CN108208972A - Anti- PM2.5 active carbon masks - Google Patents

Anti- PM2.5 active carbon masks Download PDF

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Publication number
CN108208972A
CN108208972A CN201810010688.XA CN201810010688A CN108208972A CN 108208972 A CN108208972 A CN 108208972A CN 201810010688 A CN201810010688 A CN 201810010688A CN 108208972 A CN108208972 A CN 108208972A
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woven fabrics
active carbon
rotating speed
revs
spun
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CN201810010688.XA
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CN108208972B (en
Inventor
袁强
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Jiangsu Kangnuo Medical Devices Co.,Ltd.
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Xiantao Tripod Labour Protection Products Co Ltd
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    • AHUMAN NECESSITIES
    • A41WEARING APPAREL
    • A41DOUTERWEAR; PROTECTIVE GARMENTS; ACCESSORIES
    • A41D13/00Professional, industrial or sporting protective garments, e.g. surgeons' gowns or garments protecting against blows or punches
    • A41D13/05Professional, industrial or sporting protective garments, e.g. surgeons' gowns or garments protecting against blows or punches protecting only a particular body part
    • A41D13/11Protective face masks, e.g. for surgical use, or for use in foul atmospheres
    • A41D13/1192Protective face masks, e.g. for surgical use, or for use in foul atmospheres with antimicrobial agent

Abstract

The invention discloses a kind of anti-PM2.5 active carbon masks, the ear-hang button loop including filter disc, on the left of filter disc and the ear-hang button loop on the right side of filter disc, institute's filter disc include successively from inside to outside:First non-woven fabrics, filter paper, active carbon nonwoven fabric, the second non-woven fabrics.The anti-PM2.5 active carbon masks of the present invention, good permeability, light comfortable, hygienic environment-protecting, the activated carbon non-woven layer of cloth contained can in environment PM2.5, dust particle, sulfide, nitride, organic hydrocarbon compounds, metal ion and bacterium, the multiple isolation of harmful substances such as virus, harmful substance is removed, the air of clean safety is provided for human body.

Description

Anti- PM2.5 active carbon masks
Technical field
The present invention relates to a kind of anti-PM2.5 masks, more particularly to a kind of active carbon mask of anti-PM2.5.
Background technology
Mask be worn over nose and mouth for filter disengaging mouth and nose air, to reach the gas of blocking harmful, smell, winged Foam passes in and out the apparatus of wearer's mouth and nose, is mostly made with cloth or paper etc..PM2.5 is that diameter is less than or equal to 2.5 microns in air Pellet, PM2.5 contain pernicious gas and heavy metal substance, and PM2.5 is small and light, it is difficult to which natural subsidence is to ground On, long-term floating in air, and adsorbs a large amount of poisonous and harmful substances, thus very big to human health damage.Exploitation is a kind of It can effectively stop that the mask of PM2.5 has become a top priority.But traditional mask generally use multilayer gauze or nonwoven Cloth overlapping is fabricated to mask, mask covering mouth and nose during use, in order to reached molecule in air filtering or Either the number of plies of non-woven fabrics or increase gauze or non-woven fabrics when aerial dirt count is very big it is necessary to increase gauze Textile density, the permeability of such mask will reduce, in use, people can be allowed to breathe difficulty increase, feel bored, breathe out simultaneously Moisture row do not go out, people is allowed to feel very uncomfortable.The present invention has studied a kind of anti-PM2.5 mouthfuls containing activated carbon non-woven layer of cloth Cover, active carbon nonwoven fabric have good absorption property, and thickness is uniform, good permeability, free from extraneous odour, and carbon content is high, activated carbon Grain is not easily to fall off, and PM2.5, microorganism, virus etc. in air filtering were come by the good adsorptivity of activated carbon, prevents air dirty Dye endangers health.
The anti-PM2.5 active carbon masks of invention, good permeability, light comfortable, hygienic environment-protecting, the active carbon nonwoven fabric contained Layer can in environment PM2.5, dust particle, sulfide, nitride, organic hydrocarbon compounds, metal ion and bacterium, virus Etc. the multiple isolation of harmful substances, remove harmful substance, clean, safe air be provided for human body.
Invention content
The present invention provides anti-PM2.5 active carbon masks.The present invention adopts the following technical scheme that:
A kind of anti-PM2.5 active carbon masks, the ear-hang button loop including filter disc, on the left of filter disc and the ear on the right side of filter disc Button loop is hung, institute's filter disc includes successively from inside to outside:First non-woven fabrics, filter paper, active carbon nonwoven fabric, the second non-woven fabrics.
Heretofore described left side is close to the side of left ear when wearing mask, close to right when mask is is worn in the right side The side of ear;The inside is proximate to the side of wearer, and the outside refers to the side far from wearer.
A kind of anti-PM2.5 active carbon masks, which is characterized in that the ear-hang including filter disc, on the left of filter disc is fastened with a rope, string, etc. and is located at Ear-hang button loop on the right side of filter disc, institute's filter disc include successively from inside to outside:First non-woven fabrics, filter paper, third non-woven fabrics, activated carbon without Woven fabric, the second non-woven fabrics.
Preferably, first non-woven fabrics, the second non-woven fabrics be PP spun-bonded non-woven fabrics or PET non-woven fabrics, the filter paper For PP melt spraying non-woven fabrics.
Preferably, the third non-woven fabrics is PP spun-bonded non-woven fabrics or PET non-woven fabrics.
It is further preferred that first non-woven fabrics, the second non-woven fabrics, third non-woven fabrics are PP spun-bonded non-woven fabrics, specifically Using PP spun-bonded non-woven fabrics, the grammes per square metre of PP spun-bonded non-woven fabrics is 28g/m2, thickness 0.2-0.4mm.
It is further preferred that the grammes per square metre of the PP melt spraying non-woven fabrics is 50g/m2, level n 95, thickness 0.3-0.6mm.
It is further preferred that the active carbon nonwoven fabric is terylene active carbon nonwoven fabric, grammes per square metre 32g/m2, thickness is The mass ratio of 0.1-0.3mm, contained terylene and activated carbon is 13:3.
Preferably, the PM2.5 filter efficiencies of the anti-PM2.5 active carbon masks are >=98%.
