CN108046702A - A kind of production technology of high-intensity building materials and its application - Google Patents
A kind of production technology of high-intensity building materials and its application Download PDFInfo
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- CN108046702A CN108046702A CN201711390220.XA CN201711390220A CN108046702A CN 108046702 A CN108046702 A CN 108046702A CN 201711390220 A CN201711390220 A CN 201711390220A CN 108046702 A CN108046702 A CN 108046702A
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- building materials
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Classifications
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
- C04B28/02—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing hydraulic cements other than calcium sulfates
- C04B28/04—Portland cements
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2201/00—Mortars, concrete or artificial stone characterised by specific physical values
- C04B2201/50—Mortars, concrete or artificial stone characterised by specific physical values for the mechanical strength
Abstract
Production technology and its application the invention discloses a kind of high-intensity building materials, this method is used portland cement, hydroxyapatite, hydroxypropyl methyl cellulose is added in pulverizer and crushes, material must be pulverized and mixed, the distilled water for then adding in its 10 times of quality is ultrasonically treated, xanthans is added in into obtained ultrasonic mixing material, tri-methyl-amyl triethoxysilane, vinyl trimethoxy silicon, it is agitated to obtain intermediate blend, heat obtained intermediate blend, add in the linear Lauxite of thermosetting property, it is agitated again to obtain final mixture, finally final mixture material is injected in box mould, aging is kept the temperature under the conditions of 85 95 DEG C for 24 hours, room temperature is cooled to up to product.The construction material being prepared, simple for process, at low cost and material self-strength is high, has a good application prospect in architectural engineering.
Description
Technical field
The present invention relates to this technical fields of construction material, are related specifically to a kind of production technology of high-intensity building materials
And its application.
Background technology
New Building Materials mainly include novel wall material, NEW PAINT SYSTEMS FOR BUILDINGS, novel building plastics, novel building dress
Exterior material, new waterproof and sealing material totally five part.Novel wall construction material refers to new material resource, energy consumption
It is low, a large amount of to utilize local supplies and waste resource;To environment, to personal friendly harmless and be conducive to ecological environmental protection, maintain
The balance of ecological environment;Meanwhile it can recycle.New Building Materials have the characteristics that high-strength light at present:Lightweight master
Refer to that material is porous, bulk density is small.It is high-strength be primarily referred to as material intensity it is higher.
However, often complex production process, raw material are not easy to obtain the high-intensity building materials used at present in building field,
It is of high cost, and product durability is bad, this just needs to develop new composite material to substitute existing construction material.
The content of the invention
In order to solve the above technical problems, the present invention provides production technology and its application of a kind of high-intensity building materials, it should
Method must be pulverized and mixed using portland cement, hydroxyapatite, hydroxypropyl methyl cellulose to be added in pulverizer and crush
Material, the distilled water for then adding in its 10 times of quality are ultrasonically treated, and xanthans, front three are added in into obtained ultrasonic mixing material
Base amyl triethoxysilane, vinyl trimethoxy silicon, agitated to obtain intermediate blend, the intermediate mixing heated
Object adds in the linear Lauxite of thermosetting property, then it is agitated obtain final mixture, final mixture material is finally injected into box mould
In tool, keep the temperature aging for 24 hours under the conditions of 85-95 DEG C, be cooled to room temperature up to product.The construction material being prepared, technique
Simply, at low cost and material self-strength is high, has a good application prospect in architectural engineering.
The purpose of the present invention can be achieved through the following technical solutions:
A kind of production technology of high-intensity building materials, comprises the following steps:
(1) by 25-35 parts of 55-65 parts of portland cement, 35-45 parts of hydroxyapatite, hydroxypropyl methyl cellulose additions
It is crushed into pulverizer, material must be pulverized and mixed;
(2) distilled water of its 10 times of quality is added in being pulverized and mixed in material of obtaining, is then ultrasonically treated, at ultrasound
It is 70-80 DEG C to manage temperature, obtains ultrasonic mixing object;
(3) 16-20 parts of xanthans, tri-methyl-amyl triethoxysilane 8-12 are added in into obtained ultrasonic mixing material
Part, 4-6 parts of vinyltrimethoxysilane adjust the rotating speed of mixer as 300-400r/min, and agitated 25min obtains centre
Mixture;
(4) obtained intermediate blend is heated, is warming up to 95 DEG C, adds in linear Lauxite 5-8 parts of thermosetting property, then with
1200r/min stirs 25min, obtains final mixture, then final mixture material is injected in box mould, in 85-95 DEG C of item
Aging is kept the temperature under part for 24 hours, is cooled to room temperature up to product.
