CN108017934A - A kind of ink sun-proof pink chromogen paratonere and preparation method - Google Patents
A kind of ink sun-proof pink chromogen paratonere and preparation method Download PDFInfo
- Publication number
- CN108017934A CN108017934A CN201610958466.1A CN201610958466A CN108017934A CN 108017934 A CN108017934 A CN 108017934A CN 201610958466 A CN201610958466 A CN 201610958466A CN 108017934 A CN108017934 A CN 108017934A
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- China
- Prior art keywords
- paratonere
- proof
- sun
- red
- ink
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0001—Post-treatment of organic pigments or dyes
- C09B67/0014—Influencing the physical properties by treatment with a liquid, e.g. solvents
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/006—Preparation of organic pigments
- C09B67/0065—Preparation of organic pigments of organic pigments with only non-macromolecular compounds
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
Abstract
The present invention provides a kind of ink with sun-proof pink chromogen paratonere, it includes following components in percentage by weight:Alkali red 1:1 5 20%;Glacial acetic acid 2 5%;Disodium hydrogen phosphate 2 5%;Sodium tungstate 10 15%;Sodium molybdate 20 25%;Pigment auxiliary agent 1 3%;Hydrochloric acid 30 35%;Rosin 2 5%;Liquid caustic soda 1 3%.A kind of preparation method present invention also offers ink with sun-proof pink chromogen paratonere.The present invention can solve the problems, such as that paratonere can not achieve that viscosity is low and stability is taken into account well in the prior art.
Description
Technical field
The present invention relates to pigment technology field, in particular to a kind of ink sun-proof pink chromogen paratonere and system
Preparation Method.
Background technology
As a kind of using quite varied coloring material, it is mainly used in coating, printing and dyeing, plastic products, makes pigment
The industries such as paper, rubber and ceramics, with the fast development of downstream industry, constantly expand the demand of pigment.
Traditional paratonere is in the industry using more, and with the development of technology, and more and more paratoneres are in ink
In there has also been certain application, such as NC ink, PP ink, PA ink and PU ink etc..In ink, pigment is low except needing to reach viscosity
Outside the requirement of (viscosity height easily causes the caking phenomenon of storage process, influences to use), it is also necessary to ensure the good requirement of stability,
And current paratonere also there is shortcoming can't achieve the purpose that to take into account in other words in these areas.
The content of the invention
In consideration of it, the present invention provides a kind of ink sun-proof pink chromogen paratonere and preparation method, it is intended to solves existing
There is paratonere in technology to can not achieve the problem of viscosity is low and stability is taken into account well.
For this reason, the present invention provides a kind of ink with sun-proof pink chromogen paratonere, it includes following percentage by weight
Component:
Further, above-mentioned ink includes following components in percentage by weight with sun-proof pink chromogen paratonere:Alkalescence is red
17-18%;Glacial acetic acid 3-4%;Disodium hydrogen phosphate 3-4%;Sodium tungstate 12-13%;Sodium molybdate 22-23%;Pigment auxiliary agent 1-
2%;Hydrochloric acid 32-33%;Rosin 3-4%;Liquid caustic soda 1-2%.
Further, above-mentioned ink includes following components in percentage by weight with sun-proof pink chromogen paratonere:Alkalescence is red
17.5%;Glacial acetic acid 4%;Disodium hydrogen phosphate 4%;Sodium tungstate 12.5%;Sodium molybdate 22.5%;Pigment auxiliary agent 2%;Hydrochloric acid
32.5%;Rosin 4%;Liquid caustic soda 2%.
Further, it is alkali red 1:1 that above-mentioned alkalescence is red:1.
The preparation method of the sun-proof pink chromogen paratonere of a kind of above-mentioned ink, it is characterised in that comprise the following steps:
1) red be put into 75-85 DEG C of water of alkalescence is dissolved in a reaction container;
2) sodium tungstate, sodium molybdate and disodium hydrogen phosphate are put into another reaction container and are dissolved;
3) it is alkaline red interior what is dissolved in the phosphorus tungsten molybdenum acid solutions addition step 1) dissolved in step 2);
4) reaction is completed, and material is rinsed, dries and crushed successively.
