CN108017974A - A kind of preparation method of fireproof coating - Google Patents
A kind of preparation method of fireproof coating Download PDFInfo
- Publication number
- CN108017974A CN108017974A CN201711446637.3A CN201711446637A CN108017974A CN 108017974 A CN108017974 A CN 108017974A CN 201711446637 A CN201711446637 A CN 201711446637A CN 108017974 A CN108017974 A CN 108017974A
- Authority
- CN
- China
- Prior art keywords
- parts
- speed
- fireproof coating
- dusting
- film forming
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D161/00—Coating compositions based on condensation polymers of aldehydes or ketones; Coating compositions based on derivatives of such polymers
- C09D161/20—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/18—Fireproof paints including high temperature resistant paints
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/02—Elements
- C08K3/08—Metals
- C08K2003/0812—Aluminium
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/32—Phosphorus-containing compounds
- C08K2003/321—Phosphates
- C08K2003/322—Ammonium phosphate
- C08K2003/323—Ammonium polyphosphate
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/02—Flame or fire retardant/resistant
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
Abstract
The invention relates to a kind of preparation method of fireproof coating, it comprises the following steps:1) each materials for later use of following parts by weight is taken:30 50 parts of anhydrous calcium chloride, 400 450 parts of dusting silicate fiber, 50 70 parts of chlorinated paraffin, 30 50 parts of mountain flour, 8 12 parts of aluminium powder, 15 30 parts of composite zinc phosphate, 8 10 parts of titanium dioxide, 10 20 parts of mica powder, 15 25 parts of foaming agent, 150 200 parts of film forming agent, 150 250 parts of deionized water;2) deionized water is added in dispersion cylinder, moderate-speed mixer state is opened, adds foaming agent thereto, stirs 2 3min, then the film forming agent in formula is sequentially added, after stirring 5 8min, dusting silicate fiber, chlorinated paraffin, mountain flour, aluminium powder, composite zinc phosphate, titanium dioxide, mica powder are added, increase mixing speed is at a high speed, scattered 40 50min of mashing, then rotating speed is reduced to middling speed state, and it is 19 25 DEG C to control final denseness, obtains the fireproof coating.
Description
Technical field
The invention belongs to paint field, and in particular to a kind of preparation method of Novel fire retardant coating.
Background technology
With the increase of people's awareness of safety, the application of fireproof coating is more and more extensive.But grinding for fireproof coating
System, there are still many technological difficulties, it is necessary to which the main problem solved is to improve water resistance, shorten drying time, extend fire resisting
Time, improve storage stability, increase dicoration etc..
In conclusion indoor thin section steel structure fire-resisting paint poor water resistance currently on the market, poor storage stability are resistance to
The shortcomings of fiery time is short, drying time length, decorative difference.Therefore research and development excellent performance, environmental-friendly indoor slim steel
Structure fire coating is the inexorable trend of indoor steel structure fireproof protection.
The content of the invention
In order to solve the problems in the existing technology, the present invention provides a kind of water resistance for improving fireproof coating
With the preparation method of the Novel fire retardant coating of improvement coating adhesion.
The object of the invention to solve the technical problems is realized using following technical scheme.Carried according to the present invention
A kind of preparation method of the fireproof coating gone out, the described method comprises the following steps:
1) each materials for later use of following parts by weight is taken:30-50 parts of anhydrous calcium chloride, dusting silicate fiber 400-450
Part, 50-70 parts of chlorinated paraffin, 30-50 parts of mountain flour, 8-12 parts of aluminium powder, 15-30 parts of composite zinc phosphate, 8-10 parts of titanium dioxide, cloud
10-20 parts of female powder, 15-25 parts of foaming agent, 150-200 parts of film forming agent, 150-250 parts of deionized water;
2) deionized water is added in dispersion cylinder, opens moderate-speed mixer state, add foaming agent thereto, stir 2-
3min, then sequentially adds the film forming agent in formula, after stirring 5-8min, adds dusting silicate fiber, chlorinated paraffin, stone
Then powder, aluminium powder, composite zinc phosphate, titanium dioxide, mica powder, increase mixing speed are dropped to scattered 40-50min at a high speed, is beaten
To middling speed state, it is 19-25 DEG C to control final denseness, obtains the fireproof coating for the slow-speed of revolution.
