CN108048948A - A kind of preparation method of the fire-retardant synthetic wig fiber easily painted - Google Patents
A kind of preparation method of the fire-retardant synthetic wig fiber easily painted Download PDFInfo
- Publication number
- CN108048948A CN108048948A CN201711453948.2A CN201711453948A CN108048948A CN 108048948 A CN108048948 A CN 108048948A CN 201711453948 A CN201711453948 A CN 201711453948A CN 108048948 A CN108048948 A CN 108048948A
- Authority
- CN
- China
- Prior art keywords
- solution
- preparation
- fire
- parts
- processing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F8/00—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
- D01F8/02—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from cellulose, cellulose derivatives, or proteins
-
- A—HUMAN NECESSITIES
- A41—WEARING APPAREL
- A41G—ARTIFICIAL FLOWERS; WIGS; MASKS; FEATHERS
- A41G3/00—Wigs
- A41G3/0083—Filaments for making wigs
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/07—Addition of substances to the spinning solution or to the melt for making fire- or flame-proof filaments
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F8/00—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
- D01F8/18—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from other substances
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Manufacturing & Machinery (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention discloses a kind of preparation methods of the fire-retardant synthetic wig fiber easily painted, and include the following steps：First shrimp powder is put into lye and dissolves, separate, purifying, is then mixed again with sodium alginate soln, and adds improved silica ingredient and is allocated, curing molding, washing stretching, dipping, drying and processing are finally carried out successively to mixture.The present invention has carried out the preparation method of synthetic wig fiber special improvement processing, the synthesis for effectively improving fiber uses quality, fiber made from correspondence has good intensity, corrosion resistant, fire-retardant, stability, easy coloring characteristic, great popularizing value and the market competitiveness.
Description
Technical field
The invention belongs to chemical fibre material fields, and in particular to a kind of preparation of the fire-retardant synthetic wig fiber easily painted
Method.
Background technology
In recent years, wig was come into as a kind of new fashional consumption product in people's life.Wig is referred to as " when on head
Dress ", various types of wigs meet the various demand of people.The material of wig can be divided into artificial hair and biomass wig,
Wherein artificial hair is that material composition manually is processed into fiber hair, and biomass wig is cropped by the true hair on human body etc.
It forms, the quantity of the latter is few, cost is high, and with the continuous promotion in the market for wig demand, the production of artificial hair adds
Work scale constantly expands.But anti-flammability, heat resistance, stainability, stability of existing commercially available synthetic wig fiber etc. is not still
It is too preferable, it is also necessary to further improvement processing.
The content of the invention
The purpose of the present invention is being directed to the problem of existing, a kind of preparation of the fire-retardant synthetic wig fiber easily painted is provided
Method.
The present invention is achieved by the following technical solutions：
A kind of preparation method of the fire-retardant synthetic wig fiber easily painted, includes the following steps：
（1）Shrimp powder is put into 3 ~ 5h of stir process in lye, during which heating keeps the temperature of lye to be completed for 45 ~ 50 DEG C
After filter, it is spare to obtain solution A；
（2）Sodium alginate is put into water, is stirred continuously 35 ~ 40min of processing, during which heating keep the temperature of solution for 40 ~
45 DEG C, it is spare that solution B is obtained after finishing；
（3）By step（1）The solution A and step of gained（2）The solution B of gained is according to weight ratio 1:7 ~ 9 are mixed, Ran Houjia
Enter the improved silica of its gross mass 0.2 ~ 0.4%, be stirred continuously 1 ~ 1.5h of processing, the temperature of during which heating holding solution is
35 ~ 40 DEG C, it is spare that solution C is obtained after finishing；
（4）By step（3）The solution C of gained, which is put into, carries out spinning processing in spinning box, then by conventional curing molding,
Must come into being wig fiber after washing stretching, be taken out after finally carrying out conventional dipping, drying and processing to wig fiber of coming into being.
Further, step（1）Described in lye be sodium hydroxide solution that mass fraction is 3 ~ 5%, shrimp powder and alkali
The mass volume ratio of liquid mixing is 1g：20~25ml.
Further, step（2）Described in sodium alginate and water mixing mass ratio be 5 ~ 8:100.
