CN108165173A - A kind of graphene root resistant waterproof roll - Google Patents
A kind of graphene root resistant waterproof roll Download PDFInfo
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- CN108165173A CN108165173A CN201711168581.XA CN201711168581A CN108165173A CN 108165173 A CN108165173 A CN 108165173A CN 201711168581 A CN201711168581 A CN 201711168581A CN 108165173 A CN108165173 A CN 108165173A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D195/00—Coating compositions based on bituminous materials, e.g. asphalt, tar, pitch
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/18—Fireproof paints including high temperature resistant paints
-
- E—FIXED CONSTRUCTIONS
- E04—BUILDING
- E04D—ROOF COVERINGS; SKY-LIGHTS; GUTTERS; ROOF-WORKING TOOLS
- E04D5/00—Roof covering by making use of flexible material, e.g. supplied in roll form
- E04D5/10—Roof covering by making use of flexible material, e.g. supplied in roll form by making use of compounded or laminated materials, e.g. metal foils or plastic films coated with bitumen
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Architecture (AREA)
- Civil Engineering (AREA)
- Structural Engineering (AREA)
- Paints Or Removers (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
The invention discloses a kind of graphene root resistant waterproof roll, including tire base and dip-coating the modified asphalt layer on tire base, which is made of following components and parts by weight：48 60 parts of pitch, 40 48 parts of rubber powder, 10 15 parts of SBS modifier, 10 15 parts of graphene oxide, 35 parts of fire retardant, 5 10 parts of machine oil, chemical 5 10 parts of root resistance agent, 0.5 1 parts of filler material, 0.5 2 parts of SBS modified asphalt stabilizers.Graphene root resistant waterproof roll of the present invention is enhanced on pulling force, heat resistance, resistance to ag(e)ing, low temperature flexibility.
Description
Technical field
The invention belongs to building material technical fields, and in particular to a kind of graphene root resistant waterproof roll.
Background technology
To improve housing conditions and living environment, the green plant in roof is increasingly paid attention to by people, at present, western developed country,
Such as the building roof greening technique that the states such as the U.S., Japan, Singapore use, to improving city environmental quality, beautification rapidly
Urban environment plays huge effect.Roof greening has protection top of building, extends building service life；Mitigate city
City's discharge pressure；The energy is saved, heat insulating effect is good；Sound insulation and noise reduction acts on and improves air quality, mesoclimate, and can
Play the role of beautifying the environment.
But in routine use of the existing roof greening in building course and after building up, equal destructible roof is prevented
Water and drainage system, so as to cause roof leak.The roof greening system of building is generally glued using common in the prior art
The outer heat preservation system that knot mortar and decorative mortar are formed is also easy to produce cracking, infiltration etc., fails so as to cause thermal insulation of roof waterproof；And
If there is the root system of plant of very strong penetration capacity building roof can be formed and wear as waterproof layer using conventional waterproof coiled material
Thoroughly, cause waterproof damage layer and cause roof leak, once roof leakage, will just face entire roofing is rooted out, repair and
High reparation will be formed and reform a series of catastrophic problems of expense.
Therefore, while studying, develop one kind with high-effective water-proof, having can prevent from preparing the high-strength waterproof volume punctured
Material is applied to roof greening, can be citizen, be that society brings welfare, has important social effect and application value.
Chinese patent application No. is 201220422929.X provides a kind of planted roof root resistant waterproof roll, packet
The compound plies of copper foil is included, the two sides of the compound plies of copper foil are respectively equipped with SBS modified asphalt layers, the SBS modified pitch
The outer surface of layer is equipped with protective layer；The SBS modified asphalt layers are made of the SBS modified pitch for being added with chemical root resistance agent.
Chinese patent application No. is 201310069167.9 provides a kind of combination modified pitch root-resistant puncturing waterproof volume
Material and preparation method thereof is combined by face layer, upper waterproof layer, tire base, lower waterproof layer and bottom；Upper waterproof layer and lower waterproof
The material composition and weight percent proportioning of layer are as follows；The material of the upper waterproof layer and lower waterproof layer forms and weight percent
Proportioning is as follows：Pitch 20~60%；Machine oil 15~20%；Polyolefin 2~15%；SBS3~15%；Wollastonite powder 10~
25%；Silicon carbide whisker powder 1~5%；Silicon nitride crystal whisker powder 1~5%；Calcium carbonate crystal whisker powder 1~10%；It is nano oxidized
Zinc 0.1~6%；Chemical root resistance agent 0.5~5.0%.