The present invention has the following advantages compared with prior art:
Preparation method of the present invention is simple, prepares product and belongs to green environmental protection coating, which not only has fire resistance period
Long, decoration performance is good, the features such as caking property is good, water resistance is excellent.
Embodiment
Further to illustrate that the present invention to reach the technological means and effect that predetermined goal of the invention is taken, ties below
Preferred embodiment is closed, to being described in detail according to a kind of its embodiment of the preparation method of fireproof coating proposed by the present invention
As after.
Embodiment 1
A kind of preparation method of fireproof coating of the present invention, the described method comprises the following steps:
1) each materials for later use of following parts by weight is taken:30 parts of anhydrous calcium chloride, 400 parts of dusting silicate fiber, chlorination stone
70 parts of wax, 30 parts of mountain flour, 8 parts of aluminium powder, 15 parts of composite zinc phosphate, 8 parts of titanium dioxide, 10 parts of mica powder, 25 parts of foaming agent, film forming
200 parts of agent, 150 parts of deionized water.
2) deionized water is added in dispersion cylinder, opens moderate-speed mixer state, add foaming agent thereto, stir 2min,
Then sequentially add the film forming agent in formula, after stirring 5min, add dusting silicate fiber, chlorinated paraffin, mountain flour, aluminium powder,
Then composite zinc phosphate, titanium dioxide, mica powder, increase mixing speed reduce rotating speed to middling speed to scattered 40min at a high speed, is beaten
State, it is 22 DEG C to control final denseness, obtains the fireproof coating.
Wherein dusting silicate fiber is one kind in ammonium polyphosphate, pentaerythrite and melamine;It is wherein described into
Film is amino resins and the mixture of allyl resin, its weight ratio is 3:1.
Embodiment 2
A kind of preparation method of fireproof coating of the present invention, the described method comprises the following steps:
1) each materials for later use of following parts by weight is taken:40 parts of anhydrous calcium chloride, 430 parts of dusting silicate fiber, chlorination stone
60 parts of wax, 40 parts of mountain flour, 10 parts of aluminium powder, 22 parts of composite zinc phosphate, 9 parts of titanium dioxide, 15 parts of mica powder, 20 parts of foaming agent, film forming
170 parts of agent, 200 parts of deionized water.
2) deionized water is added in dispersion cylinder, opens moderate-speed mixer state, add foaming agent thereto, stir 3min,
Then sequentially add the film forming agent in formula, after stirring 8min, add dusting silicate fiber, chlorinated paraffin, mountain flour, aluminium powder,
Then composite zinc phosphate, titanium dioxide, mica powder, increase mixing speed reduce rotating speed to middling speed to scattered 50min at a high speed, is beaten
State, it is 25 DEG C to control final denseness, obtains the fireproof coating.
Wherein described dusting silicate fiber is any two the mixing in ammonium polyphosphate, pentaerythrite and melamine
Thing.The film forming agent is amino resins and the mixture of allyl resin, its weight ratio is 3: 1.
Embodiment 3
A kind of preparation method of fireproof coating of the present invention, the described method comprises the following steps:
1) each materials for later use of following parts by weight is taken:50 parts of anhydrous calcium chloride, 450 parts of dusting silicate fiber, chlorination stone
50 parts of wax, 50 parts of mountain flour, 12 parts of aluminium powder, 30 parts of composite zinc phosphate, 10 parts of titanium dioxide, 20 parts of mica powder, 15 parts of foaming agent, into
150 parts of film, 250 parts of deionized water.
3) deionized water is added in dispersion cylinder, opens moderate-speed mixer state, add foaming agent thereto, stir 3min,
Then sequentially add the film forming agent in formula, after stirring 7min, add dusting silicate fiber, chlorinated paraffin, mountain flour, aluminium powder,
Then composite zinc phosphate, titanium dioxide, mica powder, increase mixing speed reduce rotating speed to middling speed to scattered 45min at a high speed, is beaten
State, it is 19 DEG C to control final denseness, obtains the fireproof coating.
