CN108059801A - A kind of high grade of transparency plate base-material of automation equipment and preparation method thereof - Google Patents
A kind of high grade of transparency plate base-material of automation equipment and preparation method thereof Download PDFInfo
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- CN108059801A CN108059801A CN201711094989.7A CN201711094989A CN108059801A CN 108059801 A CN108059801 A CN 108059801A CN 201711094989 A CN201711094989 A CN 201711094989A CN 108059801 A CN108059801 A CN 108059801A
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- parts
- automation equipment
- high grade
- plate base
- auxiliary agent
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L67/00—Compositions of polyesters obtained by reactions forming a carboxylic ester link in the main chain; Compositions of derivatives of such polymers
- C08L67/02—Polyesters derived from dicarboxylic acids and dihydroxy compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J5/00—Manufacture of articles or shaped materials containing macromolecular substances
- C08J5/04—Reinforcing macromolecular compounds with loose or coherent fibrous material
- C08J5/0405—Reinforcing macromolecular compounds with loose or coherent fibrous material with inorganic fibres
- C08J5/043—Reinforcing macromolecular compounds with loose or coherent fibrous material with inorganic fibres with glass fibres
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2367/00—Characterised by the use of polyesters obtained by reactions forming a carboxylic ester link in the main chain; Derivatives of such polymers
- C08J2367/02—Polyesters derived from dicarboxylic acids and dihydroxy compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2427/00—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Derivatives of such polymers
- C08J2427/02—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Derivatives of such polymers not modified by chemical after-treatment
- C08J2427/12—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Derivatives of such polymers not modified by chemical after-treatment containing fluorine atoms
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2237—Oxides; Hydroxides of metals of titanium
- C08K2003/2241—Titanium dioxide
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/10—Transparent films; Clear coatings; Transparent materials
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
Abstract
High grade of transparency plate base-material the invention discloses a kind of automation equipment and preparation method thereof, is made of the raw material of following parts by weight：20 ~ 40 parts of 1,4 cyclohexanedimethanoester ester of polyethylene terephthalate, 10 ~ 20 parts of polytrifluorochloroethylene, 2 ~ 6 parts of polyvinyl butyral, 2 ~ 5 parts of coumarone indene resin, 2 ~ 4 parts of polyvinylpyrrolidone, 2 ~ 6 parts of transparent glass fibre, 0.5 ~ 1.5 part of dodecafluoroheptyl methacrylate, 4 ~ 10 parts of vinyl three (β methoxy ethoxies) silane, 2 ~ 4 parts of tributyl citrate, 1 ~ 2 part of Triallyl isocyanurate, 4 ~ 10 parts of inorganic modified auxiliary agent, 1 ~ 4 part of other auxiliary agents.The present invention uses polyethylene terephthalate 1, after 4 cyclohexanedimethanoester esters are compounded with other various raw materials, greatly strengthen the mechanical strength of automation equipment composite material, there is excellent transparent performance simultaneously, mechanical property and comprehensive performance are good, it is tested through practical application, the present invention is a kind of automation equipment base material of the excellent transparency.
Description
Technical field
The present invention relates to technical field of composite materials, and in particular to a kind of high grade of transparency plate base-material of automation equipment
And preparation method thereof.
Background technology
The continuous development of science and technology has driven the continuous progress of automatic technology, and so far, automation equipment is widely used in workers and peasants
Industry, military affairs, scientific research, transportation, business, medical treatment, service and household electrical appliances etc..The machine prepared using automatic technology
The process that device or device were operated or controlled automatically by regulated procedure or instruction in the case of unmanned intervene, automates skill
Art can not only free people from heavy manual labor, part mental labour and danger, severe working environment,
The organ dysfunction of people can be extended simultaneously, greatlys improve labor productivity, enhance the energy of the human cognitive world and reforming world
Power.
