CN108041672A - A kind of preparation method of non-fiber matrix Novel reconstructed tobacco leaf product - Google Patents
A kind of preparation method of non-fiber matrix Novel reconstructed tobacco leaf product Download PDFInfo
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- CN108041672A CN108041672A CN201711324580.XA CN201711324580A CN108041672A CN 108041672 A CN108041672 A CN 108041672A CN 201711324580 A CN201711324580 A CN 201711324580A CN 108041672 A CN108041672 A CN 108041672A
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- Prior art keywords
- preparation
- product
- fiber matrix
- prepared
- tobacco leaf
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 241000208125 Nicotiana Species 0.000 title claims abstract description 46
- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 46
- 239000000835 fiber Substances 0.000 title claims abstract description 15
- 239000011159 matrix material Substances 0.000 title claims abstract description 13
- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- 239000000463 material Substances 0.000 claims abstract description 33
- 235000019504 cigarettes Nutrition 0.000 claims abstract description 12
- 230000001953 sensory effect Effects 0.000 claims abstract description 10
- 238000010345 tape casting Methods 0.000 claims abstract description 9
- 239000000843 powder Substances 0.000 claims abstract description 8
- 238000001303 quality assessment method Methods 0.000 claims abstract description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 8
- 238000002485 combustion reaction Methods 0.000 claims abstract description 6
- 239000012764 mineral filler Substances 0.000 claims abstract description 5
- MDYZKJNTKZIUSK-UHFFFAOYSA-N tyloxapol Chemical compound O=C.C1CO1.CC(C)(C)CC(C)(C)C1=CC=C(O)C=C1 MDYZKJNTKZIUSK-UHFFFAOYSA-N 0.000 claims abstract description 5
- 239000000853 adhesive Substances 0.000 claims abstract description 4
- 230000001070 adhesive effect Effects 0.000 claims abstract description 4
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 12
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims description 10
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical group OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 10
- 238000011002 quantification Methods 0.000 claims description 7
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 6
- 229910000019 calcium carbonate Inorganic materials 0.000 claims description 5
- 235000011187 glycerol Nutrition 0.000 claims description 5
- 239000001508 potassium citrate Substances 0.000 claims description 5
- 229960002635 potassium citrate Drugs 0.000 claims description 5
- QEEAPRPFLLJWCF-UHFFFAOYSA-K potassium citrate (anhydrous) Chemical compound [K+].[K+].[K+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O QEEAPRPFLLJWCF-UHFFFAOYSA-K 0.000 claims description 5
- 235000011082 potassium citrates Nutrition 0.000 claims description 5
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims description 4
- 229920001661 Chitosan Polymers 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 4
- 235000010413 sodium alginate Nutrition 0.000 claims description 4
- 239000000661 sodium alginate Substances 0.000 claims description 4
- 229940005550 sodium alginate Drugs 0.000 claims description 4
- 229910000278 bentonite Inorganic materials 0.000 claims description 3
- 239000000440 bentonite Substances 0.000 claims description 3
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 claims description 3
- SVICABYXKQIXBM-UHFFFAOYSA-L potassium malate Chemical compound [K+].[K+].[O-]C(=O)C(O)CC([O-])=O SVICABYXKQIXBM-UHFFFAOYSA-L 0.000 claims description 3
- 239000001415 potassium malate Substances 0.000 claims description 3
- 235000011033 potassium malate Nutrition 0.000 claims description 3
- 239000004408 titanium dioxide Substances 0.000 claims description 3
- 229920002134 Carboxymethyl cellulose Polymers 0.000 claims description 2
- FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 claims description 2
- 229920002907 Guar gum Polymers 0.000 claims description 2
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims description 2
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 claims description 2
- 239000002253 acid Substances 0.000 claims description 2
- 229920006184 cellulose methylcellulose Polymers 0.000 claims description 2
- 239000003795 chemical substances by application Substances 0.000 claims description 2
