CN108102396A - A kind of high-quality slender joss stick engraving column wax and preparation method - Google Patents

A kind of high-quality slender joss stick engraving column wax and preparation method Download PDF

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Publication number
CN108102396A
CN108102396A CN201810058586.5A CN201810058586A CN108102396A CN 108102396 A CN108102396 A CN 108102396A CN 201810058586 A CN201810058586 A CN 201810058586A CN 108102396 A CN108102396 A CN 108102396A
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CN
China
Prior art keywords
wax
joss stick
slender joss
quality slender
column
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Application number
CN201810058586.5A
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Chinese (zh)
Inventor
姜颖
刘小青
莫欣欣
魏晓星
侯婷婷
Original Assignee
青岛金王应用化学股份有限公司
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Priority to CN201810058586.5A priority Critical patent/CN108102396A/en
Publication of CN108102396A publication Critical patent/CN108102396A/en

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    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L91/00Compositions of oils, fats or waxes; Compositions of derivatives thereof
    • C08L91/06Waxes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B44DECORATIVE ARTS
    • B44CPRODUCING DECORATIVE EFFECTS; MOSAICS; TARSIA WORK; PAPERHANGING
    • B44C3/00Processes, not specifically provided for elsewhere, for producing ornamental structures
    • B44C3/04Modelling plastic materials, e.g. clay
    • B44C3/046Modelling plastic materials, e.g. clay using a modelling surface, e.g. plate
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/02Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
    • C08L2205/025Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure

Abstract

The present invention provides a kind of high-quality slender joss stick engraving column wax and preparation method.High-quality slender joss stick engraving column wax provided by the invention is used as in the preparation using the fluorubber with good oil resistivity and stability prepares mold.Fluorubber mold when essence additive amount is higher will not dissolved element, the problem of into without candle is caused change colour during storage, ensure that the high-quality slender joss stick quality for carving column wax, reduction problem after sale.It in addition, fluorubber mold has higher structural strength, can be recycled for multiple times, thus, it is possible to reduce the high-quality slender joss stick engraving waxed standby cost of column.

Description

A kind of high-quality slender joss stick engraving column wax and preparation method

Technical field

The present invention relates to candle field more particularly to a kind of high-quality slender joss stick engraving column wax and preparation methods.

Background technology

Candle is a kind of common daily necessities in daily life.According to the difference of purpose of usage, candle is divided into daily illumination Two major class of candle and craftwork candle, thus candle can be widely applied for birthday party, church festival, weddings and funerals and tune In the activity of solar term atmosphere.

Pillar candle, i.e. column wax are a kind of common candle in making candle for domestic illumination and craftwork candle.In the table of column wax The patterns such as face engraving flowers and plants, personage, event and building enable to column wax to form the distinctive engraving column wax of tool.Carve column wax It needs, using softer rubber mold, such as to there is softness, good toughness, easily carry pattern, easy mold release and spy easy to operate in the preparation The nitrile rubber mould of point, before use, inside needs to be carved with pattern in advance the rubber mold, so that the column wax surface prepared With depiction.

Engraving column wax would generally add in essence in the preparation, so that the engraving column wax prepared sends fragrance in burning.When When the additive amount of essence is more than 1.5-2%, nitrile rubber mold easily dissolves out fractions, which so that carving column wax is putting There is the phenomenon that surface discolouration during putting.If engraving column wax there is surface discolouration, seriously affect engraving column wax appearance and Quality, and then influence the sale of candle and handle after sale.

The content of the invention

The present invention provides a kind of high-quality slender joss stick engraving column wax and preparation method, easy in storage to solve existing high-quality slender joss stick engraving column wax The problem of discoloration.

A kind of high-quality slender joss stick engraving column wax of present invention offer, which is used as using fluorubber prepares mold.Fluorine rubber Glue is the synthesis macromolecular elastomer containing fluorine atom on the carbon atom of main chain or side chain.Fluorubber have excellent heat resistance, Inoxidizability, oil resistivity, corrosion resistance and resistance to weathering.The oil resistivity of fluorubber so that fluorubber is higher in essence content When will not dissolve out component, into the quality assurance for without candle is caused to change colour, realizing candle product.At present, it will usually Fluorubber includes fluororubber 23, fluororubber 26, inclined fluoroether rubber, perfluoroelastomers and fluorine silicone rubber etc..In the present invention In embodiment, used fluorubber selects oil resistivity fluorubber to prepare fluorubber mold.

