CN108148398A - A kind of wear-resistant ceramic material and its preparation method and application - Google Patents
A kind of wear-resistant ceramic material and its preparation method and application Download PDFInfo
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- CN108148398A CN108148398A CN201711409836.7A CN201711409836A CN108148398A CN 108148398 A CN108148398 A CN 108148398A CN 201711409836 A CN201711409836 A CN 201711409836A CN 108148398 A CN108148398 A CN 108148398A
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- resistant ceramic
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K13/00—Use of mixtures of ingredients not covered by one single of the preceding main groups, each of these compounds being essential
- C08K13/04—Ingredients characterised by their shape and organic or inorganic ingredients
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B33—ADDITIVE MANUFACTURING TECHNOLOGY
- B33Y—ADDITIVE MANUFACTURING, i.e. MANUFACTURING OF THREE-DIMENSIONAL [3-D] OBJECTS BY ADDITIVE DEPOSITION, ADDITIVE AGGLOMERATION OR ADDITIVE LAYERING, e.g. BY 3-D PRINTING, STEREOLITHOGRAPHY OR SELECTIVE LASER SINTERING
- B33Y70/00—Materials specially adapted for additive manufacturing
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/24—Acids; Salts thereof
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/32—Phosphorus-containing compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/16—Nitrogen-containing compounds
- C08K5/17—Amines; Quaternary ammonium compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K7/00—Use of ingredients characterised by shape
- C08K7/22—Expanded, porous or hollow particles
- C08K7/24—Expanded, porous or hollow particles inorganic
- C08K7/26—Silicon- containing compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/32—Phosphorus-containing compounds
- C08K2003/321—Phosphates
- C08K2003/324—Alkali metal phosphate
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/14—Polymer mixtures characterised by other features containing polymeric additives characterised by shape
- C08L2205/16—Fibres; Fibrils
Abstract
The invention discloses a kind of wear-resistant ceramic materials and its preparation method and application.The wear-resistant ceramic material includes the raw material of following parts by weight：30 55 parts of nylon fiber, 10 25 parts of ceramic, 11 17 parts of dimethylamino isopropanol, 14 18 parts of tertiary sodium phosphate, 8 16 parts of Cyanuric Chloride, 69 parts of modenite powder, 49 parts of isopropyl titanate, 26 parts of potassium aluminate.The wear-resistant ceramic material of the present invention is prepared by nylon fiber, ceramic, dimethylamino isopropanol, tertiary sodium phosphate, Cyanuric Chloride, modenite powder, isopropyl titanate and potassium aluminate, wear-resisting property is good, with excellent mechanical property and corrosion resistance, preparation process is simple, it is easy to accomplish industrialized production.
Description
Technical field
The present invention relates to a kind of ceramics, specifically a kind of wear-resistant ceramic material and its preparation method and application.
Background technology
3D printing also referred to as increasing material manufacturing, is one kind of rapid shaping technique, is known as " the third time industrial revolution "
Core technology.Compared with traditional manufacturing technology, 3D printing does not need to manufacture mold in advance, it is not necessary to which removal is big in the fabrication process
The material of amount also can be obtained by final products without going through complicated forging technology, therefore, structure can be realized in production
Optimization saves material and saves the energy.3D printing technique be suitable for new product development, quick-acting single and parts in small batch manufacture,
The manufacture of complicated shape part, the design of mold and manufacture etc., be also suitable for the manufacture of difficult-to-machine material, configuration design inspection,
Assembly test and Rapid reverse engineering etc..Therefore, 3D printing industry receives concern more and more extensive both at home and abroad, under becoming
One tool rising industry with broad prospects for development.And current low close 3D printing ceramic material is seldom, greatly limits 3D
The selection of printed material.And existing 3D printing ceramic material wear-resisting property is poor, has one to ceramic material after long-time service
Fixed damage.Therefore, the present invention provides a kind of wear-resistant ceramic material and its preparation method and application.
Invention content
The purpose of the present invention is to provide a kind of wear-resistant ceramic material and its preparation method and application, to solve above-mentioned background
The problem of being proposed in technology.
To achieve the above object, the present invention provides following technical solution：
A kind of wear-resistant ceramic material includes the raw material of following parts by weight：30-55 parts of nylon fiber, ceramic 10-25
Part, 11-17 parts of dimethylamino isopropanol, 14-18 parts of tertiary sodium phosphate, 8-16 parts of Cyanuric Chloride, 6-9 parts of modenite powder, metatitanic acid
4-9 parts of isopropyl ester, 2-6 parts of potassium aluminate.