Further, it is alkali red 1:1 that above-mentioned alkalescence is red:1.
Further, above-mentioned steps 1) in, water temperature is 80 DEG C.
Ink provided by the present invention sun-proof pink chromogen paratonere and preparation method, are when prepared by described matching somebody with somebody
Method so that the stability for obtaining paratonere is improved, and viscosity reduces, and the storage characteristics of product can be improved, so that effectively
Ground solves the problems, such as that paratonere can not achieve that viscosity is low and stability is taken into account well in the prior art.
Embodiment
The exemplary embodiment of the disclosure is described in more detail below.Although show the exemplary implementation of the disclosure
Example, it being understood, however, that may be realized in various forms the disclosure without should be limited by embodiments set forth here.On the contrary,
These embodiments are provided to facilitate a more thoroughly understanding of the present invention, and can completely be communicated to the scope of the present disclosure
Those skilled in the art.
It is a kind of ink provided in an embodiment of the present invention sun-proof pink chromogen paratonere and preparation method below.The ink
Obtained with sun-proof pink chromogen paratonere by following proportioning, gross weight is in terms of 500KG.
Experiment condition is with reference to the existing determination condition progress for paratonere in the prior art, such as national standard, OK
Described in industry standard, details are not described herein.
According to above-described embodiment it can be seen that, ink provided by the present invention sun-proof pink chromogen paratonere and preparation side
Method, by described with when preparation method, since glossiness and tinctorial strength are all improved, so that obtained face
Expect that red stability is improved, and viscosity reduces, and the storage characteristics of product can be improved, so as to efficiently solve the prior art
Middle paratonere can not achieve the problem of viscosity is low and stability is taken into account well.
The ink is made with sun-proof pink chromogen paratonere by following preparation method, and this method comprises the following steps:
1) in the water of the red arbitrary temp (preferably 80 DEG C of status) being put between 75-85 DEG C of alkalescence in a reaction container
Dissolving;
2) sodium tungstate, sodium molybdate and disodium hydrogen phosphate are put into another reaction container and are dissolved;
3) it is alkaline red interior what is dissolved in the phosphorus tungsten molybdenum acid solutions addition step 1) dissolved in step 2);
4) reaction is completed, and material is rinsed, dries and crushed successively.
Wherein, above-mentioned alkalescence is red is specifically as follows alkali red 1:1:1.
Obviously, various changes and modifications can be made to the invention without departing from essence of the invention by those skilled in the art
God and scope.In this way, if these modifications and changes of the present invention belongs to the scope of the claims in the present invention and its equivalent technologies
Within, then the present invention is also intended to comprising including these modification and variations.
Claims (7)
1. the sun-proof pink chromogen paratonere of a kind of ink, it is characterised in that including following components in percentage by weight:
2. the sun-proof pink chromogen paratonere of a kind of ink according to claim 1, it is characterised in that including following weight
The component of percentage:Alkali red 1:1 7-18%;Glacial acetic acid 3-4%;Disodium hydrogen phosphate 3-4%;Sodium tungstate 12-13%;Sodium molybdate
22-23%;Pigment auxiliary agent 1-2%;Hydrochloric acid 32-33%;Rosin 3-4%;Liquid caustic soda 1-2%.
3. the sun-proof pink chromogen paratonere of a kind of ink according to claim 1, it is characterised in that including following weight
The component of percentage:Alkali red 1:1 7.5%;Glacial acetic acid 4%;Disodium hydrogen phosphate 4%;Sodium tungstate 12.5%;Sodium molybdate 22.5%;
Pigment auxiliary agent 2%;Hydrochloric acid 32.5%;Rosin 4%;Liquid caustic soda 2%.