- 229940045110 chitosan Drugs 0.000 claims description 2
- 235000010417 guar gum Nutrition 0.000 claims description 2
- 239000000665 guar gum Substances 0.000 claims description 2
- 229960002154 guar gum Drugs 0.000 claims description 2
- 229960003975 potassium Drugs 0.000 claims description 2
- 239000011591 potassium Substances 0.000 claims description 2
- 229910052700 potassium Inorganic materials 0.000 claims description 2
- 239000011975 tartaric acid Substances 0.000 claims description 2
- 235000002906 tartaric acid Nutrition 0.000 claims description 2
- 239000003607 modifier Substances 0.000 claims 2
- 239000000945 filler Substances 0.000 claims 1
- 239000003595 mist Substances 0.000 claims 1
- 239000000047 product Substances 0.000 abstract description 20
- 239000002994 raw material Substances 0.000 abstract description 7
- 239000013589 supplement Substances 0.000 abstract description 4
- 238000005303 weighing Methods 0.000 abstract 1
- 238000000034 method Methods 0.000 description 9
- 239000000523 sample Substances 0.000 description 6
- 229920001131 Pulp (paper) Polymers 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 235000019505 tobacco product Nutrition 0.000 description 2
- 230000002411 adverse Effects 0.000 description 1
- 239000013068 control sample Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 239000000686 essence Substances 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000013355 food flavoring agent Nutrition 0.000 description 1
- 238000005194 fractionation Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- AVTYONGGKAJVTE-OLXYHTOASA-L potassium L-tartrate Chemical compound [K+].[K+].[O-]C(=O)[C@H](O)[C@@H](O)C([O-])=O AVTYONGGKAJVTE-OLXYHTOASA-L 0.000 description 1
- 239000001472 potassium tartrate Substances 0.000 description 1
- 229940111695 potassium tartrate Drugs 0.000 description 1
- 235000011005 potassium tartrates Nutrition 0.000 description 1
- 238000013441 quality evaluation Methods 0.000 description 1
- 238000007613 slurry method Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/14—Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/12—Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco
- A24B15/14—Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco made of tobacco and a binding agent not derived from tobacco
Abstract
A kind of preparation method of non-fiber matrix Novel reconstructed tobacco leaf product, it is spare including 1) weighing the mineral filler, 5 20% tobacco powder, 5 12% Alevaire, 1 3% combustion rate regulator, 5 20% tobacco extract that weight percent is 60 80%;2) material in step 1) is sufficiently mixed in homogeneous tank with water;3) 2 7% according to material total weight in step 1) weigh adhesive, prepare the solution as 2% concentration;4) prepared solution in step 3) is added in the material mixed in step 2);5) prepared material in step 4) is shaped using the tape casting, dry, chopping;6) after product prepared by step 5) being made cigarette sample, tar and CO burst sizes is detected, and carries out sensory quality assessment.Product of the present invention has the characteristics that low tar, low CO burst sizes, without papery breath, can be as effective supplement of existing papermaking reconstituted tobacco, while can expand raw material Application Range.
Description
Technical field
The present invention relates to reconstituted tobacco technical fields, are specifically a kind of preparation of non-fiber matrix Novel reconstructed tobacco leaf product
Method.
Background technology
At present, important formula composition of the papermaking-method reconstituted tobaccos as cigarette, has effectively played the effect of reducing tar and reducing harm.
In order to meet molding needs of manufacturing paper with pulp, papermaking-method reconstituted tobaccos add in the fibre compositions such as wood pulp in process of production.Since it is special
Different fibre fractionation, on the one hand, the CO burst sizes of papermaking-method reconstituted tobaccos are higher, the addition of the fibre compositions such as another aspect wood pulp
Distinctive papery breath can be generated during burning, reconstituted tobacco product sensory quality can be adversely affected.Existing
The burst size of papermaking-method reconstituted tobaccos CO how is reduced on the basis of having and papery breath also becomes an industry general character problem.