Further, the crushing mesh number of pulverizer is preferably 200 mesh in the step (1), and revolution is preferably 15000r/
min。
Further, ultrasonic power is preferably 600W in the step (2), and ultrasonic time is preferably 60-80min.
Further, the rotating speed of the mixer in the step (3) is preferably 350r/min.
Further, the application the invention also discloses the high-intensity building materials in architectural engineering.
Compared with prior art, the present invention its advantage is:
(1) production technology of high-intensity building materials of the invention is used portland cement, hydroxyapatite, hydroxypropyl
Methylcellulose is added in pulverizer and crushes, and must be pulverized and mixed material, and the distilled water for then adding in its 10 times of quality carries out ultrasound
Processing adds in xanthans, tri-methyl-amyl triethoxysilane, vinyl trimethoxy silicon into obtained ultrasonic mixing material,
Intermediate blend that is agitated to obtain intermediate blend, heating adds in the linear Lauxite of thermosetting property, then agitated obtains
Final mixture finally injects final mixture material in box mould, keeps the temperature aging for 24 hours under the conditions of 85-95 DEG C, is cooled to
Room temperature is up to product.The construction material being prepared, simple for process, at low cost and material self-strength is high, in architectural engineering
In have a good application prospect.
(2) present invention employs xanthans, tri-methyl-amyl triethoxysilane, vinyl trimethoxy silicon these types are former
Material is mixed with construction material with ultrasonic mixing material, effective modification has been carried out to construction material, although in these modifying process
Material therefor be not first Application in construction material, but according to a certain ratio amount combination after, be aided with corresponding processing mode, give
The construction material being finally prepared brings increasing substantially in performance, this is never to report in previous research
It crosses, plays the role of for the technique effect for realizing the present invention conclusive.
Specific embodiment
The technical solution of invention is described in detail with reference to specific embodiment.
Embodiment 1
(1) 55 parts of portland cement, 35 parts of hydroxyapatite, 25 parts of hydroxypropyl methyl cellulose are added in pulverizer
It crushes, pulverizer revolution is 15000r/min, and crushing mesh number is 200 mesh, must be pulverized and mixed material;
(2) distilled water of its 10 times of quality is added in being pulverized and mixed in material of obtaining, is then ultrasonically treated, at ultrasound
Reason temperature obtains ultrasonic mixing object for 70 DEG C, ultrasonic power 600W, ultrasonic time 60min;
(3) 16 parts of xanthans, 8 parts of tri-methyl-amyl triethoxysilane, ethylene are added in into obtained ultrasonic mixing material
4 parts of base trimethoxy silane adjusts the rotating speed of mixer as 350r/min, and agitated 25min obtains intermediate blend;
(4) obtained intermediate blend is heated, is warming up to 95 DEG C, adds in linear 5 parts of the Lauxite of thermosetting property, then with
1200r/min stirs 25min, obtains final mixture, then final mixture material is injected in box mould, under the conditions of 85 DEG C
It keeps the temperature aging for 24 hours, is cooled to room temperature up to product.
The performance test results of high-intensity building materials obtained are as shown in table 1.
