CN208213185U - Bundle pipe type reaction module in butanone oximino silane crosslinking agent continuous production process - Google Patents

Bundle pipe type reaction module in butanone oximino silane crosslinking agent continuous production process Download PDF

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Publication number
CN208213185U
CN208213185U CN201820239218.6U CN201820239218U CN208213185U CN 208213185 U CN208213185 U CN 208213185U CN 201820239218 U CN201820239218 U CN 201820239218U CN 208213185 U CN208213185 U CN 208213185U
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China
Prior art keywords
cooling water
main body
material main
pipe type
reaction module
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CN201820239218.6U
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Inventor
曾曼华
尹述柏
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HUBEI XIANLIN CHEMICAL INDUSTRY Co Ltd
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HUBEI XIANLIN CHEMICAL INDUSTRY Co Ltd
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Abstract

Bundle pipe type reaction module in butanone oximino silane crosslinking agent continuous production process, including cooling water distributor box, cooling water pipe, material main body, variable diameter materail tube, cooling water collection box, one side of material main body is equipped with cooling water distributor box, described material main body the other side is equipped with cooling water collection box, the cooling water distributor box is equipped with cooling water inlet, the cooling water distributor box is connect with cooling water pipe end, variable diameter materail tube is axially arranged in the material main body, the variable diameter materail tube has expansion segment and contraction section, cooling water pipe is additionally provided in the material main body;The cooling water collection box is connect with cooling water pipe end, and groove is equipped at the top of the material main body, and the material main body bottom is equipped with plush copper.The utility model is suitable for that the reaction time is shorter or the violent reaction of reaction, temperature-controllable, securely and reliably.For intermittent reaction process to be transformed, reaction efficiency is improved, realizes continuous production.

Description

Bundle pipe type reaction module in butanone oximino silane crosslinking agent continuous production process
Technical field
The utility model relates to technical field of chemical production equipment, especially butanone oximino silane crosslinking agent continuous production mistake Bundle pipe type reaction module in journey.
Background technique
The tank reactor of intermittently operated, be all reactants are primary before operation be added, with the progress of reaction, Temperature in the kettle, concentration and reaction speed all change over time, always until being reached scheduled conversion ratio discharging.Currently, Batch still is widely applied because its structure is simple and convenient to operate, flexibility is big, but the charging of batch still, discharging, inspection And non-cutting time needed for cleaning equipment etc. is long, causes labor intensity high, production efficiency is low, therefore is badly in need of researching and developing a kind of bundle pipe type Reaction module is to solve prior art deficiency.
Utility model content
The purpose of this utility model is in view of the shortcomings of the prior art, providing butanone oximino silane crosslinking agent continuous production process In bundle pipe type reaction module, to solve the problems, such as above-mentioned background technique.
To solve prior art problem, the technical solution adopted in the utility model is: a kind of butanone oximino silane crosslinking agent Bundle pipe type reaction module in continuous production process, including cooling water distributor box, cooling water pipe, material main body, variable diameter material Pipe, cooling water collection box, one side of material main body are equipped with cooling water distributor box, and described material main body the other side is equipped with cold But water collector, the cooling water distributor box are equipped with cooling water inlet, and the cooling water distributor box and cooling water pipe end connect It connects, variable diameter materail tube is axially arranged in the material main body, the variable diameter materail tube has expansion segment and contraction section, the substrate Cooling water pipe is additionally provided in ontology;The cooling water collection box is connect with cooling water pipe end, is equipped at the top of the material main body Groove, the material main body bottom are equipped with plush copper.
Preferably, the variable diameter materail tube expansion segment diameter 6~40mm, 3~20mm of the contraction section diameter, the receipts 10~1000mm of contracting segment length;
Preferably, the variable diameter materail tube expansion segment diameter is 8~12mm;The variable diameter materail tube contraction section diameter is 4~6mm, the contraction segment length are 200~500mm.
Collect preferably, the bundle pipe type reaction module is constituted after connecting up and down with other bundle pipe type reaction module Beam tube type reaction module combined application.
Another embodiment, bundle pipe type reaction module include upper perforated plate, lower perforated plate, variable diameter materail tube, shell, institute Case top is stated equipped with upper perforated plate, the housing bottom is equipped with lower perforated plate, and the shell side is equipped with cooling water inlet, the shell Body the other side is equipped with cooling water outlet.
The utility model is suitable for that the reaction time is shorter or the violent reaction of reaction, temperature-controllable, securely and reliably.For changing Intermittent reaction process is made, reaction efficiency is improved, realizes continuous production.The utility model is equipped with unified concave-convex seal groove, It extends and connects for two or more bundle pipe type reaction modules, guarantee material residence time in reaction tube.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of the utility model;
Fig. 2 is another embodiment of the utility model.
Specific embodiment
The utility model is more fully retouched below with reference to relevant drawings for the ease of understanding the utility model, It states.The preferred embodiment of the utility model is given in attached drawing.But the utility model can be realized in different forms, It is not limited to the examples described herein.Opposite, purpose of providing these embodiments is makes disclosure to the utility model Content is more thorough and comprehensive.
As shown in Figure 1, the bundle pipe type reaction module in butanone oximino silane crosslinking agent continuous production process, including cooling Water distributor box 1, cooling water pipe 2, material main body 3, variable diameter materail tube 4, cooling water collection box 5,3 one side of material main body are set There is cooling water distributor box 1, described 3 the other side of material main body is equipped with cooling water collection box 5, and the cooling water distributor box is equipped with Cooling water inlet 6, the cooling water distributor box are connect with 2 end of cooling water pipe, and more transverse directions are equipped in the material main body and are set The cooling water pipe set, the heat generated for taking away reaction, makes reaction temperature be constant at design value.It is axial in the material main body Equipped with multiple variable diameter materail tubes 4, the variable diameter materail tube is equipped with expansion segment 8 and contraction section 9, and diameter 6 at the expansion segment~ 40mm, preferred diameter are 8~12mm.3~20mm of diameter at the contraction section, preferred diameter are 4~6mm.The contraction 10~1000mm of segment length, preferred segment length of shrinking is 200~500mm.4 local diameter of variable diameter materail tube becomes smaller, and is formed and is become Diameter channel, material form fierce turbulent flow herein, convenient for mixing rapidly.Cooling water collection box is connect with cooling water pipe end, cooling Water collector is equipped with cooling water outlet 10.Groove 7 is equipped at the top of the material main body, the material main body bottom is equipped with plush copper 11。
As shown in Fig. 2, another embodiment of the utility model, butanone oximino silane crosslinking agent continuous production process In bundle pipe type reaction module, including upper perforated plate 11, lower perforated plate 12, variable diameter materail tube 4, shell 13, the case top set There is upper perforated plate 11, the housing bottom is equipped with lower perforated plate 13, and the shell side is equipped with cooling water inlet 6, and the shell is another Side is equipped with cooling water outlet 10.
Its working principle is that: two strands of materials enter from 4 opening of variable diameter materail tube to be formed fierce turbulent flow herein and mixes rapidly Merge reaction;Heat of reaction is transferred to rapidly cooling water pipe by material main body, and takes bundle pipes out of by cooling water in cooling water pipe Formula reaction module, to guarantee that reaction temperature is stablized in control range;The bundle pipe type reaction module is suitable for the reaction time Reaction shorter or that reaction is violent, temperature-controllable, securely and reliably.For intermittent reaction process to be transformed, reaction efficiency is improved, in fact Existing continuous production.
Bundle pipe type reaction module is equipped with unified concave-convex seal groove, expands for two or more bundle pipe type reaction modules Exhibition connection, guarantees material residence time in reaction tube.On bundle pipe type reaction module and other bundle pipe type reaction module Bundle pipe type reaction module combined application is constituted after lower series connection
Embodiment described in the utility model is only the description carried out to preferred embodiments of the present invention, not The utility model conception and scope is defined, not departing from the utility model relates under the premise of thought, work in this field The various changes and improvements that journey technical staff makes the technical solution of the utility model should all fall into the protection of the utility model Range, the claimed technology of the utility model is interior to be used, and is all described in the claims.