Further, step（3）Described in the preparation method of improved silica include the following steps：
A. by hexadecyl amide propyl amine oxide, nonylphenol polyoxyethylene ether and ethanol solution according to mass ratio 1:0.4：8~9
Common mixing is put into reaction kettle, after being stirred continuously 20 ~ 25min of processing, then ammonium hydroxide is added dropwise into reaction kettle, is stirred continuously place
After managing 10 ~ 15min, then ethyl orthosilicate is added in into reaction kettle, be stirred continuously after 45 ~ 50min of processing mixture A is spare；
B. the modified solution of its gross mass 15 ~ 20% is added into the mixture A obtained by step a, then heating is kept in reaction kettle
Temperature for 64 ~ 68 DEG C, and the pressure in reaction kettle is increased into 0.45 ~ 0.50MPa, is carried out after being stirred continuously 25 ~ 30min of processing
The filter residue of gained is finally put into drying box after 50 ~ 60min of drying process and is taken out by filtering；The modified solution by
The material composition of following parts by weight：30 ~ 35 parts of carbon nanotubes, 10 ~ 15 parts of nanometer pomegranate mountain flours, 3 ~ 5 parts of furazolidones, 5 ~ 8 parts
Methyl methacrylate, 3 ~ 6 parts of dimethyl suflfates, 2 ~ 4 parts of cetyl benzenesulfonic acid sodiums, 320 ~ 340 parts of water.
Further, the volume fraction of ethyl alcohol is 50 ~ 55% in the ethanol solution described in step a.
Further, the dripping quantity of the ammonium hydroxide described in step a is the 14 ~ 18% of ethanol solution gross mass, the positive silicic acid
The additive amount of ethyl ester is 5.0 ~ 5.4 times of ethanol solution gross mass.
Further, it is 80 ~ 85 DEG C that the temperature in drying box is controlled during drying process described in step b.
Also there are the technical solution seen and shrimp is used for synthetic wig fiber, such as Application No. in the prior art：
201210457178.X discloses a kind of preparation method of synthetic wig fiber, takes full advantage of krill, and is made
Synthetic wig fiber there is good intensity, fire-retardant, easy coloring characteristic, but with continuous promotion of the people to product requirement,
Its wig fibre cannot meet the needs of contemporary people.In this regard, preparation method of the present invention to synthetic wig fiber
Improvement processing has been carried out, still using shrimp powder and sodium alginate as main material composition, and has been with the addition of a kind of special modification dioxy
SiClx ingredient, this improved silica are using ethyl orthosilicate as silicon source, and ethanol solution is solvent, and ammonium hydroxide is catalyst, modified
Solution is modifying agent, and hexadecyl amide propyl amine oxide and nonylphenol polyoxyethylene ether are activating agent and template, are made jointly
The silica filler with porous, more whisker structures, carbon nanotubes, nanometer pomegranate mountain flour in modified solution can enhance
The heatproof flame-retardant of silica, the hollow structure of carbon nanotubes can further promote whole colorability again, this two kinds into
Divide during silica generates, be effectively fixed therein, modified effect is good, and stability is high, changing after final process
Property silica surface characteristic it is good, compatible bond strength between the bulk composition of wig fiber is high, effectively improves whole
Use quality and value.
The present invention has the following advantages compared with prior art：
The present invention has carried out the preparation method of synthetic wig fiber special improvement processing, and effectively improving the synthesis of fiber makes
With quality, fiber made from correspondence has good intensity, corrosion resistant, fire-retardant, stability, easy coloring characteristic, great to promote the use of
Value and the market competitiveness.
Specific embodiment
Embodiment 1
A kind of preparation method of the fire-retardant synthetic wig fiber easily painted, includes the following steps：
（1）Shrimp powder is put into stir process 3h in lye, during which heating keeps the temperature of lye as 45 DEG C, after finishing mistake
Filter, it is spare to obtain solution A；
（2）Sodium alginate is put into water, is stirred continuously processing 35min, during which heating keeps the temperature of solution as 40 DEG C, complete
It is spare that solution B is obtained after；
（3）By step（1）The solution A and step of gained（2）The solution B of gained is according to weight ratio 1:7 are mixed, and are then added in
The improved silica of its gross mass 0.2% is stirred continuously processing 1h, and during which heating keeps the temperature of solution as 35 DEG C, after finishing
It is spare to obtain solution C；
（4）By step（3）The solution C of gained, which is put into, carries out spinning processing in spinning box, then by conventional curing molding,
Must come into being wig fiber after washing stretching, be taken out after finally carrying out conventional dipping, drying and processing to wig fiber of coming into being.
Further, step（1）Described in lye be sodium hydroxide solution that mass fraction is 3%, shrimp powder and lye
The mass volume ratio of mixing is 1g：20ml.
