CN108059870A - A kind of antibiotic property offset ink and preparation method thereof - Google Patents
A kind of antibiotic property offset ink and preparation method thereof Download PDFInfo
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- CN108059870A CN108059870A CN201711431737.9A CN201711431737A CN108059870A CN 108059870 A CN108059870 A CN 108059870A CN 201711431737 A CN201711431737 A CN 201711431737A CN 108059870 A CN108059870 A CN 108059870A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
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Abstract
The present invention relates to offset ink preparing technical fields, specifically, it is related to a kind of antibiotic property offset ink and preparation method thereof, including 95~110 parts of binder, organo-mineral complexing antiseptic 8~12, auxiliary agent 5~10, by adding in the complex antimicrobials being made of bacterium antiseptic and sterile antiseptic in the present invention, it can effectively kill and inhibit the procreation of germ, really realize antibacterial effect, the dichloro-dimethyl glycolylurea in the organic antibacterial agent of addition discharges slowly in ink simultaneously, so that preparing the offset ink formed has anti-microbial property steady in a long-term, it can be effectively so that the germ on printing carrier kills and inhibits the procreation of germ after organic antibacterial agent volatilization.The place for being printed with ink on printing carrier can not only be caused to realize antibacterial, and realize the place for not having ink on printing carrier equally there is antibacterial bacteriostatic effect.
Description
Technical field：
The present invention relates to offset ink preparing technical fields, and in particular, to a kind of antibiotic property offset ink and its preparation
Method.
Background technology：
Offset ink is mainly the coloured material for the flow-like being made of pigment, auxiliary agent, high molecular polymer and solvent,
In, the primary solvent of offset ink is mineral oil and vegetable oil.The drying process that offset ink is printed onto on paper is very multiple
Miscellaneous, we, which can be understood as ink, is dried by the oxidation filming of mineral oil infiltration and vegetable oil.
As the improvement of people's living standards, higher requirement is proposed to environmental quality, health and the health of itself, it is right
In the bacterium that naked eyes can not be seen, it is potentially hazardous that people even more can not put up with its.Current market sales of offset ink is simultaneously
Do not possess anti-microbial property, the product come is printed out using these offset inks and does not also possess anti-microbial property, surface becomes easily infected by
Bacterium, it is difficult to meet the needs of people, Application No. CN201410362497.1 discloses a kind of traditional Chinese medicine ingredients containing antibiotic property
Ink is printed, zinc oxide, folium isatidis, the coptis are added in component for antibacterial, utilizes big yellow leaf, the automatic sterilization function characteristic of the coptis
Antibacterial is carried out, anti-microbial property is single, and effect is not notable, and Application No. CN1195120C is related to antibacterial ink, and use is inorganic
Carrying silver antimicrobials.It, or antibacterial effect is not notable when single carrying metal ion inorganic antiseptic adds use in ink
Product is made to change colour, the sample antibacterial effect such as obtained using zeolite or silica type the antiseptic addition of carrying silver ion in ink
Fruit reappearance is bad or not notable and more serious to the abrasion of the equipment such as three-roller during printing ink to manufacture, is not suitable for oil
Ink makes.
The content of the invention：
The present invention overcomes the defects of prior art, provides a kind of antibiotic property offset ink and preparation method thereof.
The technical problems to be solved by the invention are realized using following technical scheme：A kind of antibiotic property offset ink, by weight
Part meter is measured, including 95~110 parts of binder, Organic-inorganic composite antiseptic 8~12, auxiliary agent 5~10；
The Organic-inorganic composite antiseptic contains organic antibacterial agent and inorganic antiseptic；
In the present invention, the inorganic antiseptic is the phosphate for having loaded silver ion, zinc ion or silver zinc complex ion
Or glass micro mist, the phosphate are selected from cubic basic zirconium phosphate, bedded zirconium phosphate or sodium phosphate, elemental oxygen has Strong oxdiative
Property can sterilize, can consumingly attract the sulfydryl (- SH) on protease in bacterial body, and it is rapid together with it, make
Protease loss of activity, causes bacterial death.After bacterium is by Ag+, Zn2+, Ag+, Zn2+ understand bacterium corpse middle reaches and separate out again
Come, then contacted with other bacterium colonies, proceeded as described above again and again, so bactericidal effect is lasting.
