CN108085111A - A kind of preparation method of clean type film lubrication agent - Google Patents

A kind of preparation method of clean type film lubrication agent Download PDF

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Publication number
CN108085111A
CN108085111A CN201711409109.0A CN201711409109A CN108085111A CN 108085111 A CN108085111 A CN 108085111A CN 201711409109 A CN201711409109 A CN 201711409109A CN 108085111 A CN108085111 A CN 108085111A
Authority
CN
China
Prior art keywords
clean type
lubrication agent
preparation
type film
film
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201711409109.0A
Other languages
Chinese (zh)
Inventor
周忠太
崔素彬
周征寰
李保莉
张守鹏
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Xinxiang Hengxing Technology Co Ltd
Original Assignee
Xinxiang Hengxing Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Xinxiang Hengxing Technology Co Ltd filed Critical Xinxiang Hengxing Technology Co Ltd
Priority to CN201711409109.0A priority Critical patent/CN108085111A/en
Publication of CN108085111A publication Critical patent/CN108085111A/en
Pending legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M169/00Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
    • C10M169/04Mixtures of base-materials and additives
    • C10M169/041Mixtures of base-materials and additives the additives being macromolecular compounds only
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2211/00Organic non-macromolecular compounds containing halogen as ingredients in lubricant compositions
    • C10M2211/02Organic non-macromolecular compounds containing halogen as ingredients in lubricant compositions containing carbon, hydrogen and halogen only
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2213/00Organic macromolecular compounds containing halogen as ingredients in lubricant compositions
    • C10M2213/06Perfluoro polymers
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2213/00Organic macromolecular compounds containing halogen as ingredients in lubricant compositions
    • C10M2213/06Perfluoro polymers
    • C10M2213/062Polytetrafluoroethylene [PTFE]
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2217/00Organic macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2217/04Macromolecular compounds from nitrogen-containing monomers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10NINDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/04Detergent property or dispersant property
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10NINDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/06Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Laminated Bodies (AREA)

Abstract

The invention discloses a kind of preparation methods of clean type film lubrication agent, belong to technical field of lubricant.Technical scheme main points are:A kind of preparation method of clean type film lubrication agent, the raw material matched by following weight percent are uniformly mixed and are made at room temperature:Perfluoropolyether 20%~30%, Ultra-low molecular weight polytetrafluoroethylene PTFE particle 15%~25%, polyimides 5%~8%, surplus is fluorocarbon solvent.The use temperature range of clean type film lubrication agent produced by the present invention is wide, can be used at 60 DEG C~260 DEG C;Film forming speed is fast, good leveling property, and 10~15s forms dried layer film;Film layer insulation is non-conductive;Film layer does not flow diffusion, does not adsorb dust particle;The erosion of waterproof and other liquid;To use environment without destruction, nontoxic plurality of advantages.

Description

A kind of preparation method of clean type film lubrication agent
Technical field
The invention belongs to technical field of lubricant, and in particular to a kind of preparation method of clean type film lubrication agent.
Background technology
In electric appliance and electronic equipment, precision instrument, clock and watch, musical instrument, automobile etc., it is necessary to which a kind of clean, is pollution-free, no The conductive and significant lubricant of lubricating action, this lubricant can penetrate into and with reference to metal, paper, wood, glass, rubber etc. its The surface of its overwhelming majority forms the film of one layer of non-pickup to prevent to stick and then reduce friction, it should have good Thermal stability and chemical stability.It applies in electronic device, energy self-assembling formation insulating layer prevents conduction.Existing product is applicable in Scope face is narrow, and it is therefore necessary to develop one kind there is clean type, lubricity, insulating properties, temperature tolerance, security and film forming uniformly to have All multifunctional film lubrication agent.
The content of the invention
The technical problem to be solved by the present invention is to provide a kind of clean type films simple for process, formula is reasonable and environmental-friendly The preparation method of lubricant.
It is of the invention to adopt the following technical scheme that solve above-mentioned technical problem, a kind of preparation side of clean type film lubrication agent Method, it is characterised in that the raw material matched by following weight percent is uniformly mixed and is made at room temperature:Perfluoropolyether 20%~ 30%th, Ultra-low molecular weight polytetrafluoroethylene (PTFE)(PTFE)Particle 15%~25%, polyimides 5%~8%, surplus are fluorocarbon solvent.
Further preferably, the preparation method of the clean type film lubrication agent, it is characterised in that matched by following weight percent Raw material be uniformly mixed and be made at room temperature:Perfluoropolyether 30%, Ultra-low molecular weight polytetrafluoroethylene (PTFE)(PTFE)Particle 25%th, polyimides 5%, surplus are fluorocarbon solvent.
Further preferably, the perfluoroalkyl polyether is distillate of the boiling point at 240~260 DEG C, and the molecular weight of polyimides is 300 ~400.
Perfluoropolyether used in the present invention is distillate of the boiling point at 240~260 DEG C, has good high and low temperature, It is non-combustible, the advantages of nontoxic and low volatility;Ultra-low molecular weight polytetrafluoroethylene (PTFE)(PTFE)Particle is that tetrafluoroethene is aggregated anti- A kind of speciality polymer material of prepared by answering has the advantages that high temperature resistant, low temperature resistant, strong alkali-acid resistance, high lubrication and nontoxic. Polyimides for molecular weight in the range of 300~400, have good wear resistence and high temperatures and certain adhesiveness, favorably In the lasting holding of lubricant film layer.
The present invention has the following advantages compared with prior art:Clean type film lubrication agent produced by the present invention, has the advantage that More, the scope of application is wide, disclosure satisfy that the needs of all trades and professions such as electronic equipment, mechanical equipment, automobile, precision instrument, universal By force.Use temperature range is wide, can be used at -60 DEG C~260 DEG C;Film forming speed is fast, good leveling property, and 10~15s forms dried layer Film;Film layer insulation is non-conductive;Film layer does not flow diffusion, does not adsorb dust particle;The erosion of waterproof and other liquid;To using Environment is without destruction, nontoxic plurality of advantages.
Specific embodiment
The above of the present invention is described in further details by the following examples, but this should not be interpreted as to this The scope for inventing above-mentioned theme is only limitted to following embodiment, and all technologies realized based on the above of the present invention belong to this hair Bright scope.
Embodiment
1st, by 23kg perfluoropolyether, 15kg Ultra-low molecular weight polytetrafluoroethylene (PTFE)(PTFE)Particle, 5kg polyimides, 57kg Fluorocarbon solvent is uniformly mixed obtained clean type film lubrication agent at room temperature.
2nd, by 23kg perfluoropolyether, 20kg Ultra-low molecular weight polytetrafluoroethylene (PTFE)(PTFE)Particle, 5kg polyimides, 52kg Fluorocarbon solvent is uniformly mixed obtained clean type film lubrication agent at room temperature.
3rd, by 29kg perfluoropolyether, 15kg Ultra-low molecular weight polytetrafluoroethylene (PTFE)(PTFE)Particle, 8kg polyimides, 48kg Fluorocarbon solvent is uniformly mixed obtained clean type film lubrication agent at room temperature.
The use temperature range of clean type film lubrication agent is wide made from above-described embodiment, can make at -60 DEG C~260 DEG C With;Film forming speed is fast, good leveling property, and 10~15s forms dried layer film;Film layer insulation is non-conductive;Film layer does not flow diffusion, does not inhale Attached dust particle;The erosion of waterproof and other liquid;To use environment without destruction, nontoxic plurality of advantages.
Have been shown and described above the basic principle of the present invention, main feature and advantage, do not depart from spirit of the invention and On the premise of scope, the present invention also has various changes and modifications, these changes and improvements both fall within claimed invention Scope.