Chinese patent application No. is 201310738653.5 provides a kind of planted roof root resistant waterproof roll, packet
Include 28~30 parts of pitch, SBS2~6 part, SBR3~6 part, APP1.6~7 part, 15~23 parts of compound lard, 3~6 parts of fire retardant,
Resistance to 10~13 parts of plasticizer of migration, 23~24 parts of Corvic, 8~10 parts of portland cement powder, nano zine oxide 1.0~
1.2 parts, 1~5 part of dibasic lead phosphite, 2~8 parts of ternary chlorine vinegar resin, 1~5 part of ABS resin, 909 anti-freezing type adhesive glues 15
~22 parts, 10~12 parts of polypropylene fiber silk and chemical 0.8~1.2 part of root resistance agent.
Chinese patent application No. is 201410322553.9 provides a kind of compound root-resistant puncturing of planted roof and prevents
Water coiled material intersects film including bitumen layer on tire base of tire base, dip-coating and high density strength, and the bitumen layer is by following parts by weight
Several component compositions：700~1500 parts of 10# pitches, 700~1500 parts of 90# pitches, 600~1200 parts of rubber powder, SBS50~250
Part, APP50~250 part, IPP0~150 part, 100~400 parts of machine oil, 1000~1800 parts of mountain flour, chemical root resistance agent 20~80
Part.
Chinese patent application No. is 201310738653.5 provides a kind of planted roof root resistant waterproof roll, packet
Include 28~30 parts of pitch, SBS2~6 part, SBR3~6 part, APP1.6~7 part, 15~23 parts of compound lard, 3~6 parts of fire retardant,
Resistance to 10~13 parts of plasticizer of migration, 23~24 parts of Corvic, 8~10 parts of portland cement powder, nano zine oxide 1.0~
1.2 parts, 1~5 part of dibasic lead phosphite, 2~8 parts of ternary chlorine vinegar resin, 1~5 part of ABS resin, 909 anti-freezing type adhesive glues 15
~22 parts, 10~12 parts of polypropylene fiber silk and chemical 0.8~1.2 part of root resistance agent.
Invention content
On planted roof root resistant waterproof roll, although there are many formulas of bitumen layer in above-mentioned background technology,
But the performance of waterproof roll still can further be enhanced.
Applicant passes through certain retrieval and research and development, adjusts the formula of bitumen layer, to reach it is a kind of in pulling force, it is heat-resisting
The effect that can enhance in property, resistance to ag(e)ing, low temperature flexibility.For this purpose, applicant is made that experiment many times, many is tested
Kind different component and dosage, have paid creative work, have just obtained the present invention.
The purpose of the present invention is to provide a kind of resistance to of graphenes that can enhance on pulling force, heat resistance, low temperature flexibility
Puncture waterproof roll.
Used technical solution is：
A kind of graphene root resistant waterproof roll, it is described to change including tire base and dip-coating the modified asphalt layer on tire base
Property bitumen layer is made of following components and parts by weight：
Further, the pitch is 90#Pitch.
Further, the rubber powder is nylon rubber powder.
Further, the SBS modified asphalt stabilizers are polyolefins.
In the technical solution of the present invention, SBS modifier and pitch are mixed to form modified pitch, which can carry
Lower temperature resistance, elasticity and the flexibility of high entire product and the resistance to ag(e)ing for improving entire product.
Fire retardant improves the anti-flammability of product, can be additive flame retardant, reduce the combustibility of the organic materials such as pitch.
Machine oil can improve the lubricity of product and improve the compatibility of the entire each component of product.
SBS modified asphalt stabilizers increase the stability of entire formula mixture, improve SBS modifier and pitch
Compatibility has the function that improve modified pitch storage stability.
Graphene oxide is because after oxidized, oxygen-containing functional group increases and makes property more active compared with graphene thereon.Application
People has found that the addition of graphene oxide can improve pulling force, heat resistance, resistance to ag(e)ing, the low temperature flexibility of product entirety.
The content of each component is repeatedly to grope to adjust through applicant, enables each component preferably phase being entirely formulated
It is molten to form entire product.
During preparation, the mixing of pitch, rubber powder and SBS modifier is warming up to 180~190 DEG C, is then added while stirring
Enter fire retardant, machine oil, chemical root resistance agent, filler material, SBS modified asphalt stabilizers, it is equal finally to add graphene oxide stirring
It is even, modified asphalt layer is made；Then by modified asphalt layer dip-coating on tire base up to graphene root resistant waterproof roll.It is necessary
When, it can be in the further coating surface spacer material layer of modified asphalt layer, such as PE films.
The beneficial effects of the present invention are：
The graphene root resistant waterproof roll of the present invention obtains on pulling force, heat resistance, resistance to ag(e)ing, low temperature flexibility
Enhancing.
Specific embodiment
Technical scheme of the present invention is further described, but only from the numerous realities of applicant with reference to embodiment and comparative example
The section Example and comparative example enumerated in testing, the present invention claims protection domain be not limited thereto.