It is provided by the invention it is high-quality slender joss stick engraving column wax in, it is high-quality slender joss stick engraving column wax prepare raw material include paraffin, stearic acid and Additive, wherein, additive includes essence.When fluorubber mold is used to prepare high-quality slender joss stick engraving column wax, added in candle Fragrance content can be the 1-5% of candle gross mass.More there is a choosing, the additive amount of fragrance is the 2- of candle gross mass in candle 5%.In embodiments of the present invention, a diameter of 6-10cm of prepared high-quality slender joss stick engraving column wax, is highly 8-20cm.

The present invention also provides a kind of high-quality slender joss stick engraving waxed Preparation Methods of column, and high-quality slender joss stick engraving column wax is prepared using fluorubber mold.

Specifically, the high-quality slender joss stick engraving waxed Preparation Method of column includes:

S01:Wax material is weighed, wax material is melt-blended at a temperature of 70-120 DEG C, form blended wax;Wherein, wax material is system Raw material used in standby candle, including paraffin, stearic acid and additive.

S02:Dyestuff and essence are added in blended wax, is stirred evenly, forms wax liquor.

S03:Wax liquor is cast at a temperature of 50-110 DEG C in fluorubber mold.

S04:It is cast to the wax liquor in fluorubber mold to cool down, be molded at a temperature of 5-35 DEG C, forms candle;Wherein, wax The wax liquor that temperature is 50-110 DEG C is continuously replenished in liquid cooling procedure.A diameter of 6-10cm is highly 8-20cm

Different shape, appearance or pattern are formed by carving, modifying etc. by high-quality slender joss stick engraving column wax prepared by the above method Candle.However, the engraving of later stage candle needs to realize that this undoubtedly adds production cost by craft or machine.To reduce Manufacturing cost with figuratum high-quality slender joss stick engraving column wax, fluorubber mould inner wall is carved with decorative pattern or pattern, so that the height prepared Perfume engraving column wax is accompanied with pattern.Fluorubber mould inner wall is carved with decorative pattern or pattern and can also realize with the high-quality slender joss stick of depiction The batch production of column wax is carved, improves production efficiency.

The technical solution that the embodiment of the present invention provides can include the following benefits:

The present invention provides a kind of high-quality slender joss stick engraving column wax of high-quality slender joss stick column wax and preparation method.High-quality slender joss stick column wax provided by the invention is high-quality slender joss stick Engraving column wax is used as using the fluorubber with good oil resistivity and stability prepares mold in the preparation.Fluorubber mold is in perfume (or spice) Smart additive amount it is higher when will not dissolved element, the problem of into without candle is caused to change colour during storage, guarantee The quality of the high-quality slender joss stick engraving column wax of high-quality slender joss stick candle, reduces problem after sale.In addition, fluorubber mold has higher structural strength, It can be recycled for multiple times, thus, it is possible to reduce the high-quality slender joss stick engraving waxed standby cost of column of high-quality slender joss stick candle.

It should be appreciated that above general description and following detailed description are only exemplary and explanatory, not It can the limitation present invention.

Description of the drawings

In order to illustrate more clearly of the technical solution of the application, letter will be made to attached drawing needed in the embodiment below Singly introduce, it should be apparent that, for those of ordinary skills, without having to pay creative labor, It can also be obtained according to these attached drawings other attached drawings.

Fig. 1 is the flow diagram of the high-quality slender joss stick engraving waxed Preparation Method of column provided in an embodiment of the present invention.

Specific embodiment

Attached drawing 1 is refer to, attached drawing 1 shows that the flow of the high-quality slender joss stick engraving waxed Preparation Method of column provided in an embodiment of the present invention is shown It is intended to.The description of following specific embodiments is based on attached drawing 1.

Embodiment 1

The embodiment of the present invention provides a kind of high-quality slender joss stick engraving column wax, the high-quality slender joss stick engraving column wax using fluorubber die casting into Type.Specifically preparation method includes high-quality slender joss stick engraving column wax:

S101:Wax material is weighed, wax material is melt-blended at a temperature of 90 DEG C, form blended wax;Wherein, the composition of wax material is pressed Mass fraction includes:Including paraffin 75%, stearic acid 20%, soft wax 2% and auxiliary agent 2%;

S102:Dyestuff and essence are added in blended wax, is stirred evenly, forms wax liquor;Wherein, the additive amount of essence is wax Candle prepares the 1% of raw material gross mass;The weight of dyestuff can be neglected;

S103:Wax liquor is cast at a temperature of 80 DEG C in the fluorubber mold of diameter 7cm × high 14cm;

S104:It is cast to the wax liquor in fluorubber mold to cool down, be molded at a temperature of 5 DEG C, forms candle;Wherein, wax liquor The wax liquor that temperature is 80 DEG C is continuously replenished in cooling procedure.Last time mends wax postcooling 2-24h and forms high-quality slender joss stick engraving column wax.