In the present invention, the organic antibacterial agent is sodium dichloro cyanurate, Efficacious Disinfeitant, dichloro-dimethyl sea
Because, one kind in two cyanuric acid of chlorine bromine or and its mixture, preferably dichloro-dimethyl glycolylurea, its available chlorine content be
More than 70%, there is stronger sterilizing ability, irritation and corrosivity are weak, can be suitable for people, animal, environment, and stablize
Property it is high, dichloro-dimethyl glycolylurea discharge slowly in ink so for preparing the offset ink of formation with antibacterial steady in a long-term
Performance.
By adding in the complex antimicrobials being made of bacterium antiseptic and sterile antiseptic in the present invention, can effectively kill simultaneously
Inhibit the procreation of germ, really realize antibacterial effect, while the dichloro-dimethyl glycolylurea in the organic antibacterial agent added is in ink
Middle release is slow so that preparing the offset ink of formation has anti-microbial property steady in a long-term, can after organic antibacterial agent volatilization
The effective germ caused on printing carrier kills and inhibits the procreation of germ.It can not only to be printed on printing carrier
Antibacterial is realized in the place of ink, and not having on printing carrier the place of ink to realize antibacterial bacteriostatic effect.
The binder includes hard resin, refined soybean oil, soya fatty acid fat, wherein, hard resin：It is refined
Soybean oil：The mass ratio of soya fatty acid fat is (0.4~1.3)：1：(2~14).
Chinese medicine group agent is further included in the binder, the Chinese medicine group agent is included in folium artemisiae argyi, honeysuckle, dandelion
A kind of or mixture, the folium artemisiae argyi, honeysuckle, the grain size of dandelion granule folium artemisiae argyi, gold in 0.4~1.6um, the present invention
Honeysuckle flower, dandelion are to buy in the market, and the present invention does not have particular/special requirement to it.
The Chinese medicine group agent：The mass ratio of binder is (0.1~0.15)：1.
In the Organic-inorganic composite antiseptic, organic antibacterial agent：The weight ratio of inorganic antiseptic is 1：(1.3~
2)。
The auxiliary agent is included in viscosity-controlling agent, emulsion resistance auxiliary agent, dispersant, antiwear additive, drier or barras oil
One or more combinations.
The binder is made by the steps：
(1) hard resin, refined soybean oil, soya fatty acid ester are added in four mouthfuls of reaction flasks, is heated to 160 DEG C
It is melted completely to resin, under conditions of nitrogen protection, 75rpm rotating speeds, is continuously heating to 180 DEG C, when heat preservation 1 is small, is set
Lipoprotein solution A；
(2) above-mentioned solution A is cooled to 145 DEG C, adds in alumina gel agent, Chinese medicine group agent is warming up to 170 DEG C, and heat preservation 0.5 is small
When, viscosimetric if viscosity is less than 75000mPas/25 DEG C, continues heat preservation and surveyed a viscosity every 15 minutes, until viscosity reaches
To 85000~90000mPas/25 DEG C；If viscosity is more than standard value, extremely closed with reserved soya fatty acid ester adjustment viscosity
Lattice.
The preparation method of the antibiotic property offset ink, comprises the following steps：
S1, binder is prepared；
S2, the binder being prepared and other residual components are mixed, put into homogenizer, with 16000 revs/min
The rotating speed of clock obtains mixture after being dispersed with stirring 3h；
S3, mixture being put into ball-milling treatment in ball mill again, the grain size for making gained slurry is less than 15 μm, and according to need
Adjust viscosity to get.
