CN108219594A - A kind of environmental protection pearly-lustre mill base - Google Patents
A kind of environmental protection pearly-lustre mill base Download PDFInfo
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- CN108219594A CN108219594A CN201711222710.9A CN201711222710A CN108219594A CN 108219594 A CN108219594 A CN 108219594A CN 201711222710 A CN201711222710 A CN 201711222710A CN 108219594 A CN108219594 A CN 108219594A
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- pearly
- mill base
- lustre
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D17/00—Pigment pastes, e.g. for mixing in paints
- C09D17/001—Pigment pastes, e.g. for mixing in paints in aqueous medium
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- Life Sciences & Earth Sciences (AREA)
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Abstract
The present invention relates to a kind of environmentally friendly pearly-lustre mill base, the environmental protection pearly-lustre mill base includes following raw material：55~68 parts of pearlite slurry,25~28 parts of pigment,15~18 parts of stearic acid,5~8 parts of zinc stearate,3~7 parts of mould inhibitor,21~27 parts of glycerine,35~45 parts of deionized water,12~16 parts of stearic acid diethylene glycol dilaurate,6~11 parts of hydroxyethyl cellulose,18~24 parts of talcum powder,9~15 parts of 11~14 parts of styrax and silica gel,The present invention carries out scientific and reasonable proportioning using Novel environment-friendlymaterial material,The raw material of conventional Environmental Safety is used in formula,Environmental protection pearly-lustre mill base safety obtained is good,Uniform coloring,It is easy to use,Good economy performance,It manufactures at low cost,With good potentiality,Environmentally protective few harm,Meet polycyclic aromatic hydrocarbons (PAH) inspection specification,Polycyclic aromatic hydrocarbons (PAH) is not detected,Meet Environmental Safety requirement,Environmental protection pearly-lustre mill base of the invention is widely used in medical treatment,Health,Coating,The fields such as machine and food.
Description
Technical field
The present invention relates to environmentally friendly mill base field of material technology, and in particular to a kind of environmental protection pearly-lustre mill base.
Background technology
Mill base, also known as color, i.e. pigment coordinate dispersant based on plasticizer, the high concentration formed by means of machine finish
Cream colored agent, suitable for Toy Industry, silica gel medical equipment, PVC trade marks, silica gel trade mark, PVC artificial leather and EVA foamed products,
Numerous industry fields such as acryl plank (organic glass).
Pearlite slurry is a kind of sheet coating of high refractive index, and good luster can show a kind of metal-like of flicker, extensively
It is general to be used for the coating such as car, furniture, machine or resin button, the surface treatment of craftwork.
But phthalate is used in the pearly-lustre mill base occurred in the market as plasticizer, it is right with carcinogenicity
Ecological environment and human health cause potential threat.Therefore, it is necessary to a kind of new environmentally friendly pearly-lustre mill bases.
Invention content
To solve the above problems, a kind of the present invention is intended to provide environmental protection pearly-lustre mill base.
Purpose to realize the present invention, the technical solution adopted is that：A kind of environmental protection pearly-lustre mill base, the environmental protection pearly-lustre mill base packet
Following raw material are included：It is 55~68 parts of pearlite slurry, 25~28 parts of pigment, 15~18 parts of stearic acid, 5~8 parts of zinc stearate, mould proof
3~7 parts of agent, 21~27 parts of glycerine, 35~45 parts of deionized water, 12~16 parts of stearic acid diethylene glycol dilaurate, hydroxyethyl cellulose 6
9~15 parts of~11 parts, 18~24 parts of talcum powder, 11~14 parts of styrax and silica gel.
Preferably, the environmentally friendly pearly-lustre mill base is also added with 1~3 part of environmentally friendly color paste stabilizer.
Preferably, the environmentally friendly color paste stabilizer includes 30~40% organic tin stabilizer, 20~40% antimony organics
Stabilizer and 10~30% organic zinc stabilizer.