Automation equipment be applied to all trades and professions, species is various, for example automated machine equipment, automated office equipment,
Automate lifestyle device etc., the materials such as different shape, plate of specification that automation equipment is prepared by different processing technologys
Soft and hardware control assembly is packed or assembled, the base-material of existing processing assembling plate is black or other are opaque
Material, and that the preferable assembly of transparency is prepared is visual with good aesthetics and equipment operation for transparent base material
Property, there is certain market-oriented demand.
The content of the invention
In view of the shortcomings of the prior art, a kind of plate base-material with the high grade of transparency the present invention provides automation equipment
And preparation method thereof.
The present invention solve the technical solution that uses of above-mentioned technical problem for：A kind of high grade of transparency plate of automation equipment
Base-material is made of following raw material：Polyethylene terephthalate -1,4 cyclohexane dimethanol ester, triallyl isocyanide urea
Acid esters, polytrifluorochloroethylene, coumarone-indene resin, polyvinylpyrrolidone, polyvinyl butyral, transparent glass fibre,
Dodecafluoroheptyl methacrylate, vinyl three ('beta '-methoxy ethyoxyl) silane, tributyl citrate, inorganic modified auxiliary agent,
Other auxiliary agents；
The parts by weight of the raw material are：Polyethylene terephthalate -20 ~ 40 parts of 1,4 cyclohexane dimethanol ester gathers
10 ~ 20 parts of chlorotrifluoroethylene, 2 ~ 5 parts of coumarone-indene resin, 2 ~ 4 parts of polyvinylpyrrolidone, polyvinyl butyral 2 ~ 6
Part, 2 ~ 6 parts of transparent glass fibre, 0.5 ~ 1.5 part of dodecafluoroheptyl methacrylate, vinyl three ('beta '-methoxy ethyoxyl) silicon
4 ~ 10 parts of alkane, 2 ~ 4 parts of tributyl citrate, 1 ~ 2 part of Triallyl isocyanurate, 4 ~ 10 parts of inorganic modified auxiliary agent, other help
1 ~ 4 part of agent.
Further, the inorganic modified auxiliary agent is the 800 gentle phase titanic oxides of mesh transparent powder, mass parts ratio for 1 ~
3：1.
Further, other described auxiliary agents are antimony pentoxide, 2,5- ditert-butylhydro quinones and 2- hydroxyl -4- first
Oxygroup benzophenone it is compound, for further improving the comprehensive stability of composite material.
A kind of high grade of transparency plate base-material of automation equipment, its preparation method comprise the following steps：
（1）Raw material is on the waiting list according to the parts by weight；
（2）By the polyethylene terephthalate being on the waiting list -1,4 cyclohexane dimethanol ester, Triallyl isocyanurate,
Polytrifluorochloroethylene, polyvinyl butyral, coumarone-indene resin, polyvinylpyrrolidone, ten difluoro heptan of methacrylic acid
Ester, vinyl three ('beta '-methoxy ethyoxyl) silane, tributyl citrate, inorganic modified auxiliary agent and the mixing of other auxiliary agents add in extremely
Further melting mixing in double screw extruder；
（3）Transparent glass fibre is added in from side spout into above-mentioned extruder；
（4）Setting double screw extruder squeezes out under certain condition, is granulated and obtains composite material of the invention.
Preferably, the certain condition is：Each area's temperature of double screw extruder control 210 ~ 240 DEG C, rotating speed 350 ~
400RPM, rate of feeding are 40 ~ 50RPM.
Compared with prior art, what the present invention possessed has the beneficial effect that：
A kind of high grade of transparency plate base-material of automation equipment of the present invention uses polyethylene terephthalate -1,4- rings
Hexane diformazan alcohol ester is main material, is enhanced through transparent glass fibre and with after other various raw material compoundings, greatly strengthening automatic
To change the mechanical strength of equipment composite material, while there is excellent transparent performance, mechanical property and comprehensive performance are good,
It is tested through practical application, the present invention is a kind of automation equipment base material of the excellent transparency.
Specific embodiment
With reference to specific embodiment, the present invention is described further.
