed liquids connect
Receive slot;16 rise indicator light;17 decline indicator light;18 rising buttons;19 declines buttons
Specific embodiment
Below in conjunction with the accompanying drawings and specific embodiment is described in further detail the present invention.
A kind of remote instantaneous sample device of mixer-settler material liquid outlet, it is clear including ball valve 1, sampling bottle channel 2, mixing
Expansion in clear slot 14, sampling part, control cabinet 13, feed liquid receiving slit 15, wherein 14 right side connection sampling part of mixer-settler
Big section 12, expanding reach 12 are a groove structure, and available for keeping in material, sampling part includes motor 3, stent 4, upper limit position switch
5th, lower position switch 6, discharge nozzle 7, transmission shaft 8, sampling bottle rack 9, sampling bottle 10, sampling probe 11, expanding reach 12, in sampling portion
Divide Hu stent 4 top installation motor 3, motor 3 drives transmission shaft 8, and the connection of transmission shaft 8 samples bottle rack 9, samples bottle rack
Sampling bottle 10 is inserted into 9 sustainable sampling bottles 10,11 upper end of sampling probe, and expanding reach 12 is inserted into lower end;On having respectively on stent 4
Limit switch 5, lower position switch 6, the height available for limitation sampling bottle rack 9;Ball valve 1 is located at 2 top of sampling bottle channel, takes
Sample bottle 10 can enter sampling bottle channel 2 from ball valve 1
Sampling part connects feed liquid receiving slit 15 by discharge nozzle 7, while sampling part also connects control cabinet by conducting wire
13, control cabinet 13 includes rising indicator light 16, declines indicator light 17, rising button 18, declines button 19;
A kind of remote instantaneous sample method of mixer-settler material liquid outlet, includes the following steps:
S1:Ball valve 1 is opened, the sampling bottle 10 for being up to vacuum degree 0.08MPa is sent into from sampling bottle channel 2 in hot cell;
S2:By 13 rising button 15 of control cabinet, rising indicator light 16 is bright, and motor 3 drives transmission shaft 8, makes on sampling stent 9
It rises, runs into limit switch 5 and be automatically stopped rising;
S3:Sampling bottle 10 is put on sampling bottle rack 9 with manipulator
S4:By 13 declines button 19 of control cabinet, motor 3 drives transmission shaft 8, declines sampling stent 9, touch lower position switch
6 are automatically stopped decline, and sampling probe 11 is inserted into sampling bottle 10 at this time, and feed liquid is inhaled under vacuum in sampling bottle 10;
S5:13 rising button 16 of control cabinet, motor 3 drive transmission shaft 8, sampling stent 9 are made to increase, runs into limit switch 5
Stop, being removed sampling bottle 10 with manipulator.
Claims (10)
1. a kind of remote instantaneous sample device of mixer-settler material liquid outlet, it is characterised in that:Including ball valve (1), sampling bottle
Channel (2), mixer-settler (14), sampling part, control cabinet (13), feed liquid receiving slit (15), wherein mixer-settler (14)
Expanding reach (12) in right side connection sampling part, sampling part include motor (3), stent (4), upper limit position switch (5), lower limit
Bit switch (6), transmission shaft (8), sampling bottle rack (9), sampling bottle (10), sampling probe (11), expanding reach (12), in sampling part
Installation motor (3) above Hu stent (4), motor (3) drives transmission shaft (8), and transmission shaft (8) connection samples bottle rack (9),
It samples bottle rack (9) and can support sampling bottle (10), sampling bottle (10) is inserted into sampling probe (11) upper end, and expanding reach is inserted into lower end
(12);There are upper limit position switch (5), lower position switch (6) on stent (4) respectively, the height available for limitation sampling bottle rack (9)
Degree;For ball valve (1) positioned at sampling bottle channel (2) top, sampling bottle (10) can be from ball valve (1) into sampling bottle channel (2).
2. a kind of remote instantaneous sample device of mixer-settler material liquid outlet according to claim 1, it is characterised in that:
The sampling part connects feed liquid receiving slit (15) by discharge nozzle (7).
3. a kind of remote instantaneous sample device of mixer-settler material liquid outlet according to claim 2, it is characterised in that:
The sampling part also connects control cabinet (13) by conducting wire.
4. a kind of remote instantaneous sample device of mixer-settler material liquid outlet according to claim 1, it is characterised in that:
The expanding reach (12) is a groove structure, available for keeping in material.
5. a kind of remote instantaneous sample device of mixer-settler material liquid outlet according to claim 1, it is characterised in that:
The control cabinet (13) is including rising indicator light (16), declining indicator light (17), rising button (18), declines button (19).
A kind of 6. remote instantaneous sample method of mixer-settler material liquid outlet as claimed in claim 3, it is characterised in that:Packet
Include following steps:
S1:Ball valve (1) is opened, sampling bottle (10) is sent into from sampling bottle channel (2) in hot cell;
S2:By control cabinet (13) rising button (15), rising indicator light (16) is bright, and motor (3) driving transmission shaft (8) makes sampling
Stent (9) rises;
S3:Sampling bottle (10) is put on sampling bottle rack (9);
S4:By control cabinet (13) declines button (19), motor (3) driving transmission shaft (8) declines sampling stent (9), touches lower limit
Bit switch (6) is automatically stopped decline, and sampling probe (11) is inserted into sampling bottle (10) at this time, and feed liquid is inhaled into takes under vacuum
In sample bottle (10);
S5:Control cabinet (13) rising button (16), motor (3) driving transmission shaft (8) rise sampling stent (9), run into limiting
It switchs (5) to stop, being removed sampling bottle (10) with manipulator.
7. a kind of remote instantaneous sample method of mixer-settler material liquid outlet according to claim 6, it is characterised in that:
In the S1, sampling bottle (10) vacuum degree is 0.08Mpa.
8. a kind of remote instantaneous sample method of mixer-settler material liquid outlet according to claim 6, it is characterised in that:
In the S2, sampling stent (9) runs into limit switch (5) and is automatically stopped rising.
9. a kind of remote instantaneous sample method of mixer-settler material liquid outlet according to claim 6, it is characterised in that:
In the S5, after running into limit switch (5) stopping, sampling bottle (10) is removed with manipulator.
10. a kind of remote instantaneous sample method of mixer-settler material liquid outlet according to claim 6, feature exist
In:In the S3, sampling bottle (10) is put on sampling bottle rack (9) with manipulator.
Priority Applications (1)
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CN201611149979.4A CN108225829A (en) | 2016-12-14 | 2016-12-14 | A kind of remote instantaneous sample device and method of mixer-settler material liquid outlet |
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CN201611149979.4A CN108225829A (en) | 2016-12-14 | 2016-12-14 | A kind of remote instantaneous sample device and method of mixer-settler material liquid outlet |
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CN108225829A true CN108225829A (en) | 2018-06-29 |
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CN201611149979.4A Pending CN108225829A (en) | 2016-12-14 | 2016-12-14 | A kind of remote instantaneous sample device and method of mixer-settler material liquid outlet |
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Cited By (1)
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---|---|---|---|---|
CN109406211A (en) * | 2018-11-15 | 2019-03-01 | 中国核电工程有限公司 | Radioactivity material automatic sampling device |
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Application publication date: 20180629 |