Embodiment 2
(1) 60 parts of portland cement, 40 parts of hydroxyapatite, 30 parts of hydroxypropyl methyl cellulose are added in pulverizer
It crushes, pulverizer revolution is 15000r/min, and crushing mesh number is 200 mesh, must be pulverized and mixed material;
(2) distilled water of its 10 times of quality is added in being pulverized and mixed in material of obtaining, is then ultrasonically treated, at ultrasound
Reason temperature obtains ultrasonic mixing object for 75 DEG C, ultrasonic power 600W, ultrasonic time 70min;
(3) 18 parts of xanthans, 10 parts of tri-methyl-amyl triethoxysilane, ethylene are added in into obtained ultrasonic mixing material
5 parts of base trimethoxy silane adjusts the rotating speed of mixer as 350r/min, and agitated 25min obtains intermediate blend;
(4) obtained intermediate blend is heated, is warming up to 95 DEG C, adds in linear 7 parts of the Lauxite of thermosetting property, then with
1200r/min stirs 25min, obtains final mixture, then final mixture material is injected in box mould, under the conditions of 90 DEG C
It keeps the temperature aging for 24 hours, is cooled to room temperature up to product.
The performance test results of high-intensity building materials obtained are as shown in table 1.
Embodiment 3
(1) 65 parts of portland cement, 45 parts of hydroxyapatite, 35 parts of hydroxypropyl methyl cellulose are added in pulverizer
It crushes, pulverizer revolution is 15000r/min, and crushing mesh number is 200 mesh, must be pulverized and mixed material;
(2) distilled water of its 10 times of quality is added in being pulverized and mixed in material of obtaining, is then ultrasonically treated, at ultrasound
Reason temperature obtains ultrasonic mixing object for 80 DEG C, ultrasonic power 600W, ultrasonic time 80min;
(3) 20 parts of xanthans, 12 parts of tri-methyl-amyl triethoxysilane, ethylene are added in into obtained ultrasonic mixing material
6 parts of base trimethoxy silane adjusts the rotating speed of mixer as 350r/min, and agitated 25min obtains intermediate blend;
(4) obtained intermediate blend is heated, is warming up to 95 DEG C, adds in linear 8 parts of the Lauxite of thermosetting property, then with
1200r/min stirs 25min, obtains final mixture, then final mixture material is injected in box mould, under the conditions of 95 DEG C
It keeps the temperature aging for 24 hours, is cooled to room temperature up to product.
The performance test results of high-intensity building materials obtained are as shown in table 1.
Comparative example 1
(1) 60 parts of portland cement, 40 parts of hydroxyapatite, 30 parts of hydroxypropyl methyl cellulose are added in pulverizer
It crushes, pulverizer revolution is 15000r/min, and crushing mesh number is 200 mesh, must be pulverized and mixed material;
(2) distilled water of its 10 times of quality is added in being pulverized and mixed in material of obtaining, is then ultrasonically treated, at ultrasound
Reason temperature obtains ultrasonic mixing object for 75 DEG C, ultrasonic power 600W, ultrasonic time 70min;
(3) ultrasonic mixing object is heated, is warming up to 95 DEG C, adds in linear 7 parts of the Lauxite of thermosetting property, then with 1200r/min
25min is stirred, obtains final mixture, then final mixture material is injected in box mould, aging is kept the temperature under the conditions of 90 DEG C
For 24 hours, room temperature is cooled to up to product.
The performance test results of construction material obtained are as shown in table 1.
Comparative example 2
(1) 60 parts of portland cement, 40 parts of hydroxyapatite, 30 parts of hydroxypropyl methyl cellulose are added in pulverizer
It crushes, pulverizer revolution is 15000r/min, and crushing mesh number is 200 mesh, must be pulverized and mixed material;
(2) distilled water of its 10 times of quality is added in being pulverized and mixed in material of obtaining, is then ultrasonically treated, at ultrasound
Reason temperature obtains ultrasonic mixing object for 75 DEG C, ultrasonic power 600W, ultrasonic time 70min;
(3) 18 parts of xanthans, 10 parts of tri-methyl-amyl triethoxysilane, adjustment are added in into obtained ultrasonic mixing material
The rotating speed of mixer is 350r/min, and agitated 25min obtains intermediate blend;
(4) obtained intermediate blend is heated, is warming up to 95 DEG C, adds in linear 7 parts of the Lauxite of thermosetting property, then with
1200r/min stirs 25min, obtains final mixture, then final mixture material is injected in box mould, under the conditions of 90 DEG C
It keeps the temperature aging for 24 hours, is cooled to room temperature up to product.
The performance test results of construction material obtained are as shown in table 1.
