CN108126662A - 一种微环境污染治理的吸附器制备方法 - Google Patents
一种微环境污染治理的吸附器制备方法 Download PDFInfo
- Publication number
- CN108126662A CN108126662A CN201810126181.0A CN201810126181A CN108126662A CN 108126662 A CN108126662 A CN 108126662A CN 201810126181 A CN201810126181 A CN 201810126181A CN 108126662 A CN108126662 A CN 108126662A
- Authority
- CN
- China
- Prior art keywords
- pollution control
- temperature
- microenvironment
- zeolite
- absorber preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/20—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising free carbon; comprising carbon obtained by carbonising processes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D49/00—Separating dispersed particles from gases, air or vapours by other methods
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
- B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
- B01J20/12—Naturally occurring clays or bleaching earth
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
- B01J20/14—Diatomaceous earth
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
- B01J20/16—Alumino-silicates
- B01J20/165—Natural alumino-silicates, e.g. zeolites
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
- B01J20/28014—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their form
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/30—Processes for preparing, regenerating, or reactivating
- B01J20/3007—Moulding, shaping or extruding
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/30—Processes for preparing, regenerating, or reactivating
- B01J20/3078—Thermal treatment, e.g. calcining or pyrolizing
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2220/00—Aspects relating to sorbent materials
- B01J2220/40—Aspects relating to the composition of sorbent or filter aid materials
- B01J2220/42—Materials comprising a mixture of inorganic materials
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2220/00—Aspects relating to sorbent materials
- B01J2220/40—Aspects relating to the composition of sorbent or filter aid materials
- B01J2220/48—Sorbents characterised by the starting material used for their preparation
- B01J2220/4875—Sorbents characterised by the starting material used for their preparation the starting material being a waste, residue or of undefined composition
- B01J2220/4887—Residues, wastes, e.g. garbage, municipal or industrial sludges, compost, animal manure; fly-ashes
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Analytical Chemistry (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Geochemistry & Mineralogy (AREA)
- Life Sciences & Earth Sciences (AREA)
- Dispersion Chemistry (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Engineering & Computer Science (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
Abstract
本发明涉及一种微环境污染治理的吸附器制备方法。将陶粉、沸石、硅藻泥、生活垃圾颗粒混合均匀,在温度为120~200℃、压力为0.5~3MPa条件下挤成棒条,在温度为750~850℃、无氧条件下、时间为3‑67h制备成高温炭,然后在850‑950℃下、在水蒸气环境中处理5‑60min,冷却,即得。本发明制备方法简单,成本低,且得到的产品能够对各种污染物具有处理作用,使用寿命长。