Wherein described dusting silicate fiber is the mixture in ammonium polyphosphate, pentaerythrite and melamine.Described
Film forming agent is amino resins and the mixture of allyl resin, its weight ratio is 3:1.
The above described is only a preferred embodiment of the present invention, limitation in any form is not done to the present invention,
Although the present invention is disclosed above with preferred embodiment, but is not limited to the present invention, any to be familiar with this professional technology
Personnel, without departing from the scope of the present invention, when the technology contents using the disclosure above make a little change or repair
The equivalent embodiment for equivalent variations is adornd, as long as being the content without departing from technical solution of the present invention, the technology according to the present invention is real
Verify any simple modification, equivalent change and modification made for any of the above embodiments, still fall within the model of technical solution of the present invention
In enclosing.
Claims (1)
1. a kind of preparation method of fireproof coating, it is characterised in that the described method comprises the following steps::
1) each materials for later use of following parts by weight is taken:30-50 parts of anhydrous calcium chloride, 400-450 parts of dusting silicate fiber, chlorination
50-70 parts of paraffin, 30-50 parts of mountain flour, 8-12 parts of aluminium powder, 15-30 parts of composite zinc phosphate, 8-10 parts of titanium dioxide, mica powder 10-20
Part, 15-25 parts of foaming agent, 150-200 parts of film forming agent, 150-250 parts of deionized water;
2) deionized water is added in dispersion cylinder, opens moderate-speed mixer state, add foaming agent thereto, stir 2-3min, so
Sequentially add the film forming agent in formula afterwards, after stirring 5-8min, add dusting silicate fiber, chlorinated paraffin, mountain flour, aluminium powder,
Then composite zinc phosphate, titanium dioxide, mica powder, increase mixing speed reduce rotating speed into scattered 40-50min at a high speed, is beaten
Fast state, it is 19-25 DEG C to control final denseness, obtains the fireproof coating.
Priority Applications (1)
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CN201711446637.3A CN108017974A (en) | 2017-12-27 | 2017-12-27 | A kind of preparation method of fireproof coating |
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CN201711446637.3A CN108017974A (en) | 2017-12-27 | 2017-12-27 | A kind of preparation method of fireproof coating |
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CN108017974A true CN108017974A (en) | 2018-05-11 |
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CN201711446637.3A Pending CN108017974A (en) | 2017-12-27 | 2017-12-27 | A kind of preparation method of fireproof coating |
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Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1740253A (en) * | 2005-09-16 | 2006-03-01 | 湖南华迪电力环保工程技术有限公司 | Anticorrosive flue paint |
CN101724302A (en) * | 2009-12-02 | 2010-06-09 | 山东鲁阳股份有限公司 | Light inorganic silicate fiber reinforcing fireproof paint and preparation method thereof |
CN103694827A (en) * | 2013-12-30 | 2014-04-02 | 河北晨阳工贸集团有限公司 | Fireproof coating and preparation method thereof |
CN106032443A (en) * | 2015-09-06 | 2016-10-19 | 洛阳新巨能高热技术有限公司 | Preparation method of fireproof coating |
-
2017
- 2017-12-27 CN CN201711446637.3A patent/CN108017974A/en active Pending
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1740253A (en) * | 2005-09-16 | 2006-03-01 | 湖南华迪电力环保工程技术有限公司 | Anticorrosive flue paint |
CN101724302A (en) * | 2009-12-02 | 2010-06-09 | 山东鲁阳股份有限公司 | Light inorganic silicate fiber reinforcing fireproof paint and preparation method thereof |
CN103694827A (en) * | 2013-12-30 | 2014-04-02 | 河北晨阳工贸集团有限公司 | Fireproof coating and preparation method thereof |
CN106032443A (en) * | 2015-09-06 | 2016-10-19 | 洛阳新巨能高热技术有限公司 | Preparation method of fireproof coating |
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Application publication date: 20180511 |
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