Preferably, 1~2 part of γ-FeO (OH), FeCO are also added in the environmentally friendly pearly-lustre mill base3And CaTiO3It is mixed
Object is closed, wherein, γ-FeO (OH), FeCO3And CaTiO3Adding proportion be 1~3:1:1~2.
Preferably, 3~5 parts of antifoaming agent is also added in the environmentally friendly pearly-lustre mill base, wherein, antifoaming agent is dodecyl
The mixture of sulfonate and lauryl sulfate, wherein, the ratio of dodecane sulfonate and lauryl sulfate for 2~
3:3~5.
Preferably, the manufacturing method of the environmentally friendly pearly-lustre mill base is：
1) is ground：Whole zinc stearate, stearic acid diethylene glycol dilaurate, hydroxyethyl cellulose, talcum powder and silica gel are turned
Enter into three-roll grinder and rough lapping 3~5 times is carried out with the grinding rate of 60~100r/min, obtain effective nominal diameter and do not surpass
Cross the uniformly mixed particle of 0.5cm；
2) mixes colours：30~40% antifoaming agent, pearlite slurry, pigment and glycerine are dissolved in deionized water, use high-speed stirring
It mixes machine to be stirred with the stir speed (S.S.) of 2500~3000r/min so that pearlite slurry mixes completely with glycerine, pigment and deionized water
It closes uniformly, color uniformly thick pearly-lustre mill base is made；
3) disperses：The ground hybrid particles of step 1 are transferred in dispersion machine, are added in while being dispersed with stirring
Thick pearly-lustre mill base made from step 2 after thick pearly-lustre mill base is added completely into, adds remaining antifoaming agent, stearic acid, mould proof
Agent, styrax, environmentally friendly color paste stabilizer, γ-FeO (OH), FeCO3And CaTiO3Dispersion 3~6h of stirring is carried out, is transferred to after dispersion
It is ground to horizontal bar type circulation horizontal grinder；
4) is ground again：The scattered material of step 3 is put into horizontal bar type circulation horizontal grinder, with 100~
The grinding rate of 150r/min is ground 3~5 times, and the grain size for being ground to mill base internal particle is 6~10nm, obtains environmentally friendly pearly-lustre color
Slurry.
Beneficial effects of the present invention are：Environmental protection pearly-lustre mill base of the invention carries out scientific and reasonable match using Novel environment-friendlymaterial material
Than the raw material of conventional Environmental Safety being used in formula, environmental protection pearly-lustre mill base safety obtained is good, uniform coloring, user
Just, good economy performance, manufactures at low cost, the potentiality having had, and environmentally protective few harm meets polycyclic aromatic hydrocarbons (PAH) inspection specification, not
Polycyclic aromatic hydrocarbons (PAH) is detected, meets Environmental Safety requirement, present invention environmental protection pearly-lustre mill base is widely used in medical treatment, health, coating, machine
With the fields such as food.
Description of the drawings
Fig. 1 is the raw material proportioning table of environmentally friendly pearly-lustre mill base of the invention.
Specific embodiment
Below in conjunction with the attached drawing in the embodiment of the present invention, the technical solution in the embodiment of the present invention is carried out clear, complete
Site preparation describes, it is clear that described embodiment is only part of the embodiment of the present invention, instead of all the embodiments.It is based on
Embodiment in the present invention, those of ordinary skill in the art are obtained every other without making creative work
Embodiment shall fall within the protection scope of the present invention.
Embodiment 1
Refering to Figure 1, the technical solution adopted by the present invention is：A kind of environmental protection pearly-lustre mill base, the environmental protection pearly-lustre color
Slurry includes following raw material：66 parts of pearlite slurry, 26 parts of pigment, 15 parts of stearic acid, 5 parts of zinc stearate, 4 parts of mould inhibitor, glycerine
24 parts, 43 parts of deionized water, 15 parts of stearic acid diethylene glycol dilaurate, 10 parts of hydroxyethyl cellulose, 22 parts of talcum powder, 13 parts of styrax
With 12 parts of silica gel.
Wherein, the environmentally friendly pearly-lustre mill base is also added with 2 parts of environmentally friendly color paste stabilizer.