Description
技术领域
本发明涉及一种微环境污染治理的吸附器制备方法,属于环保技术领域。
背景技术
微环境是指公交车内环境、地铁内环境、出租车内环境、家居环境以及所有公共场合的环境。我们日常生活中随时接触的“微环境”,比如刚装修好的新家、爸爸的二手烟、新入手的爱车等等。这些微环境容易产生粉尘、甲醛、臭氧等污染物,其危害性不亚于大环境的雾霾等污染物。
针对微环境污染治理的产品比如硅藻泥、活性炭、纳米二氧化钛等,存在产品性能单一、成本高、使用寿命短等缺点。
发明内容
有鉴于此,本发明提供了一种微环境污染治理的吸附器制备方法,制备方法简单,成本低,且得到的产品能够对各种污染物具有处理作用,使用寿命长。
本发明解决其技术问题所采用的技术方案是:
一种微环境污染治理的吸附器制备方法,将陶粉、沸石、硅藻泥、生活垃圾颗粒混合均匀,在温度为120~200℃、压力为0.5~3MPa条件下挤成棒条,在温度为750~850℃、无氧条件下、时间为3-67h制备成高温炭,然后在850-950℃下、在水蒸气环境中处理5-60min,冷却,即得。
按照陶粉、沸石、硅藻泥和生活垃圾颗粒质量比为0.1~10:0.1~10:0.1~10:10。
所述陶粉、沸石、硅藻泥和生活垃圾颗粒均破碎成粉状,粒径为50-150微米。
所述无氧条件每立方米的空间中为氧化性气体的含量低于50ppm。
所述冷却过程按照1-2℃/h的降温速率来降温,降温至室温。
所述水蒸气环境为每立方米的空间中水蒸气的含量为50-500g。
本发明采用陶粉、沸石、硅藻泥、生活垃圾颗粒为原料,通过高压下挤压、高温下碳化和水蒸气下高温处理,可以得到高活性的活性炭,同时使得陶粉、沸石、硅藻泥均匀负载在活性炭上,同时可以发挥各个组分的特点,使得产品的性能得到最大的发挥。
本发明有益效果为:制备方法简单,成本低,其产品可吸附微环境中的有害气体和微细颗粒物,且吸附效果好,使用寿命长,同是实现生活垃圾资源化利用。
具体实施方式
现在结合实施例具体对本发明作进一步详细的说明。
一种微环境污染治理的吸附器制备方法,将陶粉、沸石、硅藻泥、生活垃圾颗粒混合均匀,在温度为120~200℃、压力为0.5~3MPa条件下挤成棒条,在温度为750~850℃、无氧条件下、时间为3-67h制备成高温炭,然后在850-950℃下、在水蒸气环境中处理5-60min,冷却,即得。
按照陶粉、沸石、硅藻泥和生活垃圾颗粒质量比为0.1~10:0.1~10:0.1~10:10。
所述陶粉、沸石、硅藻泥和生活垃圾颗粒均破碎成粉状,粒径为50-150微米。
所述无氧条件每立方米的空间中为氧化性气体的含量低于50ppm。
所述冷却过程按照1-2℃/h的降温速率来降温,降温至室温。
所述水蒸气环境为每立方米的空间中水蒸气的含量为50-500g。
实施例一
一种微环境污染治理的吸附器制备方法,将陶粉、沸石、硅藻泥、生活垃圾颗粒混合均匀,在温度为185℃、压力为2.1MPa条件下挤成棒条,在温度为795℃、无氧条件下、时间为55h制备成高温炭,然后在895℃下、在水蒸气环境中处理40min,冷却,即得。
按照陶粉、沸石、硅藻泥和生活垃圾颗粒质量比为5:5:5:10。
所述陶粉、沸石、硅藻泥和生活垃圾颗粒均破碎成粉状,粒径为85微米。
所述无氧条件每立方米的空间中为氧化性气体的含量低于50ppm。
所述冷却过程按照1.5℃/h的降温速率来降温,降温至室温。
所述水蒸气环境为每立方米的空间中水蒸气的含量为120g。
实施例二
一种微环境污染治理的吸附器制备方法,将陶粉、沸石、硅藻泥、生活垃圾颗粒混合均匀,在温度为185℃、压力为2.1MPa条件下挤成棒条,在温度为795℃、无氧条件下、时间为40h制备成高温炭,然后在895℃下、在水蒸气环境中处理35min,冷却,即得。
按照陶粉、沸石、硅藻泥和生活垃圾颗粒质量比为8:6:7:10。
所述陶粉、沸石、硅藻泥和生活垃圾颗粒均破碎成粉状,粒径为110微米。
所述无氧条件每立方米的空间中为氧化性气体的含量低于50ppm。
所述冷却过程按照1.3℃/h的降温速率来降温,降温至室温。
所述水蒸气环境为每立方米的空间中水蒸气的含量为200g。
实施例3
一种微环境污染治理的吸附器制备方法,将陶粉、沸石、硅藻泥、生活垃圾颗粒混合均匀,在温度为145℃、压力为0.98MPa条件下挤成棒条,在温度为790℃、无氧条件下、时间为21h制备成高温炭,然后在915℃下、在水蒸气环境中处理40min,冷却,即得。
按照陶粉、沸石、硅藻泥和生活垃圾颗粒质量比为3:7:5:10。
所述陶粉、沸石、硅藻泥和生活垃圾颗粒均破碎成粉状,粒径为120微米。
所述无氧条件每立方米的空间中为氧化性气体的含量低于50ppm。
所述冷却过程按照1.8℃/h的降温速率来降温,降温至室温。
所述水蒸气环境为每立方米的空间中水蒸气的含量为200g。
最后说明的是,以上实施例仅用以说明本发明的技术方案而非限制,尽管参照较佳实施例对本发明进行了详细说明,本领域的普通技术人员应当理解,可以对本发明的技术方案进行修改或者等同替换,而不脱离本发明技术方案的宗旨和范围,其均应涵盖在本发明的权利要求范围当中。
Claims (6)
1.一种微环境污染治理的吸附器制备方法,其特征在于,将陶粉、沸石、硅藻泥、生活垃圾颗粒混合均匀,在温度为120~200℃、压力为0.5~3MPa条件下挤成棒条,在温度为750~850℃、无氧条件下、时间为3-67h制备成高温炭,然后在850-950℃下、在水蒸气环境中处理5-60min,冷却,即得。
2.如权利要求1所述的一种微环境污染治理的吸附器制备方法,其特征在于,按照陶粉、沸石、硅藻泥和生活垃圾颗粒质量比为0.1~10:0.1~10:0.1~10:10。
3.如权利要求1所述的一种微环境污染治理的吸附器制备方法,其特征在于,所述陶粉、沸石、硅藻泥和生活垃圾颗粒均破碎成粉状,粒径为50-150微米。
4.如权利要求1所述的一种微环境污染治理的吸附器制备方法,其特征在于,所述无氧条件每立方米的空间中为氧化性气体的含量低于50ppm。
5.如权利要求1所述的一种微环境污染治理的吸附器制备方法,其特征在于,所述冷却过程按照1-2℃/h的降温速率来降温,降温至室温。
6.如权利要求1所述的一种微环境污染治理的吸附器制备方法,其特征在于,所述水蒸气环境为每立方米的空间中水蒸气的含量为50-500g。
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201810126181.0A CN108126662A (zh) | 2018-02-08 | 2018-02-08 | 一种微环境污染治理的吸附器制备方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201810126181.0A CN108126662A (zh) | 2018-02-08 | 2018-02-08 | 一种微环境污染治理的吸附器制备方法 |