Embodiment 1
The graphene root resistant waterproof roll of the present embodiment, including tire base and dip-coating the modified asphalt layer on tire base,
The modified asphalt layer is made of following components and parts by weight：
Embodiment 2
The graphene root resistant waterproof roll of the present embodiment, including tire base and dip-coating the modified asphalt layer on tire base,
The modified asphalt layer is made of following components and parts by weight：
Embodiment 3
The graphene root resistant waterproof roll of the present embodiment, including tire base and dip-coating the modified asphalt layer on tire base,
The modified asphalt layer is made of following components and parts by weight：
Embodiment 4
The graphene root resistant waterproof roll of the present embodiment, including tire base and dip-coating the modified asphalt layer on tire base,
The modified asphalt layer is made of following components and parts by weight：
Embodiment 5
The graphene root resistant waterproof roll of the present embodiment, including tire base and dip-coating the modified asphalt layer on tire base,
The modified asphalt layer is made of following components and parts by weight：
Comparative example 1-5
Graphene oxide will be added without in the modified pitch layer formula of embodiment 1-5, other components and its content correspond to real
It applies a 1-5 to remain unchanged, is contrasted a 1-5.
By graphene root resistant waterproof roll made from above each embodiment and comparative example, performance inspection is carried out to it
It surveys, obtains the following table 1：
Table 1
The detection method of graphene root resistant waterproof roll is consistent made from this each embodiment and comparative example, such as draws
Power, heat resistance, low temperature flexibility, impermeability are tested using the standard of GB18242-2008d, and root-resistant puncturing experiment uses
The standard of JC/T1075-2008 is tested.Puncture resistant ability is judged according to the physical property and root-resistant puncturing performance of product
Out.The comprehensive performances such as low temperature flexibility, puncture resistant ability can embody resistance to ag(e)ing.
As can be known from the above table, relative to comparative example, the addition of graphene oxide is drawing graphene root resistant waterproof roll
Power, resistance to ag(e)ing, is enhanced on low temperature flexibility heat resistance, is improved in each lower limit value, amplification exceeds
Expection, achieves unexpected technique effect！
On this basis, applicant further retrieves discovery：
Chinese patent application No. is 201710583187.6 provides a kind of roof greening waterproof roll, including base material
Layer, the substrate layer are glass carpet veneer, and the waterproof roll further includes the self-adhesive modified asphalt layer for being arranged on substrate layer upper surface,
The toughness waterproof layer of substrate layer lower surface is arranged on, the self-adhesive modified asphalt layer upper surface is equipped with reinforced waterproofing layer, described to add
Strong waterproof layer upper surface is equipped with root-resistant puncturing layer, and the toughness waterproof layer lower surface is equipped with PE films.The toughness waterproof layer is stone
Black alkene/natural rubber nano composite material layer.The reinforced waterproofing layer is epoxy resin/graphite alkene nanometer composite layer.Institute
Root-resistant puncturing layer is stated as poly- N, N- dimethacrylamide/stannic oxide/graphene nano composite layer.
Chinese patent application No. is 201620833967.2 provides a kind of root resistant waterproof roll, prevents including toughness
Water layer, the toughness waterproof layer are arranged on toughness and strengthen in layer surface, and the toughness enhancement layer is arranged on the surface of bitumen layer, institute
It states bitumen layer to be arranged on waterproof matrix, another exposed surface of the waterproof matrix and toughness waterproof layer is equipped with sealer.
The toughness waterproof layer is graphene modified polyurethane coating.The toughness enhancement layer is compound for graphene/natural rubber nano
Material.
Chinese patent application No. is 201610333427.2 provides a kind of novel high-performance waterproof roll, including base
(1), modified layer (2)；The base (1) is formed using scrim surfaces coating conductive nanometer slurry, and the modified layer, which uses, to be changed
Property high molecular material is made.The conductive nanometer slurry includes resin, conductive nanometer material, auxiliary agent, cosolvent mixing system
Into.The resin is at least one of epoxy resin, polyurethane resin, acrylic resin, alkyd resin；The conductive nanometer
Material is at least one of carbon nanotube, graphene, carbon black, graphite；The auxiliary agent includes dispersant, antifoaming agent, levelling agent, profit
At least one of humectant, adhesion promoter, color fixing agent；The cosolvent is water, ethylene glycol monomethyl ether, propylene glycol monomethyl ether acetic acid
At least one of ester, propylene-glycol ethyl ether, dimethylbenzene.The modified layer (2) is using pitch, softening agent, modifying agent, filler material, work(
Energy property film (3), pre- immersion oil are mixed, and the functional film (3) is arranged on the modified layer (2) surface.