Claims (3)

1. a kind of preparation method of clean type film lubrication agent, it is characterised in that the raw material matched by following weight percent is at room temperature It is uniformly mixed and is made:Perfluoropolyether 20%~30%, Ultra-low molecular weight polytetrafluoroethylene PTFE particle 15%~25%, polyamides Imines 5%~8%, surplus are fluorocarbon solvent.
2. the preparation method of clean type film lubrication agent according to claim 1, it is characterised in that matched somebody with somebody by following weight percent The raw material of ratio is uniformly mixed and is made at room temperature:Perfluoropolyether 30%, Ultra-low molecular weight polytetrafluoroethylene PTFE particle 25%th, polyimides 5%, surplus are fluorocarbon solvent.
3. the preparation method of the face washing mud according to claim 1 for high-efficiency cleaning face, it is characterised in that:The fluorine Polyethers is distillate of the boiling point at 240~260 DEG C, and the molecular weight of polyimides is 300~400.
CN201711409109.0A 2017-12-22 2017-12-22 A kind of preparation method of clean type film lubrication agent Pending CN108085111A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201711409109.0A CN108085111A (en) 2017-12-22 2017-12-22 A kind of preparation method of clean type film lubrication agent

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201711409109.0A CN108085111A (en) 2017-12-22 2017-12-22 A kind of preparation method of clean type film lubrication agent

Publications (1)

Publication Number Publication Date
CN108085111A true CN108085111A (en) 2018-05-29

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201711409109.0A Pending CN108085111A (en) 2017-12-22 2017-12-22 A kind of preparation method of clean type film lubrication agent

Country Status (1)

Country Link
CN (1) CN108085111A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111412372A (en) * 2020-04-15 2020-07-14 山东军沃科技有限公司 Shell case lengthening water-free cleaning processing technology

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102618362A (en) * 2012-02-27 2012-08-01 深圳市优宝惠新材料科技有限公司 Friction-reducing lubricating coating composition
CN104560263A (en) * 2014-12-26 2015-04-29 齐磊 Lubricating agent provided with high temperature resistance and used for rail transit
CN105018195A (en) * 2015-06-23 2015-11-04 东莞市佳丹润滑油有限公司 Special lubricant for plastic part assembly, and preparation method thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102618362A (en) * 2012-02-27 2012-08-01 深圳市优宝惠新材料科技有限公司 Friction-reducing lubricating coating composition
CN104560263A (en) * 2014-12-26 2015-04-29 齐磊 Lubricating agent provided with high temperature resistance and used for rail transit
CN105018195A (en) * 2015-06-23 2015-11-04 东莞市佳丹润滑油有限公司 Special lubricant for plastic part assembly, and preparation method thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111412372A (en) * 2020-04-15 2020-07-14 山东军沃科技有限公司 Shell case lengthening water-free cleaning processing technology

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Application publication date: 20180529

RJ01 Rejection of invention patent application after publication