CN108144408A - A kind of recovery system for organic solvent and its recovery method - Google Patents

A kind of recovery system for organic solvent and its recovery method Download PDF

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Publication number
CN108144408A
CN108144408A CN201710382615.9A CN201710382615A CN108144408A CN 108144408 A CN108144408 A CN 108144408A CN 201710382615 A CN201710382615 A CN 201710382615A CN 108144408 A CN108144408 A CN 108144408A
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CN
China
Prior art keywords
adsorption tank
organic solvent
tank
condenser
air
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710382615.9A
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Chinese (zh)
Inventor
唐源欣
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Guangzhou Dili Environmental Protection Technology Co Ltd
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Guangzhou Dili Environmental Protection Technology Co Ltd
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Priority to CN201710382615.9A priority Critical patent/CN108144408A/en
Publication of CN108144408A publication Critical patent/CN108144408A/en
Pending legal-status Critical Current

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2253/00Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/10Inorganic adsorbents
    • B01D2253/102Carbon
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2257/00Components to be removed
    • B01D2257/70Organic compounds not provided for in groups B01D2257/00 - B01D2257/602
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2259/00Type of treatment
    • B01D2259/40Further details for adsorption processes and devices
    • B01D2259/40083Regeneration of adsorbents in processes other than pressure or temperature swing adsorption
    • B01D2259/40088Regeneration of adsorbents in processes other than pressure or temperature swing adsorption by heating
    • B01D2259/4009Regeneration of adsorbents in processes other than pressure or temperature swing adsorption by heating using hot gas

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Analytical Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Treating Waste Gases (AREA)
  • Separation Of Gases By Adsorption (AREA)

Abstract

A kind of recovery system for organic solvent and its recovery method, it is related to technical field of environment protection equipment;It includes air collecting box, filter, aerial cooler, centrifugal high pressure fan, jet chimney, proportion separating tank, adsorption tank, floss hole, condenser, vacuum pump;The side of the air collecting box is connected with filter, aerial cooler and centrifugal high pressure fan in turn, centrifugal high pressure fan is connect by pumping pipeline with several adsorption tanks being set up in parallel, activated carbon is provided in adsorption tank, the side wall of adsorption tank is connected with jet chimney, and floss hole is provided at the top of adsorption tank;The adsorption tank is connect by vacuum pump with condenser, and condenser is connect with proportion separating tank.A kind of recovery system for organic solvent and its recovery method of the present invention, the steam consumption in desorption process is greatly saved, the operating cost of organic solvent recovery process and the treating capacity of waste water are reduced, the condition for reducing solvent and being decomposed since desorption time is long.

