CN108101504A - A kind of high whiteness ceramic idiosome and preparation method thereof - Google Patents
A kind of high whiteness ceramic idiosome and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a kind of high whiteness ceramic idiosomes and preparation method thereof, and high whiteness ceramic idiosome is prepared by the component of following parts by weight：In white 68 parts of sodium sand, 6 10 parts of water mill potassium sand, 12 17 parts of medium temperature white sand, 68 parts of mud washing, 2.5 4 parts of Guangxi sodium stone, 8 12 parts of high potassium sand, 4.5 6 parts of medium temperature sand, 58 parts of bentonite, 10 14 parts of Huaiji sand, 14 18 parts of Yangshan mountain flour, 24 parts of talcum mud, 12 15 parts of mixed soil, 47 parts of high alumina mountain flour, brighten 35 parts of complexing agent.The whiteness of the high whiteness ceramic idiosome can increase by 10 degree or more, and without radioactive composite material, cost is cheap compared to the ceramic idiosome containing zirconium silicate, about reduces by 1/3 cost of material.
Description
Technical field
The present invention relates to a kind of ceramic making technologies more particularly to a kind of high whiteness ceramic idiosome and preparation method thereof.
Background technology
At present, as existing ceramic idiosome is more and more lower with material quality, utilization of the white embryo brick to idiosome is produced at present
There are two types of conventional methods, the first is most conventional methods：Zirconium silicate is introduced in idiosome raw material, although the method can be certain
Degree increases the whiteness of idiosome, but its cost of material is high, and the market price of zirconium silicate is 1.2 ten thousand/ton, and the radioactivity of zirconium silicate
It is too strong, it is hazardous to the human body.Another is using relatively high-grade washing raw material, and the whitening effect of the method is limited,
And cost is also relatively expensive.
The content of the invention
For overcome the deficiencies in the prior art, one of the objects of the present invention is to provide a kind of high whiteness ceramic idiosomes.It should
The whiteness of high whiteness ceramic idiosome can increase by 10 degree or more, and without radioactive composite material, cost, which is compared, contains zirconium silicate
Ceramic idiosome is cheap, about reduces by 1/3 cost of material.
The second object of the present invention is to provide a kind of ceramic idiosome production method for increasing idiosome whiteness.The preparation method
Suitable for primary producing line, better whitening effect, cost of material is lower.
An object of the present invention adopts the following technical scheme that realization：A kind of high whiteness ceramic idiosome, by following parts by weight
Several components are prepared：In white 6-8 part of sodium sand, 6-10 parts of water mill potassium sand, 12-17 parts of medium temperature white sand, 6-8 parts of mud washing, extensively
Western 2.5-4 parts of sodium stone, 8-12 parts of high potassium sand, 4.5-6 parts of medium temperature sand, 5-8 parts of bentonite, sand 10-14 parts of Huaiji, Yangshan mountain flour
14-18 parts, 2-4 parts of talcum mud, 12-15 parts of mixed soil, 4-7 parts of high alumina mountain flour, brighten 3-5 parts of complexing agent.
It is further, described that brighten alumina powder and mass fraction that complexing agent is 80-95% by mass fraction be 5-8%
Barium carbonate composition, the sum of mass fraction of said components is 100%.
The second object of the present invention adopts the following technical scheme that realization：A kind of ceramic idiosome making side for increasing idiosome whiteness
Method, including,
The step of ball milling：Dispensing is carried out according to the formula ratio of high whiteness ceramic idiosome, then carries out ball milling using ball mill
8-12h；
The step of slurry iron-removing, sieving：It is filtered using the sieve of 70-90 mesh, except iron, obtains mud；
The aging step of mud：It will be except the mud after iron aging 1 day at ambient temperature；
The step of powder is made：Powder is made using spray tower in mud after will be aging；
The aging step of powder：Powder is placed in aging 1 day under room temperature；
The step of powder is except iron, sieving：Powder after will be aging is filtered, using the sieve of 10-30 mesh except iron, is obtained
Embryo material；
The step of compacting, shaping：Embryo material is placed in press, under the action of mold, is suppressed, is then sent to burning
Shaping is fired in stove.
