CN108066206A - A kind of dark hair hair tonic shampoo and preparation method thereof - Google Patents
A kind of dark hair hair tonic shampoo and preparation method thereof Download PDFInfo
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- CN108066206A CN108066206A CN201711270043.1A CN201711270043A CN108066206A CN 108066206 A CN108066206 A CN 108066206A CN 201711270043 A CN201711270043 A CN 201711270043A CN 108066206 A CN108066206 A CN 108066206A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/006—Antidandruff preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q7/00—Preparations for affecting hair growth
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Abstract
The invention discloses a kind of dark hair hair tonic shampoos, are prepared by component as follows in parts by weight：0.05 0.09 parts of 11 30 parts of Eclipta prostrata extracting solution, 5 15 parts of extracting solution of south dodder seed, 12 45 parts of tuber of multiflower knotweed extracting solution, 5 18 parts of angelica extract, 59 parts of surfactant, 48 parts of foam improver and essence.The present invention also provides a kind of preparation methods of dark hair hair tonic shampoo.The raw material of the shampoo of the present invention uses Herba ecliptae, Semen Cuscutae extract, tuber of multiflower knotweed extract and angelica extract, rather than Chinese medicine is in itself, the drug effect of Chinese medicine is played to maximize, possess cleaning, it is anti-dandruff on the basis of, also have effects that hair tonic, black hair, nourishing and maintenance scalp.
Description
Technical field
The present invention relates to a kind of shampoos more particularly to a kind of dark hair hair tonic shampoo and preparation method thereof.
Background technology
Shampoo refers to a kind of hair products with functions such as anti-dandruff, treatment oil function and hair dyeings, in shampoo
Containing Multiple components, the comprehensive function of these compositions can play the function of cleaning scalp and hair.More and more people occur
Common hair problem, the shampoos such as alopecia, hair are dried up, dandruff increases have become day indispensable in people's daily life
Articles for use, most people wash once or wash once for two days head for one day to solve the problems, such as hair, and shampoo on the market is mostly at present
Petroleum hydrocarbon chemical synthesis raw material shampoo, this shampoo of long-time service, the problems such as short-tempered hair, withered, bifurcated can be caused,
Therefore, there is the shampoo of more traditional Chinese medicine ingredients again on the market.
But there are following defects for the shampoo of existing traditional Chinese medicine ingredients：
The shampoo of existing Chinese medicine ingredient be originally traditional Chinese medicine ingredients in itself, by traditional Chinese medicine ingredients tanning mixing and emulsifying be prepared into
Shampoo, but the traditional Chinese medicine ingredients for passing through tanning can not fully be extracted its active ingredient, effect cannot reach optimal
Also waste raw material.
The content of the invention
It, should one of the objects of the present invention is to provide a kind of dark hair hair tonic shampoo for overcome the deficiencies in the prior art
The raw material of shampoo uses Herba ecliptae, Semen Cuscutae extract, tuber of multiflower knotweed extract and angelica extract rather than Chinese medicine
Itself, make Chinese medicine drug effect play maximize, possess cleaning, it is anti-dandruff on the basis of, also with hair tonic, black hair, nourishing and
The effect of conserving scalp.
Second object of the present invention is to provide for a kind of preparation method of dark hair hair tonic shampoo, which will
Eclipta prostrata, Semen Cuscutae, the tuber of multiflower knotweed and Radix Angelicae Sinensis extract respectively is made extract, by extract mix add again surfactant,
Foam improver and essence are sufficiently stirred, and obtain hair tonic, black hair, nourishing and the dark hair hair tonic shampoo for conserving scalp.
An object of the present invention adopts the following technical scheme that realization：
A kind of dark hair hair tonic shampoo is prepared by component as follows in parts by weight：
Further, shampoo is prepared by component as follows in parts by weight：
Further, shampoo is prepared by component as follows in parts by weight：
Further, the surfactant for one or both of Gleditschiasaponin, Tea Saponin and sapindoside with
On.
Further, the foam improver is coconut acid diethanolamide and/or coconut oil acyl propyl glycine betaine.
