CN108085969A - The antiseptic finish method of knitting wool - Google Patents

The antiseptic finish method of knitting wool Download PDF

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Publication number
CN108085969A
CN108085969A CN201711191652.8A CN201711191652A CN108085969A CN 108085969 A CN108085969 A CN 108085969A CN 201711191652 A CN201711191652 A CN 201711191652A CN 108085969 A CN108085969 A CN 108085969A
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China
Prior art keywords
parts
knitting wool
working fluid
chinese
liquid
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CN201711191652.8A
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Chinese (zh)
Inventor
杨海峰
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Huzhou Zhili Plastic Plastic Technology Co Ltd
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Huzhou Zhili Plastic Plastic Technology Co Ltd
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Priority to CN201711191652.8A priority Critical patent/CN108085969A/en
Publication of CN108085969A publication Critical patent/CN108085969A/en
Pending legal-status Critical Current

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    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/144Alcohols; Metal alcoholates
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/184Carboxylic acids; Anhydrides, halides or salts thereof
    • D06M13/1845Aromatic mono- or polycarboxylic acids
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/184Carboxylic acids; Anhydrides, halides or salts thereof
    • D06M13/203Unsaturated carboxylic acids; Anhydrides, halides or salts thereof
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M16/00Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/02Natural fibres, other than mineral fibres
    • D06M2101/10Animal fibres
    • D06M2101/12Keratin fibres or silk

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Biochemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Microbiology (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The present invention relates to a kind of antiseptic finish methods of knitting wool, comprise the following steps:(1)Chinese herbal medicine is cleaned into removal of impurities, after drying and crushing, adds water to cook, liquid is obtained by filtration;(2)Liquid is sieved, then by being evaporated in vacuo, obtains concentrated extract;(3)Diatomite and activated carbon are added in concentrated extract, is filtered after stirring, adds sodium benzoate, potassium sorbate and ethyl alcohol, is uniformly mixed, 300 mesh sieves is crossed, obtains working fluid;(4)By knitting wool and working fluid in mass ratio 5~8:1 mixing, then plus the mass ratio of water configuration knitting wool and dilution working fluid is 1:20~25, it impregnates, then heats to 40~55 DEG C, keep the temperature 30min, then 65~80 DEG C are warming up to, and 30min is kept the temperature, is washed, drying.Knitting wool after processed can prevent moth from multiplying, multiplying, also the effect with antiseptic and inhibiting bacteria function, there is good washability, and not influence the feel of knitting wool in itself, available for knit a sweater, the winter warmings articles for use such as cap, scarf, socks, gloves.