Wherein, the environmentally friendly color paste stabilizer include 30% organic tin stabilizer, 40% organic antimony stabilizer and
30% organic zinc stabilizer.
Wherein, 1 part of γ-FeO (OH), FeCO are also added in the environmentally friendly pearly-lustre mill base3And CaTiO3Mixture,
Wherein, γ-FeO (OH), FeCO3And CaTiO3Adding proportion be 3:1:1.
Wherein, 3 parts of antifoaming agent is also added in the environmentally friendly pearly-lustre mill base, wherein, antifoaming agent is dodecyl sodium sulfonate
The mixture of salt and lauryl sulfate, wherein, the ratio of dodecane sulfonate and lauryl sulfate is 2:3.
Embodiment 2
Refering to Figure 1, the technical solution adopted by the present invention is：A kind of environmental protection pearly-lustre mill base, the environmental protection pearly-lustre color
Slurry includes following raw material：60 parts of pearlite slurry, 26 parts of pigment, 16 parts of stearic acid, 6 parts of zinc stearate, 5 parts of mould inhibitor, glycerine
25 parts, 40 parts of deionized water, 14 parts of stearic acid diethylene glycol dilaurate, 8 parts of hydroxyethyl cellulose, 20 parts of talcum powder, 12 parts of styrax
With 10 parts of silica gel.
Wherein, the environmentally friendly pearly-lustre mill base is also added with 2 parts of environmentally friendly color paste stabilizer.
Wherein, the environmentally friendly color paste stabilizer include 35% organic tin stabilizer, 35% organic antimony stabilizer and
30% organic zinc stabilizer.
Wherein, 2 parts of γ-FeO (OH), FeCO are also added in the environmentally friendly pearly-lustre mill base3And CaTiO3Mixture,
Wherein, γ-FeO (OH), FeCO3And CaTiO3Adding proportion be 2:1:2.
Wherein, 5 parts of antifoaming agent is also added in the environmentally friendly pearly-lustre mill base, wherein, antifoaming agent is dodecyl sodium sulfonate
The mixture of salt and lauryl sulfate, wherein, the ratio of dodecane sulfonate and lauryl sulfate is 3:4.
Embodiment 3
Refering to Figure 1, the technical solution adopted by the present invention is：A kind of environmental protection pearly-lustre mill base, the environmental protection pearly-lustre color
Slurry includes following raw material：68 parts of pearlite slurry, 25 parts of pigment, 15 parts of stearic acid, 8 parts of zinc stearate, 3 parts of mould inhibitor, glycerine
27 parts, 35 parts of deionized water, 16 parts of stearic acid diethylene glycol dilaurate, 6 parts of hydroxyethyl cellulose, 24 parts of talcum powder, 11 parts of styrax
With 15 parts of silica gel.
Wherein, the environmentally friendly pearly-lustre mill base is also added with 1 part of environmentally friendly color paste stabilizer.
Wherein, the environmentally friendly color paste stabilizer include 30% organic tin stabilizer, 40% organic antimony stabilizer and
30% organic zinc stabilizer.
Wherein, 2 parts of γ-FeO (OH), FeCO are also added in the environmentally friendly pearly-lustre mill base3And CaTiO3Mixture,
Wherein, γ-FeO (OH), FeCO3And CaTiO3Adding proportion be 1:1:2.
Wherein, 3 parts of antifoaming agent is also added in the environmentally friendly pearly-lustre mill base, wherein, antifoaming agent is dodecyl sodium sulfonate
The mixture of salt and lauryl sulfate, wherein, the ratio of dodecane sulfonate and lauryl sulfate is 2:5.
Embodiment 4
Refering to Figure 1, the technical solution adopted by the present invention is：A kind of environmental protection pearly-lustre mill base, the environmental protection pearly-lustre color
Slurry includes following raw material：55 parts of pearlite slurry, 28 parts of pigment, 15 parts of stearic acid, 8 parts of zinc stearate, 3 parts of mould inhibitor, glycerine
27 parts, 35 parts of deionized water, 16 parts of stearic acid diethylene glycol dilaurate, 6 parts of hydroxyethyl cellulose, 24 parts of talcum powder, 11 parts of styrax
With 15 parts of silica gel.