The content of the invention
In view of the deficiencies of the prior art, the present invention provides a kind of preparation side of non-fiber matrix Novel reconstructed tobacco leaf product
Method, the product have the characteristics that low tar, low CO burst sizes, without papery breath, being capable of having as existing papermaking reconstituted tobacco
Effect supplement, while raw material Application Range can be expanded, alleviate the pressure that there is lack of raw materials such as tobacco chippings, for entire tobacco business
With highly important innovation and realistic meaning.
Technical solution is used by the present invention solves above-mentioned technical problem:A kind of non-fiber matrix Novel reconstructed cigarette is provided
The preparation method of leaf product, includes the following steps:
1) weight percent is weighed as the mineral filler of 60-80%, the tobacco powder of 5-20%, Alevaire, the 1-3% of 5-12%
Combustion rate regulator, the tobacco extract of 5-20%, it is spare;
2) material in step 1) is sufficiently mixed in homogeneous tank with water, speed of agitator 500-1000rpm, the time is
10-30min;
3) adhesive is weighed according to the 2-7% of material total weight in step 1), prepares the solution as 2% concentration;
4) prepared solution in step 3) is added in the material mixed in step 2), be sufficiently stirred, speed of agitator
500-1000rpm, time 10-20min;
5) prepared material in step 4) is shaped using the tape casting, dry, chopping, wherein quantification of 80-120g/
M2, drying temperature are 110-130 DEG C;
6) after product prepared by step 5) being made cigarette sample, tar and CO burst sizes is detected, and carries out aesthetic quality
Evaluation.
Further, the mineral filler is the mixing of one or both of calcium carbonate, titanium dioxide and bentonite.
Further, the Alevaire is one kind in glycerine, propylene glycol.
Further, the combustion rate regulator is potassium citrate, tartaric acid acid potassium, one kind in potassium malate or two
The mixing of kind.
Further, described adhesive is the mixing of one or both of sodium alginate, chitosan, guar gum, CMC.
Reconstituted tobacco product prepared by the present invention has the characteristics that low tar, low CO burst sizes, without papery breath, Neng Gouzuo
For effective supplement of existing papermaking reconstituted tobacco, while raw material Application Range can be expanded, alleviate tobacco chippings etc. there is lack of raw materials
Pressure has highly important innovation and realistic meaning for entire tobacco business.
Specific embodiment
In order to make the purpose , technical scheme and advantage of the present invention be clearer, with reference to embodiments, to the present invention
It is further elaborated.The specific embodiments described herein are merely illustrative of the present invention, is not used to limit this hair
It is bright.
Embodiment 1
1) weigh weight percent be 60% calcium carbonate, 20% tobacco powder, 10% glycerine, 3% potassium citrate,
7% tobacco extract, it is spare;
2) material in 1) is sufficiently mixed in homogeneous tank with water, speed of agitator 500rpm, time 15min;
3) 3% according to material total weight in 1) weighs sodium alginate, prepares the solution as 2% concentration;
4) in the material mixed during 2) prepared solution in 3) is added in, it is sufficiently stirred, speed of agitator 700rpm, when
Between be 20min;
5) prepared material in 4) is shaped using the tape casting, dry, chopping, wherein quantification of 90g/m2, dry temperature
It spends for 110 DEG C;
6) after the product 5) prepared being made cigarette sample, tar and CO burst sizes is detected, and carries out sensory quality assessment.
Embodiment 2
1) weigh weight percent be 80% titanium dioxide, 6% tobacco powder, 8% propylene glycol, 1% potassium tartrate,
5% tobacco extract, it is spare;
2) material in 1) is sufficiently mixed in homogeneous tank with water, speed of agitator 800rpm, time 25min;
3) 5% according to material total weight in 1) weighs CMC, prepares the solution as 2% concentration;
4) in the material mixed during 2) prepared solution in 3) is added in, it is sufficiently stirred, speed of agitator 800rpm, when
Between be 15min;
5) prepared material in 4) is shaped using the tape casting, dry, chopping, wherein quantification of 100g/m2, dry temperature
It spends for 120 DEG C;
6) after the product 5) prepared being made cigarette sample, tar and CO burst sizes is detected, and carries out sensory quality assessment.