Realize that second object of the present invention can reach by adopting the following technical scheme that：
A kind of preparation method of dark hair hair tonic shampoo, including,
Material preparation step：Eclipta prostrata, Semen Cuscutae, the tuber of multiflower knotweed and Radix Angelicae Sinensis are cleaned, then dried, it is spare；
Extraction step：After Eclipta prostrata ultramicro grinding, using the ethanol solution extraction that concentration is 70% three times, obtain
Eclipta prostrata extracting solution；
Second extraction step：Take Semen Cuscutae, add in glacial acetic acid solution, add cellulase, water carries, filter after, obtain
To extracting solution of south dodder seed；
Extraction step three times：Take the tuber of multiflower knotweed, using 70% ethanol solution refluxing extraction three times, alkaline condition be concentrated in vacuo
Afterwards, tuber of multiflower knotweed extracting solution is obtained；
Four extraction steps：Radix Angelicae Sinensis smashes it through 20 mesh sieves, merges filter using 95% ethanol solution circumfluence distillation three times
Liquid decompression filters, and angelica extract is obtained after vacuum distillation；
Blend step：Eclipta prostrata extracting solution, extracting solution of south dodder seed, tuber of multiflower knotweed extracting solution and angelica extract are mixed by proportioning
It closes, adds surfactant, foam improver and essence and be sufficiently stirred, obtain dark hair hair tonic shampoo.
Further, in an extraction step, the weight ratio of Eclipta prostrata and ethanol solution is 1：(25-28).
Further, in the second extraction step, the pH of glacial acetic acid solution is 3-4；Semen Cuscutae and the weight of cellulase
Amount is than being 2：(1-3).
Further, in the extraction step three times, refluxing extraction is specially three times：Extraction 2h for the first time, ethanol solution
Weight ratio with the tuber of multiflower knotweed is 10：1；The weight ratio of second of extraction 2h, ethanol solution and the tuber of multiflower knotweed is 8：1；Third time extraction 1h, second
The weight ratio of alcoholic solution and the tuber of multiflower knotweed is 8：1.
Further, in four extraction steps, circumfluence distillation is specially three times：Extraction 8h, ethyl alcohol are molten for the first time
The weight ratio of liquid and Radix Angelicae Sinensis is 8：1；The weight ratio of second of extraction 6h, ethanol solution and Radix Angelicae Sinensis is 6：1；Third time extraction 6h,
The weight ratio of ethanol solution and Radix Angelicae Sinensis is 6：1.
The beneficial effects of the present invention are：
1st, dark hair hair tonic shampoo of the invention, the raw material of the shampoo using Herba ecliptae, Semen Cuscutae extract,
Tuber of multiflower knotweed extract and angelica extract rather than Chinese medicine in itself, make Chinese medicine drug effect play maximize, possess cleaning,
On the basis of anti-dandruff, also there is hair tonic, black hair, nourishing and maintenance scalp；
2nd, the preparation method of dark hair hair tonic shampoo of the present invention, the preparation method is by Eclipta prostrata, Semen Cuscutae, the tuber of multiflower knotweed and Radix Angelicae Sinensis
It extracts respectively and extract is made, extract mixing is added surfactant, foam improver and essence again is sufficiently stirred, and obtains
Hair tonic, black hair, nourishing and the dark hair hair tonic shampoo for conserving scalp.
Specific embodiment
In the following, with reference to specific embodiment, the present invention is described further, it is necessary to which explanation is, what is do not collided
Under the premise of, new embodiment can be formed between various embodiments described below or between each technical characteristic in any combination.
A kind of dark hair hair tonic shampoo is prepared by component as follows in parts by weight：
As the mode that further carries out, shampoo is prepared by component as follows in parts by weight：
As the mode that further carries out, shampoo is prepared by component as follows in parts by weight：
As the mode that further carries out, the surfactant is in Gleditschiasaponin, Tea Saponin and sapindoside
It is one or more kinds of.
As the mode that further carries out, the foam improver is coconut acid diethanolamide and/or coconut oleoyl third
Base glycine betaine.