A kind of anti-PM2.5 active carbon masks, the ear-hang button loop including filter disc, on the left of filter disc and the ear on the right side of filter disc Button loop is hung, institute's filter disc includes successively from inside to outside:First non-woven fabrics, filter paper, active carbon nonwoven fabric, the second non-woven fabrics, described One non-woven fabrics be PP spun-bonded non-woven fabrics, second non-woven fabrics be antibacterial PP spun-bonded non-woven fabrics, the antibacterial PP spun-bonded non-woven fabrics Processing method be:Antimicrobial fluid is uniformly sprayed on PP spun-bonded non-woven fabrics surface, antimicrobial fluid fountain height is 80-150g/m2, after sprinkling PP spun-bonded non-woven fabrics are 3-6 hours dry at 65-75 DEG C, obtain antibacterial PP spun-bonded non-woven fabrics.Preferably, the filter paper is PP Melt spraying non-woven fabrics, grammes per square metre 50g/m2, level n 95, thickness 0.3-0.6mm.Preferably, the grammes per square metre of PP spun-bonded non-woven fabrics is 28g/m2, thickness 0.2-0.4mm.Preferably, the active carbon nonwoven fabric be terylene active carbon nonwoven fabric, grammes per square metre 32g/m2, Thickness is 0.1-0.3mm, and the mass ratio of contained terylene and activated carbon is 13:3.
Preferably, the preparation method of the anti-PM2.5 active carbon masks is:By cutting out to obtain length as 17.5- 20.5cm, the first non-woven fabrics, filter paper, active carbon nonwoven fabric, the second non-woven fabrics that width is 9.5-11.5cm, by the first nonwoven Cloth, filter paper, active carbon nonwoven fabric, the second non-woven fabrics stack successively, are sutured at edge position, obtain filter disc, then suture The ear-hang button loop on the right side of ear-hang button loop and filter disc on the left of filter disc, obtains anti-PM2.5 active carbon masks.
Preferably, the preparation method of the antimicrobial fluid includes the following steps:(1) 45-65g tartaric acid is added to 900- 1000g mass fractions are in the ethanol water of 65-85%, 65-85g soybean proteins are added in, at 35-45 DEG C, with 150-300 Rev/min rotating speed stir 2-4 hour, the sodium-chloride water solution of 800-1000g mass fractions for 1.5-3% is added in, in 35-45 DEG C, stirred 30-50 minute with 150-300 revs/min of rotating speed, 15-18 DEG C of preservation 2-4 hours is placed in, then with 5000-8000 Rev/min rotating speed centrifuge 30-50 minute, take centrifugation after sediment, sediment is 6-8 hours dry at 40-50 DEG C, crushing 20-50 mesh sieve is crossed, obtains modified soybean protein;(2) 2-4g sodium alginates are added to 100-150g and are pre-heated to 65-75 DEG C Water in, stirred 30-50 minute with 200-300 revs/min of rotating speed at 65-75 DEG C, be cooled to 45-55 DEG C, addition 0.5- The soybean protein that 1.5g xanthans, 0.1-0.3g tartaric acid, 1.5-4.5g are modified, at 45-55 DEG C, with 200-500 revs/min Rotating speed stirs 35-55 minutes, adds in 1-3g calcium chloride, at 45-55 DEG C, with 200-500 revs/min of 35-55 points of rotating speed stirring Clock obtains antimicrobial fluid.
Preferably, the preparation method of the antimicrobial fluid includes the following steps:(1) 45-65g tartaric acid is added to 900- 1000g mass fractions are in the ethanol water of 65-85%, 65-85g soybean proteins are added in, at 35-45 DEG C, with 150-300 Rev/min rotating speed stir 2-4 hour, the sodium-chloride water solution of 800-1000g mass fractions for 1.5-3% is added in, in 35-45 DEG C, stirred 30-50 minute with 150-300 revs/min of rotating speed, 15-18 DEG C of preservation 2-4 hours is placed in, then with 5000-8000 Rev/min rotating speed centrifuge 30-50 minute, take centrifugation after sediment, sediment is 6-8 hours dry at 40-50 DEG C, crushing 20-50 mesh sieve is crossed, obtains modified soybean protein;(2) it is pomelo peel fresh 250-300g is small in 55-65 DEG C of dry 48-60 When, 500-800 mesh sieve is smashed it through, obtains shaddock peel powder, 2-4g sodium alginates are added to 100-150g is pre-heated to 65-75 DEG C water in, stirred 30-50 minute with 200-300 revs/min of rotating speed at 65-75 DEG C, addition 2-7g shaddock peel powders, in 65- 75 DEG C are stirred 120-150 minute with 200-500 revs/min of rotating speed, are cooled to 45-50 DEG C, addition 0.5-1.5g xanthans, The soybean protein that 0.1-0.3g tartaric acid, 1.5-4.5g are modified stirs 35- at 45-55 DEG C, with 200-500 revs/min of rotating speed 55 minutes, 1-3g calcium chloride, the antibacterial auxiliary agents of 0-0.06g are added in, 35- is stirred at 45-55 DEG C, with 200-500 revs/min of rotating speed 55 minutes, obtain antimicrobial fluid.
It is further preferred that the preparation method of the antimicrobial fluid includes the following steps:(1) 45g tartaric acid is added to 900g mass fractions are in 65% ethanol water, add in 65g soybean proteins, are stirred at 35 DEG C, with 150 revs/min of rotating speed It mixes 2 hours, adds in the sodium-chloride water solution that 800g mass fractions are 1.5%, 30 are stirred at 35 DEG C, with 150 revs/min of rotating speed Minute, it is placed in 15 DEG C and preserves 2 hours, then centrifuged 30 minutes with 5000 revs/min of rotating speed, take the sediment after centrifugation, it will Sediment is 6 hours dry at 40 DEG C, crushed 20 mesh sieve, obtains modified soybean protein;(2) the fresh pomelo peels of 250g are existed 55 DEG C of dryings 48 hours smash it through 500 mesh sieve, obtain shaddock peel powder, 2g sodium alginates are added to 100g is pre-heated to 65 DEG C water in, stirred 30 minutes with 200 revs/min of rotating speed at 65 DEG C, 5g shaddock peel powders added in, at 65 DEG C with 200 revs/min Rotating speed stir 120 minutes, be cooled to 45 DEG C, add in the soybean protein that 0.5g xanthans, 0.1g tartaric acid, 1.5g are modified, 45 DEG C, stirred 35 minutes with 200 revs/min of rotating speed, add in 1g calcium chloride, the antibacterial auxiliary agents of 0.03g, 45 DEG C, with 200 turns/ The rotating speed of minute stirs 35 minutes, obtains antimicrobial fluid.
The antibacterial auxiliary agent is nisin and/or tea polyphenols.
It is further preferred that it is 1 in mass ratio that the antibacterial auxiliary agent, which is nisin and tea polyphenols,:(3-5's) is mixed Close object.
The present invention also provides a kind of antibacterial PP spun-bonded non-woven fabrics, which is characterized in that the processing side of antibacterial PP spun-bonded non-woven fabrics Method is:Antimicrobial fluid is uniformly sprayed on PP spun-bonded non-woven fabrics surface, antimicrobial fluid fountain height is 80-150g/m2, by PP spunbonds after sprinkling Non-woven fabrics is 3-6 hours dry at 65-75 DEG C, obtains antibacterial PP spun-bonded non-woven fabrics.
