CN108212068A - Bundle pipe type reaction module in butanone oximino silane crosslinking agent continuous flow procedure - Google Patents
Bundle pipe type reaction module in butanone oximino silane crosslinking agent continuous flow procedure Download PDFInfo
- Publication number
- CN108212068A CN108212068A CN201810138621.4A CN201810138621A CN108212068A CN 108212068 A CN108212068 A CN 108212068A CN 201810138621 A CN201810138621 A CN 201810138621A CN 108212068 A CN108212068 A CN 108212068A
- Authority
- CN
- China
- Prior art keywords
- cooling water
- main body
- material main
- pipe type
- reducing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 238000006243 chemical reaction Methods 0.000 title claims abstract description 51
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 title claims abstract description 26
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 title claims abstract description 13
- 239000003431 cross linking reagent Substances 0.000 title claims abstract description 13
- 125000005646 oximino group Chemical group 0.000 title claims abstract description 13
- 229910000077 silane Inorganic materials 0.000 title claims abstract description 13
- 238000000034 method Methods 0.000 title claims abstract description 12
- 239000000498 cooling water Substances 0.000 claims abstract description 57
- 239000000463 material Substances 0.000 claims abstract description 33
- 230000008602 contraction Effects 0.000 claims abstract description 13
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims abstract description 4
- 229910052802 copper Inorganic materials 0.000 claims abstract description 4
- 239000010949 copper Substances 0.000 claims abstract description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 2
- 238000010924 continuous production Methods 0.000 abstract description 3
- 230000035484 reaction time Effects 0.000 abstract description 3
- 238000005516 engineering process Methods 0.000 description 3
- 238000007599 discharging Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 230000008859 change Effects 0.000 description 1
- 238000012824 chemical production Methods 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 230000036632 reaction speed Effects 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/0013—Controlling the temperature of the process
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/24—Stationary reactors without moving elements inside
- B01J19/2405—Stationary reactors without moving elements inside provoking a turbulent flow of the reactants, such as in cyclones, or having a high Reynolds-number
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/24—Stationary reactors without moving elements inside
- B01J19/2415—Tubular reactors
- B01J19/242—Tubular reactors in series
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/02—Silicon compounds
- C07F7/08—Compounds having one or more C—Si linkages
- C07F7/0834—Compounds having one or more O-Si linkage
- C07F7/0892—Compounds with a Si-O-N linkage
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
- B01J2219/00092—Tubes
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Silicon Polymers (AREA)
Abstract
Bundle pipe type reaction module in butanone oximino silane crosslinking agent continuous flow procedure, including cooling water distributor box, cooling water pipe, material main body, reducing materail tube, cooling water collection box, one side of material main body is equipped with cooling water distributor box, described material main body the other side is equipped with cooling water collection box, the cooling water distributor box is equipped with cooling water inlet, the cooling water distributor box is connect with cooling water pipe end, reducing materail tube is axially arranged in the material main body, the reducing materail tube has expansion segment and contraction section, cooling water pipe is additionally provided in the material main body；The cooling water collection box is connect with cooling water pipe end, and groove is equipped at the top of the material main body, and the material main body bottom is equipped with plush copper.The present invention is suitable for that the reaction time is shorter or the violent reaction of reaction, temperature-controllable, securely and reliably.For intermittent reaction process to be transformed, reaction efficiency is improved, realizes continuous production.
Description
Technical field
The present invention relates in technical field of chemical production equipment, particularly butanone oximino silane crosslinking agent continuous flow procedure
Bundle pipe type reaction module.
Background technology
The tank reactor of intermittently operated, be all reactants are primary before operation add in, with the progress of reaction,
Temperature in the kettle, concentration and reaction speed all change over time, always until scheduled conversion ratio discharging is reached.At present,
Batch still when its is simple in structure, easy to operate, flexibility is big by extensive use, but the charging of batch still, discharging, inspection
And non-cutting time needed for cleaning equipment etc. is long, causes labor intensity high, low production efficiency, therefore is badly in need of researching and developing a kind of bundle pipe type
Reaction module is insufficient to solve the prior art.
Invention content
The purpose of the present invention is in view of the shortcomings of the prior art, providing in butanone oximino silane crosslinking agent continuous flow procedure
Bundle pipe type reaction module, to solve the problems, such as above-mentioned background technology.