The preparation method of above-mentioned dark hair hair tonic shampoo, including,
Material preparation step：Eclipta prostrata, Semen Cuscutae, the tuber of multiflower knotweed and Radix Angelicae Sinensis are cleaned, then dried, it is spare；
Extraction step：After Eclipta prostrata ultramicro grinding, using the ethanol solution extraction that concentration is 70% three times, obtain
Eclipta prostrata extracting solution；
Second extraction step：Take Semen Cuscutae, add in glacial acetic acid solution, add cellulase, water carries, filter after, obtain
To extracting solution of south dodder seed；
Extraction step three times：Take the tuber of multiflower knotweed, using 70% ethanol solution refluxing extraction three times, alkaline condition be concentrated in vacuo
Afterwards, tuber of multiflower knotweed extracting solution is obtained；
Four extraction steps：Radix Angelicae Sinensis smashes it through 20 mesh sieves, merges filter using 95% ethanol solution circumfluence distillation three times
Liquid decompression filters, and angelica extract is obtained after vacuum distillation；
Blend step：Eclipta prostrata extracting solution, extracting solution of south dodder seed, tuber of multiflower knotweed extracting solution and angelica extract are mixed by proportioning
It closes, adds surfactant, foam improver and essence and be sufficiently stirred, obtain dark hair hair tonic shampoo.
As the mode that further carries out, in an extraction step, the weight ratio of Eclipta prostrata and ethanol solution is 1：(25-
28)。
As the mode that further carries out, in second extraction step, the pH of glacial acetic acid solution is 3-4；Semen Cuscutae and fiber
The weight ratio of plain enzyme is 2：(1-3).
As the mode that further carries out, three times in extraction step, refluxing extraction is specially three times：Extraction 2h for the first time,
The weight ratio of ethanol solution and the tuber of multiflower knotweed is 10：1；The weight ratio of second of extraction 2h, ethanol solution and the tuber of multiflower knotweed is 8：1；For the third time
The weight ratio of extraction 1h, ethanol solution and the tuber of multiflower knotweed is 8：1.
As the mode that further carries out, in four extraction steps, circumfluence distillation is specially three times：It extracts for the first time
The weight ratio of 8h, ethanol solution and Radix Angelicae Sinensis is 8：1；The weight ratio of second of extraction 6h, ethanol solution and Radix Angelicae Sinensis is 6：1；3rd
The weight ratio of secondary extraction 6h, ethanol solution and Radix Angelicae Sinensis is 6：1.
It is specific embodiment of the present invention below, used raw material, equipment etc. remove special limit in the following embodiments
It can be obtained outside fixed by buying pattern.
Embodiment 1-5：
The proportioning of 1 embodiment 1-5 of table
| Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | |
| Eclipta prostrata extracting solution | 11 | 30 | 18 | 23 | 20 |
| Extracting solution of south dodder seed | 5 | 15 | 9 | 12 | 11 |
| Tuber of multiflower knotweed extracting solution | 12 | 45 | 28 | 34 | 31 |
| Angelica extract | 5 | 18 | 10 | 14 | 12 |
| Surfactant | 5 | 9 | 6 | 8 | 7 |
| Foam improver | 4 | 8 | 5 | 7 | 6 |
| Essence | 0.05 | 0.09 | 0.06 | 0.08 | 0.07 |
Wherein, the surfactant of embodiment 1 is Gleditschiasaponin, and foam improver is coconut acid diethanolamide.
The surfactant of embodiment 2 is Tea Saponin, and foam improver is coconut oil acyl propyl glycine betaine.
The surfactant of embodiment 3 is sapindoside, and foam improver is coconut oil acyl propyl glycine betaine.
The surfactant of embodiment 4 is Gleditschiasaponin and sapindoside, and the two mass ratio is 1：1, foam improver is coconut palm
Seed oil acyl propyl glycine betaine.
The surfactant of embodiment 5 is Gleditschiasaponin and Tea Saponin, and the two mass ratio is 3：4, foam improver is coconut oil
Sour diglycollic amide and coconut oil acyl propyl glycine betaine, the two mass ratio are 1：1.