Preferably, the grammes per square metre of PP spun-bonded non-woven fabrics is 28g/m2, thickness 0.2-0.4mm.
Preferably, the preparation method of the antimicrobial fluid includes the following steps:(1) 45-65g tartaric acid is added to 900- 1000g mass fractions are in the ethanol water of 65-85%, 65-85g soybean proteins are added in, at 35-45 DEG C, with 150-300 Rev/min rotating speed stir 2-4 hour, the sodium-chloride water solution of 800-1000g mass fractions for 1.5-3% is added in, in 35-45 DEG C, stirred 30-50 minute with 150-300 revs/min of rotating speed, 15-18 DEG C of preservation 2-4 hours is placed in, then with 5000-8000 Rev/min rotating speed centrifuge 30-50 minute, take centrifugation after sediment, sediment is 6-8 hours dry at 40-50 DEG C, crushing 20-50 mesh sieve is crossed, obtains modified soybean protein;(2) 2-4g sodium alginates are added to 100-150g and are pre-heated to 65-75 DEG C Water in, stirred 30-50 minute with 200-300 revs/min of rotating speed at 65-75 DEG C, be cooled to 45-55 DEG C, addition 0.5- The soybean protein that 1.5g xanthans, 0.1-0.3g tartaric acid, 1.5-4.5g are modified, at 45-55 DEG C, with 200-500 revs/min Rotating speed stirs 35-55 minutes, adds in 1-3g calcium chloride, at 45-55 DEG C, with 200-500 revs/min of 35-55 points of rotating speed stirring Clock obtains antimicrobial fluid.
Preferably, the preparation method of the antimicrobial fluid includes the following steps:(1) 45-65g tartaric acid is added to 900- 1000g mass fractions are in the ethanol water of 65-85%, 65-85g soybean proteins are added in, at 35-45 DEG C, with 150-300 Rev/min rotating speed stir 2-4 hour, the sodium-chloride water solution of 800-1000g mass fractions for 1.5-3% is added in, in 35-45 DEG C, stirred 30-50 minute with 150-300 revs/min of rotating speed, 15-18 DEG C of preservation 2-4 hours is placed in, then with 5000-8000 Rev/min rotating speed centrifuge 30-50 minute, take centrifugation after sediment, sediment is 6-8 hours dry at 40-50 DEG C, crushing 20-50 mesh sieve is crossed, obtains modified soybean protein;(2) it is pomelo peel fresh 250-300g is small in 55-65 DEG C of dry 48-60 When, 500-800 mesh sieve is smashed it through, obtains shaddock peel powder, 2-4g sodium alginates are added to 100-150g is pre-heated to 65-75 DEG C water in, stirred 30-50 minute with 200-300 revs/min of rotating speed at 65-75 DEG C, addition 2-7g shaddock peel powders, in 65- 75 DEG C are stirred 120-150 minute with 200-500 revs/min of rotating speed, are cooled to 45-50 DEG C, addition 0.5-1.5g xanthans, The soybean protein that 0.1-0.3g tartaric acid, 1.5-4.5g are modified stirs 35- at 45-55 DEG C, with 200-500 revs/min of rotating speed 55 minutes, 1-3g calcium chloride, the antibacterial auxiliary agents of 0-0.06g are added in, 35- is stirred at 45-55 DEG C, with 200-500 revs/min of rotating speed 55 minutes, obtain antimicrobial fluid.
It is further preferred that the preparation method of the antimicrobial fluid includes the following steps:(1) 45g tartaric acid is added to 900g mass fractions are in 65% ethanol water, add in 65g soybean proteins, are stirred at 35 DEG C, with 150 revs/min of rotating speed It mixes 2 hours, adds in the sodium-chloride water solution that 800g mass fractions are 1.5%, 30 are stirred at 35 DEG C, with 150 revs/min of rotating speed Minute, it is placed in 15 DEG C and preserves 2 hours, then centrifuged 30 minutes with 5000 revs/min of rotating speed, take the sediment after centrifugation, it will Sediment is 6 hours dry at 40 DEG C, crushed 20 mesh sieve, obtains modified soybean protein;(2) the fresh pomelo peels of 250g are existed 55 DEG C of dryings 48 hours smash it through 500 mesh sieve, obtain shaddock peel powder, 2g sodium alginates are added to 100g is pre-heated to 65 DEG C water in, stirred 30 minutes with 200 revs/min of rotating speed at 65 DEG C, 5g shaddock peel powders added in, at 65 DEG C with 200 revs/min Rotating speed stir 120 minutes, be cooled to 45 DEG C, add in the soybean protein that 0.5g xanthans, 0.1g tartaric acid, 1.5g are modified, 45 DEG C, stirred 35 minutes with 200 revs/min of rotating speed, add in 1g calcium chloride, the antibacterial auxiliary agents of 0.03g, 45 DEG C, with 200 turns/ The rotating speed of minute stirs 35 minutes, obtains antimicrobial fluid.
The antibacterial auxiliary agent is nisin and/or tea polyphenols.
It is further preferred that it is 1 in mass ratio that the antibacterial auxiliary agent, which is nisin and tea polyphenols,:(3-5's) is mixed Close object.
The present invention also provides application of the above-mentioned antibacterial PP spun-bonded non-woven fabrics in anti-PM2.5 active carbon masks.
The anti-PM2.5 active carbon masks of invention, good permeability, light comfortable, hygienic environment-protecting, the active carbon nonwoven fabric contained Layer can in environment PM2.5, dust particle, sulfide, nitride, organic hydrocarbon compounds, metal ion and bacterium, virus Etc. the multiple isolation of harmful substances, remove harmful substance, clean, safe air be provided for human body.
On the basis of common knowledge of the art, above-mentioned each optimum condition, can be each preferably to get the present invention in any combination Embodiment.
Specific embodiment
It is further illustrated the present invention below by the mode of embodiment, but does not therefore limit the present invention to the reality It applies among a range.Test method without specific conditions in the following example, according to conventional methods and conditions or according to quotient Product specification selects.
In following embodiments, primary raw material and instrument used are as follows:
PP spun-bonded non-woven fabrics, grammes per square metre 28g/m2, thickness 0.3mm bought from Jiangxi Dong Ju Industrial Co., Ltd.s.
PP melt spraying non-woven fabrics, i.e. polypropylene melt blown non-woven fabric, grammes per square metre 50g/m2, level n 95, thickness 0.5mm, purchase From Jiangxi Dong Ju Industrial Co., Ltd.s, medium is detected:NaCl particles, grain size:0.3um, flow 85L/min.
