CN108017974A - A kind of preparation method of fireproof coating - Google Patents

A kind of preparation method of fireproof coating Download PDF

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Publication number
CN108017974A
CN108017974A CN201711446637.3A CN201711446637A CN108017974A CN 108017974 A CN108017974 A CN 108017974A CN 201711446637 A CN201711446637 A CN 201711446637A CN 108017974 A CN108017974 A CN 108017974A
Authority
CN
China
Prior art keywords
parts
speed
fireproof coating
dusting
film forming
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201711446637.3A
Other languages
Chinese (zh)
Inventor
王红超
贾留宽
贾若龙
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
LUOYANG SHENJIA KILN CO Ltd
Original Assignee
LUOYANG SHENJIA KILN CO Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by LUOYANG SHENJIA KILN CO Ltd filed Critical LUOYANG SHENJIA KILN CO Ltd
Priority to CN201711446637.3A priority Critical patent/CN108017974A/en
Publication of CN108017974A publication Critical patent/CN108017974A/en
Pending legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D161/00Coating compositions based on condensation polymers of aldehydes or ketones; Coating compositions based on derivatives of such polymers
    • C09D161/20Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/18Fireproof paints including high temperature resistant paints
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00Use of inorganic substances as compounding ingredients
    • C08K3/02Elements
    • C08K3/08Metals
    • C08K2003/0812Aluminium
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00Use of inorganic substances as compounding ingredients
    • C08K3/32Phosphorus-containing compounds
    • C08K2003/321Phosphates
    • C08K2003/322Ammonium phosphate
    • C08K2003/323Ammonium polyphosphate
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2201/00Properties
    • C08L2201/02Flame or fire retardant/resistant
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/03Polymer mixtures characterised by other features containing three or more polymers in a blend

Abstract

The invention relates to a kind of preparation method of fireproof coating, it comprises the following steps:1) each materials for later use of following parts by weight is taken:30 50 parts of anhydrous calcium chloride, 400 450 parts of dusting silicate fiber, 50 70 parts of chlorinated paraffin, 30 50 parts of mountain flour, 8 12 parts of aluminium powder, 15 30 parts of composite zinc phosphate, 8 10 parts of titanium dioxide, 10 20 parts of mica powder, 15 25 parts of foaming agent, 150 200 parts of film forming agent, 150 250 parts of deionized water;2) deionized water is added in dispersion cylinder, moderate-speed mixer state is opened, adds foaming agent thereto, stirs 2 3min, then the film forming agent in formula is sequentially added, after stirring 5 8min, dusting silicate fiber, chlorinated paraffin, mountain flour, aluminium powder, composite zinc phosphate, titanium dioxide, mica powder are added, increase mixing speed is at a high speed, scattered 40 50min of mashing, then rotating speed is reduced to middling speed state, and it is 19 25 DEG C to control final denseness, obtains the fireproof coating.