The preparation method of the dark hair hair tonic shampoo of embodiment 1-5 follows the steps below, and step includes,
Material preparation step：Eclipta prostrata, Semen Cuscutae, the tuber of multiflower knotweed and Radix Angelicae Sinensis are cleaned, then dried, it is spare；
Extraction step：After Eclipta prostrata ultramicro grinding, using the ethanol solution extraction that concentration is 70% three times, every time
The weight ratio of Eclipta prostrata and ethanol solution is 1：(25-28) obtains Eclipta prostrata extracting solution；
Second extraction step：Semen Cuscutae is taken, is added in glacial acetic acid solution, the pH of glacial acetic acid solution is 3-4, adds fiber
The weight ratio of plain enzyme, Semen Cuscutae and cellulase is 2：(1-3), water carries, filter after, obtain extracting solution of south dodder seed；
Extraction step three times：Take the tuber of multiflower knotweed, using 70% ethanol solution refluxing extraction three times, alkaline condition be concentrated in vacuo
Afterwards, tuber of multiflower knotweed extracting solution is obtained；Refluxing extraction is specially three times：The weight ratio of extraction 2h for the first time, ethanol solution and the tuber of multiflower knotweed is 10：
1；The weight ratio of second of extraction 2h, ethanol solution and the tuber of multiflower knotweed is 8：1；The weight of third time extraction 1h, ethanol solution and the tuber of multiflower knotweed
Than for 8：1；
Four extraction steps：Radix Angelicae Sinensis smashes it through 20 mesh sieves, merges filter using 95% ethanol solution circumfluence distillation three times
Liquid decompression filters, and angelica extract is obtained after vacuum distillation；Circumfluence distillation is specially three times：Extraction 8h, ethyl alcohol are molten for the first time
The weight ratio of liquid and Radix Angelicae Sinensis is 8：1；The weight ratio of second of extraction 6h, ethanol solution and Radix Angelicae Sinensis is 6：1；Third time extraction 6h,
The weight ratio of ethanol solution and Radix Angelicae Sinensis is 6：1；
Blend step：Eclipta prostrata extracting solution, extracting solution of south dodder seed, tuber of multiflower knotweed extracting solution and angelica extract are mixed by proportioning
It closes, adds surfactant, foam improver and essence and be sufficiently stirred, obtain dark hair hair tonic shampoo.
Comparative example 1：
1 difference from Example 1 of comparative example is, the component of comparative example 1 is Eclipta prostrata, Semen Cuscutae, the tuber of multiflower knotweed and Radix Angelicae Sinensis,
Preparation method is to be mixed again with remaining ingredient after boiling Eclipta prostrata, Semen Cuscutae, the tuber of multiflower knotweed and Radix Angelicae Sinensis.
Comparative example 2：
2 difference from Example 1 of comparative example is, surfactant-free, foam improver and essence in comparative example 2.
Effect assessment and performance detection
First, physical and chemical index
According to the regulation of GB/T 29679-2013, physical and chemical index is carried out to the shampoo of embodiment 1-5 and comparative example 1-2
Detection, testing result are as follows：
2 physical and chemical index result of table
By table 2 as it can be seen that embodiment 1-5 and comparative example 1 are satisfied by the regulation of GB/T 29679-2013, and embodiment 3-5
Effect is better than embodiment 1-2, wherein, 5 effect of embodiment is best.And the foam of comparative example 1 is smaller, substance content is low, comparison
Heat resistance, cold resistance, foam size and the substance content of example 2 are unsatisfactory for providing.
2nd, clinical test
70 volunteers are chosen, are divided into 7 groups, every group of 10 people, 70 volunteers are tight with alopecia, dandruff in various degree
The symptoms such as weight, white hair, respectively using the shampoo three months of embodiment 1-5 and comparative example 1-2, effect is as follows：
3 clinical detection result of table
By table 3 as it can be seen that the shampoo of embodiment 1-5, which can generate, reduces dandruff, blackening hair, the new work of growth
With, and the effect of embodiment 3-5 is better than embodiment 1-2, wherein, the effect of embodiment 5 is best, and 1 dandruff of comparative example is less
It reduces, 2 fruit not yet in effect of comparative example, this illustrates that the effect of the shampoo of the present invention is generated by the synergy between component, only
Corresponding effect only can not be obtained with traditional Chinese medicine ingredients, is maximized moreover, can play the drug effect of Chinese medicine using extracting solution,
Possess cleaning, it is anti-dandruff on the basis of, also have effects that hair tonic, black hair, nourishing and maintenance scalp.