Description

The antiseptic finish method of knitting wool
Technical field
The present invention relates to knitting wool manufacture field, more particularly, to a kind of antiseptic finish method of knitting wool.
Background technology
Knitting wool can be used for being compiled into the heating clothes such as sweater, gloves, socks, seems indispensable in winter, but maintains Come but very enervated, especially with respect to the moth problem of knitting wool and wool product, often influence its service life, but relatively hold It is easily ignored.In addition to keeping the daily nursings such as knitting wool and wool product aeration-drying, it is also necessary to work out a kind of from knitting wool Itself start with and carry out the mothproof processing method of insect prevention, to extend the service life of knitting wool.
The content of the invention
The object of the present invention is to provide a kind of antiseptic finish methods of knitting wool.
The object of the invention is achieved by the following technical programs:
A kind of antiseptic finish method of knitting wool is provided, is comprised the following steps:
(1)Chinese herbal medicine is cleaned into removal of impurities, after drying and crushing, 10~20 times of water is added in and decocts 40~60min, liquid is obtained by filtration;
(2)Liquid is crossed into 200 mesh sieves, then by being evaporated in vacuo, the concentration that mass percentage concentration is 55~80% is obtained and extracts Liquid;
(3)Diatomite and activated carbon are added in concentrated extract, then stirring 10~15min decolorations filter, add benzene first 5~10 parts of sour 0.02~0.05 part of sodium, 0.07~0.09 part of potassium sorbate and ethyl alcohol are uniformly mixed, and are crossed 300 mesh sieves, are added Work liquid;
(4)By knitting wool and working fluid in mass ratio 5~8:1 mixing, then plus water configures knitting wool with diluting the mass ratio of working fluid For 1:20~25,5~10min is impregnated, is then warming up to 40~55 DEG C with the rate of 2~3 DEG C/min, keeps the temperature 30min, then with 1 The rate of~2 DEG C/min is warming up to 65~80 DEG C, keeps the temperature 30min, then washes, and dries.
Further, the Chinese herbal medicine is grouped by each group of following weight fraction:3~6 parts of softleaf ash root-bark, rhizome of cyrtomium 12~17 Part, 6~10 parts of dryopteris fragrans, 9~15 parts of Cynanchum otophyllum Schneid, 4~8 parts of 16~31 Fen , pivots of granatum storage, 10~15 parts of Chinese gall, gold 1~3 part is not changed, 5~8 parts of Chinese prickly ash.
Preferably, the Chinese herbal medicine is grouped by each group of following parts by weight:3.5~5.5 parts of softleaf ash root-bark, rhizome of cyrtomium 14~ 16 parts, 7~9 parts of dryopteris fragrans, 11~14 parts of Cynanchum otophyllum Schneid, 5~7 parts of 20~28 Fen , pivots of granatum storage, 11~13 parts of Chinese gall, Invaluable 1.5~2.5 parts, 6~7.5 parts of Chinese prickly ash.
Preferably, the Chinese herbal medicine is grouped by each group of following parts by weight:4.5 parts of softleaf ash root-bark, 15 parts of rhizome of cyrtomium, androconium 8 parts of fern of hair, 13 parts of Cynanchum otophyllum Schneid, 6 parts of 25 Fen , pivots of granatum storage, 12 parts of Chinese gall, invaluable 2 parts, 7 parts of Chinese prickly ash.
Compared with prior art, the invention has the advantages that:
The present invention provides a kind of antiseptic finish method of knitting wool, it is processed after knitting wool can prevent moth from multiplying, multiplying, also have There is the effect of antiseptic and inhibiting bacteria function, storage for a long time is not easy mouldy, there is good washability, and does not influence the feel of knitting wool in itself, can For knitting a sweater, the winter warmings articles for use such as cap, scarf, socks, gloves, greatly prolong the service life.
Specific embodiment
With reference to specific embodiment, the present invention is further illustrated.
Embodiment 1