Compared with prior art, beneficial effects of the present invention are：
1st, can effectively be killed in the present invention by adding in the complex antimicrobials being made of bacterium antiseptic and sterile antiseptic
And inhibit the procreation of germ, really realize antibacterial effect, while the dichloro-dimethyl glycolylurea in the organic antibacterial agent added is in oil
It is discharged in ink slow so that preparing the offset ink of formation has anti-microbial property steady in a long-term, energy after organic antibacterial agent volatilization
Enough effective germs caused on printing carrier kill and inhibit the procreation of germ.It can not only to print on printing carrier
Antibacterial is realized in the place for having ink, and realizing does not have the place of ink is similary to have antibacterial bacteriostatic effect on printing carrier；
2nd, Chinese medicine group agent is added in binder, any direction in binder of the plant fiber in one side Chinese medicine group agent
Stretching, extension, greatly improves the tension of offset ink and the ability of anti-twist deformation so that reliable and stable after printing, the opposing party
Face, the antimicrobial component in Chinese medicine group agent is readily volatilized, can realize antibacterial effect rapidly, and after the agent of Chinese medicine group is failed, volatilization is slow
Slow organic antibacterial agent takes over Chinese medicine group agent and continues to realize antibacterial effect, so that the antibacterial ability of the present invention is greatly carried
Height, good anti-bacterial effect, durable antibacterial effect are stablized.
Specific embodiment：
In order to be easy to understand the technical means, the creative features, the aims and the efficiencies achieved by the present invention, tie below
Specific embodiment is closed, the present invention is furture elucidated.
Embodiment 1：
A kind of antibiotic property offset ink includes the material composition of following parts by weight：In in 100 parts of binder, binder
8 parts of medicine group agent, 4 parts of organic antibacterial agent, 6 parts of inorganic antiseptic, 7 parts of auxiliary agent；
The Chinese medicine group agent includes the grain size of folium artemisiae argyi, honeysuckle, the mixture in dandelion and the mixture for 1um,
Hard resin in binder：Refined soybean oil：The mass ratio of soya fatty acid fat is 1：1：8, auxiliary agent is viscosity-controlling agent, resists
Composition in emulsion adjuvant, dispersant, antiwear additive, drier or barras oil.
The preparation method of above-mentioned antibiotic property offset ink comprises the following steps：
S1, binder is prepared；
S2, the binder being prepared and other residual components are mixed, put into homogenizer, with 16000 revs/min
The rotating speed of clock obtains mixture after being dispersed with stirring 3h；
S3, mixture being put into ball-milling treatment in ball mill again, the grain size for making gained slurry is less than 15 μm, and according to need
Adjust viscosity to get.
In the experiment, the ball mill used is AX- vertical mixing ball milling of the Wuxi into the production of inscription drying equipment Co., Ltd
Machine；
The stirred tank that the homogenizer used produces for golden 100,000,000,000 Machinery Co., Ltd.s of Dongguan City.
Embodiment 2：
A kind of antibiotic property offset ink includes the material composition of following parts by weight：Chinese medicine in 95 parts of binder, binder
6 parts of agent of group, 4 parts of organic antibacterial agent, 6 parts of inorganic antiseptic, 7 parts of auxiliary agent；
The Chinese medicine group agent includes the grain size of folium artemisiae argyi, honeysuckle, the mixture in dandelion and the mixture for 1um,
Hard resin in binder：Refined soybean oil：The mass ratio of soya fatty acid fat is 1：1：8, auxiliary agent is viscosity-controlling agent, resists
Composition in emulsion adjuvant, dispersant, antiwear additive, drier or barras oil.
The preparation method of above-mentioned antibiotic property offset ink comprises the following steps：
S1, binder is prepared；
S2, the binder being prepared and other residual components are mixed, put into homogenizer, with 16000 revs/min
The rotating speed of clock obtains mixture after being dispersed with stirring 3h；
S3, mixture being put into ball-milling treatment in ball mill again, the grain size for making gained slurry is less than 15 μm, and according to need
Adjust viscosity to get.
Embodiment 3：
A kind of antibiotic property offset ink includes the material composition of following parts by weight：In in 110 parts of binder, binder
9 parts of medicine group agent, 4 parts of organic antibacterial agent, 6 parts of inorganic antiseptic, 7 parts of auxiliary agent；
The Chinese medicine group agent includes the grain size of folium artemisiae argyi, honeysuckle, the mixture in dandelion and the mixture for 1um,
Hard resin in binder：Refined soybean oil：The mass ratio of soya fatty acid fat is 1：1：8, auxiliary agent is viscosity-controlling agent, resists
Composition in emulsion adjuvant, dispersant, antiwear additive, drier or barras oil.
