CN108003795A - Electronic jacquard machine finishing agent and preparation method thereof - Google Patents
Electronic jacquard machine finishing agent and preparation method thereof Download PDFInfo
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- CN108003795A CN108003795A CN201711393008.9A CN201711393008A CN108003795A CN 108003795 A CN108003795 A CN 108003795A CN 201711393008 A CN201711393008 A CN 201711393008A CN 108003795 A CN108003795 A CN 108003795A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09G—POLISHING COMPOSITIONS; SKI WAXES
- C09G1/00—Polishing compositions
- C09G1/04—Aqueous dispersions
Abstract
The invention discloses a kind of electronic jacquard machine finishing agent and preparation method thereof, wherein, the preparation method includes：1) in the presence of a solvent, polyether-modified heptamethyltrisiloxane and sodium dihydrogen phosphate are mixed, mixed liquor M1 is made；2) sodium metasilicate, triethanolamine, sodium citrate and borax are added into mixed liquor M1, mixture M 2 is made；3) sodium pyrophosphate and disodium ethylene diamine tetraacetate, obtained electronic jacquard machine finishing agent are added into mixture M 2.The present invention mixes polyether-modified heptamethyltrisiloxane and sodium dihydrogen phosphate, sodium metasilicate, triethanolamine, sodium citrate and borax are added into above-mentioned mixed liquor again, further, sodium pyrophosphate and disodium ethylene diamine tetraacetate are added thereto, so that the electronic jacquard machine finishing agent being mixed to prepare by above-mentioned material can effectively improve the surface brightness of electronic jacquard machine, and then its performance is greatly improved, reduce manual maintenance cost.
Description
Technical field
The present invention relates to brightener Material Field, and in particular, to electronic jacquard machine finishing agent and its preparation side
Method.
Background technology
For electronic jacquard machine as important Weaving device, the application in daily textile enterprise is extremely wide.And in reality
During use, often with the extension of usage time, electronic jacquard machine surface can cause its surface because the influence such as being aoxidized
Light is lost, so that its easily depreciation, so as to need artificially to be safeguarded, considerably increases artificial maintenance cost.
Therefore it provides a kind of brightness that can effectively maintain its surface, the electronic jacquard machine of artificial maintenance cost is reduced
The problem of with finishing agent and preparation method thereof being urgent need to resolve of the present invention.
The content of the invention
For the above-mentioned prior art, it is an object of the invention to overcome, electronic jacquard machine surface can be because being subject in the prior art
The influences such as oxidation cause its surface to lose light, so that its easily depreciation, so as to need artificially to be safeguarded, greatly increases
The problems such as artificial maintenance cost, so as to provide a kind of brightness that can effectively maintain its surface, reduce artificial maintenance into
This electronic jacquard machine finishing agent and preparation method thereof.
To achieve these goals, the present invention provides a kind of preparation method of electronic jacquard machine finishing agent, its
In, the preparation method includes：
1) in the presence of a solvent, polyether-modified heptamethyltrisiloxane and sodium dihydrogen phosphate are mixed, are made mixed
Close liquid M1；
2) sodium metasilicate, triethanolamine, sodium citrate and borax are added into mixed liquor M1, mixture M 2 is made；
3) sodium pyrophosphate and disodium ethylene diamine tetraacetate, obtained electronic jacquard machine surface-brightening are added into mixture M 2
Agent.
Present invention also offers a kind of electronic jacquard machine finishing agent according to made from preparation method described above.
Through the above technical solutions, the present invention mixes polyether-modified heptamethyltrisiloxane and sodium dihydrogen phosphate, then to
Sodium metasilicate, triethanolamine, sodium citrate and borax are added in above-mentioned mixed liquor, further, add thereto sodium pyrophosphate and
Disodium ethylene diamine tetraacetate, so that the electronic jacquard machine finishing agent being mixed to prepare by above-mentioned material can be effective
The surface brightness of electronic jacquard machine is improved, and then greatly improves its performance, reduces manual maintenance cost.
Other features and advantages of the present invention will be described in detail in subsequent specific embodiment part.
Embodiment
The embodiment of the present invention is described in detail below.It is it should be appreciated that described herein specific
Embodiment is merely to illustrate and explain the present invention, and is not intended to limit the invention.