As further embodiment of the present invention：Include the raw material of following parts by weight：35-50 parts of nylon fiber, ceramics are micro-
14-20 parts of powder, 12-15 parts of dimethylamino isopropanol, 15-17 parts of tertiary sodium phosphate, 10-12 parts of Cyanuric Chloride, modenite powder 7-9
Part, 5-7 parts of isopropyl titanate, 3-5 parts of potassium aluminate.
As further embodiment of the present invention：Include the raw material of following parts by weight：42 parts of nylon fiber, ceramic 16
Part, 13 parts of dimethylamino isopropanol, 16 parts of tertiary sodium phosphate, 11 parts of Cyanuric Chloride, 8 parts of modenite powder, 6 parts of isopropyl titanate,
4 parts of potassium aluminate.
A kind of preparation method of wear-resistant ceramic material, includes the following steps：(1) nylon fiber and ceramic are mixed,
It is placed at 180-205 DEG C and is uniformly mixed, mixing speed 350-500r/min；(2) upwards step gains in add in tertiary sodium phosphate,
Modenite powder and potassium aluminate are placed at 210-220 DEG C and are uniformly mixed, mixing speed 150-220r/min；(3) institute is walked upwards
It obtains and isopropyl titanate, Cyanuric Chloride and dimethylamino isopropanol is added in object, be placed at 220-235 DEG C and be uniformly mixed, stirring speed
It spends for 100-200r/min；(4) by upper step gains by extruder squeeze out to get.
As further embodiment of the present invention：Step (1) incorporation time is 15-30min；Step (2) incorporation time is 10-
20min；Step (3) incorporation time is 20-40min.
A kind of wear-resistant ceramic material is used for 3D printing technique field.
Compared with prior art, the beneficial effects of the invention are as follows：
The wear-resistant ceramic material of the present invention passes through nylon fiber, ceramic, dimethylamino isopropanol, tertiary sodium phosphate, three
Polychlorostyrene cyanogen, modenite powder, isopropyl titanate and potassium aluminate are prepared, and wear-resisting property is good, have excellent mechanical property and
Corrosion resistance, preparation process are simple, it is easy to accomplish industrialized production.
Specific embodiment
The technical solution of this patent is described in more detail With reference to embodiment.
Embodiment 1
A kind of wear-resistant ceramic material includes the raw material of following parts by weight：30 parts of nylon fiber, 10 parts of ceramic, two
11 parts of methylamino isopropanol, 14 parts of tertiary sodium phosphate, 8 parts of Cyanuric Chloride, 6 parts of modenite powder, 4 parts of isopropyl titanate, potassium aluminate 2
Part.
A kind of preparation method of wear-resistant ceramic material, includes the following steps：(1) nylon fiber and ceramic are mixed,
It is placed at 180 DEG C and is uniformly mixed, mixing speed 350r/min；(2) tertiary sodium phosphate, modenite are added in step gains upwards
Powder and potassium aluminate are placed at 210 DEG C and are uniformly mixed, mixing speed 150r/min；Incorporation time is 15min；Incorporation time is
10min；(3) isopropyl titanate, Cyanuric Chloride and dimethylamino isopropanol are added in step gains upwards, is placed at 220 DEG C and mixes
Close uniform, mixing speed 100r/min；Incorporation time is 20min；(4) by upper step gains by extruder squeeze out to get.
The wear-resistant ceramic material can be used for 3D printing technique field.
Embodiment 2
A kind of wear-resistant ceramic material includes the raw material of following parts by weight：55 parts of nylon fiber, 25 parts of ceramic, two
17 parts of methylamino isopropanol, 18 parts of tertiary sodium phosphate, 16 parts of Cyanuric Chloride, 9 parts of modenite powder, 9 parts of isopropyl titanate, potassium aluminate
6 parts.
A kind of preparation method of wear-resistant ceramic material, includes the following steps：(1) nylon fiber and ceramic are mixed,
It is placed at 205 DEG C and is uniformly mixed, mixing speed 500r/min；(2) tertiary sodium phosphate, modenite are added in step gains upwards
Powder and potassium aluminate are placed at 220 DEG C and are uniformly mixed, mixing speed 220r/min；Incorporation time is 30min；Incorporation time is
20min；(3) isopropyl titanate, Cyanuric Chloride and dimethylamino isopropanol are added in step gains upwards, is placed at 235 DEG C and mixes
Close uniform, mixing speed 200r/min；Incorporation time is 40min；(4) by upper step gains by extruder squeeze out to get.
The wear-resistant ceramic material can be used for 3D printing technique field.
Embodiment 3
A kind of wear-resistant ceramic material includes the raw material of following parts by weight：42 parts of nylon fiber, 16 parts of ceramic, two
13 parts of methylamino isopropanol, 16 parts of tertiary sodium phosphate, 11 parts of Cyanuric Chloride, 8 parts of modenite powder, 6 parts of isopropyl titanate, potassium aluminate
4 parts.