Further, step（2）Described in sodium alginate and water mixing mass ratio be 5:100.
Further, step（3）Described in the preparation method of improved silica include the following steps：
A. by hexadecyl amide propyl amine oxide, nonylphenol polyoxyethylene ether and ethanol solution according to mass ratio 1:0.4：8 is common
It is put into mixing in reaction kettle, after being stirred continuously processing 20min, then ammonium hydroxide is added dropwise into reaction kettle, is stirred continuously processing
After 10min, then ethyl orthosilicate is added in into reaction kettle, be stirred continuously processing 45min after mixture A it is spare；
B. the modified solution of its gross mass 15% is added into the mixture A obtained by step a, then heating is kept in reaction kettle
Temperature is 64 DEG C, and the pressure in reaction kettle is increased to 0.45MPa, is filtered after being stirred continuously processing 25min, finally by institute
The filter residue obtained is put into drying box after drying process 50min and is taken out；The modified solution by following parts by weight substance
Composition：30 parts of carbon nanotubes, 10 parts of nanometer pomegranate mountain flours, 3 parts of furazolidones, 5 parts of methyl methacrylates, 3 parts of dimethyl sulfates
Ester, 2 parts of cetyl benzenesulfonic acid sodiums, 320 parts of water.
Further, the volume fraction of ethyl alcohol is 50% in the ethanol solution described in step a.
Further, the dripping quantity of the ammonium hydroxide described in step a is the 14% of ethanol solution gross mass, the positive silicic acid second
The additive amount of ester is 5.0 times of ethanol solution gross mass.
Further, it is 80 DEG C that the temperature in drying box is controlled during drying process described in step b.
Embodiment 2
A kind of preparation method of the fire-retardant synthetic wig fiber easily painted, includes the following steps：
（1）Shrimp powder is put into stir process 4h in lye, during which heating keeps the temperature of lye as 48 DEG C, after finishing mistake
Filter, it is spare to obtain solution A；
（2）Sodium alginate is put into water, is stirred continuously processing 37min, during which heating keeps the temperature of solution as 43 DEG C, complete
It is spare that solution B is obtained after；
（3）By step（1）The solution A and step of gained（2）The solution B of gained is according to weight ratio 1:8 are mixed, and are then added in
The improved silica of its gross mass 0.3% is stirred continuously processing 1.2h, and during which heating keeps the temperature of solution to be completed for 37 DEG C
It is spare that solution C is obtained afterwards；
（4）By step（3）The solution C of gained, which is put into, carries out spinning processing in spinning box, then by conventional curing molding,
Must come into being wig fiber after washing stretching, be taken out after finally carrying out conventional dipping, drying and processing to wig fiber of coming into being.
Further, step（1）Described in lye be sodium hydroxide solution that mass fraction is 4%, shrimp powder and lye
The mass volume ratio of mixing is 1g：23ml.
Further, step（2）Described in sodium alginate and water mixing mass ratio be 7:100.
Further, step（3）Described in the preparation method of improved silica include the following steps：
A. by hexadecyl amide propyl amine oxide, nonylphenol polyoxyethylene ether and ethanol solution according to mass ratio 1:0.4：8.6
Common mixing is put into reaction kettle, after being stirred continuously processing 23min, then ammonium hydroxide is added dropwise into reaction kettle, is stirred continuously processing
After 12min, then ethyl orthosilicate is added in into reaction kettle, be stirred continuously processing 48min after mixture A it is spare；
B. the modified solution of its gross mass 17% is added into the mixture A obtained by step a, then heating is kept in reaction kettle
Temperature is 66 DEG C, and the pressure in reaction kettle is increased to 0.48MPa, is filtered after being stirred continuously processing 27min, finally by institute
The filter residue obtained is put into drying box after drying process 55min and is taken out；The modified solution by following parts by weight substance
Composition：33 parts of carbon nanotubes, 12 parts of nanometer pomegranate mountain flours, 4 parts of furazolidones, 7 parts of methyl methacrylates, 5 parts of dimethyl sulfates
Ester, 3 parts of cetyl benzenesulfonic acid sodiums, 330 parts of water.
Further, the volume fraction of ethyl alcohol is 52% in the ethanol solution described in step a.
Further, the dripping quantity of the ammonium hydroxide described in step a is the 16% of ethanol solution gross mass, the positive silicic acid second
The additive amount of ester is 5.2 times of ethanol solution gross mass.