The endpoint of disclosed scope and any value are not limited to the accurate scope or value herein, these scopes or
Value should be understood to comprising the value close to these scopes or value.For number range, between the endpoint value of each scope, respectively
It can be combined with each other between the endpoint value of a scope and single point value, and individually between point value and obtain one or more
New number range, these number ranges should be considered as specific open herein.
The present invention provides a kind of preparation method of electronic jacquard machine finishing agent, wherein, the preparation method bag
Include：
1) in the presence of a solvent, polyether-modified heptamethyltrisiloxane and sodium dihydrogen phosphate are mixed, are made mixed
Close liquid M1；
2) sodium metasilicate, triethanolamine, sodium citrate and borax are added into mixed liquor M1, mixture M 2 is made；
3) sodium pyrophosphate and disodium ethylene diamine tetraacetate, obtained electronic jacquard machine surface-brightening are added into mixture M 2
Agent.
The present invention mixes polyether-modified heptamethyltrisiloxane and sodium dihydrogen phosphate, then adds silicon into above-mentioned mixed liquor
Sour sodium, triethanolamine, sodium citrate and borax, further, add sodium pyrophosphate and disodium ethylene diamine tetraacetate thereto, from
And enable the table for effectively improving electronic jacquard machine with finishing agent by the electronic jacquard machine that above-mentioned material is mixed to prepare
Face brightness, and then its performance is greatly improved, reduce manual maintenance cost.
In a kind of preferred embodiment of the present invention, in step 1), the solvent is selected from water and/or ethanol.
The dosage of above-mentioned raw materials can select in wide scope, for example, in a kind of implementation being more highly preferred to of the present invention
In mode, in step 1), relative to the solvent of 1000 parts by weight, the dosage of the polyether-modified heptamethyltrisiloxane is
10-60 parts by weight, the dosage of the sodium dihydrogen phosphate is 5-30 parts by weight.
In further preferred embodiment, in step 2), relative to the mixed liquor M1 of 1000 parts by weight, the silicon
The dosage of sour sodium is 10-20 parts by weight, and the dosage of the triethanolamine is 5-15 parts by weight, and the dosage of the sodium citrate is
10-20 parts by weight, the dosage of the borax is 5-10 parts by weight.
The present invention another preferred embodiment in, in step 2), the mixed process include the first mixing section and
Second mixing section；
And first mixing section is mixed to be placed under conditions of temperature is 40-60 DEG C；
Second mixing section is mixed to be placed under conditions of temperature is 65-80 DEG C.
In a kind of preferred embodiment of the present invention, the incorporation time of first mixing section is 10-30min；
The incorporation time of second mixing section is 5-15min.
It is described relative to the mixture M 2 of 1000 parts by weight in step 3) in a kind of embodiment being more highly preferred to
The dosage of sodium pyrophosphate is 10-30 parts by weight, and the dosage of the disodium ethylene diamine tetraacetate is 5-20 parts by weight.
Present invention also offers a kind of electronic jacquard machine finishing agent according to made from preparation method described above.
The present invention will be described in detail by way of examples below.
Embodiment 1
1) under the conditions of existing for the water in 1000 parts by weight, by the polyether-modified heptamethyltrisiloxane of 10 parts by weight and 5 weights
The mixing of part sodium dihydrogen phosphate is measured, mixed liquor M1 is made；
2) 10 parts by weight sodium metasilicate, 5 parts by weight triethanolamines, 10 parts by weight are added into the mixed liquor M1 of 1000 parts by weight
After sodium citrate and 5 parts by weight boraxs are placed in temperature to carry out mixing 10min under conditions of 40 DEG C, then it is 65 DEG C to be placed in temperature
Under the conditions of carry out mixing 5min, be made mixture M 2；
3) 10 parts by weight sodium pyrophosphates and 5 parts by weight ethylenediamine tetra-acetic acids two are added into the mixture M 2 of 1000 parts by weight
Sodium, is made electronic jacquard machine finishing agent A1.