Terylene active carbon nonwoven fabric:Grammes per square metre is 32g/m2, thickness 0.2mm, the mass ratio of contained terylene and activated carbon is 13:3.It buys from Jiangxi Hao Rui industrial materials Co., Ltd.
Ear-hang is fastened with a rope, string, etc., material nylon.
Tartaric acid, No. CAS:526-83-0.
Ethyl alcohol, No. CAS:64-17-5, purity 99.5%.
Soybean protein, No. CAS:9010-10-0, specifically used soybean protein isolate, content 90%, food-grade.
Sodium chloride, No. CAS:7647-14-5.
Pomelo peel, Rutaceae citrus shaddock (Classification system:Citrus maxima (Burm) Merr.) fruit shaddock The crust of son.
Sodium alginate, No. CAS:9005-38-3.
Xanthans, No. CAS:11138-66-2.
Calcium chloride, No. CAS:10043-52-4.
Tea polyphenols, No. CAS:84650-60-2.
Nisin, also known as streptococcus lactis peptide are a kind of peptide materials that streptococcus lactis generates, by 34 amino acid Residue forms, and is pale solid powder.It can be degraded by the enzyme in human body, digestion, be that one kind is efficient, safe and nontoxic, make without pair Antiseptics for natural food.No. CAS:1414-45-5.
In following embodiments, used test method and key instrument are as follows:
PM2.5 filter efficiencies are tested:PM2.5 filter efficiency tests are carried out to the anti-PM2.5 active carbon masks of the present invention, A concentration of 300 μ g/m of PM2.5 in the Laboratory Module of 500L3, under the conditions of 25 DEG C, relative humidity are 65%, 3min is first passed through in advance Ventilation ensure to measure and stablize, then the air in Laboratory Module is filtered with anti-PM2.5 active carbon masks, flow 8L/ Min after filtering in 60 minutes, is measured using AM510pm2.5 testers after the filtering of anti-PM2.5 active carbon masks PM2.5 concentration.PM2.5 filter efficiencies=and (the PM2.5 concentration before filtering-the PM2.5 concentration after mask filters)/before filtering PM2.5 concentration × 100%.
Anti-microbial property test:Reference《GB15979-2002 disposable sanitary articles sanitary standards》Appendix C《Product bactericidal properties Energy, bacteriostasis property and stability test method》The antibacterial nonwoven cloth layer of the anti-PM2.5 active carbon masks of the present invention is sterilized Rate is tested, and action time is 5 minutes.Test strain is Escherichia coli (ATCC25922) and Candida albicans (ATCC10321).
Surface anti humility performance test:Moisture resistance is carried out to the antibacterial nonwoven cloth layer of the anti-PM2.5 active carbon masks of the present invention It can test, test method reference《The requirement of GB 19083-2010 medical protective masks technology》.Test water is deionized water, temperature Spend is 20 ± 2 DEG C.
It is further illustrated the present invention below by the mode of embodiment, unless otherwise specified, used number is attached most importance to Measure number.
Embodiment 1
Anti- PM2.5 active carbon masks:Ear-hang button loop including filter disc, on the left of filter disc and the ear-hang on the right side of filter disc Button loop, institute's filter disc include successively from inside to outside:First non-woven fabrics, filter paper, active carbon nonwoven fabric, the second non-woven fabrics.
First non-woven fabrics, the second non-woven fabrics are PP spun-bonded non-woven fabrics.
The active carbon nonwoven fabric is terylene active carbon nonwoven fabric.
The filter paper is PP melt spraying non-woven fabrics.
The processing method of anti-PM2.5 active carbon masks is:By cutting out to obtain, length is 17.5cm, width is 9.5cm's First non-woven fabrics, filter paper, active carbon nonwoven fabric, the second non-woven fabrics, by the first non-woven fabrics, filter paper, active carbon nonwoven fabric, Two non-woven fabrics stack successively, are sutured at edge position, obtain filter disc, then suture on the right side of ear-hang button loop and the filter disc on the left of filter disc Ear-hang button loop, obtain anti-PM2.5 active carbon masks.
The anti-PM2.5 active carbon masks of the present invention, are provided with active carbon nonwoven fabric, activated carbon has extremely strong adsorptivity, greatly It is big improve mask to particulate matter, aerosol, microorganism filter effect, be 98% to PM2.5 filter efficiencies.
Embodiment 2
Anti- PM2.5 active carbon masks, the ear-hang button loop including filter disc, on the left of filter disc and the ear-hang on the right side of filter disc Button loop, institute's filter disc include successively from inside to outside:First non-woven fabrics, filter paper, third non-woven fabrics, active carbon nonwoven fabric, the second nonwoven Cloth.
First non-woven fabrics, the second non-woven fabrics, third non-woven fabrics are PP spun-bonded non-woven fabrics.
The active carbon nonwoven fabric is terylene active carbon nonwoven fabric.
The filter paper is PP melt spraying non-woven fabrics.
The processing method of anti-PM2.5 active carbon masks is:By cutting out to obtain, length is 17.5cm, width is 9.5cm's First non-woven fabrics, filter paper, third non-woven fabrics, active carbon nonwoven fabric, the second non-woven fabrics, by the first non-woven fabrics, filter paper, third Non-woven fabrics, active carbon nonwoven fabric, the second non-woven fabrics stack successively, are sutured at edge position, obtain filter disc, then suture filter disc Ear-hang button loop on the right side of the ear-hang button loop and filter disc in left side, obtains anti-PM2.5 active carbon masks.
Anti- PM2.5 active carbon masks are 99.5% to PM2.5 filter efficiencies.
Embodiment 3
Anti- PM2.5 active carbon masks:Ear-hang button loop including filter disc, on the left of filter disc and the ear-hang on the right side of filter disc Button loop, institute's filter disc include successively from inside to outside:First non-woven fabrics, filter paper, active carbon nonwoven fabric, the second non-woven fabrics.
First non-woven fabrics be PP spun-bonded non-woven fabrics, grammes per square metre 28g/m2, thickness 0.3mm.
The active carbon nonwoven fabric be terylene active carbon nonwoven fabric, grammes per square metre 32g/m2, thickness 0.2mm, contained terylene Mass ratio with activated carbon is 13:3.
The filter paper be PP melt spraying non-woven fabrics, grammes per square metre 50g/m2, level n 95, thickness 0.5mm.
Second non-woven fabrics is antibacterial PP spun-bonded non-woven fabrics, and the grammes per square metre of PP spun-bonded non-woven fabrics used is 28g/m2, thickness For 0.3mm, the processing method of the antibacterial PP spun-bonded non-woven fabrics is:It is 0.5m to area2PP spun-bonded non-woven fabrics surface it is uniform Antimicrobial fluid is sprayed, antimicrobial fluid fountain height is 80g/m2, it is after sprinkling that PP spun-bonded non-woven fabrics are 3 hours dry at 65 DEG C, obtain antibacterial PP spun-bonded non-woven fabrics.