Present embodiment discloses a kind of antiseptic finish methods of knitting wool, comprise the following steps:
(1)By 3 parts of softleaf ash root-bark, 17 parts of rhizome of cyrtomium, 6 parts of dryopteris fragrans, 15 parts of Cynanchum otophyllum Schneid, 8 parts of 16 Fen , pivots of granatum storage, Chinese gall 10 parts, invaluable 3 parts, 5 parts of Chinese prickly ash, which is cleaned, to clean, and after drying and crushing, adds in 20 times of water and decocts 40min, liquid is obtained by filtration;
(2)Liquid is crossed into 200 mesh sieves, then by being evaporated in vacuo, obtains the concentrated extract that mass percentage concentration is 80%;
(3)Diatomite and activated carbon are added in concentrated extract, is filtered after stirring 10min, add 0.05 part of sodium benzoate, 10 parts of 0.07 part of potassium sorbate and ethyl alcohol are uniformly mixed, and are crossed 300 mesh sieves, are obtained working fluid;
(4)By knitting wool and working fluid in mass ratio 5:1 mixing, then plus the mass ratio of water configuration knitting wool and dilution working fluid is 1: 25,5min is impregnated, is then warming up to 40 DEG C with the rate of 3 DEG C/min, 30min is kept the temperature, then 65 is warming up to the rate of 2 DEG C/min DEG C, 30min is kept the temperature, is then washed, is dried.
Embodiment 2
Present embodiment discloses a kind of antiseptic finish methods of knitting wool, comprise the following steps:
(1)By 6 parts of softleaf ash root-bark, 12 parts of rhizome of cyrtomium, 10 parts of dryopteris fragrans, 9 parts of Cynanchum otophyllum Schneid, 4 parts of 31 Fen , pivots of granatum storage, Chinese gall 15 parts, invaluable 1 part, 8 parts of Chinese prickly ash, which is cleaned, to clean, and after drying and crushing, adds in 10 times of water and decocts 60min, liquid is obtained by filtration;
(2)Liquid is crossed into 200 mesh sieves, then by being evaporated in vacuo, obtains the concentrated extract that mass percentage concentration is 55%;
(3)Diatomite and activated carbon are added in concentrated extract, is filtered after stirring 15min, add 0.02 part of sodium benzoate, 5 parts of 0.09 part of potassium sorbate and ethyl alcohol are uniformly mixed, and are crossed 300 mesh sieves, are obtained working fluid;
(4)By knitting wool and working fluid in mass ratio 8:1 mixing, then plus the mass ratio of water configuration knitting wool and dilution working fluid is 1: 20,10min is impregnated, is then warming up to 55 DEG C with the rate of 2 DEG C/min, 30min is kept the temperature, then is warming up to the rate of 1 DEG C/min 80 DEG C, 30min is kept the temperature, is then washed, dried.
Embodiment 3
Present embodiment discloses a kind of antiseptic finish methods of knitting wool, comprise the following steps:
(1)By 3.5 parts of softleaf ash root-bark, 16 parts of rhizome of cyrtomium, 7 parts of dryopteris fragrans, 14 parts of Cynanchum otophyllum Schneid, 7 parts, five times of 20 Fen , pivots of granatum storage 11 parts of son, invaluable 2.5 parts, 6 parts of Chinese prickly ash, which is cleaned, to clean, and after drying and crushing, adds in 12 times of water and decocts 45min, medicine is obtained by filtration Liquid;
(2)Liquid is crossed into 200 mesh sieves, then by being evaporated in vacuo, obtains the concentrated extract that mass percentage concentration is 60%;
(3)Diatomite and activated carbon are added in concentrated extract, is filtered after stirring 12min, add 0.03 part of sodium benzoate, 8 parts of 0.08 part of potassium sorbate and ethyl alcohol are uniformly mixed, and are crossed 300 mesh sieves, are obtained working fluid;
(4)By knitting wool and working fluid in mass ratio 6:1 mixing, then plus the mass ratio of water configuration knitting wool and dilution working fluid is 1: 22,8min is impregnated, is then warming up to 48 DEG C with the rate of 2.5 DEG C/min, 30min is kept the temperature, then is heated up with the rate of 1.5 DEG C/min To 70 DEG C, 30min is kept the temperature, is then washed, dried.
Embodiment 4