Embodiment 2
1) under the conditions of existing for the water in 1000 parts by weight, by the polyether-modified heptamethyltrisiloxane of 60 parts by weight and 30 weights
The mixing of part sodium dihydrogen phosphate is measured, mixed liquor M1 is made；
2) 20 parts by weight sodium metasilicate, 15 parts by weight triethanolamines, 20 weight are added into the mixed liquor M1 of 1000 parts by weight
After part sodium citrate and 10 parts by weight boraxs are placed in temperature to carry out mixing 30min under conditions of 60 DEG C, then temperature is placed in as 80
Mixing 15min is carried out under conditions of DEG C, mixture M 2 is made；
3) 30 parts by weight sodium pyrophosphates and 20 parts by weight ethylenediamine tetra-acetic acids are added into the mixture M 2 of 1000 parts by weight
Disodium, is made electronic jacquard machine finishing agent A2.
Embodiment 3
1) under the conditions of existing for the water in 1000 parts by weight, by the polyether-modified heptamethyltrisiloxane of 30 parts by weight and 20 weights
The mixing of part sodium dihydrogen phosphate is measured, mixed liquor M1 is made；
2) 15 parts by weight sodium metasilicate, 10 parts by weight triethanolamines, 15 weight are added into the mixed liquor M1 of 1000 parts by weight
After part sodium citrate and 8 parts by weight boraxs are placed in temperature to carry out mixing 20min under conditions of 50 DEG C, then temperature is placed in as 70 DEG C
Under conditions of carry out mixing 10min, be made mixture M 2；
3) 20 parts by weight sodium pyrophosphates and 10 parts by weight ethylenediamine tetra-acetic acids are added into the mixture M 2 of 1000 parts by weight
Disodium, is made electronic jacquard machine finishing agent A3.
Embodiment 4
It is prepared by the preparation method according to embodiment 1, unlike, the use of the polyether-modified heptamethyltrisiloxane
Measure as 5 parts by weight, the dosage of the sodium dihydrogen phosphate is 2 parts by weight, and electronic jacquard machine finishing agent A4 is made.
Embodiment 5
It is prepared by the preparation method according to embodiment 2, unlike, the dosage of the sodium metasilicate is 5 parts by weight, described
The dosage of triethanolamine is 2 parts by weight, and the dosage of the sodium citrate is 5 parts by weight, and the dosage of the borax is 2 parts by weight,
Electronic jacquard machine finishing agent A5 is made.
Embodiment 6
It is prepared by the preparation method according to embodiment 3, unlike, for be placed directly within temperature be 20 DEG C in step 2)
Under the conditions of mix 5min, electronic jacquard machine finishing agent A6 is made.
Comparative example 1
It is prepared by the preparation method according to embodiment 1, unlike, be added without polyether-modified heptamethyltrisiloxane and
Triethanolamine, is made brightener D1.
Comparative example 2
It is prepared by the preparation method according to embodiment 2, unlike, sodium citrate, borax and sodium pyrophosphate are added without,
Brightener D2 is made.
Test case
After above-mentioned A1-A6, D1 and D2 are soaked test piece respectively, test piece is cleaned, detects its brightness, then by above-mentioned examination
After piece is placed 1 month, its brightness is detected again, obtains that the results are shown in Table 1.
Table 1
| Numbering | Brightness | Brightness after 1 month |
| A1 | Strip is bright | Strip is bright |
| A2 | Strip is bright | Strip is bright |
| A3 | Strip is bright | Strip is bright |
| A4 | Strip is bright | It is more bright |
| A5 | Strip is bright | It is more bright |
| A6 | Strip is bright | It is more bright |
| D1 | Strip is more bright | It is silent |
| D2 | Strip is more bright | It is silent |
The preferred embodiment of the present invention described in detail above, still, during present invention is not limited to the embodiments described above
Detail, in the range of the technology design of the present invention, a variety of simple variants can be carried out to technical scheme, this
A little simple variants belong to protection scope of the present invention.
It is further to note that each particular technique feature described in above-mentioned embodiment, in not lance
In the case of shield, can be combined by any suitable means, in order to avoid unnecessary repetition, the present invention to it is various can
The combination of energy no longer separately illustrates.