Embodiment 1：A kind of high grade of transparency plate base-material of automation equipment, is made of following raw material：Gather to benzene two
Formic acid glycol ester -1,4 cyclohexane dimethanol ester, Triallyl isocyanurate, coumarone-indene resin, polyvinylpyrrolidine
Alkanone, polytrifluorochloroethylene, polyvinyl butyral, transparent glass fibre, dodecafluoroheptyl methacrylate, vinyl three
('beta '-methoxy ethyoxyl) silane, tributyl citrate, inorganic modified auxiliary agent, other auxiliary agents；
The parts by weight of the raw material are：Polyethylene terephthalate -30 parts of 1,4 cyclohexane dimethanol ester, poly- three
15 parts of fluorine vinyl chloride, 3 parts of coumarone-indene resin, 3 parts of polyvinylpyrrolidone, 4 parts of polyvinyl butyral, transparent glass
4 parts of fiber, 1 part of dodecafluoroheptyl methacrylate, 7 parts of vinyl three ('beta '-methoxy ethyoxyl) silane, tributyl citrate 3
Part, 1.5 parts of Triallyl isocyanurate, 7 parts of inorganic modified auxiliary agent, 2 parts of other auxiliary agents.
Further, the inorganic modified auxiliary agent is the 800 gentle phase titanic oxides of mesh transparent powder, and mass parts ratio is 2：
1。
Further, other described auxiliary agents are antimony pentoxide, 2,5- ditert-butylhydro quinones and 2- hydroxyl -4- first
Oxygroup benzophenone it is compound, for further improving the comprehensive stability of composite material.
Embodiment 2：The high grade of transparency plate base-material of a kind of automation equipment, by the raw material group of following parts by weight
Into：Polyethylene terephthalate -20 parts of 1,4 cyclohexane dimethanol ester, 10 parts of polytrifluorochloroethylene, coumarone-indenes tree
2 parts of fat, 2 parts of polyvinylpyrrolidone, 2 parts of polyvinyl butyral, 2 parts of transparent glass fibre, ten difluoro of methacrylic acid
0.5 part of heptyl ester, 4 parts of vinyl three ('beta '-methoxy ethyoxyl) silane, 2 parts of tributyl citrate, Triallyl isocyanurate 1
Part, 4 parts of inorganic modified auxiliary agent, 1 part of other auxiliary agents.
Further, the inorganic modified auxiliary agent is the 800 gentle phase titanic oxides of mesh transparent powder, and mass parts ratio is 1：
1；Other described auxiliary agents are antimony pentoxide, 2,5- ditert-butylhydro quinones and ESCALOL 567
It is compound.
Embodiment 3：The high grade of transparency plate base-material of a kind of automation equipment, by the raw material group of following parts by weight
Into：Polyethylene terephthalate -40 parts of 1,4 cyclohexane dimethanol ester, 20 parts of polytrifluorochloroethylene, coumarone-indenes tree
5 parts of fat, 4 parts of polyvinylpyrrolidone, 6 parts of polyvinyl butyral, 6 parts of transparent glass fibre, ten difluoro of methacrylic acid
1.5 parts of heptyl ester, 10 parts of vinyl three ('beta '-methoxy ethyoxyl) silane, 4 parts of tributyl citrate, Triallyl isocyanurate
2 parts, 10 parts of inorganic modified auxiliary agent, 4 parts of other auxiliary agents.
Further, the inorganic modified auxiliary agent is the 800 gentle phase titanic oxides of mesh transparent powder, and mass parts ratio is 3：
1；Other described auxiliary agents are antimony pentoxide, 2,5- ditert-butylhydro quinones and ESCALOL 567
It is compound.