Embodiment 3
1) weigh weight percent be 70% calcium carbonate, 15% tobacco powder, 5% glycerine, 3% potassium malate,
7% tobacco extract, it is spare;
2) material in 1) is sufficiently mixed in homogeneous tank with water, speed of agitator 900rpm, time 25min;
3) 5% according to material total weight in 1) weighs chitosan, prepares the solution as 2% concentration;
4) in the material mixed during 2) prepared solution in 3) is added in, it is sufficiently stirred, speed of agitator 900rpm, when
Between be 20min;
5) prepared material in 4) is shaped using the tape casting, dry, chopping, wherein quantification of 110g/m2, dry temperature
It spends for 130 DEG C;
6) after the product 5) prepared being made cigarette sample, tar and CO burst sizes is detected, and carries out sensory quality assessment.
Embodiment 4
1) weigh weight percent be 75% calcium carbonate, 8% tobacco powder, 9% propylene glycol, 2% potassium citrate,
6% tobacco extract, it is spare;
2) material in 1) is sufficiently mixed in homogeneous tank with water, speed of agitator 600rpm, time 30min;
3) 5% according to material total weight in 1) weighs sodium alginate, prepares the solution as 2% concentration;
4) in the material mixed during 2) prepared solution in 3) is added in, it is sufficiently stirred, speed of agitator 850rpm, when
Between be 20min;
5) prepared material in 4) is shaped using the tape casting, dry, chopping, wherein quantification of 115g/m2, dry temperature
It spends for 130 DEG C;
6) after the product 5) prepared being made cigarette sample, tar and CO burst sizes is detected, and carries out sensory quality assessment.
Embodiment 5
1) weigh weight percent be 70% bentonite, 10% tobacco powder, 10% glycerine, 3% potassium citrate,
7% tobacco extract, it is spare;
2) material in 1) is sufficiently mixed in homogeneous tank with water, speed of agitator 650rpm, time 20min;
3) 3% according to material total weight in 1) weighs chitosan, prepares the solution as 2% concentration;
4) in the material mixed during 2) prepared solution in 3) is added in, it is sufficiently stirred, speed of agitator 900rpm, when
Between be 15min;
5) prepared material in 4) is shaped using the tape casting, dry, chopping, wherein quantification of 115g/m2, dry temperature
It spends for 120 DEG C;
6) after the product 5) prepared being made cigarette sample, tar and CO burst sizes is detected, and carries out sensory quality assessment.
The tar of Examples 1 to 5 Novel reconstructed tobacco leaf product and CO burst size testing results are as shown in table 1.
1 testing result of table
Tar content (mg/ branch)) | CO burst sizes (mg/ branch) | |
Control sample | 6.5 | 13.5 |
Embodiment 1 | 2.3 | 6.2 |
Embodiment 2 | 3.1 | 5.8 |
Embodiment 3 | 2.2 | 7.3 |
Embodiment 4 | 2.8 | 6.8 |
Embodiment 5 | 3.5 | 5.2 |
As can be seen from Table 1, compared with existing reconstituted tobacco, using the Novel reconstructed tobacco leaf product of the method for the present invention preparation
Tar and CO burst sizes are significantly reduced.By sensory quality assessment, the Novel reconstructed cigarette prepared using the method for the present invention
Leaf product sensory stable quality meets the demand of cigarette product.
The present invention uses mineral filler as main matrix, selective addition expanded by heating and the adjustable bonding of Filling power
Agent, Alevaire, combustion rate regulator, tobacco material and essence and flavoring agent etc., are uniformly mixed by homogenizer, are molded with the tape casting
Technology (thick slurry method) prepares the Novel reconstructed tobacco leaf product of non-fiber matrix.The product has low tar, low CO burst sizes, nothing
The features such as papery breath, can be as effective supplement of existing papermaking reconstituted tobacco, while raw material Application Range can be expanded, alleviate
The pressure that there is lack of raw materials such as tobacco chippings has highly important innovation and realistic meaning for entire tobacco business.