The preparation method of the antimicrobial fluid is as follows:(1) 45g tartaric acid is added to the ethyl alcohol that 900g mass fractions are 65% In aqueous solution, 65g soybean proteins are added in, is stirred 2 hours at 35 DEG C, with 150 revs/min of rotating speed, adds in 800g mass fractions It for 1.5% sodium-chloride water solution, is stirred 30 minutes at 35 DEG C, with 150 revs/min of rotating speed, is placed in 15 DEG C and preserves 2 hours, Then 30min is centrifuged with 5000 revs/min of rotating speed, takes the sediment after centrifugation, sediment dried 6 hours at 40 DEG C, powder Broken 20 mesh of mistake sieve, obtains modified soybean protein;(2) 2g sodium alginates are added to 100g to be pre-heated in 65 DEG C of water, 65 DEG C are stirred 30 minutes with 200 revs/min of rotating speed, are cooled to 45 DEG C, are added in 0.5g xanthans, 0.1g tartaric acid, 1.5g and are changed Property soybean protein, stirred 35 minutes at 45 DEG C, with 200 revs/min of rotating speed, add in 1g calcium chloride, 45 DEG C, with 200 turns/ The rotating speed of minute stirs 35 minutes, obtains antimicrobial fluid.
The processing method of anti-PM2.5 active carbon masks is:By cutting out to obtain, length is 17.5cm, width is 9.5cm's First non-woven fabrics, filter paper, active carbon nonwoven fabric, the second non-woven fabrics, by the first non-woven fabrics, filter paper, active carbon nonwoven fabric, Two non-woven fabrics stack successively, are sutured at edge position, obtain filter disc, then suture on the right side of ear-hang button loop and the filter disc on the left of filter disc Ear-hang button loop, obtain anti-PM2.5 active carbon masks.
Comparative example 1
Anti- PM2.5 active carbon masks:Ear-hang button loop including filter disc, on the left of filter disc and the ear-hang on the right side of filter disc Button loop, institute's filter disc include successively from inside to outside:First non-woven fabrics, filter paper, active carbon nonwoven fabric, the second non-woven fabrics.
First non-woven fabrics be PP spun-bonded non-woven fabrics, grammes per square metre 28g/m2, thickness 0.3mm.
The active carbon nonwoven fabric be terylene active carbon nonwoven fabric, grammes per square metre 32g/m2, thickness 0.2mm, contained terylene Mass ratio with activated carbon is 13:3.
The filter paper be PP melt spraying non-woven fabrics, grammes per square metre 50g/m2, level n 95, thickness 0.5mm.
Second non-woven fabrics is antibacterial PP spun-bonded non-woven fabrics, and the grammes per square metre of PP spun-bonded non-woven fabrics used is 28g/m2, thickness For 0.3mm, the processing method of the antibacterial PP spun-bonded non-woven fabrics is:It is 0.5m to area2PP spun-bonded non-woven fabrics surface it is uniform Antimicrobial fluid is sprayed, antimicrobial fluid fountain height is 80g/m2, it is after sprinkling that PP spun-bonded non-woven fabrics are 3 hours dry at 65 DEG C, obtain antibacterial PP spun-bonded non-woven fabrics.
The preparation method of the antimicrobial fluid is as follows:2g sodium alginates are added to 100g to be pre-heated in 65 DEG C of water, 65 DEG C are stirred 30 minutes with 200 revs/min of rotating speed, are cooled to 45 DEG C, 0.5g xanthans, 1.5g soybean proteins are added in, 45 DEG C, stirred 35 minutes with 200 revs/min of rotating speed, add in 1g calcium chloride, 35 stirred at 45 DEG C, with 200 revs/min of rotating speed Minute, obtain antimicrobial fluid.
The processing method of anti-PM2.5 active carbon masks is:By cutting out to obtain, length is 17.5cm, width is 9.5cm's First non-woven fabrics, filter paper, active carbon nonwoven fabric, the second non-woven fabrics, by the first non-woven fabrics, filter paper, active carbon nonwoven fabric, Two non-woven fabrics stack successively, are sutured at edge position, obtain filter disc, then suture on the right side of ear-hang button loop and the filter disc on the left of filter disc Ear-hang button loop, obtain anti-PM2.5 active carbon masks.
Embodiment 4
Anti- PM2.5 active carbon masks:Ear-hang button loop including filter disc, on the left of filter disc and the ear-hang on the right side of filter disc Button loop, institute's filter disc include successively from inside to outside:First non-woven fabrics, filter paper, active carbon nonwoven fabric, the second non-woven fabrics.
First non-woven fabrics be PP spun-bonded non-woven fabrics, grammes per square metre 28g/m2, thickness 0.3mm.
The active carbon nonwoven fabric be terylene active carbon nonwoven fabric, grammes per square metre 32g/m2, thickness 0.2mm, contained terylene Mass ratio with activated carbon is 13:3.
The filter paper be PP melt spraying non-woven fabrics, grammes per square metre 50g/m2, level n 95, thickness 0.5mm.
Second non-woven fabrics is antibacterial PP spun-bonded non-woven fabrics, and the grammes per square metre of PP spun-bonded non-woven fabrics used is 28g/m2, thickness For 0.3mm, the processing method of the antibacterial PP spun-bonded non-woven fabrics is:It is 0.5m to area2PP spun-bonded non-woven fabrics surface it is uniform Antimicrobial fluid is sprayed, antimicrobial fluid fountain height is 80g/m2, it is after sprinkling that PP spun-bonded non-woven fabrics are 3 hours dry at 65 DEG C, obtain antibacterial PP spun-bonded non-woven fabrics.
The preparation method of the antimicrobial fluid is as follows:(1) 45g tartaric acid is added to the ethyl alcohol that 900g mass fractions are 65% In aqueous solution, 65g soybean proteins are added in, is stirred 2 hours at 35 DEG C, with 150 revs/min of rotating speed, adds in 800g mass fractions It for 1.5% sodium-chloride water solution, is stirred 30 minutes at 35 DEG C, with 150 revs/min of rotating speed, is placed in 15 DEG C and preserves 2 hours, Then 30min is centrifuged with 5000 revs/min of rotating speed, takes the sediment after centrifugation, sediment dried 6 hours at 40 DEG C, powder Broken 20 mesh of mistake sieve, obtains modified soybean protein;(2) it is pomelo peel fresh 250g is 48 hours dry at 55 DEG C, it smashes it through 500 mesh sieve, obtain shaddock peel powder, 2g sodium alginates are added to 100g is pre-heated in 65 DEG C of water, 65 DEG C with 200 turns/ The rotating speed of minute stirs 30 minutes, adds in 3g shaddock peel powders, is stirred 120 minutes with 200 revs/min of rotating speed at 65 DEG C, cooling To 45 DEG C, the soybean protein that 0.5g xanthans, 0.1g tartaric acid, 1.5g are modified is added in, at 45 DEG C, with 200 revs/min of rotating speed Stirring 35 minutes adds in 1g calcium chloride, is stirred 35 minutes at 45 DEG C, with 200 revs/min of rotating speed, obtains antimicrobial fluid.