Present embodiment discloses a kind of antiseptic finish methods of knitting wool, comprise the following steps:
(1)By 5.5 parts of softleaf ash root-bark, 14 parts of rhizome of cyrtomium, 9 parts of dryopteris fragrans, 11 parts of Cynanchum otophyllum Schneid, 5 parts, five times of 28 Fen , pivots of granatum storage 13 parts of son, invaluable 1.5 parts, 7.5 parts of Chinese prickly ash, which is cleaned, to clean, and after drying and crushing, adds in 15 times of water and decocts 50min, be obtained by filtration Liquid;
(2)Liquid is crossed into 200 mesh sieves, then by being evaporated in vacuo, obtains the concentrated extract that mass percentage concentration is 70%;
(3)Diatomite and activated carbon are added in concentrated extract, is filtered after stirring 14min, add 0.04 part of sodium benzoate, 6 parts of 0.07 part of potassium sorbate and ethyl alcohol are uniformly mixed, and are crossed 300 mesh sieves, are obtained working fluid;
(4)By knitting wool and working fluid in mass ratio 7:1 mixing, then plus the mass ratio of water configuration knitting wool and dilution working fluid is 1: 24,6min is impregnated, is then warming up to 50 DEG C with the rate of 2 DEG C/min, 30min is kept the temperature, then 72 is warming up to the rate of 2 DEG C/min DEG C, 30min is kept the temperature, is then washed, is dried.
Embodiment 5
Present embodiment discloses a kind of antiseptic finish methods of knitting wool, comprise the following steps:
(1)By 4 parts of softleaf ash root-bark, 14.5 parts of rhizome of cyrtomium, 7.5 parts of dryopteris fragrans, 12 parts of Cynanchum otophyllum Schneid, 22 Fen , pivots of granatum store 5.5 parts, 11.5 parts of Chinese gall, invaluable 1.8 parts, 6.5 parts of Chinese prickly ash, which is cleaned, to clean, and after drying and crushing, adds in 15 times of water and decocts 55min, mistake Filter obtains liquid;
(2)Liquid is crossed into 200 mesh sieves, then by being evaporated in vacuo, obtains the concentrated extract that mass percentage concentration is 60%;
(3)Diatomite and activated carbon are added in concentrated extract, is filtered after stirring 11min, add 0.05 part of sodium benzoate, 9 parts of 0.09 part of potassium sorbate and ethyl alcohol are uniformly mixed, and are crossed 300 mesh sieves, are obtained working fluid;
(4)By knitting wool and working fluid in mass ratio 6:1 mixing, then plus the mass ratio of water configuration knitting wool and dilution working fluid is 1: 23,7min is impregnated, is then warming up to 50 DEG C with the rate of 3 DEG C/min, 30min is kept the temperature, then 78 is warming up to the rate of 1 DEG C/min DEG C, 30min is kept the temperature, is then washed, is dried.
Embodiment 6
Present embodiment discloses a kind of antiseptic finish methods of knitting wool, comprise the following steps:
(1)By 4.5 parts of softleaf ash root-bark, 15 parts of rhizome of cyrtomium, 8 parts of dryopteris fragrans, 13 parts of Cynanchum otophyllum Schneid, 6 parts, five times of 25 Fen , pivots of granatum storage 12 parts of son, invaluable 2 parts, 7 parts of Chinese prickly ash, which is cleaned, to clean, and after drying and crushing, adds in 12 times of water and decocts 45min, liquid is obtained by filtration;
(2)Liquid is crossed into 200 mesh sieves, then by being evaporated in vacuo, obtains the concentrated extract that mass percentage concentration is 60%;
(3)Diatomite and activated carbon are added in concentrated extract, is filtered after stirring 10~15min, adds sodium benzoate 8 parts of 0.03 part, 0.08 part of potassium sorbate and ethyl alcohol are uniformly mixed, and are crossed 300 mesh sieves, are obtained working fluid;
(4)By knitting wool and working fluid in mass ratio 6:1 mixing, then plus the mass ratio of water configuration knitting wool and dilution working fluid is 1: 22,8min is impregnated, is then warming up to 48 DEG C with the rate of 2.5 DEG C/min, 30min is kept the temperature, then is warming up to the rate of 1 DEG C/min 68 DEG C, 30min is kept the temperature, is then washed, dried.