To solve prior art problem, the technical solution adopted by the present invention is:A kind of butanone oximino silane crosslinking agent is continuous
Bundle pipe type reaction module in production process, including cooling water distributor box, cooling water pipe, material main body, reducing materail tube, cold
But water collector, one side of material main body are equipped with cooling water distributor box, and described material main body the other side is equipped with cooling water
Collector, the cooling water distributor box are equipped with cooling water inlet, and the cooling water distributor box is connect with cooling water pipe end, institute
It states and reducing materail tube is axially arranged in material main body, the reducing materail tube has expansion segment and contraction section, the material main body
Inside it is additionally provided with cooling water pipe；The cooling water collection box is connect with cooling water pipe end, and groove is equipped at the top of the material main body,
The material main body bottom is equipped with plush copper.
Preferably, the reducing materail tube expansion segment diameter 6~40mm, 3~20mm of the contraction section diameter, the receipts
10~1000mm of contracting segment length；
Preferably, a diameter of 8~12mm of reducing materail tube expansion segment；The reducing materail tube contraction section a diameter of 4~
6mm, the contraction segment length is 200~500mm.
Collect preferably, the bundle pipe type reaction module is formed after connecting up and down with other bundle pipe type reaction module
Beam tube type reaction module combination application.
Another embodiment, bundle pipe type reaction module include upper perforated plate, lower perforated plate, reducing materail tube, housing, institute
Case top is stated equipped with upper perforated plate, the housing bottom is equipped with lower perforated plate, and the housing side is equipped with cooling water inlet, the shell
Body the other side is equipped with cooling water outlet.
The present invention is suitable for that the reaction time is shorter or the violent reaction of reaction, temperature-controllable, securely and reliably.For between transformation
Having a rest property reaction process improves reaction efficiency, realizes continuous production.The present invention is equipped with unified concave-convex seal groove, for two
Or multiple bundle pipe type reaction module extension connections, ensure material residence time in reaction tube.
Description of the drawings
Fig. 1 is the structure diagram of the present invention；
Fig. 2 is another embodiment of the invention.
Specific embodiment
For the ease of understanding the present invention, the present invention is described more fully below with reference to relevant drawings.In attached drawing
Give the present invention preferred embodiment.But the present invention can realize in different forms, however it is not limited to be retouched herein
The embodiment stated.Opposite, the purpose for providing these embodiments is made to the disclosure more thorough and comprehensive.
As shown in Figure 1, the bundle pipe type reaction module in butanone oximino silane crosslinking agent continuous flow procedure, including cooling
Water distributor box 1, cooling water pipe 2, material main body 3, reducing materail tube 4, cooling water collection box 5,3 one side of material main body are set
There is cooling water distributor box 1, described 3 the other side of material main body is equipped with cooling water collection box 5, and the cooling water distributor box is equipped with
Cooling water inlet 6, the cooling water distributor box are connect with 2 end of cooling water pipe, are set in the material main body equipped with more transverse directions
The cooling water pipe put for taking away the heat that reaction generates, makes reaction temperature be constant at design value.It is axial in the material main body
Equipped with multiple reducing materail tubes 4, the reducing materail tube is equipped with expansion segment 8 and contraction section 9, and diameter 6 at the expansion segment~
40mm, preferred a diameter of 8~12mm.3~20mm of diameter at the contraction section, preferred a diameter of 4~6mm.The contraction
10~1000mm of segment length, preferred segment length of shrinking is 200~500mm.4 local diameter of reducing materail tube becomes smaller, and is formed and become
Diameter channel, material form fierce turbulent flow herein, convenient for mixing rapidly.Cooling water collection box is connect with cooling water pipe end, cooling
Water collector is equipped with cooling water outlet 10.Groove 7 is equipped at the top of the material main body, the material main body bottom is equipped with plush copper
11。
As shown in Fig. 2, another embodiment of the present invention, in butanone oximino silane crosslinking agent continuous flow procedure
Bundle pipe type reaction module, including upper perforated plate 11, lower perforated plate 12, reducing materail tube 4, housing 13, the case top is equipped with upper
Tube sheet 11, the housing bottom are equipped with lower perforated plate 13, and the housing side is equipped with cooling water inlet 6, described housing the other side
Equipped with cooling water outlet 10.