Wherein, the environmentally friendly pearly-lustre mill base is also added with 1 part of environmentally friendly color paste stabilizer.
Wherein, the environmentally friendly color paste stabilizer include 40% organic tin stabilizer, 40% organic antimony stabilizer and
20% organic zinc stabilizer.
Wherein, 2 parts of γ-FeO (OH), FeCO are also added in the environmentally friendly pearly-lustre mill base3And CaTiO3Mixture,
Wherein, γ-FeO (OH), FeCO3And CaTiO3Adding proportion be 1:1:2.
Wherein, 5 parts of antifoaming agent is also added in the environmentally friendly pearly-lustre mill base, wherein, antifoaming agent is dodecyl sodium sulfonate
The mixture of salt and lauryl sulfate, wherein, the ratio of dodecane sulfonate and lauryl sulfate is 3:3.
Embodiment 5
Refering to Figure 1, the technical solution adopted by the present invention is：A kind of environmental protection pearly-lustre mill base, the environmental protection pearly-lustre color
Slurry includes following raw material：55 parts of pearlite slurry, 25 parts of pigment, 15 parts of stearic acid, 5 parts of zinc stearate, 3 parts of mould inhibitor, glycerine
21 parts, 35 parts of deionized water, 12 parts of stearic acid diethylene glycol dilaurate, 6 parts of hydroxyethyl cellulose, 18 parts of talcum powder, 11 parts of styrax
With 9 parts of silica gel.
Wherein, the environmentally friendly pearly-lustre mill base is also added with 1 part of environmentally friendly color paste stabilizer.
Wherein, the environmentally friendly color paste stabilizer include 30% organic tin stabilizer, 40% organic antimony stabilizer and
30% organic zinc stabilizer.
Wherein, 1 part of γ-FeO (OH), FeCO are also added in the environmentally friendly pearly-lustre mill base3And CaTiO3Mixture,
Wherein, γ-FeO (OH), FeCO3And CaTiO3Adding proportion be 1:1:1.
Wherein, 4 parts of antifoaming agent is also added in the environmentally friendly pearly-lustre mill base, wherein, antifoaming agent is dodecyl sodium sulfonate
The mixture of salt and lauryl sulfate, wherein, the ratio of dodecane sulfonate and lauryl sulfate is 2:3.
Embodiment 6
Refering to Figure 1, the technical solution adopted by the present invention is：A kind of environmental protection pearly-lustre mill base, the environmental protection pearly-lustre color
Slurry includes following raw material：68 parts of pearlite slurry, 28 parts of pigment, 18 parts of stearic acid, 8 parts of zinc stearate, 7 parts of mould inhibitor, glycerine
27 parts, 45 parts of deionized water, 16 parts of stearic acid diethylene glycol dilaurate, 11 parts of hydroxyethyl cellulose, 24 parts of talcum powder, 14 parts of styrax
With 15 parts of silica gel.
Wherein, the environmentally friendly pearly-lustre mill base is also added with 3 parts of environmentally friendly color paste stabilizer.
Wherein, the environmentally friendly color paste stabilizer include 40% organic tin stabilizer, 30% organic antimony stabilizer and
30% organic zinc stabilizer.
Wherein, 2 parts of γ-FeO (OH), FeCO are also added in the environmentally friendly pearly-lustre mill base3And CaTiO3Mixture,
Wherein, γ-FeO (OH), FeCO3And CaTiO3Adding proportion be 3:1:2.
Wherein, 4 parts of antifoaming agent is also added in the environmentally friendly pearly-lustre mill base, wherein, antifoaming agent is dodecyl sodium sulfonate
The mixture of salt and lauryl sulfate, wherein, the ratio of dodecane sulfonate and lauryl sulfate is 3:5.