Further, in the step of ball milling, the high whiteness ceramic idiosome by following parts by weight component prepare and
Into：In white 6-8 parts of sodium sand, 6-10 parts of water mill potassium sand, 12-17 parts of medium temperature white sand, 6-8 parts of mud washing, 2.5-4 parts of Guangxi sodium stone,
High 8-12 parts of potassium sand, 4.5-6 parts of medium temperature sand, 5-8 parts of bentonite, sand 10-14 parts of Huaiji, mountain flour 14-18 parts of Yangshan, talcum mud 2-
4 parts, 12-15 parts of mixed soil, 4-7 parts of high alumina mountain flour, brighten 3-5 parts of complexing agent；It is described brighten complexing agent by mass fraction be 80-
The barium carbonate that 95% alumina powder and mass fraction is 5-8% forms, and the sum of mass fraction of said components is 100%.
Further, in the step of ball milling, time of the ball milling is 10h, and after ball milling, powder fineness is controlled 250
Mesh, screen over-size 0.8-1.0%.
Further, in the step of slurry iron-removing, sieving, the step is in triplicate.
Further, in the step of slurry iron-removing, sieving, the mesh number of the sieve is 80 mesh.
Further, in powder except in the step of iron, sieving, the mesh number of the sieve is 20 mesh.
Further, in the step of compacting, shaping, the condition of the compacting is as follows：Using the pressure of 28000-30000N
Power is suppressed, and compacting frequency is 4.6 times/min.
Further, in the step of compacting, shaping, the condition of the firing is as follows：In 1175 DEG C of -1180 DEG C of conditions
Under, fire 48-55min.
Compared with prior art, the beneficial effects of the present invention are：
The present invention replaces original zirconium silicate by adding in the composite whitening agent of aluminium oxide and barium carbonate, without radioactive
Composite material, cost cheaply about reduce by 1/3 cost of material compared to the ceramic idiosome containing zirconium silicate；In addition the requirement of its whiteness
Similarly reach the ceramic idiosome whiteness containing zirconium silicate.Compared with the ceramic idiosome without brightening agent, high whiteness of the invention pottery
The whiteness of porcelain idiosome can increase by 10 degree or more.
Description of the drawings
Fig. 1 is its whiteness comparison diagram of the idiosome of same size size made from embodiment 1 and comparative example 1-2.
In figure, A is ceramic idiosome made from comparative example 1；B is ceramic idiosome made from embodiment 1；C is made for comparative example 2
Ceramic idiosome.
Specific embodiment
In the following, with reference to attached drawing and specific embodiment, the present invention is described further, it is necessary to which explanation is, not
Under the premise of conflicting, new implementation can be formed between various embodiments described below or between each technical characteristic in any combination
Example.
In the present invention, if not refering in particular to, all parts, percentage are unit of weight, used equipment and raw material etc.
It is commercially available or commonly used in the art.Method in following embodiments is the normal of this field unless otherwise instructed
Rule method.
A kind of high whiteness ceramic idiosome, is prepared by the component of following parts by weight：In white 6-8 parts of sodium sand, water mill potassium
6-10 parts of sand, 12-17 parts of medium temperature white sand, 6-8 parts of mud washing, 2.5-4 parts of Guangxi sodium stone, 8-12 parts of high potassium sand, medium temperature sand 4.5-6
Part, 5-8 parts of bentonite, sand 10-14 parts of Huaiji, mountain flour 14-18 parts of Yangshan, 2-4 parts of talcum mud, 12-15 parts of mixed soil, high alumina stone
4-7 parts of powder brightens 3-5 parts of complexing agent.
It is specifically, described that brighten alumina powder and mass fraction that complexing agent is 80-95% by mass fraction be 5-8%'s
Barium carbonate forms, and the sum of mass fraction of said components is 100%.
Wherein, the present invention replaces original zirconium silicate (market price by adding in the composite whitening agent of aluminium oxide and barium carbonate
1.2 ten thousand/ton), the composite whitening agent market price of aluminium oxide and barium carbonate is 5.5 thousand/ton, therefore can reduce cost of material, and
And without radioactive composite material.
A kind of ceramic idiosome production method for increasing idiosome whiteness, including,
The step of ball milling：Dispensing is carried out according to the formula ratio of above-mentioned high whiteness ceramic idiosome, is then carried out using ball mill
Ball milling 8-12h；Preferably, the time of the ball milling is 10h, and after ball milling, powder fineness is controlled in 250 mesh, screen over-size 0.8-
1.0%.
The step of slurry iron-removing, sieving：It is filtered using the sieve of 70-90 mesh, except iron, obtains mud；Preferably, institute
The mesh number for stating sieve is 80 mesh.In triplicate, the present invention carries out multiple the step of removing iron to the step, is conducive to increase the white of green body
Degree.