The preparation method of above-mentioned antibiotic property offset ink comprises the following steps：
S1, binder is prepared；
S2, the binder being prepared and other residual components are mixed, put into homogenizer, with 16000 revs/min
The rotating speed of clock obtains mixture after being dispersed with stirring 3h；
S3, mixture being put into ball-milling treatment in ball mill again, the grain size for making gained slurry is less than 15 μm, and according to need
Adjust viscosity to get.
Embodiment 4：
A kind of antibiotic property offset ink includes the material composition of following parts by weight：In in 100 parts of binder, binder
8 parts of medicine group agent, 3.5 parts of organic antibacterial agent, 4.5 parts of inorganic antiseptic, 7 parts of auxiliary agent；
The Chinese medicine group agent includes the grain size of folium artemisiae argyi, honeysuckle, the mixture in dandelion and the mixture for 1um,
Hard resin in binder：Refined soybean oil：The mass ratio of soya fatty acid fat is 1：1：8, auxiliary agent is viscosity-controlling agent, resists
Composition in emulsion adjuvant, dispersant, antiwear additive, drier or barras oil.
The preparation method of above-mentioned antibiotic property offset ink comprises the following steps：
S1, binder is prepared；
S2, the binder being prepared and other residual components are mixed, put into homogenizer, with 16000 revs/min
The rotating speed of clock obtains mixture after being dispersed with stirring 3h；
S3, mixture being put into ball-milling treatment in ball mill again, the grain size for making gained slurry is less than 15 μm, and according to need
Adjust viscosity to get.
Embodiment 5：
A kind of antibiotic property offset ink includes the material composition of following parts by weight：In in 100 parts of binder, binder
8 parts of medicine group agent, 5 parts of organic antibacterial agent, 7 parts of inorganic antiseptic, 7 parts of auxiliary agent；
The Chinese medicine group agent includes the grain size of folium artemisiae argyi, honeysuckle, the mixture in dandelion and the mixture for 1um,
Hard resin in binder：Refined soybean oil：The mass ratio of soya fatty acid fat is 1：1：8, auxiliary agent is viscosity-controlling agent, resists
Composition in emulsion adjuvant, dispersant, antiwear additive, drier or barras oil.
The preparation method of above-mentioned antibiotic property offset ink comprises the following steps：
S1, binder is prepared；
S2, the binder being prepared and other residual components are mixed, put into homogenizer, with 16000 revs/min
The rotating speed of clock obtains mixture after being dispersed with stirring 3h；
S3, mixture being put into ball-milling treatment in ball mill again, the grain size for making gained slurry is less than 15 μm, and according to need
Adjust viscosity to get.
Comparative example 1：
A kind of antibiotic property offset ink includes the material composition of following parts by weight：Chinese medicine in 90 parts of binder, binder
5 parts of agent of group, 4 parts of organic antibacterial agent, 6 parts of inorganic antiseptic, 7 parts of auxiliary agent；
The Chinese medicine group agent includes the grain size of folium artemisiae argyi, honeysuckle, the mixture in dandelion and the mixture for 1um,
Hard resin in binder：Refined soybean oil：The mass ratio of soya fatty acid fat is 1：1：8, auxiliary agent is viscosity-controlling agent, resists
Composition in emulsion adjuvant, dispersant, antiwear additive, drier or barras oil.
The preparation method of above-mentioned antibiotic property offset ink comprises the following steps：
S1, binder is prepared；
S2, the binder being prepared and other residual components are mixed, put into homogenizer, with 16000 revs/min
The rotating speed of clock obtains mixture after being dispersed with stirring 3h；
S3, mixture being put into ball-milling treatment in ball mill again, the grain size for making gained slurry is less than 15 μm, and according to need
Adjust viscosity to get.
Comparative example 2：
A kind of antibiotic property offset ink includes the material composition of following parts by weight：In in 120 parts of binder, binder
10 parts of medicine group agent, 4 parts of organic antibacterial agent, 6 parts of inorganic antiseptic, 7 parts of auxiliary agent；
The Chinese medicine group agent includes the grain size of folium artemisiae argyi, honeysuckle, the mixture in dandelion and the mixture for 1um,
Hard resin in binder：Refined soybean oil：The mass ratio of soya fatty acid fat is 1：1：8, auxiliary agent is viscosity-controlling agent, resists
Composition in emulsion adjuvant, dispersant, antiwear additive, drier or barras oil.