Publications (1)
Publication Number | Publication Date |
---|---|
CN108126662A true CN108126662A (zh) | 2018-06-08 |
Family
ID=62430730
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201810126181.0A Pending CN108126662A (zh) | 2018-02-08 | 2018-02-08 | 一种微环境污染治理的吸附器制备方法 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN108126662A (zh) |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1509257A (zh) * | 2002-01-31 | 2004-06-30 | ���弼����˾ | 微孔过滤介质、包含它的过滤体系以及制造和使用方法 |
CN103537255A (zh) * | 2013-07-28 | 2014-01-29 | 王泽辉 | 一种具有分解、杀菌性能的纳米氧化物陶瓷净化吸附材料 |
CN104556027A (zh) * | 2014-12-11 | 2015-04-29 | 惠州学院 | 一种荔枝核活性炭的制备方法 |
CN105056748A (zh) * | 2015-07-15 | 2015-11-18 | 中南林业科技大学 | 一种室内空气自动净化生物器的制备方法 |
CN106732401A (zh) * | 2016-12-26 | 2017-05-31 | 广西筑梦三体科技有限公司 | 一种吸收挥发性有机物的陶瓷膜及其制备方法 |
-
2018
- 2018-02-08 CN CN201810126181.0A patent/CN108126662A/zh active Pending
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1509257A (zh) * | 2002-01-31 | 2004-06-30 | ���弼����˾ | 微孔过滤介质、包含它的过滤体系以及制造和使用方法 |
CN103537255A (zh) * | 2013-07-28 | 2014-01-29 | 王泽辉 | 一种具有分解、杀菌性能的纳米氧化物陶瓷净化吸附材料 |
CN104556027A (zh) * | 2014-12-11 | 2015-04-29 | 惠州学院 | 一种荔枝核活性炭的制备方法 |
CN105056748A (zh) * | 2015-07-15 | 2015-11-18 | 中南林业科技大学 | 一种室内空气自动净化生物器的制备方法 |
CN106732401A (zh) * | 2016-12-26 | 2017-05-31 | 广西筑梦三体科技有限公司 | 一种吸收挥发性有机物的陶瓷膜及其制备方法 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
TWI826408B (zh) | 用於催化甲醛氧化的催化劑及其製備與用途 | |
CN110548488B (zh) | 一种生物炭基富氮复合材料、其制备和应用 | |
CN111359582A (zh) | 一种石墨烯复合气凝胶除甲醛材料及制备方法 | |
CN105214706B (zh) | 一种用于废气处理的催化陶瓷烧结环及制备方法 | |
CN108147835B (zh) | 一种以细菌纤维素为生物模板制备具有多级孔结构的陶瓷块体的方法 | |
CN112121790A (zh) | 核壳结构型锰系催化剂及其制备方法 | |
CN112473404A (zh) | 一种具有zif-8笼状结构的混合基质碳分子筛膜的制备方法及应用 | |
CN107670641B (zh) | 一种石墨烯空气净化材料及其制备方法 | |
CN108126662A (zh) | 一种微环境污染治理的吸附器制备方法 | |
CN102671626B (zh) | 净化空气用炭陶的制备工艺 | |
CN110368897B (zh) | 一种煤焦油基超高比表面积含氮多孔炭及其制备方法和应用 | |
CN115254070B (zh) | 一种可高温脱附的复合蜂窝吸附材料及其制备方法和应用 | |
CN110237783B (zh) | 一种提高炭气凝胶抗氧化性能的方法以及由此制得的改性炭气凝胶 | |
CN100588457C (zh) | 一种吸附co2用超级活性炭粉体的成型方法 | |
CN114984913B (zh) | 一种新型碳捕集材料的制备方法及应用 | |
CN103979536B (zh) | 一种二噁英吸附专用活性炭的制备方法 | |
CN114471143B (zh) | 一种缺陷氧化铝调质的宽温脱硫剂及其制备方法及应用 | |
CN102744091B (zh) | 多孔无机陶瓷膜-石墨烯-N改性TiO2光触媒材料及其制备方法 | |
CN110437720B (zh) | 一种室内有害气体吸附型水性聚氨酯涂料及其制备方法 | |
KR102181924B1 (ko) | 나노 금속분말을 이용한 유해가스 제거용 고효율 활성탄소 제조 방법 | |
CN111888837A (zh) | 用于空气净化的环保复合新材料及其制备方法 | |
CN112108115A (zh) | 室温催化降解多种有机物的炭基复合材料的制备方法及测试装置 | |
CN107573094B (zh) | 一种用于高温环境的微孔陶粒过滤介质及其制备方法 | |
CN113198477A (zh) | 一种Co3O4-NiO-石墨烯气凝胶催化剂材料的制备方法 | |
CN100525884C (zh) | 一种用于去除空气中有机挥发物的复合净化剂的制备方法 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
PB01 | Publication | ||
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180608 |
|
RJ01 | Rejection of invention patent application after publication |