Refering to Figure 1, the technical solution adopted by the present invention is：A kind of environmental protection pearly-lustre mill base, the environmental protection pearly-lustre color
The manufacturing method of slurry is：
1) is ground：Whole zinc stearate, stearic acid diethylene glycol dilaurate, hydroxyethyl cellulose, talcum powder and silica gel are turned
Enter into three-roll grinder and rough lapping 4 times is carried out with the grinding rate of 90r/min, obtain effective nominal diameter no more than 0.5cm
Uniformly mixed particle；
2) mixes colours：35% antifoaming agent, pearlite slurry, pigment and glycerine are dissolved in deionized water, use homogenizer
It is stirred with the stir speed (S.S.) of 2800r/min so that pearlite slurry is uniformly mixed completely with glycerine, pigment and deionized water, system
Obtain color uniformly thick pearly-lustre mill base；
3) disperses：The ground hybrid particles of step 1 are transferred in dispersion machine, are added in while being dispersed with stirring
Thick pearly-lustre mill base made from step 2 after thick pearly-lustre mill base is added completely into, adds remaining antifoaming agent, stearic acid, mould proof
Agent, styrax, environmentally friendly color paste stabilizer, γ-FeO (OH), FeCO3And CaTiO3Dispersion stirring 5h is carried out, list is transferred to after dispersion
Thick stick formula circulation horizontal grinder is ground；
4) is ground again：The scattered material of step 3 is put into horizontal bar type circulation horizontal grinder, with 120r/min
Grinding rate grind 4 times, be ground to the grain size of mill base internal particle as 8nm, obtain environmentally friendly pearly-lustre mill base.
In the present invention, the environmentally friendly pearly-lustre mill base of the present invention carries out scientific and reasonable proportioning using Novel environment-friendlymaterial material, will be normal
The raw material for advising Environmental Safety is used in formula, and environmental protection pearly-lustre mill base safety obtained is good, and uniform coloring is easy to use, economical
Property it is good, manufacture at low cost, the potentiality having had, environmentally protective few harm meets polycyclic aromatic hydrocarbons (PAH) inspection specification, do not detect polycyclic
Aromatic hydrocarbon, meets Environmental Safety requirement, and present invention environmental protection pearly-lustre mill base is widely used in medical treatment, health, coating, machine and food etc.
Field.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
Understanding without departing from the principles and spirit of the present invention can carry out these embodiments a variety of variations, modification, replace
And modification, the scope of the present invention is defined by the appended.
Claims (6)
1. a kind of environmental protection pearly-lustre mill base, it is characterised in that：The environmental protection pearly-lustre mill base includes following raw material：Pearlite slurry 55~
68 parts, 25~28 parts of pigment, 15~18 parts of stearic acid, 5~8 parts of zinc stearate, 3~7 parts of mould inhibitor, 21~27 parts of glycerine, go
35~45 parts of ionized water, 12~16 parts of stearic acid diethylene glycol dilaurate, 6~11 parts of hydroxyethyl cellulose, 18~24 parts of talcum powder, peace
Breath fragrant 11~14 parts and 9~15 parts of silica gel.
2. a kind of environmentally friendly pearly-lustre mill base according to claim 1, it is characterised in that：The environmental protection pearly-lustre mill base is also added with
1~3 part of environmentally friendly color paste stabilizer.
3. a kind of environmentally friendly pearly-lustre mill base according to claim 2, it is characterised in that：The environmental protection color paste stabilizer includes
30~40% organic tin stabilizer, 20~40% organic antimony stabilizers and 10~30% organic zinc stabilizer.
4. a kind of environmentally friendly pearly-lustre mill base according to claim 1, it is characterised in that：It is also added in the environmental protection pearly-lustre mill base
There are 1~2 part of γ-FeO (OH), FeCO3And CaTiO3Mixture, wherein, γ-FeO (OH), FeCO3And CaTiO3Addition
Ratio is 1~3:1:1~2.