Comparative example 3
(1) 60 parts of portland cement, 40 parts of hydroxyapatite, 30 parts of hydroxypropyl methyl cellulose are added in pulverizer
It crushes, pulverizer revolution is 15000r/min, and crushing mesh number is 200 mesh, must be pulverized and mixed material;
(2) distilled water of its 10 times of quality is added in being pulverized and mixed in material of obtaining, is then ultrasonically treated, at ultrasound
Reason temperature obtains ultrasonic mixing object for 75 DEG C, ultrasonic power 600W, ultrasonic time 70min;
(3) 18 parts of xanthans, 5 parts of vinyltrimethoxysilane, adjustment stirring are added in into obtained ultrasonic mixing material
The rotating speed of machine is 350r/min, and agitated 25min obtains intermediate blend;
(4) obtained intermediate blend is heated, is warming up to 95 DEG C, adds in linear 7 parts of the Lauxite of thermosetting property, then with
1200r/min stirs 25min, obtains final mixture, then final mixture material is injected in box mould, under the conditions of 90 DEG C
It keeps the temperature aging for 24 hours, is cooled to room temperature up to product.
The performance test results of construction material obtained are as shown in table 1.
Comparative example 4
(1) 60 parts of portland cement, 40 parts of hydroxyapatite, 30 parts of hydroxypropyl methyl cellulose are added in pulverizer
It crushes, pulverizer revolution is 15000r/min, and crushing mesh number is 200 mesh, must be pulverized and mixed material;
(2) distilled water of its 10 times of quality is added in being pulverized and mixed in material of obtaining, is then ultrasonically treated, at ultrasound
Reason temperature obtains ultrasonic mixing object for 75 DEG C, ultrasonic power 600W, ultrasonic time 70min;
(3) 10 parts of tri-methyl-amyl triethoxysilane, vinyl trimethoxy are added in into obtained ultrasonic mixing material
5 parts of silane adjusts the rotating speed of mixer as 350r/min, and agitated 25min obtains intermediate blend;
(4) obtained intermediate blend is heated, is warming up to 95 DEG C, adds in linear 7 parts of the Lauxite of thermosetting property, then with
1200r/min stirs 25min, obtains final mixture, then final mixture material is injected in box mould, under the conditions of 90 DEG C
It keeps the temperature aging for 24 hours, is cooled to room temperature up to product.
The performance test results of construction material obtained are as shown in table 1.
The construction material obtained of embodiment 1-3 and comparative example 1-4 are subjected to compression strength, bending strength, stretching respectively
This several performance tests of intensity.
Table 1
Compression strength (MPa) | Bending strength (MPa) | Tensile strength (MPa) | |
Embodiment 1 | 31.8 | 27.0 | 56.3 |
Embodiment 2 | 32.5 | 28.1 | 57.5 |
Embodiment 3 | 32.4 | 27.8 | 57.2 |
Comparative example 1 | 28.6 | 22.8 | 52.3 |
Comparative example 2 | 29.0 | 23.9 | 53.6 |
Comparative example 3 | 29.3 | 23.5 | 53.4 |
Comparative example 4 | 28.9 | 23.1 | 52.8 |
The production technology of the construction material of the present invention is used portland cement, hydroxyapatite, hydroxypropyl methyl fiber
Element is added in pulverizer and crushes, and must be pulverized and mixed material, and the distilled water for then adding in its 10 times of quality is ultrasonically treated, Xiang get
To ultrasonic mixing material in add in xanthans, tri-methyl-amyl triethoxysilane, vinyl trimethoxy silicon, it is agitated to obtain
Intermediate blend, the intermediate blend heated add in the linear Lauxite of thermosetting property, then agitated are finally mixed
Material finally injects final mixture material in box mould, keeps the temperature aging for 24 hours under the conditions of 85-95 DEG C, is cooled to room temperature to obtain the final product
Product.The construction material being prepared, simple for process, at low cost and material self-strength is high, has in architectural engineering good
Good application prospect.Also, present invention employs xanthans, tri-methyl-amyl triethoxysilane, vinyl trimethoxy silicon
These types of raw material is mixed with construction material with ultrasonic mixing material, effective modification has been carried out to construction material, although these change
Property used in the process of material be not first Application in construction material, but according to a certain ratio amount combination after, be aided with corresponding place
Reason mode brings increasing substantially in performance to the construction material being finally prepared, this is in previous research
It is never to report, plays the role of for the technique effect for realizing the present invention conclusive.