Embodiment 4：The high grade of transparency plate base-material of a kind of automation equipment, by the raw material group of following parts by weight
Into：Polyethylene terephthalate -40 parts of 1,4 cyclohexane dimethanol ester, 10 parts of polytrifluorochloroethylene, coumarone-indenes tree
5 parts of fat, 4 parts of polyvinylpyrrolidone, 6 parts of polyvinyl butyral, 2 parts of transparent glass fibre, ten difluoro of methacrylic acid
1.5 parts of heptyl ester, 4 parts of vinyl three ('beta '-methoxy ethyoxyl) silane, 4 parts of tributyl citrate, Triallyl isocyanurate 1
Part, 10 parts of inorganic modified auxiliary agent, 4 parts of other auxiliary agents.
Further, the inorganic modified auxiliary agent is the 800 gentle phase titanic oxides of mesh transparent powder, and mass parts ratio is 3：
2；Other described auxiliary agents are antimony pentoxide, 2,5- ditert-butylhydro quinones and ESCALOL 567
It is compound.
Embodiment 5：The high grade of transparency plate base-material of a kind of automation equipment, by the raw material group of following parts by weight
Into：Polyethylene terephthalate -25 parts of 1,4 cyclohexane dimethanol ester, 13 parts of polytrifluorochloroethylene, coumarone-indenes tree
2 ~ 5 parts of fat, 3 parts of polyvinylpyrrolidone, 5 parts of polyvinyl butyral, 5 parts of transparent glass fibre, methacrylic acid 12
0.8 part of fluorine heptyl ester, 5 parts of vinyl three ('beta '-methoxy ethyoxyl) silane, 3 parts of tributyl citrate, triallyl isocyanuric acid
1.2 parts of ester, 8 parts of inorganic modified auxiliary agent, 3 parts of other auxiliary agents.
Further, the inorganic modified auxiliary agent is the 800 gentle phase titanic oxides of mesh transparent powder, and mass parts ratio is 5：
3；Other described auxiliary agents are antimony pentoxide, 2,5- ditert-butylhydro quinones and ESCALOL 567
It is compound.
A kind of high grade of transparency plate base-material of automation equipment described in above-described embodiment 1 ~ 5, preparation side
Method comprises the following steps：
（1）Raw material is on the waiting list according to the parts by weight；
（2）After the polyethylene terephthalate being on the waiting list -1,4 cyclohexane dimethanol ester is crushed with triallyl isocyanide
Urea acid esters, polytrifluorochloroethylene, polyvinyl butyral, coumarone-indene resin, polyvinylpyrrolidone, methacrylic acid
Ten difluoro heptyl esters, vinyl three ('beta '-methoxy ethyoxyl) silane, tributyl citrate, inorganic modified auxiliary agent and other auxiliary agents mix
It closes and adds in the further melting mixing into double screw extruder；
（3）Transparent glass fibre is added in from side spout into above-mentioned extruder；
（4）Setting double screw extruder squeezes out under certain condition, is granulated and obtains composite material of the invention.
The certain condition is：Each area's temperature of double screw extruder controls 210 ~ 240 DEG C, 350 ~ 400RPM of rotating speed, feeds
Material speed is 40 ~ 50RPM；Specifically, each area's temperature control selections of double screw extruder are 210,215,220,225,230,
235th, 240 DEG C, rotating speed 350,360,370,380,390,400RPM, rate of feeding 40,41,42,43,44,45,46,47,48,
49、50RPM。
Normalized test, the light transmittance for the composite material that above-described embodiment 1-5 is obtained reach 82 ~ 85%, and tensile strength reaches
To 130 ~ 150MPa, 15 ~ 17KJ/m of impact strength2.As can be seen that the present invention for a kind of good mechanical performance have both it is good
The automation equipment base material of transparent performance.
It should be pointed out that the revealed content of above-described embodiment, is only the several of present pre-ferred embodiments, as long as this
Partial alteration, variation or the part modification to disclosed technology contents that field technology personnel use, and come from this
The technological essence of invention and creative thinking is not added with to be familiar with the people of this skill is easy to deduce acquisition, all do not depart from this hair
Bright patent right scope.