Embodiment 2

The embodiment of the present invention provides a kind of high-quality slender joss stick engraving column wax, the high-quality slender joss stick engraving column wax using fluorubber die casting into Type.Specifically preparation method includes high-quality slender joss stick engraving column wax:

S201:Wax material is weighed, wax material is melt-blended at a temperature of 100 DEG C, form blended wax;Wherein, the composition of wax material Include by mass fraction:Including paraffin 73%, stearic acid 20%, soft wax 2% and auxiliary agent 2%;

S202:Dyestuff and essence are added in blended wax, is stirred evenly, forms wax liquor;Wherein, the additive amount of essence is wax Candle prepares the 3% of raw material gross mass;The weight of dyestuff can be neglected;

S203:Wax liquor is cast at a temperature of 90 DEG C in the fluorubber mold of diameter 8cm × high 16cm;

S204:It is cast to the wax liquor in fluorubber mold to cool down, be molded at a temperature of 25 DEG C, forms candle;Wherein, wax liquor The wax liquor that temperature is 80 DEG C is continuously replenished in cooling procedure.Last time mends wax postcooling 2-24h and forms high-quality slender joss stick engraving column wax.

Embodiment 3

The embodiment of the present invention provides a kind of high-quality slender joss stick engraving column wax, the high-quality slender joss stick engraving column wax using fluorubber die casting into Type.Specifically preparation method includes high-quality slender joss stick engraving column wax:

S301:Wax material is weighed, wax material is melt-blended at a temperature of 100 DEG C, form blended wax;Wherein, the composition of wax material Include by mass fraction:Including paraffin 71%, stearic acid 20%, soft wax 2% and auxiliary agent 2%;

S302:Dyestuff and essence are added in blended wax, is stirred evenly, forms wax liquor;Wherein, the additive amount of essence is wax Candle prepares the 5% of raw material gross mass;The weight of dyestuff can be neglected;

S303:Wax liquor is cast at a temperature of 90 DEG C in the fluorubber mold of diameter 10cm × high 20cm;

S304:It is cast to the wax liquor in fluorubber mold to cool down, be molded at a temperature of 20 DEG C, forms candle;Wherein, wax liquor The wax liquor that temperature is 70 DEG C is continuously replenished in cooling procedure.Last time mends wax postcooling 2-24h and forms high-quality slender joss stick engraving column wax.

Embodiment 4

The embodiment of the present invention provides a kind of high-quality slender joss stick engraving column wax, the high-quality slender joss stick engraving column wax using fluorubber die casting into Type.Specifically preparation method includes high-quality slender joss stick engraving column wax:

S401:Wax material is weighed, wax material is melt-blended at a temperature of 70 DEG C, form blended wax;Wherein, the composition of wax material is pressed Mass fraction includes:Including paraffin 74%, stearic acid 20%, soft wax 2% and auxiliary agent 2%;

S402:Dyestuff and essence are added in blended wax, is stirred evenly, forms wax liquor;Wherein, the additive amount of essence is wax Candle prepares the 2% of raw material gross mass;The weight of dyestuff can be neglected;

S403:Wax liquor is cast at a temperature of 50 DEG C in the fluorubber mold of diameter 6cm × high 8cm;

S404:It is cast to the wax liquor in fluorubber mold to cool down, be molded at a temperature of 10 DEG C, forms candle;Wherein, wax liquor The wax liquor that temperature is 50 DEG C is continuously replenished in cooling procedure.Last time mends wax postcooling 2-24h and forms high-quality slender joss stick engraving column wax.