The above description is merely a specific embodiment, but protection scope of the present invention is not limited thereto, any
Belong to those skilled in the art in the technical scope disclosed by the present invention, the change or replacement that can be readily occurred in all should
It is included within the scope of the present invention.Therefore, protection scope of the present invention should be subject to the protection scope in claims.
Claims (5)
1. a kind of preparation method of non-fiber matrix Novel reconstructed tobacco leaf product, it is characterised in that include the following steps:
1) weigh weight percent for the mineral filler of 60-80%, the tobacco powder of 5-20%, 5-12% Alevaire, 1-3% combustion
Rate modifier, the tobacco extract of 5-20% are burnt, it is spare;
2) material in step 1) is sufficiently mixed in homogeneous tank with water, speed of agitator 500-1000rpm, time 10-
30min;
3) adhesive is weighed according to the 2-7% of material total weight in step 1), prepares the solution as 2% concentration;
4) prepared solution in step 3) is added in the material mixed in step 2), be sufficiently stirred, speed of agitator 500-
1000rpm, time 10-20min;
5) prepared material in step 4) is shaped using the tape casting, dry, chopping, wherein quantification of 80-120g/m2, it is dry
Temperature is 110-130 DEG C;
6) after product prepared by step 5) being made cigarette sample, tar and CO burst sizes is detected, and carries out sensory quality assessment.
2. the preparation method of non-fiber matrix Novel reconstructed tobacco leaf product as described in claim 1, it is characterised in that:The ore deposit
Object filler is the mixing of one or both of calcium carbonate, titanium dioxide and bentonite.
3. the preparation method of non-fiber matrix Novel reconstructed tobacco leaf product as described in claim 1, it is characterised in that:The mist
Agent is glycerine, one kind in propylene glycol.
4. the preparation method of non-fiber matrix Novel reconstructed tobacco leaf product as described in claim 1, it is characterised in that:The combustion
Burning rate modifier is the mixing of one or both of potassium citrate, tartaric acid acid potassium, potassium malate.
5. the preparation method of non-fiber matrix Novel reconstructed tobacco leaf product as described in claim 1, it is characterised in that:It is described viscous
Mixture is the mixing of one or both of sodium alginate, chitosan, guar gum, CMC.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201711324580.XA CN108041672A (en) | 2017-12-13 | 2017-12-13 | A kind of preparation method of non-fiber matrix Novel reconstructed tobacco leaf product |
Applications Claiming Priority (1)
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---|---|---|---|
CN201711324580.XA CN108041672A (en) | 2017-12-13 | 2017-12-13 | A kind of preparation method of non-fiber matrix Novel reconstructed tobacco leaf product |
Publications (1)
Publication Number | Publication Date |
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CN108041672A true CN108041672A (en) | 2018-05-18 |
Family
ID=62132235
Family Applications (1)
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CN201711324580.XA Pending CN108041672A (en) | 2017-12-13 | 2017-12-13 | A kind of preparation method of non-fiber matrix Novel reconstructed tobacco leaf product |
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CN (1) | CN108041672A (en) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112384082A (en) * | 2018-06-29 | 2021-02-19 | 菲利普莫里斯生产公司 | Casting apparatus and method for producing a cast web of alkaloid containing material |
WO2021208931A1 (en) * | 2020-04-16 | 2021-10-21 | 广东省金叶科技开发有限公司 | Cigarette core material pulping method and pulp, cigarette core material and preparation method therefor |
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CN112384082A (en) * | 2018-06-29 | 2021-02-19 | 菲利普莫里斯生产公司 | Casting apparatus and method for producing a cast web of alkaloid containing material |
WO2021208931A1 (en) * | 2020-04-16 | 2021-10-21 | 广东省金叶科技开发有限公司 | Cigarette core material pulping method and pulp, cigarette core material and preparation method therefor |
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