The aging step of mud：It will be except the mud after iron aging 1 day at ambient temperature；
The step of powder is made：Powder is made using spray tower in mud after will be aging；
The aging step of powder：Powder is placed in aging 1 day under room temperature；
The step of powder is except iron, sieving：Powder after will be aging is filtered, using the sieve of 10-30 mesh except iron, is obtained
Embryo material；Preferably, the mesh number of the sieve is 20 mesh.
The step of compacting, shaping：Embryo material is placed in press, under the action of mold, is suppressed, the item of the compacting
Part is as follows：It is suppressed using the pressure of 28000-30000N, compacting frequency is 4.6 times/min.Be then sent to burn stove in into
Row forms by a firing.The condition of the firing is as follows：Under the conditions of 1175 DEG C -1180 DEG C, 48-55min is fired.
It is specific embodiment of the present invention below, used raw material, equipment etc. remove special limit in the following embodiments
It can be obtained outside fixed by buying pattern.
Embodiment 1-3 and comparative example 1-2：
The proportioning according to the form below 1 weighs raw material respectively, is prepared in accordance with the following steps, the difference is that added
Raw material proportioning is different, prepares product, specifically refers to table 1：
Table 1：Embodiment 1-3 and comparative example 1-2 raw material proportioning tables
The production method of the high whiteness ceramic idiosome of embodiment 1-3, including,
The step of ball milling：Dispensing is carried out according to the formula ratio of above-mentioned ceramic idiosome, then carries out ball milling using ball mill
10h；After ball milling, powder fineness is controlled in 250 mesh, screen over-size 0.8-1.0%.
The step of slurry iron-removing, sieving：It is filtered using the sieve of 80 mesh, except iron, obtains mud；
The aging step of mud：It will be except the mud after iron aging 1 day at ambient temperature；
The step of powder is made：Powder is made using spray tower in mud after will be aging；
The aging step of powder：Powder is placed in aging 1 day under room temperature；
The step of powder is except iron, sieving：Powder after will be aging is filtered, using the sieve of 20 mesh except iron, obtains embryo
Material；
The step of compacting, shaping：Embryo material is placed in press, under the action of mold, is suppressed, the item of the compacting
Part is as follows：It is suppressed using the pressure of 28000-30000N, compacting frequency is 4.6 times/min.Be then sent to burn stove in into
Row forms by a firing.The condition of the firing is as follows：Under the conditions of 1175 DEG C -1180 DEG C, 48-55min is fired.
Effect assessment and performance detection
1. according in GBT/5950 construction materials and nonmetal mineral product to whiteness measuring method, to embodiment 1, comparative example
The whiteness of the ceramic idiosome of 1-2 is detected, and detection project and result are referring to table 2 and Fig. 1.
Table 2：Embodiment 1-3 and comparative example 1-2 whiteness test results
Tests prove that brightening agent composite material of the invention introduces 3% in idiosome, the increased whiteness of institute, with drawing
It is identical to enter the 2% increased whiteness degree of existing brightening agent zirconium silicate institute, idiosome temperature will not be impacted, whiteness can increase by 10
It is more than degree.In addition with the increase of addition, whiteness can also raise.
The above embodiment is only the preferred embodiment of the present invention, it is impossible to the scope of protection of the invention is limited with this,
The variation and replacement for any unsubstantiality that those skilled in the art is done on the basis of the present invention belong to institute of the present invention
Claimed scope.
Claims (10)
1. a kind of high whiteness ceramic idiosome, which is characterized in that be prepared by the component of following parts by weight：In white sodium sand 6-8
Part, 6-10 parts of water mill potassium sand, 12-17 parts of medium temperature white sand, 6-8 parts of mud washing, 2.5-4 parts of Guangxi sodium stone, 8-12 parts of high potassium sand, in
Warm sand 4.5-6 parts, 5-8 parts of bentonite, sand 10-14 parts of Huaiji, mountain flour 14-18 parts of Yangshan, 2-4 parts of talcum mud, mixed soil 12-15
Part, 4-7 parts of high alumina mountain flour brighten 3-5 parts of complexing agent.
2. high whiteness ceramic idiosome as described in claim 1, which is characterized in that the complexing agent that brightens is by mass fraction
The barium carbonate that the alumina powder and mass fraction of 80-95% is 5-8% forms, and the sum of mass fraction of said components is 100%.