A kind of preparation method of wear-resistant ceramic material, includes the following steps：(1) nylon fiber and ceramic are mixed,
It is placed at 190 DEG C and is uniformly mixed, mixing speed 400r/min；(2) tertiary sodium phosphate, modenite are added in step gains upwards
Powder and potassium aluminate are placed at 215 DEG C and are uniformly mixed, mixing speed 170r/min；Incorporation time is 20min；Incorporation time is
15min；(3) isopropyl titanate, Cyanuric Chloride and dimethylamino isopropanol are added in step gains upwards, is placed at 230 DEG C and mixes
Close uniform, mixing speed 160r/min；Incorporation time is 30min；(4) by upper step gains by extruder squeeze out to get.
The wear-resistant ceramic material can be used for 3D printing technique field.
Embodiment 4
A kind of wear-resistant ceramic material includes the raw material of following parts by weight：35 parts of nylon fiber, 14 parts of ceramic, two
12 parts of methylamino isopropanol, 15 parts of tertiary sodium phosphate, 10 parts of Cyanuric Chloride, 7 parts of modenite powder, 5 parts of isopropyl titanate, potassium aluminate
3 parts.
A kind of preparation method of wear-resistant ceramic material, includes the following steps：(1) nylon fiber and ceramic are mixed,
It is placed at 185 DEG C and is uniformly mixed, mixing speed 380r/min；(2) tertiary sodium phosphate, modenite are added in step gains upwards
Powder and potassium aluminate are placed at 215 DEG C and are uniformly mixed, mixing speed 165r/min；Incorporation time is 18min；Incorporation time is
12min；(3) isopropyl titanate, Cyanuric Chloride and dimethylamino isopropanol are added in step gains upwards, is placed at 228 DEG C and mixes
Close uniform, mixing speed 128r/min；Incorporation time is 22min；(4) by upper step gains by extruder squeeze out to get.
The wear-resistant ceramic material can be used for 3D printing technique field.
Embodiment 5
A kind of wear-resistant ceramic material includes the raw material of following parts by weight：50 parts of nylon fiber, 20 parts of ceramic, two
15 parts of methylamino isopropanol, 17 parts of tertiary sodium phosphate, 12 parts of Cyanuric Chloride, 9 parts of modenite powder, 7 parts of isopropyl titanate, potassium aluminate
5 parts.
A kind of preparation method of wear-resistant ceramic material, includes the following steps：(1) nylon fiber and ceramic are mixed,
It is placed at 200 DEG C and is uniformly mixed, mixing speed 450r/min；(2) tertiary sodium phosphate, modenite are added in step gains upwards
Powder and potassium aluminate are placed at 215 DEG C and are uniformly mixed, mixing speed 210r/min；Incorporation time is 25min；Incorporation time is
16min；(3) isopropyl titanate, Cyanuric Chloride and dimethylamino isopropanol are added in step gains upwards, is placed at 230 DEG C and mixes
Close uniform, mixing speed 180r/min；Incorporation time is 32min；(4) by upper step gains by extruder squeeze out to get.
The wear-resistant ceramic material can be used for 3D printing technique field.
Comparative example 1
A kind of wear-resistant ceramic material includes the raw material of following parts by weight：50 parts of nylon fiber, 20 parts of ceramic, phosphorus
Sour 17 parts of trisodium, 12 parts of Cyanuric Chloride, 9 parts of modenite powder, 7 parts of isopropyl titanate, 5 parts of potassium aluminate.
A kind of preparation method of wear-resistant ceramic material, includes the following steps：(1) nylon fiber and ceramic are mixed,
It is placed at 200 DEG C and is uniformly mixed, mixing speed 450r/min；(2) tertiary sodium phosphate, modenite are added in step gains upwards
Powder and potassium aluminate are placed at 215 DEG C and are uniformly mixed, mixing speed 210r/min；Incorporation time is 25min；Incorporation time is
16min；(3) isopropyl titanate and Cyanuric Chloride are added in step gains upwards, is placed at 230 DEG C and is uniformly mixed, mixing speed
For 180r/min；Incorporation time is 32min；(4) by upper step gains by extruder squeeze out to get.The wear-resistant ceramic material
Available for 3D printing technique field.
Comparative example 2
A kind of wear-resistant ceramic material includes the raw material of following parts by weight：50 parts of nylon fiber, 20 parts of ceramic, two
15 parts of methylamino isopropanol, 17 parts of tertiary sodium phosphate, 9 parts of modenite powder, 7 parts of isopropyl titanate, 5 parts of potassium aluminate.