Embodiment 5

The embodiment of the present invention provides a kind of high-quality slender joss stick engraving column wax, the high-quality slender joss stick engraving column wax using fluorubber die casting into Type.Specifically preparation method includes high-quality slender joss stick engraving column wax:

S501:Wax material is weighed, wax material is melt-blended at a temperature of 120 DEG C, form blended wax;Wherein, the composition of wax material Include by mass fraction:Including paraffin 72%, stearic acid 20%, soft wax 2% and auxiliary agent 2%;

S502:Dyestuff and essence are added in blended wax, is stirred evenly, forms wax liquor;Wherein, the additive amount of essence is wax Candle prepares the 4% of raw material gross mass;The weight of dyestuff can be neglected;

S503:Wax liquor is cast at a temperature of 110 DEG C in the fluorubber mold of diameter 8cm × high 16cm;

S504:It is cast to the wax liquor in fluorubber mold to cool down, be molded at a temperature of 35 DEG C, forms candle;Wherein, wax liquor The wax liquor that temperature is 110 DEG C is continuously replenished in cooling procedure.Last time mends wax postcooling 2-24h and forms high-quality slender joss stick engraving column wax.

Embodiment 6

The embodiment of the present invention provides a kind of high-quality slender joss stick engraving column wax, the high-quality slender joss stick engraving column wax using fluorubber die casting into Type.Specifically preparation method includes high-quality slender joss stick engraving column wax:

S601:Wax material is weighed, wax material is melt-blended at a temperature of 90 DEG C, form blended wax;Wherein, the composition of wax material is pressed Mass fraction includes:Including paraffin 74%, stearic acid 20%, soft wax 2% and auxiliary agent 2%;

S602:Dyestuff and essence are added in blended wax, is stirred evenly, forms wax liquor;Wherein, the additive amount of essence is wax Candle prepares the 2% of raw material gross mass;The weight of dyestuff can be neglected;

S603:Wax liquor is cast at a temperature of 80 DEG C in the fluorubber mold of diameter 8cm × high 16cm;

S604:It is cast to the wax liquor in fluorubber mold to cool down, be molded at a temperature of 25 DEG C, forms candle;Wherein, wax liquor The wax liquor that temperature is 60 DEG C is continuously replenished in cooling procedure.Last time mends wax postcooling 2-24h and forms high-quality slender joss stick engraving column wax.

Comparative example

The present invention provides a kind of high-quality slender joss stick engraving column wax prepared using nitrile rubber mold, the preparation of the high-quality slender joss stick engraving column wax Method includes:

S1:Wax material is weighed, wax material is melt-blended at a temperature of 100 DEG C, form blended wax;Wherein, the composition of wax material is pressed Mass fraction includes:Including paraffin 73%, stearic acid 20%, soft wax 2% and auxiliary agent 2%;

S2:Dyestuff and essence are added in blended wax, is stirred evenly, forms wax liquor;Wherein, the additive amount of essence is candle Prepare the 3% of raw material gross mass;

S3:Wax liquor is cast at a temperature of 90 DEG C in the nitrile rubber mold of diameter 8cm × high 16cm;

S4:It is cast to the wax liquor in nitrile rubber mold to cool down, be molded at a temperature of 25 DEG C, forms candle;Wherein, wax liquor The wax liquor that temperature is 80 DEG C is continuously replenished in cooling procedure.Last time mends wax postcooling 2-24h and forms high-quality slender joss stick engraving column wax.

It is steady that embodiment 1-6 and the high-quality slender joss stick engraving column wax prepared by comparative example carry out appearance, fragrance and color after the cooling period Qualitative detection, wherein, colour stability detection refers to embodiment 1-6 and high-quality slender joss stick engraving column wax prepared by comparative example in the same terms It is lower preserve one month, six months, 1 year and 2 years after color detection.The concrete outcome of detection refer to table 1.

Table 1:The testing result of embodiment 1-6 and the high-quality slender joss stick engraving column wax prepared by comparative example

Analytical table 1 is understood, with the increase of essence content, the fragrance of the high-quality slender joss stick engraving column wax prepared by fluorubber mold by Gradual change is dense, and the color of candle does not have much variations within 2 years.The preparation process flow and preparation of embodiment 2 and comparative example Condition is identical, is only that the mold selected is different.Comparative example 2 and comparative example are understood, are prepared by nitrile rubber mold high-quality slender joss stick Engraving column wax starts to change colour after storing 6 months, and with the extension of time, color change is more serious.And by fluorubber mold For the high-quality slender joss stick engraving column wax prepared within storage 2 years, color has no much variations.It follows that prepared by fluorubber mold High-quality slender joss stick engraving column wax has very long storage time, and will not change colour in longer storage time, ensure that high-quality slender joss stick carving The quality of production of column wax is carved, reduces problem after sale.