Description

A kind of preparation method of fireproof coating
Technical field
The invention belongs to paint field, and in particular to a kind of preparation method of Novel fire retardant coating.
Background technology
With the increase of people's awareness of safety, the application of fireproof coating is more and more extensive.But grinding for fireproof coating System, there are still many technological difficulties, it is necessary to which the main problem solved is to improve water resistance, shorten drying time, extend fire resisting Time, improve storage stability, increase dicoration etc..
In conclusion indoor thin section steel structure fire-resisting paint poor water resistance currently on the market, poor storage stability are resistance to The shortcomings of fiery time is short, drying time length, decorative difference.Therefore research and development excellent performance, environmental-friendly indoor slim steel Structure fire coating is the inexorable trend of indoor steel structure fireproof protection.
The content of the invention
In order to solve the problems in the existing technology, the present invention provides a kind of water resistance for improving fireproof coating With the preparation method of the Novel fire retardant coating of improvement coating adhesion.
The object of the invention to solve the technical problems is realized using following technical scheme.Carried according to the present invention A kind of preparation method of the fireproof coating gone out, the described method comprises the following steps:
1) each materials for later use of following parts by weight is taken:30-50 parts of anhydrous calcium chloride, dusting silicate fiber 400-450 Part, 50-70 parts of chlorinated paraffin, 30-50 parts of mountain flour, 8-12 parts of aluminium powder, 15-30 parts of composite zinc phosphate, 8-10 parts of titanium dioxide, cloud 10-20 parts of female powder, 15-25 parts of foaming agent, 150-200 parts of film forming agent, 150-250 parts of deionized water;
2) deionized water is added in dispersion cylinder, opens moderate-speed mixer state, add foaming agent thereto, stir 2- 3min, then sequentially adds the film forming agent in formula, after stirring 5-8min, adds dusting silicate fiber, chlorinated paraffin, stone Then powder, aluminium powder, composite zinc phosphate, titanium dioxide, mica powder, increase mixing speed are dropped to scattered 40-50min at a high speed, is beaten To middling speed state, it is 19-25 DEG C to control final denseness, obtains the fireproof coating for the slow-speed of revolution.
The present invention has the following advantages compared with prior art:
Preparation method of the present invention is simple, prepares product and belongs to green environmental protection coating, which not only has fire resistance period Long, decoration performance is good, the features such as caking property is good, water resistance is excellent.
Embodiment
Further to illustrate that the present invention to reach the technological means and effect that predetermined goal of the invention is taken, ties below Preferred embodiment is closed, to being described in detail according to a kind of its embodiment of the preparation method of fireproof coating proposed by the present invention As after.
Embodiment 1
A kind of preparation method of fireproof coating of the present invention, the described method comprises the following steps:
1) each materials for later use of following parts by weight is taken:30 parts of anhydrous calcium chloride, 400 parts of dusting silicate fiber, chlorination stone 70 parts of wax, 30 parts of mountain flour, 8 parts of aluminium powder, 15 parts of composite zinc phosphate, 8 parts of titanium dioxide, 10 parts of mica powder, 25 parts of foaming agent, film forming 200 parts of agent, 150 parts of deionized water.
2) deionized water is added in dispersion cylinder, opens moderate-speed mixer state, add foaming agent thereto, stir 2min, Then sequentially add the film forming agent in formula, after stirring 5min, add dusting silicate fiber, chlorinated paraffin, mountain flour, aluminium powder, Then composite zinc phosphate, titanium dioxide, mica powder, increase mixing speed reduce rotating speed to middling speed to scattered 40min at a high speed, is beaten State, it is 22 DEG C to control final denseness, obtains the fireproof coating.
Wherein dusting silicate fiber is one kind in ammonium polyphosphate, pentaerythrite and melamine;It is wherein described into Film is amino resins and the mixture of allyl resin, its weight ratio is 3:1.
Embodiment 2
A kind of preparation method of fireproof coating of the present invention, the described method comprises the following steps:
1) each materials for later use of following parts by weight is taken:40 parts of anhydrous calcium chloride, 430 parts of dusting silicate fiber, chlorination stone 60 parts of wax, 40 parts of mountain flour, 10 parts of aluminium powder, 22 parts of composite zinc phosphate, 9 parts of titanium dioxide, 15 parts of mica powder, 20 parts of foaming agent, film forming 170 parts of agent, 200 parts of deionized water.
2) deionized water is added in dispersion cylinder, opens moderate-speed mixer state, add foaming agent thereto, stir 3min, Then sequentially add the film forming agent in formula, after stirring 8min, add dusting silicate fiber, chlorinated paraffin, mountain flour, aluminium powder, Then composite zinc phosphate, titanium dioxide, mica powder, increase mixing speed reduce rotating speed to middling speed to scattered 50min at a high speed, is beaten State, it is 25 DEG C to control final denseness, obtains the fireproof coating.
Wherein described dusting silicate fiber is any two the mixing in ammonium polyphosphate, pentaerythrite and melamine Thing.The film forming agent is amino resins and the mixture of allyl resin, its weight ratio is 3: 1.
Embodiment 3
A kind of preparation method of fireproof coating of the present invention, the described method comprises the following steps:
1) each materials for later use of following parts by weight is taken:50 parts of anhydrous calcium chloride, 450 parts of dusting silicate fiber, chlorination stone 50 parts of wax, 50 parts of mountain flour, 12 parts of aluminium powder, 30 parts of composite zinc phosphate, 10 parts of titanium dioxide, 20 parts of mica powder, 15 parts of foaming agent, into 150 parts of film, 250 parts of deionized water.
3) deionized water is added in dispersion cylinder, opens moderate-speed mixer state, add foaming agent thereto, stir 3min, Then sequentially add the film forming agent in formula, after stirring 7min, add dusting silicate fiber, chlorinated paraffin, mountain flour, aluminium powder, Then composite zinc phosphate, titanium dioxide, mica powder, increase mixing speed reduce rotating speed to middling speed to scattered 45min at a high speed, is beaten State, it is 19 DEG C to control final denseness, obtains the fireproof coating.
Wherein described dusting silicate fiber is the mixture in ammonium polyphosphate, pentaerythrite and melamine.Described Film forming agent is amino resins and the mixture of allyl resin, its weight ratio is 3:1.
The above described is only a preferred embodiment of the present invention, limitation in any form is not done to the present invention, Although the present invention is disclosed above with preferred embodiment, but is not limited to the present invention, any to be familiar with this professional technology Personnel, without departing from the scope of the present invention, when the technology contents using the disclosure above make a little change or repair The equivalent embodiment for equivalent variations is adornd, as long as being the content without departing from technical solution of the present invention, the technology according to the present invention is real Verify any simple modification, equivalent change and modification made for any of the above embodiments, still fall within the model of technical solution of the present invention In enclosing.