A kind of preparation method of wear-resistant ceramic material, includes the following steps：(1) nylon fiber and ceramic are mixed,
It is placed at 200 DEG C and is uniformly mixed, mixing speed 450r/min；(2) tertiary sodium phosphate, modenite are added in step gains upwards
Powder and potassium aluminate are placed at 215 DEG C and are uniformly mixed, mixing speed 210r/min；Incorporation time is 25min；Incorporation time is
16min；(3) isopropyl titanate and dimethylamino isopropanol are added in step gains upwards, is placed at 230 DEG C and is uniformly mixed, stir
Speed is mixed as 180r/min；Incorporation time is 32min；(4) by upper step gains by extruder squeeze out to get.The wear-resisting pottery
Ceramic material can be used for 3D printing technique field.
Comparative example 3
A kind of wear-resistant ceramic material includes the raw material of following parts by weight：50 parts of nylon fiber, 20 parts of ceramic, phosphorus
Sour 17 parts of trisodium, 9 parts of modenite powder, 7 parts of isopropyl titanate, 5 parts of potassium aluminate.
A kind of preparation method of wear-resistant ceramic material, includes the following steps：(1) nylon fiber and ceramic are mixed,
It is placed at 200 DEG C and is uniformly mixed, mixing speed 450r/min；(2) tertiary sodium phosphate, modenite are added in step gains upwards
Powder and potassium aluminate are placed at 215 DEG C and are uniformly mixed, mixing speed 210r/min；Incorporation time is 25min；Incorporation time is
16min；(3) isopropyl titanate is added in step gains upwards, is placed at 230 DEG C and is uniformly mixed, mixing speed 180r/min；
Incorporation time is 32min；(4) by upper step gains by extruder squeeze out to get.The wear-resistant ceramic material can be used for 3D printing
Technical field.
Experimental example
The wear-resistant ceramic material prepared to embodiment 5 and comparative example 1-3 is tested for the property, and as a result see the table below.
Table
The better embodiment of this patent is explained in detail above, but this patent is not limited to above-mentioned embodiment party
Formula, can also be under the premise of this patent objective not be departed from the knowledge that one skilled in the relevant art has
It makes a variety of changes.
Claims (6)
1. a kind of wear-resistant ceramic material, which is characterized in that include the raw material of following parts by weight：30-55 parts of nylon fiber, ceramics
10-25 parts of micro mist, 11-17 parts of dimethylamino isopropanol, 14-18 parts of tertiary sodium phosphate, 8-16 parts of Cyanuric Chloride, modenite powder 6-
9 parts, 4-9 parts of isopropyl titanate, 2-6 parts of potassium aluminate.
2. wear-resistant ceramic material according to claim 1, which is characterized in that include the raw material of following parts by weight：Nylon
35-50 parts of fiber, 14-20 parts of ceramic, 12-15 parts of dimethylamino isopropanol, 15-17 parts of tertiary sodium phosphate, Cyanuric Chloride 10-
12 parts, 7-9 parts of modenite powder, 5-7 parts of isopropyl titanate, 3-5 parts of potassium aluminate.
3. wear-resistant ceramic material according to claim 1, which is characterized in that include the raw material of following parts by weight：Nylon
42 parts of fiber, 16 parts of ceramic, 13 parts of dimethylamino isopropanol, 16 parts of tertiary sodium phosphate, 11 parts of Cyanuric Chloride, modenite powder
8 parts, 6 parts of isopropyl titanate, 4 parts of potassium aluminate.
4. a kind of preparation method of wear-resistant ceramic material as described in any one of claims 1-3, which is characterized in that including following step
Suddenly：（1）Nylon fiber and ceramic are mixed, is placed at 180-205 DEG C and is uniformly mixed, mixing speed 350-500r/
min；（2）Tertiary sodium phosphate, modenite powder and potassium aluminate are added in step gains upwards, is placed at 210-220 DEG C and is uniformly mixed,
Mixing speed is 150-220r/min；（3）Upwards isopropyl titanate, Cyanuric Chloride and dimethylamino isopropyl are added in step gains
Alcohol is placed at 220-235 DEG C and is uniformly mixed, mixing speed 100-200r/min；（4）Upper step gains are squeezed by extruder
Go out to get.
5. the preparation method of wear-resistant ceramic material according to claim 4, which is characterized in that step（1）Incorporation time is
15-30min；Step（2）Incorporation time is 10-20min；Step（3）Incorporation time is 20-40min.
6. a kind of wear-resistant ceramic material as described in any one of claims 1-3 is used for 3D printing technique field.
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| CN201711409836.7A CN108148398A (en) | 2017-12-23 | 2017-12-23 | A kind of wear-resistant ceramic material and its preparation method and application |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111677686A (en) * | 2020-06-03 | 2020-09-18 | 黄河水利委员会黄河水利科学研究院 | Wear-resistant mouth ring of centrifugal water pump and preparation method thereof |
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Application publication date: 20180612 |