Claims (5)

1. the bundle pipe type reaction module in butanone oximino silane crosslinking agent continuous production process, including it is cooling water distributor box, cold But water pipe, material main body, variable diameter materail tube, cooling water collection box, one side of material main body are equipped with cooling water distributor box, institute Material main body the other side is stated equipped with cooling water collection box, the cooling water distributor box is equipped with cooling water inlet, the cooling Water distributor box is connect with cooling water pipe end, and variable diameter materail tube, the variable diameter materail tube tool are axially arranged in the material main body There are expansion segment and contraction section, is additionally provided with cooling water pipe in the material main body;The cooling water collection box and cooling water pipe end Connection, the material main body top are equipped with groove, and the material main body bottom is equipped with plush copper.
2. the bundle pipe type reaction module in butanone oximino silane crosslinking agent continuous production process according to claim 1, It is characterized in that 6~40mm of the variable diameter materail tube expansion segment diameter, 3~20mm of the contraction section diameter, the contraction segment length Spend 10~1000mm.
3. the bundle pipe type in butanone oximino silane crosslinking agent continuous production process according to claim 1 or 2 reacts mould Block, it is characterised in that the variable diameter materail tube expansion segment diameter is 8~12mm;The variable diameter materail tube contraction section diameter be 4~ 6mm, the contraction segment length are 200~500mm.
4. the bundle pipe type reaction module in butanone oximino silane crosslinking agent continuous production process according to claim 1, It is characterized in that the bundle pipe type reaction module constitutes bundle pipe type after connecting up and down with other bundle pipe type reaction module Reaction module combined application.
5. the bundle pipe type reaction module in butanone oximino silane crosslinking agent continuous production process according to claim 1, Another embodiment is that bundle pipe type reaction module includes upper perforated plate, lower perforated plate, variable diameter materail tube, shell, the shell Top is equipped with upper perforated plate, and the housing bottom is equipped with lower perforated plate, and the shell side is equipped with cooling water inlet, and the shell is another Side is equipped with cooling water outlet.
CN201820239218.6U 2018-02-10 2018-02-10 Bundle pipe type reaction module in butanone oximino silane crosslinking agent continuous production process Active CN208213185U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201820239218.6U CN208213185U (en) 2018-02-10 2018-02-10 Bundle pipe type reaction module in butanone oximino silane crosslinking agent continuous production process

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201820239218.6U CN208213185U (en) 2018-02-10 2018-02-10 Bundle pipe type reaction module in butanone oximino silane crosslinking agent continuous production process

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CN208213185U true CN208213185U (en) 2018-12-11

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Country Status (1)

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Date Code Title Description
GR01 Patent grant
GR01 Patent grant
PE01 Entry into force of the registration of the contract for pledge of patent right
PE01 Entry into force of the registration of the contract for pledge of patent right

Denomination of utility model: Cluster tube reaction module in continuous production of butanone oxime silane crosslinker

Effective date of registration: 20220125

Granted publication date: 20181211

Pledgee: Bank of China Limited Xiantao branch

Pledgor: HUBEI XIANLIN CHEMICAL CO.,LTD.

Registration number: Y2022420000029