Further, it is 83 DEG C that the temperature in drying box is controlled during drying process described in step b.
Embodiment 3
A kind of preparation method of the fire-retardant synthetic wig fiber easily painted, includes the following steps：
（1）Shrimp powder is put into stir process 5h in lye, during which heating keeps the temperature of lye as 50 DEG C, after finishing mistake
Filter, it is spare to obtain solution A；
（2）Sodium alginate is put into water, is stirred continuously processing 40min, during which heating keeps the temperature of solution as 45 DEG C, complete
It is spare that solution B is obtained after；
（3）By step（1）The solution A and step of gained（2）The solution B of gained is according to weight ratio 1:9 are mixed, and are then added in
The improved silica of its gross mass 0.4% is stirred continuously processing 1.5h, and during which heating keeps the temperature of solution to be completed for 40 DEG C
It is spare that solution C is obtained afterwards；
（4）By step（3）The solution C of gained, which is put into, carries out spinning processing in spinning box, then by conventional curing molding,
Must come into being wig fiber after washing stretching, be taken out after finally carrying out conventional dipping, drying and processing to wig fiber of coming into being.
Further, step（1）Described in lye be sodium hydroxide solution that mass fraction is 5%, shrimp powder and lye
The mass volume ratio of mixing is 1g：25ml.
Further, step（2）Described in sodium alginate and water mixing mass ratio be 8:100.
Further, step（3）Described in the preparation method of improved silica include the following steps：
A. by hexadecyl amide propyl amine oxide, nonylphenol polyoxyethylene ether and ethanol solution according to mass ratio 1:0.4：9 is common
It is put into mixing in reaction kettle, after being stirred continuously processing 25min, then ammonium hydroxide is added dropwise into reaction kettle, is stirred continuously processing
After 15min, then ethyl orthosilicate is added in into reaction kettle, be stirred continuously processing 50min after mixture A it is spare；
B. the modified solution of its gross mass 20% is added into the mixture A obtained by step a, then heating is kept in reaction kettle
Temperature is 68 DEG C, and the pressure in reaction kettle is increased to 0.50MPa, is filtered after being stirred continuously processing 30min, finally by institute
The filter residue obtained is put into drying box after drying process 60min and is taken out；The modified solution by following parts by weight substance
Composition：35 parts of carbon nanotubes, 15 parts of nanometer pomegranate mountain flours, 5 parts of furazolidones, 8 parts of methyl methacrylates, 6 parts of dimethyl sulfates
Ester, 4 parts of cetyl benzenesulfonic acid sodiums, 340 parts of water.
Further, the volume fraction of ethyl alcohol is 55% in the ethanol solution described in step a.
Further, the dripping quantity of the ammonium hydroxide described in step a is the 18% of ethanol solution gross mass, the positive silicic acid second
The additive amount of ester is 5.4 times of ethanol solution gross mass.
Further, it is 85 DEG C that the temperature in drying box is controlled during drying process described in step b.
The step of above-mentioned processing of the invention（4）Using with 201210457178.X disclosed in same procedure handled.
Comparative example 1
This comparative example 1 compared with Example 2, in step（3）The commercially available silica substituting modification two of the mass parts such as middle use
Silica ingredient, method and step all same in addition.
Comparative example 2
This comparative example 2 compared with Example 2, in step（3）Processing procedure in save adding for improved silica ingredient
Add, method and step all same in addition.
Control group
Application No.：201210457178.X disclose a kind of preparation method of synthetic wig fiber.
In order to compare effect of the present invention, system is corresponded to above-described embodiment 2, comparative example 1, comparative example 2, control group
The synthetic wig fiber obtained is tested for the property, and specific correction data is as shown in table 1 below：
Table 1
| Fracture strength（cN/dt） | Limit oxygen index | Coloring | |
| Embodiment 2 | 1.73 | 36 | **** |
| Comparative example 1 | 1.54 | 30 | *** |
| Comparative example 2 | 1.30 | 24 | ** |
| Control group | 1.45 | 28 | *** |
Note：Fracture strength described in upper table 1 is tested with reference to GB/T 1039-1992；The limit oxygen index reference
GB/T 5455-1997 are tested；The coloring is to put into fiber in reactive dyeing bath foam, by identical work
After skill dyeing processing, the staining conditions of fiber surface are observed, are graded, wherein " * * * * * " represents that dyeability is optimal, " * "
Represent that dyeability is worst.