The processing method of anti-PM2.5 active carbon masks is:By cutting out to obtain, length is 17.5cm, width is 9.5cm's First non-woven fabrics, filter paper, active carbon nonwoven fabric, the second non-woven fabrics, by the first non-woven fabrics, filter paper, active carbon nonwoven fabric, Two non-woven fabrics stack successively, are sutured at edge position, obtain filter disc, then suture on the right side of ear-hang button loop and the filter disc on the left of filter disc Ear-hang button loop, obtain anti-PM2.5 active carbon masks.
Embodiment 5
Anti- PM2.5 active carbon masks:Ear-hang button loop including filter disc, on the left of filter disc and the ear-hang on the right side of filter disc Button loop, institute's filter disc include successively from inside to outside:First non-woven fabrics, filter paper, active carbon nonwoven fabric, the second non-woven fabrics.
First non-woven fabrics be PP spun-bonded non-woven fabrics, grammes per square metre 28g/m2, thickness 0.3mm.
The active carbon nonwoven fabric be terylene active carbon nonwoven fabric, grammes per square metre 32g/m2, thickness 0.2mm, contained terylene Mass ratio with activated carbon is 13:3.
The filter paper be PP melt spraying non-woven fabrics, grammes per square metre 50g/m2, level n 95, thickness 0.5mm.
Second non-woven fabrics is antibacterial PP spun-bonded non-woven fabrics, and the grammes per square metre of PP spun-bonded non-woven fabrics used is 28g/m2, thickness For 0.3mm, the processing method of the antibacterial PP spun-bonded non-woven fabrics is:It is 0.5m to area2PP spun-bonded non-woven fabrics surface it is uniform Antimicrobial fluid is sprayed, antimicrobial fluid fountain height is 80g/m2, it is after sprinkling that PP spun-bonded non-woven fabrics are 3 hours dry at 65 DEG C, obtain antibacterial PP spun-bonded non-woven fabrics.
The preparation method of the antimicrobial fluid is as follows:(1) 45g tartaric acid is added to the ethyl alcohol that 900g mass fractions are 65% In aqueous solution, 65g soybean proteins are added in, is stirred 2 hours at 35 DEG C, with 150 revs/min of rotating speed, adds in 800g mass fractions It for 1.5% sodium-chloride water solution, is stirred 30 minutes at 35 DEG C, with 150 revs/min of rotating speed, is placed in 15 DEG C and preserves 2 hours, Then it is centrifuged 30 minutes with 5000 revs/min of rotating speed, takes the sediment after centrifugation, sediment dried 6 hours at 40 DEG C, powder Broken 20 mesh of mistake sieve, obtains modified soybean protein;(2) it is pomelo peel fresh 250g is 48 hours dry at 55 DEG C, it smashes it through 500 mesh sieve, obtain shaddock peel powder, 2g sodium alginates are added to 100g is pre-heated in 65 DEG C of water, 65 DEG C with 200 turns/ The rotating speed of minute stirs 30 minutes, adds in 5g shaddock peel powders, is stirred 120 minutes with 200 revs/min of rotating speed at 65 DEG C, cooling To 45 DEG C, the soybean protein that 0.5g xanthans, 0.1g tartaric acid, 1.5g are modified is added in, at 45 DEG C, with 200 revs/min of rotating speed Stirring 35 minutes adds in 1g calcium chloride, is stirred 35 minutes at 45 DEG C, with 200 revs/min of rotating speed, obtains antimicrobial fluid.
The processing method of anti-PM2.5 active carbon masks is:By cutting out to obtain, length is 17.5cm, width is 9.5cm's First non-woven fabrics, filter paper, active carbon nonwoven fabric, the second non-woven fabrics, by the first non-woven fabrics, filter paper, active carbon nonwoven fabric, Two non-woven fabrics stack successively, are sutured at edge position, obtain filter disc, then suture on the right side of ear-hang button loop and the filter disc on the left of filter disc Ear-hang button loop, obtain anti-PM2.5 active carbon masks.
Embodiment 6
Anti- PM2.5 active carbon masks:Ear-hang button loop including filter disc, on the left of filter disc and the ear-hang on the right side of filter disc Button loop, institute's filter disc include successively from inside to outside:First non-woven fabrics, filter paper, active carbon nonwoven fabric, the second non-woven fabrics.
First non-woven fabrics be PP spun-bonded non-woven fabrics, grammes per square metre 28g/m2, thickness 0.3mm.
The active carbon nonwoven fabric be terylene active carbon nonwoven fabric, grammes per square metre 32g/m2, thickness 0.2mm, contained terylene Mass ratio with activated carbon is 13:3.
The filter paper be PP melt spraying non-woven fabrics, grammes per square metre 50g/m2, level n 95, thickness 0.5mm.
Second non-woven fabrics is antibacterial PP spun-bonded non-woven fabrics, and the grammes per square metre of PP spun-bonded non-woven fabrics used is 28g/m2, thickness For 0.3mm, the processing method of the antibacterial PP spun-bonded non-woven fabrics is:It is 0.5m to area2PP spun-bonded non-woven fabrics surface it is uniform Antimicrobial fluid is sprayed, antimicrobial fluid fountain height is 80g/m2, it is after sprinkling that PP spun-bonded non-woven fabrics are 3 hours dry at 65 DEG C, obtain antibacterial PP spun-bonded non-woven fabrics.
The preparation method of the antimicrobial fluid is as follows:(1) 45g tartaric acid is added to the ethyl alcohol that 900g mass fractions are 65% In aqueous solution, 65g soybean proteins are added in, is stirred 2 hours at 35 DEG C, with 150 revs/min of rotating speed, adds in 800g mass fractions It for 1.5% sodium-chloride water solution, is stirred 30 minutes at 35 DEG C, with 150 revs/min of rotating speed, is placed in 15 DEG C and preserves 2 hours, Then it is centrifuged 30 minutes with 5000 revs/min of rotating speed, takes the sediment after centrifugation, sediment dried 6 hours at 40 DEG C, powder Broken 20 mesh of mistake sieve, obtains modified soybean protein;(2) it is pomelo peel fresh 250g is 48 hours dry at 55 DEG C, it smashes it through 500 mesh sieve, obtain shaddock peel powder, 2g sodium alginates are added to 100g is pre-heated in 65 DEG C of water, 65 DEG C with 200 turns/ The rotating speed of minute stirs 30 minutes, adds in 7g shaddock peel powders, is stirred 120 minutes with 200 revs/min of rotating speed at 65 DEG C, cooling To 45 DEG C, the soybean protein that 0.5g xanthans, 0.1g tartaric acid, 1.5g are modified is added in, at 45 DEG C, with 200 revs/min of rotating speed Stirring 35 minutes adds in 1g calcium chloride, is stirred 35 minutes at 45 DEG C, with 200 revs/min of rotating speed, obtains antimicrobial fluid.