3. a kind of ceramic idiosome production method for increasing idiosome whiteness, it is characterised in that including,
The step of ball milling：Dispensing is carried out according to the formula ratio of high whiteness ceramic idiosome, then carries out ball milling 8- using ball mill
12h；
The step of slurry iron-removing, sieving：It is filtered using the sieve of 70-90 mesh, except iron, obtains mud；
The aging step of mud：It will be except the mud after iron aging 1 day at ambient temperature；
The step of powder is made：Powder is made using spray tower in mud after will be aging；
The aging step of powder：Powder is placed in aging 1 day under room temperature；
The step of powder is except iron, sieving：Powder after will be aging is filtered, using the sieve of 10-30 mesh except iron, obtains embryo
Material；
The step of compacting, shaping：Embryo material is placed in press, under the action of mold, is suppressed, is then sent to and burns in stove
It is fired shaping.
4. ceramic idiosome production method as claimed in claim 3, which is characterized in that in the step of ball milling, the high whiteness
Ceramic idiosome is prepared by the component of following parts by weight：In white 6-8 parts of sodium sand, 6-10 parts of water mill potassium sand, medium temperature white sand 12-
17 parts, 6-8 parts of mud washing, 2.5-4 parts of Guangxi sodium stone, 8-12 parts of high potassium sand, 4.5-6 parts of medium temperature sand, 5-8 parts of bentonite, Huaiji
Complexing agent, 12-15 parts of mixed soil, 4-7 parts of high alumina mountain flour, is brightened at 2-4 parts of talcum mud in 10-14 parts of sand, mountain flour 14-18 parts of Yangshan
3-5 parts；It is described to brighten the barium carbonate group that alumina powder and mass fraction that complexing agent is 80-95% by mass fraction are 5-8%
Into the sum of mass fraction of said components is 100%.
5. ceramic idiosome production method as claimed in claim 3, which is characterized in that in the step of ball milling, the ball milling
Time is 10h, and after ball milling, powder fineness is controlled in 250 mesh, screen over-size 0.8-1.0%.
6. ceramic idiosome production method as claimed in claim 3, which is characterized in that, should in the step of slurry iron-removing, sieving
Step is in triplicate.
7. ceramic idiosome production method as claimed in claim 3, which is characterized in that in the step of slurry iron-removing, sieving, institute
The mesh number for stating sieve is 80 mesh.
8. ceramic idiosome production method as claimed in claim 3, which is characterized in that in the step of powder removes iron, sieving, institute
The mesh number for stating sieve is 20 mesh.
9. ceramic idiosome production method as claimed in claim 3, which is characterized in that in the step of compacting, shaping, the pressure
The condition of system is as follows：It is suppressed using the pressure of 28000-30000N, compacting frequency is 4.6 times/min.
10. ceramic idiosome production method as claimed in claim 3, which is characterized in that described in the step of compacting, shaping
The condition of firing is as follows：Under the conditions of 1175 DEG C -1180 DEG C, 48-55min is fired.
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Cited By (5)
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| CN110357584A (en) * | 2019-07-04 | 2019-10-22 | 东莞市唯美装饰材料有限公司 | A method of ceramic mud is prepared using recycling ceramic wastewater |
| CN111056821A (en) * | 2019-12-31 | 2020-04-24 | 泉州阳光创艺陶瓷股份有限公司 | High-whiteness ceramic artwork and preparation method thereof |
| CN111517751A (en) * | 2020-05-19 | 2020-08-11 | 广东永航新材料实业股份有限公司 | High-whiteness zirconium-free ceramic blank and preparation method of high-whiteness zirconium-free ceramic |
| CN114956788A (en) * | 2022-07-05 | 2022-08-30 | 河源市东源鹰牌陶瓷有限公司 | High-wear-resistance ceramic tile imitating dragon ridge jade texture and preparation method thereof |
| CN115784768A (en) * | 2022-11-17 | 2023-03-14 | 安徽昆仑新材料科技有限公司 | Universal blank for water permeable ceramic tiles and forming method thereof |
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| CN114956788A (en) * | 2022-07-05 | 2022-08-30 | 河源市东源鹰牌陶瓷有限公司 | High-wear-resistance ceramic tile imitating dragon ridge jade texture and preparation method thereof |
| CN115784768A (en) * | 2022-11-17 | 2023-03-14 | 安徽昆仑新材料科技有限公司 | Universal blank for water permeable ceramic tiles and forming method thereof |
| CN115784768B (en) * | 2022-11-17 | 2023-11-28 | 安徽昆仑新材料科技有限公司 | General blank of permeable ceramic tile and forming method thereof |
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