The preparation method of above-mentioned antibiotic property offset ink comprises the following steps：
S1, binder is prepared；
S2, the binder being prepared and other residual components are mixed, put into homogenizer, with 16000 revs/min
The rotating speed of clock obtains mixture after being dispersed with stirring 3h；
S3, mixture being put into ball-milling treatment in ball mill again, the grain size for making gained slurry is less than 15 μm, and according to need
Adjust viscosity to get.
Comparative example 3：
A kind of antibiotic property offset ink includes the material composition of following parts by weight：In in 100 parts of binder, binder
8 parts of medicine group agent, 2 parts of organic antibacterial agent, 4 parts of inorganic antiseptic, 7 parts of auxiliary agent；
The Chinese medicine group agent includes the grain size of folium artemisiae argyi, honeysuckle, the mixture in dandelion and the mixture for 1um,
Hard resin in binder：Refined soybean oil：The mass ratio of soya fatty acid fat is 1：1：8, auxiliary agent is viscosity-controlling agent, resists
Composition in emulsion adjuvant, dispersant, antiwear additive, drier or barras oil.
The preparation method of above-mentioned antibiotic property offset ink comprises the following steps：
S1, binder is prepared；
S2, the binder being prepared and other residual components are mixed, put into homogenizer, with 16000 revs/min
The rotating speed of clock obtains mixture after being dispersed with stirring 3h；
S3, mixture being put into ball-milling treatment in ball mill again, the grain size for making gained slurry is less than 15 μm, and according to need
Adjust viscosity to get.
Comparative example 4：
A kind of antibiotic property offset ink includes the material composition of following parts by weight：In in 100 parts of binder, binder
8 parts of medicine group agent, 5 parts of organic antibacterial agent, 9 parts of inorganic antiseptic, 7 parts of auxiliary agent；
The Chinese medicine group agent includes the grain size of folium artemisiae argyi, honeysuckle, the mixture in dandelion and the mixture for 1um,
Hard resin in binder：Refined soybean oil：The mass ratio of soya fatty acid fat is 1：1：8, auxiliary agent is viscosity-controlling agent, resists
Composition in emulsion adjuvant, dispersant, antiwear additive, drier or barras oil.
The preparation method of above-mentioned antibiotic property offset ink comprises the following steps：
S1, binder is prepared；
S2, the binder being prepared and other residual components are mixed, put into homogenizer, with 16000 revs/min
The rotating speed of clock obtains mixture after being dispersed with stirring 3h；
S3, mixture being put into ball-milling treatment in ball mill again, the grain size for making gained slurry is less than 15 μm, and according to need
Adjust viscosity to get.
By Examples 1 to 5, offset ink test performance index that comparative example 1~4 is prepared, test method summary
It is as follows：
Viscosity test, using ink viscosity instrument YQM-1, sticky instrument is tested in the case of rotation prevents the separation of ink thin layer
Or the resistance torque ripped, it is represented with the size of the arm of force.
Fluidity testing, the ink sample of certain volume, through certain time, it is straight to be extended to cylinder under authorized pressure
Footpath size represents.
Emulsification rate is tested, and selects I type emulsion testers of RH-100- that 100 grams of water and 100 grams of sample are put into graduated cylinder
It is stirred, filters out extra moisture, claim the percentage of its mixture, be exactly the water absorption rate of the ink.
Fixed velocity test, using QB570-1983 standard testings.
Glossiness is tested, and universal 60 ° of mirror surface luster instrument LS192 is selected to measure the glossiness of ink.
Antibiotic property is tested, and the culture dish for preparing experimental strain cultivates gemma respectively, Escherichia coli, staphylococcus aureus,
Then its average colony number is respectively dropped into the ink prepared in 2 drop embodiments and comparative example, 2 is small at 1136*100 (cfu/ml)
When observe strain quantity, calculate antibiotic property, with original amount than survival strain quantity.
Test result is as shown in table 1 below：
Table 1
Basic principle, main feature and the features of the present invention of the present invention has been shown and described above.The technology of the industry
Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the above embodiments and description only describe this
The principle of invention, without departing from the spirit and scope of the present invention, various changes and modifications of the present invention are possible, these changes
Change and improvement is both fallen in the range of claimed invention.The scope of protection of present invention is by appended claims
And its equivalent thereof.