The synthesis of synthetic wig fiber made from the method for the present invention is preferable using quality it can be seen from upper table 1, intensity,
Fire-retardant, coloring properties have obtained apparent improvement, great popularizing value.
Claims (7)
1. a kind of preparation method of the fire-retardant synthetic wig fiber easily painted, which is characterized in that include the following steps：
（1）Shrimp powder is put into 3 ~ 5h of stir process in lye, during which heating keeps the temperature of lye to be completed for 45 ~ 50 DEG C
After filter, it is spare to obtain solution A；
（2）Sodium alginate is put into water, is stirred continuously 35 ~ 40min of processing, during which heating keep the temperature of solution for 40 ~
45 DEG C, it is spare that solution B is obtained after finishing；
（3）By step（1）The solution A and step of gained（2）The solution B of gained is according to weight ratio 1:7 ~ 9 are mixed, Ran Houjia
Enter the improved silica of its gross mass 0.2 ~ 0.4%, be stirred continuously 1 ~ 1.5h of processing, the temperature of during which heating holding solution is
35 ~ 40 DEG C, it is spare that solution C is obtained after finishing；
（4）By step（3）The solution C of gained, which is put into, carries out spinning processing in spinning box, then by conventional curing molding,
Must come into being wig fiber after washing stretching, be taken out after finally carrying out conventional dipping, drying and processing to wig fiber of coming into being.
A kind of 2. preparation method of fire-retardant synthetic wig fiber easily painted according to claim 1, which is characterized in that step
Suddenly（1）Described in lye be sodium hydroxide solution that mass fraction is 3 ~ 5%, the mass volume ratio that shrimp powder is mixed with lye
For 1g：20~25ml.
A kind of 3. preparation method of fire-retardant synthetic wig fiber easily painted according to claim 1, which is characterized in that step
Suddenly（2）Described in sodium alginate and water mixing mass ratio be 5 ~ 8:100.
A kind of 4. preparation method of fire-retardant synthetic wig fiber easily painted according to claim 1, which is characterized in that step
Suddenly（3）Described in the preparation method of improved silica include the following steps：
A. by hexadecyl amide propyl amine oxide, nonylphenol polyoxyethylene ether and ethanol solution according to mass ratio 1:0.4：8~9
Common mixing is put into reaction kettle, after being stirred continuously 20 ~ 25min of processing, then ammonium hydroxide is added dropwise into reaction kettle, is stirred continuously place
After managing 10 ~ 15min, then ethyl orthosilicate is added in into reaction kettle, be stirred continuously after 45 ~ 50min of processing mixture A is spare；
B. the modified solution of its gross mass 15 ~ 20% is added into the mixture A obtained by step a, then heating is kept in reaction kettle
Temperature for 64 ~ 68 DEG C, and the pressure in reaction kettle is increased into 0.45 ~ 0.50MPa, is carried out after being stirred continuously 25 ~ 30min of processing
The filter residue of gained is finally put into drying box after 50 ~ 60min of drying process and is taken out by filtering；The modified solution by
The material composition of following parts by weight：30 ~ 35 parts of carbon nanotubes, 10 ~ 15 parts of nanometer pomegranate mountain flours, 3 ~ 5 parts of furazolidones, 5 ~ 8 parts
Methyl methacrylate, 3 ~ 6 parts of dimethyl suflfates, 2 ~ 4 parts of cetyl benzenesulfonic acid sodiums, 320 ~ 340 parts of water.
A kind of 5. preparation method of fire-retardant synthetic wig fiber easily painted according to claim 4, which is characterized in that step
The volume fraction of ethyl alcohol is 50 ~ 55% in ethanol solution described in rapid a.
A kind of 6. preparation method of fire-retardant synthetic wig fiber easily painted according to claim 4, which is characterized in that step
The dripping quantity of ammonium hydroxide described in rapid a is the 14 ~ 18% of ethanol solution gross mass, and the additive amount of the ethyl orthosilicate is ethyl alcohol
5.0 ~ 5.4 times of solution gross mass.