The foregoing is merely the embodiment of the present invention, are not intended to limit the scope of the invention, every to utilize this hair
The equivalent structure or equivalent flow shift that bright description is made directly or indirectly is used in other relevant technology necks
Domain is included within the scope of the present invention.
Claims (5)
1. a kind of production technology of high-intensity building materials, which is characterized in that comprise the following steps:
(1) 55-65 parts of portland cement, 35-45 parts of hydroxyapatite, 25-35 parts of hydroxypropyl methyl cellulose are added to powder
It is crushed in broken machine, material must be pulverized and mixed;
(2) distilled water of its 10 times of quality is added in being pulverized and mixed in material of obtaining, is then ultrasonically treated, is ultrasonically treated temperature
It spends for 70-80 DEG C, obtains ultrasonic mixing object;
(3) 16-20 parts of xanthans, 8-12 parts of tri-methyl-amyl triethoxysilane, second are added in into obtained ultrasonic mixing material
4-6 parts of alkenyl trimethoxy silane adjusts the rotating speed of mixer as 300-400r/min, and agitated 25min obtains intermediate mixing
Object;
(4) obtained intermediate blend is heated, is warming up to 95 DEG C, adds in linear Lauxite 5-8 parts of thermosetting property, then with 1200r/
Min stirs 25min, obtains final mixture, then final mixture material is injected in box mould, is protected under the conditions of 85-95 DEG C
Warm aging for 24 hours, is cooled to room temperature up to product.
2. the production technology of high-intensity building materials according to claim 1, which is characterized in that powder in the step (1)
The crushing mesh number of broken machine is preferably 200 mesh, and revolution is preferably 15000r/min.
3. the production technology of high-intensity building materials according to claim 1, which is characterized in that surpass in the step (2)
Acoustical power is preferably 600W, and ultrasonic time is preferably 60-80min.
4. the production technology of high-intensity building materials according to claim 1, which is characterized in that in the step (3)
The rotating speed of mixer is preferably 350r/min.
5. according to application of the claim 1-4 any one of them high-intensity building materials in architectural engineering.
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Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1055531A (en) * | 1991-04-06 | 1991-10-23 | 武汉工业大学 | High strength composite gelatinizing material |
CN102936113A (en) * | 2011-08-15 | 2013-02-20 | 青岛理工大学 | Hybrid nanocomposite material used for buildings and preparation method thereof |
CN106009610A (en) * | 2016-06-02 | 2016-10-12 | 陈昌 | High-strength environmental-protection material and preparation method thereof |
CN106116425A (en) * | 2016-06-21 | 2016-11-16 | 安徽天锦云漆业有限公司 | A kind of crack-resistant heat-insulation wall construction material and preparation method thereof |
CN106904932A (en) * | 2017-03-01 | 2017-06-30 | 苏州顶裕节能设备有限公司 | A kind of composite with high compressive strength and preparation method thereof |
-
2017
- 2017-12-21 CN CN201711390220.XA patent/CN108046702A/en not_active Withdrawn
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1055531A (en) * | 1991-04-06 | 1991-10-23 | 武汉工业大学 | High strength composite gelatinizing material |
CN102936113A (en) * | 2011-08-15 | 2013-02-20 | 青岛理工大学 | Hybrid nanocomposite material used for buildings and preparation method thereof |
CN106009610A (en) * | 2016-06-02 | 2016-10-12 | 陈昌 | High-strength environmental-protection material and preparation method thereof |
CN106116425A (en) * | 2016-06-21 | 2016-11-16 | 安徽天锦云漆业有限公司 | A kind of crack-resistant heat-insulation wall construction material and preparation method thereof |
CN106904932A (en) * | 2017-03-01 | 2017-06-30 | 苏州顶裕节能设备有限公司 | A kind of composite with high compressive strength and preparation method thereof |
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Application publication date: 20180518 |