In addition, various embodiments of the present invention can be combined randomly, as long as it is without prejudice to originally
The thought of invention, it should equally be considered as content disclosed in this invention.
Claims (8)
1. a kind of preparation method of electronic jacquard machine finishing agent, it is characterised in that the preparation method includes：
1) in the presence of a solvent, polyether-modified heptamethyltrisiloxane and sodium dihydrogen phosphate are mixed, mixed liquor is made
M1；
2) sodium metasilicate, triethanolamine, sodium citrate and borax are added into mixed liquor M1, mixture M 2 is made；
3) sodium pyrophosphate and disodium ethylene diamine tetraacetate, obtained electronic jacquard machine finishing agent are added into mixture M 2.
2. preparation method according to claim 1, wherein, in step 1), the solvent is selected from water and/or ethanol.
3. preparation method according to claim 1 or 2, wherein, in step 1), relative to the described molten of 1000 parts by weight
Agent, the dosage of the polyether-modified heptamethyltrisiloxane is 10-60 parts by weight, and the dosage of the sodium dihydrogen phosphate is 5-30 weights
Measure part.
4. preparation method according to claim 1 or 2, wherein, in step 2), relative to the mixing of 1000 parts by weight
Liquid M1, the dosage of the sodium metasilicate are 10-20 parts by weight, and the dosage of the triethanolamine is 5-15 parts by weight, the citric acid
The dosage of sodium is 10-20 parts by weight, and the dosage of the borax is 5-10 parts by weight.
5. preparation method according to claim 1 or 2, wherein, in step 2), the mixed process includes the first mixing section
With the second mixing section；
And first mixing section is mixed to be placed under conditions of temperature is 40-60 DEG C；
Second mixing section is mixed to be placed under conditions of temperature is 65-80 DEG C.
6. preparation method according to claim 5, wherein, the incorporation time of first mixing section is 10-30min；
The incorporation time of second mixing section is 5-15min.
7. preparation method according to claim 1 or 2, wherein, in step 3), relative to the mixing of 1000 parts by weight
Thing M2, the dosage of the sodium pyrophosphate is 10-30 parts by weight, and the dosage of the disodium ethylene diamine tetraacetate is 5-20 parts by weight.
8. electronic jacquard machine surface-brightening made from the preparation method in a kind of 1-7 according to claim described in any one
Agent.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711393008.9A CN108003795A (en) | 2017-12-21 | 2017-12-21 | Electronic jacquard machine finishing agent and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711393008.9A CN108003795A (en) | 2017-12-21 | 2017-12-21 | Electronic jacquard machine finishing agent and preparation method thereof |
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| CN108003795A true CN108003795A (en) | 2018-05-08 |
Family
ID=62060296
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|---|---|---|---|
| CN201711393008.9A Pending CN108003795A (en) | 2017-12-21 | 2017-12-21 | Electronic jacquard machine finishing agent and preparation method thereof |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102002722A (en) * | 2009-08-28 | 2011-04-06 | 比亚迪股份有限公司 | Stainless steel cleaner and stainless steel cleaning method |
| CN107012458A (en) * | 2017-04-27 | 2017-08-04 | 张家港乐嘉新能源科技有限公司 | Aluminium alloy pretreatment liquid and its application method |
| CN107366000A (en) * | 2017-08-01 | 2017-11-21 | 合肥择浚电气设备有限公司 | A kind of preparation method of cleaning agent for surface of metal product |
-
2017
- 2017-12-21 CN CN201711393008.9A patent/CN108003795A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102002722A (en) * | 2009-08-28 | 2011-04-06 | 比亚迪股份有限公司 | Stainless steel cleaner and stainless steel cleaning method |
| CN107012458A (en) * | 2017-04-27 | 2017-08-04 | 张家港乐嘉新能源科技有限公司 | Aluminium alloy pretreatment liquid and its application method |
| CN107366000A (en) * | 2017-08-01 | 2017-11-21 | 合肥择浚电气设备有限公司 | A kind of preparation method of cleaning agent for surface of metal product |
Non-Patent Citations (1)
| Title |
|---|
| 唐春华: "现代镀覆技术 第一部分――镀覆前处理", 《电镀与涂饰》 * |
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Application publication date: 20180508 |
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