CN108204737A - A kind of horizontal reducing atmosphere vacuum annealing furnace - Google Patents

A kind of horizontal reducing atmosphere vacuum annealing furnace Download PDF

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Publication number
CN108204737A
CN108204737A CN201810007000.2A CN201810007000A CN108204737A CN 108204737 A CN108204737 A CN 108204737A CN 201810007000 A CN201810007000 A CN 201810007000A CN 108204737 A CN108204737 A CN 108204737A
Authority
CN
China
Prior art keywords
flue
furnace body
furnace
fire door
reducing atmosphere
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201810007000.2A
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Chinese (zh)
Inventor
匡万兵
谭俊峰
聂勇
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hunan Xin Tianli Science And Technology Ltd
Original Assignee
Hunan Xin Tianli Science And Technology Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hunan Xin Tianli Science And Technology Ltd filed Critical Hunan Xin Tianli Science And Technology Ltd
Priority to CN201810007000.2A priority Critical patent/CN108204737A/en
Publication of CN108204737A publication Critical patent/CN108204737A/en
Pending legal-status Critical Current

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Classifications

    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27BFURNACES, KILNS, OVENS, OR RETORTS IN GENERAL; OPEN SINTERING OR LIKE APPARATUS
    • F27B5/00Muffle furnaces; Retort furnaces; Other furnaces in which the charge is held completely isolated
    • F27B5/04Muffle furnaces; Retort furnaces; Other furnaces in which the charge is held completely isolated adapted for treating the charge in vacuum or special atmosphere
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27BFURNACES, KILNS, OVENS, OR RETORTS IN GENERAL; OPEN SINTERING OR LIKE APPARATUS
    • F27B5/00Muffle furnaces; Retort furnaces; Other furnaces in which the charge is held completely isolated
    • F27B5/06Details, accessories, or equipment peculiar to furnaces of these types
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27BFURNACES, KILNS, OVENS, OR RETORTS IN GENERAL; OPEN SINTERING OR LIKE APPARATUS
    • F27B5/00Muffle furnaces; Retort furnaces; Other furnaces in which the charge is held completely isolated
    • F27B5/06Details, accessories, or equipment peculiar to furnaces of these types
    • F27B5/08Arrangements of linings
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27BFURNACES, KILNS, OVENS, OR RETORTS IN GENERAL; OPEN SINTERING OR LIKE APPARATUS
    • F27B5/00Muffle furnaces; Retort furnaces; Other furnaces in which the charge is held completely isolated
    • F27B5/06Details, accessories, or equipment peculiar to furnaces of these types
    • F27B5/14Arrangements of heating devices
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27BFURNACES, KILNS, OVENS, OR RETORTS IN GENERAL; OPEN SINTERING OR LIKE APPARATUS
    • F27B5/00Muffle furnaces; Retort furnaces; Other furnaces in which the charge is held completely isolated
    • F27B5/06Details, accessories, or equipment peculiar to furnaces of these types
    • F27B5/18Arrangement of controlling, monitoring, alarm or like devices
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27MINDEXING SCHEME RELATING TO ASPECTS OF THE CHARGES OR FURNACES, KILNS, OVENS OR RETORTS
    • F27M2003/00Type of treatment of the charge
    • F27M2003/01Annealing

Landscapes

  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Furnace Details (AREA)
  • Furnace Housings, Linings, Walls, And Ceilings (AREA)

Abstract

The present invention provides a kind of horizontal reducing atmosphere vacuum annealing furnace, including rack, furnace body, fire door, flue, adiabatic heat-insulation furnace lining, heating element, vacuum system, atmosphere system, control system, safety device and radiator, vacuum system and atmosphere system are mounted on frame lower, control system installation frame rear portion;Flue is designed using height warm area, and high-temperature region is heated using U-shaped Si-Mo rod, and Si-Mo rod both sides arrangement, low-temperature space is heated using FEC ceramic fiber heaters, circumferentially arranged, height warm area is designed with diaphragm structure;Flue is designed using high and low warm area in the present invention, can effectively realize temperature gradient;Light fibre material thermal conductivity is relatively low, proportion is small, can effectively reduce the power consumption during equipment normal use;Vacuum system and atmosphere system are controlled using vacuum pump set and mass flowmenter so that vacuum degree is higher, gas flow control accuracy is preferable, reaches the index request of high, precision and frontier CVD technological experiments.