5. a kind of environmentally friendly pearly-lustre mill base according to claim 1, it is characterised in that：It is also added in the environmental protection pearly-lustre mill base
There is 3~5 parts of antifoaming agent, wherein, antifoaming agent is the mixture of dodecane sulfonate and lauryl sulfate, wherein, ten
The ratio of dialkyl group sulfonate and lauryl sulfate is 2~3:3~5.
6. a kind of environmentally friendly pearly-lustre mill base according to claim 1, it is characterised in that：The manufacturer of the environmental protection pearly-lustre mill base
Method is：
1) is ground：Whole zinc stearate, stearic acid diethylene glycol dilaurate, hydroxyethyl cellulose, talcum powder and silica gel are transferred to
Rough lapping 3~5 times is carried out with the grinding rate of 60~100r/min in three-roll grinder, effective nominal diameter is obtained and is no more than
The uniformly mixed particle of 0.5cm；
2) mixes colours：30~40% antifoaming agent, pearlite slurry, pigment and glycerine are dissolved in deionized water, use homogenizer
It is stirred with the stir speed (S.S.) of 2500~3000r/min so that pearlite slurry mixes completely with glycerine, pigment and deionized water
It is even, color uniformly thick pearly-lustre mill base is made；
3) disperses：The ground hybrid particles of step 1 are transferred in dispersion machine, step 2 is added in while being dispersed with stirring
Thick pearly-lustre mill base obtained after thick pearly-lustre mill base is added completely into, adds remaining antifoaming agent, stearic acid, mould inhibitor, rests in peace
Fragrant, environmentally friendly color paste stabilizer, γ-FeO (OH), FeCO3And CaTiO3Dispersion 3~6h of stirring is carried out, horizontal bar type is transferred to after dispersion
Circulation horizontal grinder is ground；
4) is ground again：The scattered material of step 3 is put into horizontal bar type circulation horizontal grinder, with 100~150r/min
Grinding rate grind 3~5 times, be ground to the grain size of mill base internal particle as 6~10nm, obtain environmentally friendly pearly-lustre mill base.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201711222710.9A CN108219594A (en) | 2017-11-29 | 2017-11-29 | A kind of environmental protection pearly-lustre mill base |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201711222710.9A CN108219594A (en) | 2017-11-29 | 2017-11-29 | A kind of environmental protection pearly-lustre mill base |
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| CN108219594A true CN108219594A (en) | 2018-06-29 |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110862717A (en) * | 2019-11-19 | 2020-03-06 | 江西三越新材料有限公司 | Preparation method of novel environment-friendly color paste |
| CN111393914A (en) * | 2020-05-25 | 2020-07-10 | 苏州德加画材科技有限公司 | Environment-friendly pearlescent water-based color paste and preparation method thereof |
| CN114231146A (en) * | 2021-12-22 | 2022-03-25 | 广东溢达纺织有限公司 | Impregnation slurry, impregnation rope end and preparation method thereof |
| CN117247701A (en) * | 2023-04-04 | 2023-12-19 | 广州思奇高分子材料技术有限公司 | UV-resistant silica gel paste and preparation method thereof |
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| CN105400297A (en) * | 2015-12-25 | 2016-03-16 | 上海金狮化工有限公司 | Color paste and preparation method thereof |
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| CN105400297A (en) * | 2015-12-25 | 2016-03-16 | 上海金狮化工有限公司 | Color paste and preparation method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110862717A (en) * | 2019-11-19 | 2020-03-06 | 江西三越新材料有限公司 | Preparation method of novel environment-friendly color paste |
| CN111393914A (en) * | 2020-05-25 | 2020-07-10 | 苏州德加画材科技有限公司 | Environment-friendly pearlescent water-based color paste and preparation method thereof |
| CN114231146A (en) * | 2021-12-22 | 2022-03-25 | 广东溢达纺织有限公司 | Impregnation slurry, impregnation rope end and preparation method thereof |
| CN117247701A (en) * | 2023-04-04 | 2023-12-19 | 广州思奇高分子材料技术有限公司 | UV-resistant silica gel paste and preparation method thereof |
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Application publication date: 20180629 |