A kind of 7. preparation method of fire-retardant synthetic wig fiber easily painted according to claim 4, which is characterized in that step
Control the temperature in drying box during drying process described in rapid b as 80 ~ 85 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711453948.2A CN108048948A (en) | 2017-12-28 | 2017-12-28 | A kind of preparation method of the fire-retardant synthetic wig fiber easily painted |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711453948.2A CN108048948A (en) | 2017-12-28 | 2017-12-28 | A kind of preparation method of the fire-retardant synthetic wig fiber easily painted |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108048948A true CN108048948A (en) | 2018-05-18 |
Family
ID=62128465
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711453948.2A Pending CN108048948A (en) | 2017-12-28 | 2017-12-28 | A kind of preparation method of the fire-retardant synthetic wig fiber easily painted |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108048948A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111926412A (en) * | 2020-08-27 | 2020-11-13 | 深圳千维生态纺织有限公司 | Avocado-containing fiber capable of conditioning skin and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102786817A (en) * | 2012-07-26 | 2012-11-21 | 天津大学 | Silica-supported organic alkane phase change material, and preparation method and application thereof |
| CN102808237A (en) * | 2011-06-02 | 2012-12-05 | 陈福库 | Protein composite fiber for wig and manufacturing method thereof |
| CN102926025A (en) * | 2012-11-14 | 2013-02-13 | 大连工业大学 | Preparation method of synthetic wig fiber |
-
2017
- 2017-12-28 CN CN201711453948.2A patent/CN108048948A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102808237A (en) * | 2011-06-02 | 2012-12-05 | 陈福库 | Protein composite fiber for wig and manufacturing method thereof |
| CN102786817A (en) * | 2012-07-26 | 2012-11-21 | 天津大学 | Silica-supported organic alkane phase change material, and preparation method and application thereof |
| CN102926025A (en) * | 2012-11-14 | 2013-02-13 | 大连工业大学 | Preparation method of synthetic wig fiber |
Non-Patent Citations (2)
| Title |
|---|
| 汪多仁: "《绿色化工助剂》", 31 January 2006 * |
| 纺织工业标准化研究所: "《中国纺织标准汇编 基础标准与方法标准卷（一）》", 30 June 2000, 中国标准出版社 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111926412A (en) * | 2020-08-27 | 2020-11-13 | 深圳千维生态纺织有限公司 | Avocado-containing fiber capable of conditioning skin and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103015239B (en) | Polydimethyldiallylammonium chloride modified color fixing agent and preparation method thereof | |
| CN109439124A (en) | Woodcare paint aqueous dumb light self-crosslinking acrylic lotion and its synthetic method | |
| CN106831515B (en) | The method that tetra-benzyl thiram disulfide is continuously prepared using micro-reaction device | |
| CN105178138A (en) | Semi-gloss artificial grass and preparation method thereof | |
| CN103725252B (en) | A kind of Formaldehyde-free adhesive and its preparation method and application | |
| CN107841894A (en) | A kind of water-based levelling agent of superfine fiber synthetic leather dyeing | |
| CN107964060A (en) | A kind of gradient type polyacrylate stamp lotion and preparation method thereof | |
| CN103410019A (en) | Method for preparing composite printing paste | |
| CN108048948A (en) | A kind of preparation method of the fire-retardant synthetic wig fiber easily painted | |
| CN101457411B (en) | Method for manufacturing protein cellulose fiber | |
| CN108118403A (en) | A kind of manufacture craft of the resistance to cleaning wig fiber of high intensity | |
| CN106480545A (en) | A kind of preparation method of coloring alginate fiber | |
| CN106638039A (en) | Acid dye foam printing liquid and method for chinlon thin fabric | |
| CN105463881A (en) | Cloth dyeing auxiliary agent | |
| CN107090170A (en) | Aqueous polyurethane composition, waterborne polyurethane foaming body as well as preparation method and application thereof | |
| CN107325508A (en) | A kind of resin button formula and its production technology | |
| CN110128646A (en) | A kind of composite material and preparation method thereof based on vinylite treated basalt fiber | |
| CN107524002A (en) | A kind of hard finishing method of polyvinyl fabric | |
| CN106868898A (en) | A kind of color fixing agent for improving dyefastness and its preparation method and application | |
| CN110066367A (en) | Soap-free polymerization and the styrene-acrylic emulsion and preparation method thereof with core-shell structure | |
| CN112358566A (en) | Preparation method of two-in-one emulsion for multicolor paint | |
| CN111118923A (en) | Environment-friendly textile dye and method for preparing textile fabric by using same | |
| CN110685164A (en) | Manufacturing method of flower-fragrance home textile fabric | |
| CN104448516A (en) | Bath ball for children, women and cosmetology and production process thereof | |
| CN108264049A (en) | A kind of modification process of silicon carbide micro-powder |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180518 |
|
| RJ01 | Rejection of invention patent application after publication |