Claims (4)

1. a kind of antiseptic finish method of knitting wool, which is characterized in that comprise the following steps:
(1)Chinese herbal medicine is cleaned into removal of impurities, after drying and crushing, 10~20 times of water is added in and decocts 40~60min, liquid is obtained by filtration;
(2)Liquid is crossed into 200 mesh sieves, then by being evaporated in vacuo, the concentration that mass percentage concentration is 55~80% is obtained and extracts Liquid;
(3)Diatomite and activated carbon are added in concentrated extract, is filtered after stirring 10~15min, adds sodium benzoate 5~10 parts of 0.02~0.05 part, 0.07~0.09 part of potassium sorbate and ethyl alcohol are uniformly mixed, and are crossed 300 mesh sieves, are obtained working fluid;
(4)By knitting wool and working fluid in mass ratio 5~8:1 mixing, then plus water configures knitting wool with diluting the mass ratio of working fluid For 1:20~25,5~10min is impregnated, is then warming up to 40~55 DEG C with the rate of 2~3 DEG C/min, keeps the temperature 30min, then with 1 The rate of~2 DEG C/min is warming up to 65~80 DEG C, keeps the temperature 30min, then washes, and dries.
2. the antiseptic finish method of knitting wool according to claim 1, which is characterized in that the Chinese herbal medicine is by following weight point Several each groups are grouped into:3~6 parts of softleaf ash root-bark, 12~17 parts of rhizome of cyrtomium, 6~10 parts of dryopteris fragrans, 9~15 parts of Cynanchum otophyllum Schneid, granatum 4~8 parts of 16~31 Fen , pivots storage, 10~15 parts of Chinese gall, invaluable 1~3 part, 5~8 parts of Chinese prickly ash.
3. the antiseptic finish method of knitting wool according to claim 1 or 2, which is characterized in that the Chinese herbal medicine is by following heavy The each group of amount number is grouped into:3.5~5.5 parts of softleaf ash root-bark, 14~16 parts of rhizome of cyrtomium, 7~9 parts of dryopteris fragrans, Cynanchum otophyllum Schneid 11~14 Part, 5~7 parts of 20~28 Fen , pivots of granatum storage, 11~13 parts of Chinese gall, invaluable 1.5~2.5 parts, 6~7.5 parts of Chinese prickly ash.
4. the antiseptic finish method of the knitting wool according to claim 1 or 3, which is characterized in that the Chinese herbal medicine is by following heavy The each group of amount number is grouped into:4.5 parts of softleaf ash root-bark, 15 parts of rhizome of cyrtomium, 8 parts of dryopteris fragrans, 13 parts of Cynanchum otophyllum Schneid, 25 Fen , pivots of granatum 6 parts of storage, 12 parts of Chinese gall, invaluable 2 parts, 7 parts of Chinese prickly ash.
CN201711191652.8A 2017-11-24 2017-11-24 The antiseptic finish method of knitting wool Pending CN108085969A (en)

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Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH06279220A (en) * 1994-02-17 1994-10-04 Hakugen:Kk Moth-proofing agent for clothes
CN1264542A (en) * 2000-03-17 2000-08-30 定明通 Durable vanillic mixture prepared from Chinese-meidicinal materials for preventing mildew and worm-eating and its preparing process
CN102051812A (en) * 2010-11-24 2011-05-11 东华大学 Application of botanical antibacterial mothproof multifunctional composite preparation in wool product
CN102922574A (en) * 2012-10-09 2013-02-13 莫承振 Mould-proof, insect-proof and deformation-proof medicine for environment-friendly plant woven products and treating technique for mould-proof, insect-proof and deformation-proof medicine
CN103103749A (en) * 2013-02-04 2013-05-15 东华大学 Application of plant stemona mothproofing agent on wool products
CN107326126A (en) * 2017-06-23 2017-11-07 宁波市海曙区伊万卡农业科技有限公司 A kind of Chinese herbal medicine leather and fur conditioning liquid and preparation method thereof

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH06279220A (en) * 1994-02-17 1994-10-04 Hakugen:Kk Moth-proofing agent for clothes
CN1264542A (en) * 2000-03-17 2000-08-30 定明通 Durable vanillic mixture prepared from Chinese-meidicinal materials for preventing mildew and worm-eating and its preparing process
CN102051812A (en) * 2010-11-24 2011-05-11 东华大学 Application of botanical antibacterial mothproof multifunctional composite preparation in wool product
CN102922574A (en) * 2012-10-09 2013-02-13 莫承振 Mould-proof, insect-proof and deformation-proof medicine for environment-friendly plant woven products and treating technique for mould-proof, insect-proof and deformation-proof medicine
CN103103749A (en) * 2013-02-04 2013-05-15 东华大学 Application of plant stemona mothproofing agent on wool products
CN107326126A (en) * 2017-06-23 2017-11-07 宁波市海曙区伊万卡农业科技有限公司 A kind of Chinese herbal medicine leather and fur conditioning liquid and preparation method thereof

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