The processing method of anti-PM2.5 active carbon masks is:By cutting out to obtain, length is 17.5cm, width is 9.5cm's First non-woven fabrics, filter paper, active carbon nonwoven fabric, the second non-woven fabrics, by the first non-woven fabrics, filter paper, active carbon nonwoven fabric, Two non-woven fabrics stack successively, are sutured at edge position, obtain filter disc, then suture on the right side of ear-hang button loop and the filter disc on the left of filter disc Ear-hang button loop, obtain anti-PM2.5 active carbon masks.
Embodiment 7
Anti- PM2.5 active carbon masks:Ear-hang button loop including filter disc, on the left of filter disc and the ear-hang on the right side of filter disc Button loop, institute's filter disc include successively from inside to outside:First non-woven fabrics, filter paper, active carbon nonwoven fabric, the second non-woven fabrics.
First non-woven fabrics be PP spun-bonded non-woven fabrics, grammes per square metre 28g/m2, thickness 0.3mm.
The active carbon nonwoven fabric be terylene active carbon nonwoven fabric, grammes per square metre 32g/m2, thickness 0.2mm, contained terylene Mass ratio with activated carbon is 13:3.
The filter paper be PP melt spraying non-woven fabrics, grammes per square metre 50g/m2, level n 95, thickness 0.5mm.
Second non-woven fabrics is antibacterial PP spun-bonded non-woven fabrics, and the grammes per square metre of PP spun-bonded non-woven fabrics used is 28g/m2, thickness For 0.3mm, the processing method of the antibacterial PP spun-bonded non-woven fabrics is:It is 0.5m to area2PP spun-bonded non-woven fabrics surface it is uniform Antimicrobial fluid is sprayed, antimicrobial fluid fountain height is 80g/m2, it is after sprinkling that PP spun-bonded non-woven fabrics are 3 hours dry at 65 DEG C, obtain antibacterial PP spun-bonded non-woven fabrics.
The preparation method of the antimicrobial fluid is as follows:(1) 45g tartaric acid is added to the ethyl alcohol that 900g mass fractions are 65% In aqueous solution, 65g soybean proteins are added in, is stirred 2 hours at 35 DEG C, with 150 revs/min of rotating speed, adds in 800g mass fractions It for 1.5% sodium-chloride water solution, is stirred 30 minutes at 35 DEG C, with 150 revs/min of rotating speed, is placed in 15 DEG C and preserves 2 hours, Then it is centrifuged 30 minutes with 5000 revs/min of rotating speed, takes the sediment after centrifugation, sediment dried 6 hours at 40 DEG C, powder Broken 20 mesh of mistake sieve, obtains modified soybean protein;(2) it is pomelo peel fresh 250g is 48 hours dry at 55 DEG C, it smashes it through 500 mesh sieve, obtain shaddock peel powder, 2g sodium alginates are added to 100g is pre-heated in 65 DEG C of water, 65 DEG C with 200 turns/ The rotating speed of minute stirs 30 minutes, adds in 5g shaddock peel powders, is stirred 120 minutes with 200 revs/min of rotating speed at 65 DEG C, cooling To 45 DEG C, the soybean protein that 0.5g xanthans, 0.1g tartaric acid, 1.5g are modified is added in, at 45 DEG C, with 200 revs/min of rotating speed Stirring 35 minutes adds in 1g calcium chloride, the antibacterial auxiliary agents of 0.03g, stirs 35 minutes, obtains at 45 DEG C, with 200 revs/min of rotating speed To antimicrobial fluid.The Antibacterial accessory ingredient is nisin.
The processing method of anti-PM2.5 active carbon masks is:By cutting out to obtain, length is 17.5cm, width is 9.5cm's First non-woven fabrics, filter paper, active carbon nonwoven fabric, the second non-woven fabrics, by the first non-woven fabrics, filter paper, active carbon nonwoven fabric, Two non-woven fabrics stack successively, are sutured at edge position, obtain filter disc, then suture on the right side of ear-hang button loop and the filter disc on the left of filter disc Ear-hang button loop, obtain anti-PM2.5 active carbon masks.
Embodiment 8
It is substantially the same manner as Example 7, it differs only in:Antibacterial auxiliary agent described in the present embodiment 8 is tea polyphenols.
Embodiment 9
It is substantially the same manner as Example 7, it differs only in:Antibacterial auxiliary agent described in the present embodiment 9 for nisin and Tea polyphenols are 1 in mass ratio:3 mixture.
Fungistatic effect is tested
Table 1:Sterilizing rate test result table
Escherichia coli (%) Candida albicans (%)
Embodiment 3 87.4 81.2
Embodiment 4 90.5 88.3
Embodiment 5 91.3 89.4
Embodiment 6 90.9 89.1
Embodiment 7 94.7 92.9
Embodiment 8 95.4 93.5
Embodiment 9 98.2 97.6
Comparative example 1 87.2 80.8
Surface anti humility performance test
Table 2:Spray rating
The anti-PM2.5 active carbon masks of the present invention, are provided with activated carbon non-woven layer of cloth, and activated carbon has extremely strong adsorptivity, Filtering PM2.5 particulate matters, aerosol, microorganism, virus can be isolated, more than 98% is reached to the filter efficiency of PM2.5 particulate matters, Mask also has good antibacterial and anti-wettability energy.Under the premise of gas permeability is ensured, by being sprayed to PP nonwoven surfaces Antimicrobial fluid, then drying can form the antibacterial film of one layer of good air permeability in PP nonwoven surfaces.Embodiment 3-9 mask outer layers Antibacterial PP non-woven fabrics can effectively kill the common bacterias such as Escherichia coli, Candida albicans, antibacterial PP non-woven fabrics also has good Anti-wettability energy.The antibacterial PP nonwoven surfaces of embodiment 7-9 are adsorbed with antibacterial auxiliary agent, further improve the sterilization of mask Effect.