Description

A kind of recovery system for organic solvent and its recovery method
Technical field
The present invention relates to technical field of environment protection equipment, and in particular to a kind of recovery system for organic solvent and its recovery method.
Background technology
Traditional handicraft is in desorption process, after steam is passed through, the organic solvent in activated carbon all is desorbed out, simultaneously It also needs to continue to be passed through a large amount of steam, the organic solvent for being desorbed out in adsorption tank is squeezed out into adsorption tank, is sent into condenser.This Desorption process needs 90 minutes, steam consumption 3.3t, and the wastewater flow rate of generation is 3.3t.
Invention content
Steam consumption can be greatlyd save in view of the defects and deficiencies of the prior art, the present invention intends to provide a kind of Recovery system for organic solvent and its recovery method.
To achieve the above object, the technical solution adopted by the present invention is:A kind of recovery system for organic solvent, it includes collection wind It is case, filter, aerial cooler, centrifugal high pressure fan, jet chimney, proportion separating tank, adsorption tank, floss hole, condenser, true Sky pump;The side of the air collecting box is connected with filter, aerial cooler and centrifugal high pressure fan, centrifugal high pressure fan in turn It is connect by pumping pipeline with several adsorption tanks being set up in parallel, activated carbon, the side wall connection of adsorption tank is provided in adsorption tank There is jet chimney, floss hole is provided at the top of adsorption tank;The adsorption tank is connect by vacuum pump with condenser, condenser It is connect with proportion separating tank.
A kind of recovery method of recovery system for organic solvent, it is comprised the following steps:
1st, solvent off-air is emitted in production line production process and is sent into recovery system air collecting box through collecting, by filter and Cooler pre-processes, and the exhaust gas temperature for going out cooler is down to 40 DEG C hereinafter, being pumped again by centrifugal high pressure fan into equipped with activity In the adsorption tank of charcoal;
2nd, solvent exhaust gas is tightly held by activated carbon when passing through active carbon layer in hole, and for air then through layer of charcoal, reaching discharge will The tail gas asked drains into air by adsorption tank top discharge mouth;
3rd, adsorption tank absorption certain time, when will be penetrated at the top of adsorption tank, system is passed through steam heating air lift solvent automatically, Regenerated activated carbon;
4th, after steam is passed through a period of time, organic solvent is all desorbed from activated carbon and comes out, and stopping is passed through steam, opens Vacuum pump is aspirated, and the organic solvent and water vapour that are desorbed from activated carbon is pumped after being condensed into liquid to condenser, Mixing liquid enters proportion separating tank and is automatically separated, and the solvent liquid separated enters storage tank, and waste water is exhausted directly to wastewater treatment .
Preferably, air inlet base-plate valve and outlet air base-plate valve are provided on the adsorption tank, outlet air base-plate valve and discharge Mouth connection.
Preferably, it is additionally provided with inspection socket on the adsorption tank.
Preferably, cleaning bellows are connected on the aerial cooler.
The present invention operation principle be:In desorption process, steam is passed through into adsorption tank, it will be organic molten in activated carbon Agent is desorbed out, and after all desorption comes out organic solvent from activated carbon, stopping is passed through steam, and system automatically turns on vacuum pump It is aspirated, the organic solvent and water vapour that are desorbed from activated carbon is pumped into condenser, this desorption process only needs 30 minutes, steam consumption 1.2t, the wastewater flow rate of generation was 1.2t.
With the above structure, what the present invention generated has the beneficial effect that:A kind of organic solvent recycling system of the present invention System and its recovery method, are greatly saved the steam consumption in desorption process, reduce the operation of organic solvent recovery process into The treating capacity of this and waste water, reduce solvent since desorption time is long and the condition that is decomposed.
Description of the drawings
Fig. 1 is the structure chart of the present invention;
Fig. 2 is the vertical view of Fig. 1.
Reference sign:
Air collecting box 1, filter 2, aerial cooler 3, centrifugal high pressure fan 4, jet chimney 5, proportion separating tank 6, adsorption tank 7, Floss hole 8, condenser 9, vacuum pump 10, air inlet base-plate valve 11, outlet air base-plate valve 12, cleaning bellows 13, inspection socket 14.
Specific embodiment
In order to illustrate more clearly about the embodiment of the present invention or technical scheme of the prior art, to embodiment or will show below There is attached drawing needed in technology description to be briefly described, it should be apparent that, the accompanying drawings in the following description is only this Some embodiments of invention, for those of ordinary skill in the art, without having to pay creative labor, may be used also To obtain other attached drawings according to these attached drawings.
Referring to such as Fig. 1 --- shown in Fig. 2, present embodiment adopts the following technical scheme that:A kind of organic solvent recycling System, it includes air collecting box 1, filter 2, aerial cooler 3, centrifugal high pressure fan 4, jet chimney 5, proportion separating tank 6, inhales Attached slot 7, floss hole 8, condenser 9, vacuum pump 10;The side of the air collecting box 1 is connected with filter 2, air cooling in turn Device 3 and centrifugal high pressure fan 4, centrifugal high pressure fan 4 are connect by pumping pipeline with several adsorption tanks 7 being set up in parallel, absorption Activated carbon is provided in slot 7, the side wall of adsorption tank 7 is connected with jet chimney 5, and the top of adsorption tank 7 is provided with floss hole 8;Institute The adsorption tank 7 stated is connect by vacuum pump 10 with condenser 9, and condenser 9 is connect with proportion separating tank 6.
A kind of recovery method of recovery system for organic solvent, it is comprised the following steps:
1st, solvent off-air is emitted in production line production process and is sent into recovery system air collecting box through collecting, by filter and Cooler pre-processes, and the exhaust gas temperature for going out cooler is down to 40 DEG C hereinafter, being pumped again by centrifugal high pressure fan into equipped with activity In the adsorption tank of charcoal;
2nd, solvent exhaust gas is tightly held by activated carbon when passing through active carbon layer in hole, and for air then through layer of charcoal, reaching discharge will The tail gas asked drains into air by adsorption tank top discharge mouth;
3rd, adsorption tank absorption certain time, when will be penetrated at the top of adsorption tank, system is passed through steam heating air lift solvent automatically, Regenerated activated carbon;
4th, after steam is passed through a period of time, organic solvent is all desorbed from activated carbon and comes out, and stopping is passed through steam, opens Vacuum pump is aspirated, and the organic solvent and water vapour that are desorbed from activated carbon is pumped after being condensed into liquid to condenser, Mixing liquid enters proportion separating tank and is automatically separated, and the solvent liquid separated enters storage tank, and waste water is exhausted directly to wastewater treatment .
Preferably, air inlet base-plate valve 11 and outlet air base-plate valve 12, outlet air base-plate valve 12 are provided on the adsorption tank 7 It is connect with floss hole 8.
Preferably, it is additionally provided with inspection socket 14 on the adsorption tank 7.
Preferably, cleaning bellows 13 are connected on the aerial cooler 3.
The operation principle of present embodiment is:In desorption process, steam is passed through into adsorption tank, it will be in activated carbon Organic solvent be desorbed out, when organic solvent all from activated carbon desorption come out after, stopping be passed through steam, system is opened automatically It opens vacuum pump to be aspirated, the organic solvent and water vapour that are desorbed from activated carbon be pumped into condenser, this desorption Process only needs 30 minutes, steam consumption 1.2t, and the wastewater flow rate of generation is 1.2t.
With the above structure, what present embodiment generated has the beneficial effect that:One described in present embodiment Kind recovery system for organic solvent and its recovery method, are greatly saved the steam consumption in desorption process, reduce organic solvent The operating cost of recovery process and the treating capacity of waste water, the condition for reducing solvent and being decomposed since desorption time is long.
Basic principle of the invention and main feature and advantages of the present invention has been shown and described above.The skill of the industry Art personnel it should be appreciated that the present invention is not limited to the above embodiments, the above embodiments and description only describe The principle of the present invention, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, these Changes and improvements all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and Its equivalent thereof.