The above embodiment is only the preferred embodiment of the present invention, it is impossible to the scope of protection of the invention is limited with this,
The variation and replacement for any unsubstantiality that those skilled in the art is done on the basis of the present invention belong to institute of the present invention
Claimed scope.
Claims (10)
1. a kind of dark hair hair tonic shampoo, which is characterized in that it is prepared by component as follows in parts by weight：
2. dark hair hair tonic shampoo as described in claim 1, which is characterized in that it is by component system as follows in parts by weight
It is standby to form：
3. dark hair hair tonic shampoo as described in claim 1, which is characterized in that it is by component system as follows in parts by weight
It is standby to form：
4. dark hair hair tonic shampoo as described in claim 1, which is characterized in that the surfactant is Gleditschiasaponin, tea
It is more than one or both of saponin and sapindoside.
5. dark hair hair tonic shampoo as described in claim 1, which is characterized in that the foam improver is cocinic acid diethanol acyl
Amine and/or coconut oil acyl propyl glycine betaine.
It is 6. a kind of such as the preparation method of claim 1-5 any one of them dark hair hair tonic shampoos, it is characterised in that including,
Material preparation step：Eclipta prostrata, Semen Cuscutae, the tuber of multiflower knotweed and Radix Angelicae Sinensis are cleaned, then dried, it is spare；
Extraction step：After Eclipta prostrata ultramicro grinding, using the ethanol solution extraction that concentration is 70% three times, non-irrigated lotus is obtained
Careless extracting solution；
Second extraction step：Take Semen Cuscutae, add in glacial acetic acid solution, add cellulase, water carries, filter after, obtain Tu
The sub- extracting solution of silk；
Extraction step three times：Take the tuber of multiflower knotweed, using 70% ethanol solution refluxing extraction three times, alkaline condition vacuum concentration after,
Obtain tuber of multiflower knotweed extracting solution；
Four extraction steps：Radix Angelicae Sinensis smashes it through 20 mesh sieves, and, merging filtrate subtracts using 95% ethanol solution circumfluence distillation three times
Pressure filters, and angelica extract is obtained after vacuum distillation；
Blend step：Eclipta prostrata extracting solution, extracting solution of south dodder seed, tuber of multiflower knotweed extracting solution and angelica extract are mixed by proportioning, then
It adds in surfactant, foam improver and essence to be sufficiently stirred, obtains dark hair hair tonic shampoo.
7. the preparation method of dark hair hair tonic shampoo as claimed in claim 6 a, which is characterized in that extraction step
In, the weight ratio of Eclipta prostrata and ethanol solution is 1：(25-28).
8. the preparation method of dark hair hair tonic shampoo as claimed in claim 6, which is characterized in that the second extraction step
In, the pH of glacial acetic acid solution is 3-4；The weight ratio of Semen Cuscutae and cellulase is 2：(1-3).
9. the preparation method of dark hair hair tonic shampoo as claimed in claim 6, which is characterized in that the extraction step three times
In, refluxing extraction is specially three times：The weight ratio of extraction 2h for the first time, ethanol solution and the tuber of multiflower knotweed is 10：1；Second of extraction 2h,
The weight ratio of ethanol solution and the tuber of multiflower knotweed is 8：1；The weight ratio of third time extraction 1h, ethanol solution and the tuber of multiflower knotweed is 8：1.
10. the preparation method of dark hair hair tonic shampoo as claimed in claim 6, which is characterized in that four extraction steps
In, circumfluence distillation is specially three times：The weight ratio of extraction 8h for the first time, ethanol solution and Radix Angelicae Sinensis is 8：1；Second of extraction
The weight ratio of 6h, ethanol solution and Radix Angelicae Sinensis is 6：1；The weight ratio of third time extraction 6h, ethanol solution and Radix Angelicae Sinensis is 6：1.
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| CN109303731A (en) * | 2018-11-26 | 2019-02-05 | 庄雪芸 | A kind of shampoo formula with scalp anti-aging function |
| CN111419769A (en) * | 2020-04-23 | 2020-07-17 | 广州市白云区莱媚美容美发日用化妆品厂 | Plant essence formula capable of effectively promoting hair growth and preparation method thereof |
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Application publication date: 20180525 |