Description

A kind of horizontal reducing atmosphere vacuum annealing furnace
Technical field
The present invention relates to vacuum equipment field more particularly to a kind of horizontal reducing atmosphere vacuum annealing furnace.
Background technology
Atmosphere vacuum annealing furnace serial equipment is primarily adapted for use in the development of carbon nanotube, crystalline silicon substrates plated film, nano-ZnO Controllable growth, ceramic capacitor (MLCC) the CVD techniques such as the diffusion welding (DW) of atmosphere sintering, metal material.At present, traditional gas Atmosphere vacuum annealing furnace is designed for single temperature zone, is difficult to realize the control of temperature gradient, be can not meet the requirement of CVD techniques;In boiler tube In selection, select high aluminum pipe in the past, alumina content is low, heat resistance is poor, easily in the case of a high temperature occur Cracking of furnace tube, Phenomenon of rupture causes technological experiment that cannot be normally carried out, simultaneously as boiler tube both ends and centre do not support, will also result in height Boiler tube bending in the case of temperature is even broken;In addition, vacuum system, atmosphere system use traditional mechanical pump and float stream Gauge controls, and shortcoming is that system vacuum is relatively low, gas flow control accuracy is poor, is extremely difficult to high, precision and frontier CVD techniques reality The index request tested prevents user from normal use.
Invention content
The purpose of the present invention is to provide a kind of horizontal reducing atmosphere vacuum annealing furnaces, and above-mentioned traditional atmosphere vacuum is overcome to move back Stove is difficult to realize the control of temperature gradient, and Cracking of furnace tube, bending even phenomenon of rupture, vacuum system, atmosphere system are true Reciprocal of duty cycle is relatively low, gas flow control accuracy is poor, the defects of being extremely difficult to the index request of high, precision and frontier CVD technological experiments.
To achieve the above object, the present invention provides following technical solution:
A kind of horizontal reducing atmosphere vacuum annealing furnace, including rack, furnace body, fire door, flue, adiabatic heat-insulation furnace lining, heating Element, vacuum system, atmosphere system, control system, safety device and radiator, wherein:Furnace body is mounted in rack, fire door It is connect with furnace body, flue is placed in furnace interior, and adiabatic heat-insulation furnace lining is mounted on inside flue, and heating element is in adiabatic heat-insulation furnace lining Two sides arrangement installation, vacuum system and atmosphere system be mounted on frame lower, control system installation frame rear portion, and safety fills It puts and is mounted on upper of furnace body with radiator.
Preferably, the furnace interior two sides installation guide-track groove, the company of being slidably matched between flue and guide-track groove It connects, such flue can be free to slide on guide-track groove;Lower portion of furnace body is welded on saddle, and furnace body is fixedly connected as with rack One.
Preferably, pivoted arm one end is connect by aligning device with fire door, and the pivoted arm other end passes through shaft and furnace body Connection, such fire door can rotate around the axis, be opened and closed;Aligning device is mounted on fire door outer side center position, For multidirectional adjusting fire door position.
Preferably, the flue is arranged on furnace interior, and flue both sides are equipped with idler wheel, these idler wheels and guide rail It is slidably connected between slot so that idler wheel can be free to slide on guide-track groove, and flue is equipped with interior fire door, by interior fire door The heating space of closing is formed after closing.
Preferably, the adiabatic heat-insulation furnace lining inside flue is made of multiple layer refractory.
Preferably, the temperature and pressure when control system is for measurement material sintering in real time, and can basis Material sintering process carries out atmosphere filling and displacement, opens and closes automatically heating.
Preferably, the safety device is mounted on upper of furnace body, the work in furnace interior superpressure or gas burst Make, equipment safety can be protected.
Preferably, the radiator is mounted on upper of furnace body, for reducing the surface temperature of furnace body.
Preferably, the flue is designed using height warm area, and high-temperature region is heated using U-shaped Si-Mo rod, Si-Mo rod Both sides arrange that low-temperature space is heated using FEC ceramic fiber heaters, is circumferentially arranged, height warm area is designed with diaphragm structure; Resistance to material whole Ceramics fiber light material pressure seaming in flue is assembled, is flame retardant coating successively from inside to outside, protects Warm layer and thermal insulation layer select mullite fiber, high aluminum fiber and alumina silicate fibre respectively;High-purity corundum boiler tube in flue can To free in and out flue, high-purity corundum boiler tube both ends are fixed with the steel flange with water cooling, and steel flange is detachable, silicon Rubber sealing, both ends steel flange connect vacuum system and atmosphere system respectively.
Compared with prior art, beneficial effects of the present invention are as follows:
It is structure novel of the present invention, easy to operate, adaptable, wherein:Flue is designed using high and low warm area in the present invention, It can effectively realize temperature gradient;Light fibre material thermal conductivity is relatively low, proportion is small, can effectively reduce equipment normal use process In power consumption;Vacuum system and atmosphere system are controlled using vacuum pump set and mass flowmenter so that vacuum degree is higher, gas stream It is preferable to measure control accuracy, reaches the index request of high, precision and frontier CVD technological experiments.
Description of the drawings
Fig. 1 is dimensional structure diagram of the present invention;
Fig. 2 is another angle dimensional structure diagram of the present invention;
It is marked in figure:Rack (1), furnace body (2), guide-track groove (201), saddle (202), fire door (3), pivoted arm (301), shaft (302), aligning device (303), flue (4), idler wheel (401), interior fire door (402), adiabatic heat-insulation furnace lining (5), heating element (6), vacuum system (7), atmosphere system (8), control system (9), safety device (10), radiator (11).
Specific embodiment
Below in conjunction with the attached drawing in the embodiment of the present invention, the technical solution in the embodiment of the present invention is carried out clear, complete Site preparation describes.
It please refers to Fig.1-2 present invention and a kind of technical solution is provided:A kind of horizontal reducing atmosphere vacuum annealing furnace, including rack 1st, furnace body 2, fire door 3, flue 4, adiabatic heat-insulation furnace lining 5, heating element 6, vacuum system 7, atmosphere system 8, control system 9, peace Full device 10 and radiator 11, wherein:Furnace body 2 is mounted in rack 1, and fire door 3 is connect with furnace body 2, and flue 4 is placed in furnace body 2 Inside, adiabatic heat-insulation furnace lining 5 are mounted on inside flue 4, and heating element 6 is arranged in the two sides of adiabatic heat-insulation furnace lining 5 and installed, very Empty set system 7 and atmosphere system 8 are mounted on 1 lower part of rack, 9 installation frame of control system, 1 rear portion, safety device 10 and radiator 11 are mounted on 2 top of furnace body.Guide-track groove 201 is installed in the 2 inside two sides of furnace body, slides and matches between flue 4 and guide-track groove 201 Connection is closed, such flue 4 can be free to slide on guide-track groove 201;2 lower weld of furnace body on saddle 202, and furnace body 2 with Rack 1 is connected to one.301 one end of pivoted arm is connect by aligning device 303 with fire door 3, and 301 other end of pivoted arm is by turning Axis 302 is connect with furnace body 2, and such fire door 3 302 can rotate around the shaft, be opened and closed;Aligning device 303 is mounted on On 3 outer side center position of fire door, for 3 position of multidirectional adjusting fire door.The flue 4 is arranged on inside furnace body 2,4 both sides of flue Idler wheel 401 is installed, is slidably connected between these idler wheels 401 and guide-track groove 201 so that idler wheel 401 can be in guide-track groove Free to slide on 201, flue 4 is equipped with interior fire door 402, and the heating space of closing is formed after interior fire door 402 is closed.Installation Adiabatic heat-insulation furnace lining 5 inside flue 4 is made of multiple layer refractory.The control system 9 is for measurement material in real time Temperature and pressure during sintering, and can atmosphere filling and displacement be carried out according to material sintering process, open and close automatically heating. The safety device 10 is mounted on 2 top of furnace body, works in 2 inner overpressure of furnace body or gas burst, can protect equipment safety. The radiator 11 is mounted on 2 top of furnace body, for reducing the surface temperature of furnace body 2.
Wherein:The flue 4 is heated using the design of height warm area, high-temperature region using U-shaped Si-Mo rod, Si-Mo rod both sides cloth It puts, low-temperature space is heated using FEC ceramic fiber heaters, is circumferentially arranged, height warm area is designed with diaphragm structure;In flue 4 Interior resistance to material whole Ceramics fiber light material pressure seaming is assembled, is flame retardant coating, insulating layer successively from inside to outside And thermal insulation layer, mullite fiber, high aluminum fiber and alumina silicate fibre are selected respectively;High-purity corundum boiler tube in flue 4 can be with Flue 4 is freed in and out, high-purity corundum boiler tube both ends are fixed with the steel flange with water cooling, and steel flange is detachable, silicon Rubber sealing, both ends steel flange connect vacuum system and atmosphere system respectively.
It is structure novel of the present invention, easy to operate, adaptable, wherein:Flue is designed using high and low warm area in the present invention, It can effectively realize temperature gradient;Light fibre material thermal conductivity is relatively low, proportion is small, can effectively reduce equipment normal use process In power consumption;Vacuum system and atmosphere system are controlled using vacuum pump set and mass flowmenter so that vacuum degree is higher, gas stream It is preferable to measure control accuracy, reaches the index request of high, precision and frontier CVD technological experiments.
The foregoing is only a preferred embodiment of the present invention, is not intended to restrict the invention, although with reference to aforementioned reality Example is applied the present invention is described in detail, it for those skilled in the art, still can be to aforementioned each implementation Technical solution recorded in example modifies or carries out equivalent replacement to which part technical characteristic.All essences in the present invention With within principle, any modification, equivalent replacement, improvement and so on should all be included in the protection scope of the present invention god.