It has been found that there are no a kind of formula that graphene oxide is individually added into for bitumen layer, examples in the prior art
Patent document such as above-mentioned application number 201710583187.6,201620833967.2 and 201610333427.2 has all referred to
Graphene, but all no technical inspiration is gone in the formula for adding in bitumen layer.
CN201710583187.6 is that graphene/natural rubber nano composite material layer and epoxy are set except bitumen layer
Resin/graphite alkene nanometer composite layer, each layer are separated from each other.
CN201620833967.2 be except bitumen layer setting graphene/natural rubber nano composite material layer, each layer that
This is separated.
CN201610333427.2 is that base is formed using scrim surfaces coating conductive nanometer slurry, conductive nanometer material
Material includes graphene；And it is bitumen layer that modified layer is corresponding, base and modified layer are also that each layer is separated from each other.
Graphene oxide is directly added into the formula of modified asphalt layer by the application so that graphene root-resistant puncturing obtained
Waterproof roll also achieves while being all improved in each performance such as pulling force, heat resistance, resistance to ag(e)ing, low temperature flexibility
Unexpected technique effect.
Claims (4)
1. a kind of graphene root resistant waterproof roll, which is characterized in that including tire base and dip-coating the modified pitch on tire base
Layer, the modified asphalt layer are made of following components and parts by weight：
2. graphene root resistant waterproof roll according to claim 1, which is characterized in that the pitch is 90#Pitch.
3. graphene root resistant waterproof roll according to claim 1, which is characterized in that the rubber powder is nylon glue
Powder.
4. graphene root resistant waterproof roll according to claim 1, which is characterized in that the SBS modified pitch is steady
It is polyolefins to determine agent.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201711168581.XA CN108165173A (en) | 2017-11-22 | 2017-11-22 | A kind of graphene root resistant waterproof roll |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711168581.XA CN108165173A (en) | 2017-11-22 | 2017-11-22 | A kind of graphene root resistant waterproof roll |
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| CN108165173A true CN108165173A (en) | 2018-06-15 |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109401347A (en) * | 2018-10-31 | 2019-03-01 | 山东清池防水材料股份有限公司 | A kind of waterproof roll combustion inhibitor special and preparation method thereof |
| CN110126412A (en) * | 2019-05-29 | 2019-08-16 | 崇左市豫祥科技股份有限公司 | A kind of SBS root-resistant puncturing waterproof material and preparation method thereof |
| CN111117499A (en) * | 2018-10-31 | 2020-05-08 | 山东清池防水材料股份有限公司 | Elastomer modified asphalt waterproof coiled material and preparation method thereof |
| CN113861866A (en) * | 2021-09-03 | 2021-12-31 | 惠州东方雨虹建筑材料有限责任公司 | Self-adhesion asphalt waterproof board |
| CN114958237A (en) * | 2022-06-06 | 2022-08-30 | 潍坊市宇虹防水材料(集团)有限公司 | Enhanced self-adhesive polymer modified asphalt polyester tire waterproof coiled material |
| CN116591402A (en) * | 2023-04-21 | 2023-08-15 | 湖北卓众之众防水材料有限公司 | Roof waterproof system is built to green |
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| CN107364193A (en) * | 2017-07-17 | 2017-11-21 | 合肥威斯伏新材料有限公司 | A kind of modified coiled material of waste and old waterproof roll and preparation method |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109401347A (en) * | 2018-10-31 | 2019-03-01 | 山东清池防水材料股份有限公司 | A kind of waterproof roll combustion inhibitor special and preparation method thereof |
| CN111117499A (en) * | 2018-10-31 | 2020-05-08 | 山东清池防水材料股份有限公司 | Elastomer modified asphalt waterproof coiled material and preparation method thereof |
| CN110126412A (en) * | 2019-05-29 | 2019-08-16 | 崇左市豫祥科技股份有限公司 | A kind of SBS root-resistant puncturing waterproof material and preparation method thereof |
| CN113861866A (en) * | 2021-09-03 | 2021-12-31 | 惠州东方雨虹建筑材料有限责任公司 | Self-adhesion asphalt waterproof board |
| CN114958237A (en) * | 2022-06-06 | 2022-08-30 | 潍坊市宇虹防水材料(集团)有限公司 | Enhanced self-adhesive polymer modified asphalt polyester tire waterproof coiled material |
| CN114958237B (en) * | 2022-06-06 | 2022-11-25 | 潍坊市宇虹防水材料(集团)有限公司 | Enhanced self-adhesive polymer modified asphalt polyester tire waterproof roll |
| CN116591402A (en) * | 2023-04-21 | 2023-08-15 | 湖北卓众之众防水材料有限公司 | Roof waterproof system is built to green |
| CN116591402B (en) * | 2023-04-21 | 2024-04-02 | 湖北卓众之众防水材料有限公司 | Roof waterproof system is built to green |
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Application publication date: 20180615 |