The preferred embodiment of the present invention described in detail above.It should be appreciated that those of ordinary skill in the art without Creative work is needed according to the present invention can to conceive and makes many modifications and variations.Therefore, all technologies in the art Personnel are available by logical analysis, reasoning, or a limited experiment on the basis of existing technology under this invention's idea Technical solution, all should be in the protection domain being defined in the patent claims.

Claims (10)

1. a kind of anti-PM2.5 active carbon masks, which is characterized in that the ear-hang including filter disc, on the left of filter disc is fastened with a rope, string, etc. and positioned at filter Ear-hang button loop on the right side of piece, institute's filter disc include successively from inside to outside:First non-woven fabrics, filter paper, active carbon nonwoven fabric, the second nonwoven Cloth.
2. a kind of anti-PM2.5 active carbon masks, which is characterized in that the ear-hang including filter disc, on the left of filter disc is fastened with a rope, string, etc. and positioned at filter Ear-hang button loop on the right side of piece, institute's filter disc include successively from inside to outside:First non-woven fabrics, filter paper, third non-woven fabrics, activated carbon non-woven Cloth, the second non-woven fabrics.
3. anti-PM2.5 active carbon masks according to claim 1, which is characterized in that first non-woven fabrics, the second nonwoven Cloth is PP non-woven fabrics or PET non-woven fabrics, and the filter paper is PP melt spraying non-woven fabrics.
4. anti-PM2.5 active carbon masks according to claim 2, which is characterized in that the third non-woven fabrics is PP nonwovens Cloth or PET non-woven fabrics.
5. the anti-PM2.5 active carbon masks in being appointed according to claim 1-4 described in one, which is characterized in that the anti-PM2.5 lives Property charcoal mask PM2.5 filter efficiencies be >=98%.
6. a kind of anti-PM2.5 active carbon masks, which is characterized in that the ear-hang including filter disc, on the left of filter disc is fastened with a rope, string, etc. and positioned at filter Ear-hang button loop on the right side of piece, institute's filter disc include successively from inside to outside:First non-woven fabrics, filter paper, active carbon nonwoven fabric, the second nonwoven Cloth, first non-woven fabrics are PP spun-bonded non-woven fabrics, and second non-woven fabrics is antibacterial PP spun-bonded non-woven fabrics, and the antibacterial PP is spun The processing method of bonded non-woven fabrics is:Antimicrobial fluid is uniformly sprayed on PP spun-bonded non-woven fabrics surface, antimicrobial fluid fountain height is 80-150g/ m2, it is after sprinkling that PP spun-bonded non-woven fabrics are 3-6 hours dry at 65-75 DEG C, obtain antibacterial PP spun-bonded non-woven fabrics.
7. anti-PM2.5 active carbon masks according to claim 6, which is characterized in that the preparation method packet of the antimicrobial fluid Include following steps:(1) 45-65g tartaric acid is added in the ethanol water that 900-1000g mass fractions are 65-85%, added Enter 65-85g soybean proteins, stirred 2-4 hours at 35-45 DEG C, with 150-300 revs/min of rotating speed, add in 800-1000g matter The sodium-chloride water solution that score is 1.5-3% is measured, is stirred 30-50 minutes at 35-45 DEG C, with 150-300 revs/min of rotating speed, It is placed in 15-18 DEG C to preserve 2-4 hours, then be centrifuged 30-50 minutes with 5000-8000 revs/min of rotating speed, it is heavy after centrifugation to take Starch, sediment is 6-8 hours dry at 40-50 DEG C, 20-50 mesh sieve is crushed, obtains modified soybean protein;(2) by 2- 4g sodium alginates are added to 100-150g and are pre-heated in 65-75 DEG C of water, at 65-75 DEG C with 200-300 revs/min of rotating speed Stirring 30-50 minutes is cooled to 45-55 DEG C, adds in 0.5-1.5g xanthans, 0.1-0.3g tartaric acid, 1.5-4.5g and is modified Soybean protein is stirred 35-55 minutes at 45-55 DEG C, with 200-500 revs/min of rotating speed, 1-3g calcium chloride is added in, in 45-55 DEG C, stirred 35-55 minutes with 200-500 revs/min of rotating speed, obtain antimicrobial fluid.
8. anti-PM2.5 active carbon masks according to claim 5 or 6, which is characterized in that the preparation method of the antimicrobial fluid Include the following steps:(1) 45-65g tartaric acid is added in the ethanol water that 900-1000g mass fractions are 65-85%, 65-85g soybean proteins are added in, is stirred 2-4 hours at 35-45 DEG C, with 150-300 revs/min of rotating speed, adds in 800-1000g Mass fraction is the sodium-chloride water solution of 1.5-3%, at 35-45 DEG C, with 150-300 revs/min of 30-50 points of rotating speed stirring Clock is placed in 15-18 DEG C and preserved 2-4 hours, then centrifuged 30-50 minutes with 5000-8000 revs/min of rotating speed, after taking centrifugation Sediment, sediment is 6-8 hours dry at 40-50 DEG C, crushed 20-50 mesh sieve, obtain modified soybean protein;(2) Pomelo peel fresh 250-300g is 48-60 hours dry at 55-65 DEG C, 500-800 mesh sieve is smashed it through, obtains pomelo peel 2-4g sodium alginates are added to 100-150g and are pre-heated in 65-75 DEG C of water, at 65-75 DEG C with 200-300 revs/min by powder The rotating speed of clock stirs 30-50 minutes, adds in 2-7g shaddock peel powders, is stirred at 65-75 DEG C with 200-500 revs/min of rotating speed 120-150 minutes, 45-50 DEG C is cooled to, addition 0.5-1.5g xanthans, 0.1-0.3g tartaric acid, 1.5-4.5g are modified big Legumin stirs 35-55 minutes at 45-55 DEG C, with 200-500 revs/min of rotating speed, adds in 1-3g calcium chloride, 0-0.06g suppressions Bacterium auxiliary agent is stirred 35-55 minutes at 45-55 DEG C, with 200-500 revs/min of rotating speed, obtains antimicrobial fluid;The antibacterial auxiliary agent For nisin and/or tea polyphenols.
9. a kind of antibacterial PP spun-bonded non-woven fabrics, which is characterized in that the processing method of antibacterial PP non-woven fabrics is:In PP spun-bonded non-woven fabrics Antimicrobial fluid is uniformly sprayed on surface, and antimicrobial fluid fountain height is 80-150g/m2, by PP spun-bonded non-woven fabrics in 65-75 DEG C of drying after sprinkling 3-6 hours, obtain antibacterial PP spun-bonded non-woven fabrics.
10. application of the antibacterial PP spun-bonded non-woven fabrics in anti-PM2.5 active carbon masks described in claim 9.
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CN107376860A (en) * 2017-08-25 2017-11-24 河海大学 A kind of dye sorbent and preparation method thereof

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