4. the sun-proof pink chromogen paratonere of a kind of ink according to claim 1, it is characterised in that the alkalescence is red to be
Alkali red 1:1:1.
5. a kind of a kind of ink as described in claim 1-4 is any preparation method of sun-proof pink chromogen paratonere, it is special
Sign is, comprises the following steps:
1) red be put into 75-85 DEG C of water of alkalescence is dissolved in a reaction container;
2) sodium tungstate, sodium molybdate and disodium hydrogen phosphate are put into another reaction container and are dissolved;
3) it is alkaline red interior what is dissolved in the phosphorus tungsten molybdenum acid solutions addition step 1) dissolved in the step 2);
4) reaction is completed, and material is rinsed, dries and crushed successively.
A kind of 6. ink according to claim 5 preparation method of sun-proof pink chromogen paratonere, it is characterised in that institute
It is alkali red 1:1 that it is red, which to state alkalescence,:1.
A kind of 7. ink according to claim 5 preparation method of sun-proof pink chromogen paratonere, it is characterised in that institute
State in step 1), water temperature is 80 DEG C.
Priority Applications (1)
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CN201610958466.1A CN108017934A (en) | 2016-11-03 | 2016-11-03 | A kind of ink sun-proof pink chromogen paratonere and preparation method |
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CN201610958466.1A CN108017934A (en) | 2016-11-03 | 2016-11-03 | A kind of ink sun-proof pink chromogen paratonere and preparation method |
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CN108017934A true CN108017934A (en) | 2018-05-11 |
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CN201610958466.1A Pending CN108017934A (en) | 2016-11-03 | 2016-11-03 | A kind of ink sun-proof pink chromogen paratonere and preparation method |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110845865A (en) * | 2018-08-21 | 2020-02-28 | 吴江山湖颜料有限公司 | Red-light purple pigment violet and preparation method thereof |
CN110845867A (en) * | 2018-08-21 | 2020-02-28 | 吴江山湖颜料有限公司 | Low-viscosity pigment red and preparation method thereof |
CN110982330A (en) * | 2019-11-08 | 2020-04-10 | 吴江山湖颜料有限公司 | Lightfast pink primary pigment red for solvent type ink and preparation method thereof |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1687248A (en) * | 2005-04-04 | 2005-10-26 | 吴江市横扇太湖化工厂 | Preparation process of pigment red |
CN1772815A (en) * | 2005-10-21 | 2006-05-17 | 吴江市横扇太湖化工厂 | Preparation process of pigment violet |
CN102863818A (en) * | 2012-09-18 | 2013-01-09 | 杭州红妍颜料化工有限公司 | Preparation method of pigment purple 3 |
-
2016
- 2016-11-03 CN CN201610958466.1A patent/CN108017934A/en active Pending
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1687248A (en) * | 2005-04-04 | 2005-10-26 | 吴江市横扇太湖化工厂 | Preparation process of pigment red |
CN1772815A (en) * | 2005-10-21 | 2006-05-17 | 吴江市横扇太湖化工厂 | Preparation process of pigment violet |
CN102863818A (en) * | 2012-09-18 | 2013-01-09 | 杭州红妍颜料化工有限公司 | Preparation method of pigment purple 3 |
Non-Patent Citations (1)
Title |
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周春隆 等: "《有机颜料化学及工艺学》", 31 July 2002, 中国石化出版社 * |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110845865A (en) * | 2018-08-21 | 2020-02-28 | 吴江山湖颜料有限公司 | Red-light purple pigment violet and preparation method thereof |
CN110845867A (en) * | 2018-08-21 | 2020-02-28 | 吴江山湖颜料有限公司 | Low-viscosity pigment red and preparation method thereof |
CN110982330A (en) * | 2019-11-08 | 2020-04-10 | 吴江山湖颜料有限公司 | Lightfast pink primary pigment red for solvent type ink and preparation method thereof |
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Application publication date: 20180511 |
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