Those skilled in the art will readily occur to the present invention its after considering specification and putting into practice the disclosure invented here Its embodiment.This application is intended to cover the present invention any variations, uses, or adaptations, these modifications, purposes or Person's adaptive change follows the general principle of the present invention and including undocumented common knowledge in the art of the invention Or conventional techniques.Description and embodiments are considered only as illustratively, and true scope and spirit of the invention are by following Claim is pointed out.

The invention is not limited in the precision architecture for being described above and being shown in the drawings, and can not depart from Its scope is carry out various modifications and changed.The scope of the present invention is only limited by appended claim.

Claims (10)

1. a kind of high-quality slender joss stick engraving column wax, which is characterized in that the high-quality slender joss stick engraving column wax is prepared using fluorubber mold.
2. high-quality slender joss stick engraving column wax according to claim 1, which is characterized in that the fluorubber mold includes oil resistivity fluorine rubber Sealing rubber die.
3. high-quality slender joss stick engraving column wax according to claim 1, which is characterized in that the raw material of the high-quality slender joss stick engraving column wax includes stone Wax, stearic acid and additive, the additive include essence.
4. high-quality slender joss stick engraving column wax according to claim 3, which is characterized in that the additive amount of the essence is the high-quality slender joss stick carving Carve the 1-5% of column wax gross mass.
5. it is according to claim 3 it is high-quality slender joss stick engraving column wax, which is characterized in that the additive further include soft wax, auxiliary agent and At least one of dyestuff.
6. high-quality slender joss stick engraving column wax according to claim 1, which is characterized in that the addition of essence in the high-quality slender joss stick engraving column wax It measures as the 2-5% of the high-quality slender joss stick engraving column wax gross mass.
7. high-quality slender joss stick engraving column wax according to claim 1, which is characterized in that a diameter of 6- of the high-quality slender joss stick engraving column wax 10cm is highly 8-20cm.
8. a kind of high-quality slender joss stick engraving waxed Preparation Method of column, which is characterized in that high-quality slender joss stick engraving column wax is prepared using fluorubber mold.
9. the high-quality slender joss stick engraving waxed Preparation Method of column according to claim 8, which is characterized in that the described method includes:
Wax material is weighed, the wax material is melt-blended at a temperature of 70-120 DEG C, form blended wax;
Dyestuff and essence are added in the blended wax, is stirred evenly, forms wax liquor;
The wax liquor is cast at a temperature of 50-110 DEG C in fluorubber mold;
The wax liquor being cast in the fluorubber mold is cooled down at a temperature of 5-35 DEG C, is molded, and forms candle;Wherein, institute State the wax liquor for being continuously replenished that temperature is 50-110 DEG C in wax liquor cooling procedure.
10. the high-quality slender joss stick engraving waxed Preparation Method of column according to claim 8, which is characterized in that the fluorubber mould inner wall It is carved with decorative pattern or pattern.
CN201810058586.5A 2018-01-22 2018-01-22 A kind of high-quality slender joss stick engraving column wax and preparation method CN108102396A (en)

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Application Number Priority Date Filing Date Title
CN201810058586.5A CN108102396A (en) 2018-01-22 2018-01-22 A kind of high-quality slender joss stick engraving column wax and preparation method

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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2001038740A (en) * 1999-07-29 2001-02-13 Kose Corp Elastic molding die
US20060226334A1 (en) * 2005-04-12 2006-10-12 Campbell Bruce M Malleable mold and method of use thereof
CN106853664A (en) * 2015-12-08 2017-06-16 重庆葛利兹模具技术有限公司上海分公司 A kind of processing technology of electric candle mould
CN106867683A (en) * 2017-03-01 2017-06-20 青岛金王应用化学股份有限公司 A kind of cottonseed oil candle and preparation method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2001038740A (en) * 1999-07-29 2001-02-13 Kose Corp Elastic molding die
US20060226334A1 (en) * 2005-04-12 2006-10-12 Campbell Bruce M Malleable mold and method of use thereof
CN106853664A (en) * 2015-12-08 2017-06-16 重庆葛利兹模具技术有限公司上海分公司 A kind of processing technology of electric candle mould
CN106867683A (en) * 2017-03-01 2017-06-20 青岛金王应用化学股份有限公司 A kind of cottonseed oil candle and preparation method thereof

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