Claims (1)

1. a kind of preparation method of fireproof coating, it is characterised in that the described method comprises the following steps::
1) each materials for later use of following parts by weight is taken:30-50 parts of anhydrous calcium chloride, 400-450 parts of dusting silicate fiber, chlorination 50-70 parts of paraffin, 30-50 parts of mountain flour, 8-12 parts of aluminium powder, 15-30 parts of composite zinc phosphate, 8-10 parts of titanium dioxide, mica powder 10-20 Part, 15-25 parts of foaming agent, 150-200 parts of film forming agent, 150-250 parts of deionized water;
2) deionized water is added in dispersion cylinder, opens moderate-speed mixer state, add foaming agent thereto, stir 2-3min, so Sequentially add the film forming agent in formula afterwards, after stirring 5-8min, add dusting silicate fiber, chlorinated paraffin, mountain flour, aluminium powder, Then composite zinc phosphate, titanium dioxide, mica powder, increase mixing speed reduce rotating speed into scattered 40-50min at a high speed, is beaten Fast state, it is 19-25 DEG C to control final denseness, obtains the fireproof coating.
CN201711446637.3A 2017-12-27 2017-12-27 A kind of preparation method of fireproof coating Pending CN108017974A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201711446637.3A CN108017974A (en) 2017-12-27 2017-12-27 A kind of preparation method of fireproof coating

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201711446637.3A CN108017974A (en) 2017-12-27 2017-12-27 A kind of preparation method of fireproof coating

Publications (1)

Publication Number Publication Date
CN108017974A true CN108017974A (en) 2018-05-11

Family

ID=62071637

Family Applications (1)

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CN201711446637.3A Pending CN108017974A (en) 2017-12-27 2017-12-27 A kind of preparation method of fireproof coating

Country Status (1)

Country Link
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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1740253A (en) * 2005-09-16 2006-03-01 湖南华迪电力环保工程技术有限公司 Anticorrosive flue paint
CN101724302A (en) * 2009-12-02 2010-06-09 山东鲁阳股份有限公司 Light inorganic silicate fiber reinforcing fireproof paint and preparation method thereof
CN103694827A (en) * 2013-12-30 2014-04-02 河北晨阳工贸集团有限公司 Fireproof coating and preparation method thereof
CN106032443A (en) * 2015-09-06 2016-10-19 洛阳新巨能高热技术有限公司 Preparation method of fireproof coating

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1740253A (en) * 2005-09-16 2006-03-01 湖南华迪电力环保工程技术有限公司 Anticorrosive flue paint
CN101724302A (en) * 2009-12-02 2010-06-09 山东鲁阳股份有限公司 Light inorganic silicate fiber reinforcing fireproof paint and preparation method thereof
CN103694827A (en) * 2013-12-30 2014-04-02 河北晨阳工贸集团有限公司 Fireproof coating and preparation method thereof
CN106032443A (en) * 2015-09-06 2016-10-19 洛阳新巨能高热技术有限公司 Preparation method of fireproof coating

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Application publication date: 20180511

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