Claims (5)

1. a kind of recovery system for organic solvent, it is characterised in that:It includes air collecting box, filter, aerial cooler, centrifugal high pressure Wind turbine, jet chimney, proportion separating tank, adsorption tank, floss hole, condenser, vacuum pump;The side of the air collecting box connects successively It is connected to filter, aerial cooler and centrifugal high pressure fan, centrifugal high pressure fan is set up in parallel by pumping pipeline with several Adsorption tank connects, and is provided with activated carbon in adsorption tank, the side wall of adsorption tank is connected with jet chimney, is provided at the top of adsorption tank Floss hole;The adsorption tank is connect by vacuum pump with condenser, and condenser is connect with proportion separating tank.
2. a kind of recovery method of recovery system for organic solvent, it is characterised in that it is comprised the following steps:
(1), solvent off-air is emitted in production line production process and is sent into recovery system air collecting box through collecting, passes through filter It is pre-processed with cooler, the exhaust gas temperature for going out cooler is down to 40 DEG C hereinafter, being pumped again by centrifugal high pressure fan into equipped with work In the adsorption tank of property charcoal;
(2), solvent exhaust gas is tightly held by activated carbon when passing through active carbon layer in hole, and air then through layer of charcoal, reaches discharge It is required that tail gas air is drained by adsorption tank top discharge mouth;
(3), adsorption tank absorption certain time, when will be penetrated at the top of adsorption tank, it is molten that system is passed through steam heating air lift automatically Agent is regenerated activated carbon;
(4), after steam is passed through a period of time, organic solvent is all desorbed from activated carbon and comes out, and stopping is passed through steam, opens It opens vacuum pump to be aspirated, the organic solvent and water vapour that are desorbed from activated carbon is pumped to condenser and are condensed into liquid Afterwards, mixing liquid enters proportion separating tank and is automatically separated, and the solvent liquid separated enters storage tank, and waste water is exhausted directly at waste water Manage field.
3. a kind of recovery system for organic solvent according to claim 1, it is characterised in that:It is provided on the adsorption tank Air inlet base-plate valve and outlet air base-plate valve, outlet air base-plate valve are connect with floss hole.
4. a kind of recovery system for organic solvent according to claim 1, it is characterised in that:It is also set up on the adsorption tank There is inspection socket.
5. a kind of recovery system for organic solvent according to claim 1, it is characterised in that:Connect on the aerial cooler It is connected to cleaning bellows.
CN201710382615.9A 2017-05-26 2017-05-26 A kind of recovery system for organic solvent and its recovery method Pending CN108144408A (en)

Priority Applications (1)

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CN201710382615.9A CN108144408A (en) 2017-05-26 2017-05-26 A kind of recovery system for organic solvent and its recovery method

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CN201710382615.9A CN108144408A (en) 2017-05-26 2017-05-26 A kind of recovery system for organic solvent and its recovery method

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109930416A (en) * 2019-03-20 2019-06-25 广州市帝东环保科技有限公司 A kind of vegetable fiber environmental protection material and preparation method thereof
CN110237603A (en) * 2018-11-23 2019-09-17 鹤山荣达新材料科技有限公司 A kind of novel dissolvent gas recovery system
CN113599965A (en) * 2021-08-27 2021-11-05 惠州市万绿启佳环保科技有限公司 Organic waste gas treatment process
CN113680171A (en) * 2021-08-27 2021-11-23 惠州市万绿启佳环保科技有限公司 Organic waste gas purification process

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2785692Y (en) * 2005-04-15 2006-06-07 傅太平 Organic solvent recovery device

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2785692Y (en) * 2005-04-15 2006-06-07 傅太平 Organic solvent recovery device

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110237603A (en) * 2018-11-23 2019-09-17 鹤山荣达新材料科技有限公司 A kind of novel dissolvent gas recovery system
CN109930416A (en) * 2019-03-20 2019-06-25 广州市帝东环保科技有限公司 A kind of vegetable fiber environmental protection material and preparation method thereof
CN113599965A (en) * 2021-08-27 2021-11-05 惠州市万绿启佳环保科技有限公司 Organic waste gas treatment process
CN113680171A (en) * 2021-08-27 2021-11-23 惠州市万绿启佳环保科技有限公司 Organic waste gas purification process

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Application publication date: 20180612