Claims (8)
1. a kind of antibiotic property offset ink, which is characterized in that by weight, including 95~110 parts of binder, organic and inorganic
8~12 parts of complex antimicrobials, 5~10 parts of auxiliary agent；
The Organic-inorganic composite antiseptic contains organic antibacterial agent and inorganic antiseptic；
The inorganic antiseptic is the phosphate or glass micro mist for having loaded silver ion, zinc ion or silver zinc complex ion；
The phosphate is selected from cubic basic zirconium phosphate, bedded zirconium phosphate or sodium phosphate；
The organic antibacterial agent is sodium dichloro cyanurate, Efficacious Disinfeitant, dichloro-dimethyl glycolylurea, two cyanuric acid of chlorine bromine
In one kind or and its mixture.
2. antibiotic property offset ink according to claim 1, which is characterized in that the binder include hard resin,
Refined soybean oil, soya fatty acid fat, wherein, hard resin：Refined soybean oil：The mass ratio of soya fatty acid fat is
(0.4~1.3)：1：(2~14).
3. antibiotic property offset ink according to claim 2, which is characterized in that Chinese medicine group is further included in the binder
Agent, the Chinese medicine group agent include folium artemisiae argyi, honeysuckle, one kind in dandelion or mixture, the folium artemisiae argyi, honeysuckle, Pu
The grain size of public English particle is in 0.4~1.6um.
4. antibiotic property offset ink according to claim 3, which is characterized in that the Chinese medicine group agent：The matter of binder
Amount is than being (0.1~0.15)：1.
5. antibiotic property offset ink according to claim 1, which is characterized in that the Organic-inorganic composite antiseptic
In, organic antibacterial agent：The weight ratio of inorganic antiseptic is 1：(1.3~2).
6. antibiotic property offset ink according to claim 1, which is characterized in that the auxiliary agent includes viscosity-controlling agent, resists
One or more combinations in emulsion adjuvant, dispersant, antiwear additive, drier or barras oil.
7. antibiotic property offset ink according to claim 1, which is characterized in that the binder is made as follows
It is standby：
(1) hard resin, refined soybean oil, soya fatty acid ester are added in four mouthfuls of reaction flasks, is heated to 160 DEG C to tree
Fat melts completely, under conditions of nitrogen protection, 75rpm rotating speeds, is continuously heating to 180 DEG C, when heat preservation 1 is small, it is molten to obtain resin
Liquid A；
(2) above-mentioned solution A is cooled to 145 DEG C, adds in alumina gel agent, Chinese medicine group agent is warming up to 170 DEG C, when heat preservation 0.5 is small, surveys
Viscosity if viscosity is less than 75000mPas/25 DEG C, continues heat preservation and surveyed a viscosity every 15 minutes, until viscosity reaches
85000~90000mPas/25 DEG C；If viscosity is more than standard value, extremely closed with reserved soya fatty acid ester adjustment viscosity
Lattice.
8. according to the preparation method of the antibiotic property offset ink described in any one of claim 1~7, which is characterized in that including
Following steps：
S1, binder is prepared；
S2, the binder being prepared and other residual components are mixed, put into homogenizer, with 16000 revs/min
Rotating speed obtains mixture after being dispersed with stirring 3h；
S3, mixture is put into ball-milling treatment in ball mill again, the grain size for making gained slurry is less than 15 μm, and is adjusted as needed
Save viscosity to get.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201711431737.9A CN108059870A (en) | 2017-12-26 | 2017-12-26 | A kind of antibiotic property offset ink and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711431737.9A CN108059870A (en) | 2017-12-26 | 2017-12-26 | A kind of antibiotic property offset ink and preparation method thereof |
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| CN109203741A (en) * | 2018-09-20 | 2019-01-15 | 华蓥市职业教育培训中心 | A kind of printing technology of corrugated case |
| CN112048942A (en) * | 2020-09-07 | 2020-12-08 | 安徽天翔高新特种包装材料集团有限公司 | Antibacterial cigarette tipping paper and printing process thereof |
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