Claims (8)

1. a kind of horizontal reducing atmosphere vacuum annealing furnace, which is characterized in that including rack (1), furnace body (2), fire door (3), flue (4), adiabatic heat-insulation furnace lining (5), heating element (6), vacuum system (7), atmosphere system (8), control system (9), safety device (10) and radiator (11), wherein:In rack (1), fire door (3) is connect furnace body (2) with furnace body (2), and flue (4) is put Internal in furnace body (2), adiabatic heat-insulation furnace lining (5) is internal mounted on flue (4), and heating element (6) is in adiabatic heat-insulation furnace lining (5) Two sides arrangement installation, vacuum system (7) and atmosphere system (8) are mounted on rack (1) lower part, control system (9) installation frame (1) rear portion, safety device (10) and radiator (11) are mounted on furnace body (2) top.
2. a kind of horizontal reducing atmosphere vacuum annealing furnace according to claim 1, which is characterized in that the furnace body (2) is internal Two sides installation guide-track groove (201), is slidably connected between flue (4) and guide-track groove (201), and such flue (4) can be It is free to slide on guide-track groove (201);Furnace body (2) lower weld is on saddle (202), and furnace body (2) is fixedly connected with rack (1) It is integrated.
3. a kind of horizontal reducing atmosphere vacuum annealing furnace according to claim 1, which is characterized in that pivoted arm (301) one end leads to It crosses aligning device (303) to connect with fire door (3), pivoted arm (301) other end is connect by shaft (302) with furnace body (2), such stove Door (3) (302) can rotate around the shaft, be opened and closed;Aligning device (303) is mounted on fire door (3) outer side center position It puts, for multidirectional adjusting fire door (3) position.
A kind of 4. horizontal reducing atmosphere vacuum annealing furnace according to claim 1, which is characterized in that flue (4) setting Internal in furnace body (2), flue (4) both sides are equipped with idler wheel (401), slide and match between these idler wheels (401) and guide-track groove (201) Close connection so that idler wheel (401) can be free to slide on guide-track groove (201), and flue (4) is equipped with interior fire door (402), is inciting somebody to action Interior fire door (402) forms the heating space of closing after closing.
5. a kind of horizontal reducing atmosphere vacuum annealing furnace according to claim 1, which is characterized in that in flue (4) The adiabatic heat-insulation furnace lining (5) in portion is made of multiple layer refractory.
A kind of 6. horizontal reducing atmosphere vacuum annealing furnace according to claim 1, which is characterized in that the control system (9) For measuring temperature and pressure during material sintering in real time, and can atmosphere filling and displacement be carried out according to material sintering process, from It is dynamic to open and close heating.
A kind of 7. horizontal reducing atmosphere vacuum annealing furnace according to claim 1, which is characterized in that the safety device (10) Mounted on furnace body (2) top, work in furnace body (2) inner overpressure or gas burst, equipment safety can be protected.
A kind of 8. horizontal reducing atmosphere vacuum annealing furnace according to claim 1, which is characterized in that the radiator (11) Mounted on furnace body (2) top, for reducing the surface temperature of furnace body (2).
CN201810007000.2A 2018-01-04 2018-01-04 A kind of horizontal reducing atmosphere vacuum annealing furnace Pending CN108204737A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810007000.2A CN108204737A (en) 2018-01-04 2018-01-04 A kind of horizontal reducing atmosphere vacuum annealing furnace

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201810007000.2A CN108204737A (en) 2018-01-04 2018-01-04 A kind of horizontal reducing atmosphere vacuum annealing furnace

Publications (1)

Publication Number Publication Date
CN108204737A true CN108204737A (en) 2018-06-26

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CN201810007000.2A Pending CN108204737A (en) 2018-01-04 2018-01-04 A kind of horizontal reducing atmosphere vacuum annealing furnace

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN117329860A (en) * 2023-10-05 2024-01-02 广东泛瑞新材料有限公司 Energy-saving rotary vacuum annealing furnace

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2887886Y (en) * 2005-07-08 2007-04-11 北京易西姆工业炉科技发展有限公司 Vacuum thermal-treatment furnace
CN202092461U (en) * 2011-05-27 2011-12-28 合肥高歌热处理应用技术有限公司 Vacuum atmosphere tube furnace

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2887886Y (en) * 2005-07-08 2007-04-11 北京易西姆工业炉科技发展有限公司 Vacuum thermal-treatment furnace
CN202092461U (en) * 2011-05-27 2011-12-28 合肥高歌热处理应用技术有限公司 Vacuum atmosphere tube furnace

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN117329860A (en) * 2023-10-05 2024-01-02 广东泛瑞新材料有限公司 Energy-saving rotary vacuum annealing furnace
CN117329860B (en) * 2023-10-05 2024-02-13 广东泛瑞新材料有限公司 Energy-saving rotary vacuum annealing furnace

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Application publication date: 20180626

RJ01 Rejection of invention patent application after publication