Its operation principle is：Two strands of materials enter from 4 opening of reducing materail tube to be formed fierce turbulent flow and mixes rapidly herein
Merge reaction；Heat of reaction is transferred to rapidly cooling water pipe, and take bundle pipes out of by cooling water in cooling water pipe by material main body
Formula reaction module, so as to ensure reaction temperature stabilization in control range；The bundle pipe type reaction module is suitable for the reaction time
Reaction shorter or that reaction is violent, temperature-controllable, securely and reliably.For intermittent reaction process to be transformed, reaction efficiency is improved, in fact
Existing continuous production.
Bundle pipe type reaction module is equipped with unified concave-convex seal groove, expands for two or more bundle pipe type reaction modules
Exhibition connection, ensures material residence time in reaction tube.On bundle pipe type reaction module and other bundle pipe type reaction module
Bundle pipe type reaction module combination application is formed after lower series connection
Embodiment of the present invention is only the description carried out to the preferred embodiment of the present invention, not to present inventive concept
It is defined with range, under the premise of not departing from the present invention relates to thought, engineers and technicians are to the present invention's in this field
The various modifications and improvement that technical solution is made, should all fall into protection scope of the present invention, in the claimed technology of the present invention
With whole records are in detail in the claims.
Claims (5)
1. the bundle pipe type reaction module in butanone oximino silane crosslinking agent continuous flow procedure, including cooling water distributor box, cold
But water pipe, material main body, reducing materail tube, cooling water collection box, one side of material main body are equipped with cooling water distributor box, institute
Material main body the other side is stated equipped with cooling water collection box, the cooling water distributor box is equipped with cooling water inlet, the cooling
Water distributor box is connect with cooling water pipe end, and reducing materail tube, the reducing materail tube tool are axially arranged in the material main body
There are expansion segment and contraction section, cooling water pipe is additionally provided in the material main body；The cooling water collection box and cooling water pipe end
Connection, the material main body top are equipped with groove, and the material main body bottom is equipped with plush copper.
2. the bundle pipe type reaction module in butanone oximino silane crosslinking agent continuous flow procedure according to claim 1,
It is characterized in that 6~40mm of the reducing materail tube expansion segment diameter, 3~20mm of the contraction section diameter, the contraction segment length
Spend 10~1000mm.
3. the bundle pipe type reaction mould in butanone oximino silane crosslinking agent continuous flow procedure according to claim 1 or 2
Block, it is characterised in that a diameter of 8~12mm of reducing materail tube expansion segment；The reducing materail tube contraction section a diameter of 4~
6mm, the contraction segment length is 200~500mm.
4. the bundle pipe type reaction module in butanone oximino silane crosslinking agent continuous flow procedure according to claim 1,
It is characterized in that the bundle pipe type reaction module forms bundle pipe type after connecting up and down with other bundle pipe type reaction module
Reaction module combination application.
5. the bundle pipe type reaction module in butanone oximino silane crosslinking agent continuous flow procedure according to claim 1,
Another embodiment includes upper perforated plate, lower perforated plate, reducing materail tube, housing, the housing for bundle pipe type reaction module
Top is equipped with upper perforated plate, and the housing bottom is equipped with lower perforated plate, and the housing side is equipped with cooling water inlet, and the housing is another
Side is equipped with cooling water outlet.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810138621.4A CN108212068A (en) | 2018-02-10 | 2018-02-10 | Bundle pipe type reaction module in butanone oximino silane crosslinking agent continuous flow procedure |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810138621.4A CN108212068A (en) | 2018-02-10 | 2018-02-10 | Bundle pipe type reaction module in butanone oximino silane crosslinking agent continuous flow procedure |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108212068A true CN108212068A (en) | 2018-06-29 |
Family
ID=62661543
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810138621.4A Withdrawn CN108212068A (en) | 2018-02-10 | 2018-02-10 | Bundle pipe type reaction module in butanone oximino silane crosslinking agent continuous flow procedure |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108212068A (en) |
-
2018
- 2018-02-10 CN CN201810138621.4A patent/CN108212068A/en not_active Withdrawn
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20180629 |
|
| WW01 | Invention patent application withdrawn after publication |