Claims (5)
1. a kind of high grade of transparency plate base-material of automation equipment, it is characterised in that：It is made of following raw material：Poly- terephthaldehyde
Sour glycol ester -1,4 cyclohexane dimethanol ester, Triallyl isocyanurate, coumarone-indene resin, polyvinylpyrrolidone
Ketone, polytrifluorochloroethylene, polyvinyl butyral, transparent glass fibre, dodecafluoroheptyl methacrylate, vinyl three (β-
Methoxy ethoxy) silane, tributyl citrate, inorganic modified auxiliary agent, other auxiliary agents；
The parts by weight of the raw material are：Polyethylene terephthalate -20 ~ 40 parts of 1,4 cyclohexane dimethanol ester gathers
10 ~ 20 parts of chlorotrifluoroethylene, 2 ~ 6 parts of polyvinyl butyral, 2 ~ 5 parts of coumarone-indene resin, polyvinylpyrrolidone 2 ~ 4
Part, 2 ~ 6 parts of transparent glass fibre, 0.5 ~ 1.5 part of dodecafluoroheptyl methacrylate, vinyl three ('beta '-methoxy ethyoxyl) silicon
4 ~ 10 parts of alkane, 2 ~ 4 parts of tributyl citrate, 1 ~ 2 part of Triallyl isocyanurate, 4 ~ 10 parts of inorganic modified auxiliary agent, other help
1 ~ 4 part of agent.
2. a kind of high grade of transparency plate base-material of automation equipment according to claim 1, it is characterised in that：Described
Inorganic modified auxiliary agent is the 800 gentle phase titanic oxides of mesh transparent powder, and mass parts ratio is 1 ~ 3：1.
3. a kind of high grade of transparency plate base-material of automation equipment according to claim 1, it is characterised in that：Described
Other auxiliary agents are the compound of antimony pentoxide, 2,5- ditert-butylhydro quinones and ESCALOL 567, are used for
Further improve the comprehensive stability of composite material.
4. the preparation method of the high grade of transparency plate base-material of a kind of automation equipment, which is characterized in that comprise the following steps：
（1）Raw material is on the waiting list according to the parts by weight；
（2）After the polyethylene terephthalate being on the waiting list -1,4 cyclohexane dimethanol ester is crushed with triallyl isocyanide
Urea acid esters, polytrifluorochloroethylene, polyvinyl butyral, coumarone-indene resin, polyvinylpyrrolidone, methacrylic acid
Ten difluoro heptyl esters, vinyl three ('beta '-methoxy ethyoxyl) silane, tributyl citrate, inorganic modified auxiliary agent and other auxiliary agents mix
It closes and adds in the further melting mixing into double screw extruder；
（3）Transparent glass fibre is added in from side spout into above-mentioned extruder；
（4）Setting double screw extruder squeezes out under certain condition, is granulated and obtains composite material of the invention.
5. a kind of preparation method of the high grade of transparency plate base-material of automation equipment according to claim 4, feature
It is：Step（4）The certain condition is：Each area's temperature of double screw extruder control 210 ~ 240 DEG C, rotating speed 350 ~
400RPM, rate of feeding are 40 ~ 50RPM.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711094989.7A CN108059801A (en) | 2017-11-09 | 2017-11-09 | A kind of high grade of transparency plate base-material of automation equipment and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711094989.7A CN108059801A (en) | 2017-11-09 | 2017-11-09 | A kind of high grade of transparency plate base-material of automation equipment and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108059801A true CN108059801A (en) | 2018-05-22 |
Family
ID=62135596
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711094989.7A Pending CN108059801A (en) | 2017-11-09 | 2017-11-09 | A kind of high grade of transparency plate base-material of automation equipment and preparation method thereof |
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Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106317803A (en) * | 2016-08-26 | 2017-01-11 | 张海棠 | Environment-friendly transparent cable sheathing material |
-
2017
- 2017-11-09 CN CN201711094989.7A patent/CN108059801A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106317803A (en) * | 2016-08-26 | 2017-01-11 | 张海棠 | Environment-friendly transparent cable sheathing material |
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Application publication date: 20180522 |