CN107998057A - A kind of preparation method of antibacterial moisturizing lactalbumin polysaccharide lipstick - Google Patents
A kind of preparation method of antibacterial moisturizing lactalbumin polysaccharide lipstick Download PDFInfo
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- CN107998057A CN107998057A CN201711274438.9A CN201711274438A CN107998057A CN 107998057 A CN107998057 A CN 107998057A CN 201711274438 A CN201711274438 A CN 201711274438A CN 107998057 A CN107998057 A CN 107998057A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
- A61K8/988—Honey; Royal jelly, Propolis
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/676—Ascorbic acid, i.e. vitamin C
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/927—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of insects, e.g. shellac
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/001—Preparations for care of the lips
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/81—Preparation or application process involves irradiation
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
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Abstract
The invention discloses a kind of preparation method of antibacterial moisturizing lactalbumin polysaccharide lipstick, after the fresh old leaf of Ilex Latifolia Thunb is cleaned after roller fixation and microwave high-temperature water-removing, high-temperature sterilization low temperature drying, immersion is heated after ultramicro grinding in sodium citrate aqueous solution, cellulase is added and is digested, ultrasonic wave assisted extraction, repeatedly centrifuge filtrate, merging filtrate, crystallisation by cooling freeze compound with lactalbumin, xanthans, have added base oil, the mixture such as beeswax afterwards both.Lipstick prepared by present invention lubrication sense is good, has no adverse reaction to skin, and it is strong to carry out moisturizing antibacterial, moistens lip, can effectively avoid the generation of cheilitis.
Description
Technical field
The invention belongs to daily-use chemical industry processing technique field, and in particular to a kind of antibacterial moisturizing lactalbumin polysaccharide lipstick
Preparation method.
Background technology
Ilex Latifolia Thunb is Aquifoliaceae Ilex latifolia Thunb kind aiphyllium, have clearing away heat and removing summer, eyesight-improving intelligence-developing, promote the production of body fluid to quench thirst,
The multiple efficacies such as diuresis cardiac stimulant, the cough-relieving that wets one's whistle, decompression weight-reducing, suppression cancer anti-cancer, anti-aging, promoting blood circulation arteries and veins.In recent years, to Ilex Latifolia Thunb
Research focuses mostly in terms of being processed into and sampling tea with the nutrition and health care such as tea beverage, successfully have developed bag bubble Ilex Latifolia Thunb, bitter leaves
The plurality kinds of health care food such as tea electuary, buccal lozenge of lectuce tea, compound Ilex Latifolia Thunb.The current cultivation in relation to Ilex Latifolia Thunb, processing, physiology life
Change and the research of application etc. be very active, but it is finished, deep processing, trade and Physiology and biochemistry mechanism is especially to hardship
The research of the functional component of fourth tea need further further investigated, to promote the development of the bitter leaves tea beverage utilization of resources.
The content of the invention
The present invention provides a kind of preparation method of antibacterial moisturizing lactalbumin polysaccharide lipstick, lipstick lubrication prepared by the present invention
Sense is good, has no adverse reaction to skin, and it is strong to carry out moisturizing antibacterial, moistens lip, can effectively avoid the generation of cheilitis.
The present invention is achieved by the following technical solutions:
A kind of preparation method of antibacterial moisturizing lactalbumin polysaccharide lipstick, it is characterised in that it is prepared by following steps:
(1)Ilex Latifolia Thunb is processed
Pass through successively after the fresh old leaf of 30-45 parts by weight Ilex Latifolia Thunbs is cleaned in the clear water of the powder of parts by weight of sucrose containing 2-5
In roller fixation machine, after obtaining blank after microwave high-temperature water-removing, it is put into sterilizing, drying equipment, first 115-125 DEG C of high-temperature sterilization
30-120s, is then cooled to rapidly less than 80 DEG C, low temperature drying is stand-by;
(2)Digest Ilex Latifolia Thunb
By step(1)Add 10-30 times of water and 1-2 parts by weight of lemon acid sodium, 40-50 DEG C of bar after the Ilex latifolia tea-leaf ultramicro grinding of gained
It is cooled to room temperature when processing 2-3 is small under part, adds 0.5-1 part by weight of cellulose enzymes, adjusting pH is 9-10, is placed at 20-60 DEG C
In processor for ultrasonic wave, 30-50KHz ultrasonic wave extractions 20-50 minutes, after cooling, centrifuge filtrate, lower sediment are added
Continue with the water of same volume, be so repeated 2 times, merging filtrate is stand-by;
(3)Crystallization and mixture recombination reaction
By step(2)Gains are placed in ice-water bath, are stood still for crystals, low temperature drying, are carried out after freezing, and crush and 5-15 is heavy
Part lactalbumin is measured, 10-20 parts by weight xanthans pours into 30-50 parts by weight water together, and magnetic agitation 2-4 is small at room temperature
When, 50-80 DEG C of microwave treatment after 2-5 minutes by mixed liquor carry out cryogenic freezing 6-12 it is small when, it is stand-by after defrosting;
(4)The preparation of lipstick
Under the conditions of 20-30 parts by weight of base oil and 2-5 parts by weight beeswaxs are blended in 80-90 DEG C after heating and melting, slowly with step
Suddenly(3)Gains are thoroughly mixed, and are persistently stirred 3-5 minutes, add 10-15 parts by weight vitamin Cs, 10-15 parts by weight honey
With 2-3 parts by weight fruit essences, be dried after mixing de-bubbled 1-3 it is small when, it is filling after low temperature solidification both antibacterial guarantor
Wet lactalbumin polysaccharide lipstick.
The water-removing is that Ilex Latifolia Thunb is put into 155-175 DEG C of water-removing in roller fixation machine to handle 2-5 minutes, room temperature spreading for cooling
5-15 minutes, it is delivered to microwave de-enzyming machine and carries out secondary water-removing, 180-200 DEG C of fixation time 2-5 minutes.
The high-temperature sterilization temperature is 130-140 DEG C, and sterilization time is 30-90 seconds, and low temperature drying temperature is 50-60
DEG C, when the time is 4-6 small, freeze to be refrigerated to -10--20 DEG C, in 20-30Pa, 20-40 DEG C of heating is until distillation terminates.
Base oil used is the one or more in olive oil, wheat-germ oil, coconut oil, Sweet Almond Oil and shea butter
Mixture.
It is an advantage of the invention that:
The present invention is by after roller fixation and microwave high-temperature water-removing, high-temperature sterilization low temperature is done after the fresh old leaf cleaning of Ilex Latifolia Thunb
It is dry, immersion is heated after ultramicro grinding in sodium citrate aqueous solution, cellulase is added and is digested, ultrasonic wave assisted extraction,
Repeatedly centrifuge filtrate, merging filtrate, crystallisation by cooling freeze it is compound with lactalbumin, xanthans, afterwards addition base oil, bee
The mixtures such as wax both obtained.Roller fixation causes tea aroma to be molded and promotes non-enzymatic chemical reaction, and microwave de-enzyming reduces bitter leaves
The bitter taste of tea, using ultrasonic wave added enzymolysis can more leniently decompose Ilex Latifolia Thunb tissue the characteristics of, can extract to greatest extent
Component is imitated, significantly shortens extraction time, recovery rate can be greatly improved, be polysaccharide in treated obtained extract, polyphenol
Interaction occurs between unrighted acid, with lactalbumin when heated molecule and forms gel, adding xanthans can
Heat-induced gelation plastic characteristic is influenced, forms firmer gel, it is natural products to prepare most raw material during lipstick,
Water content is high, there is good water lock moisture-keeping functions, and whey protein-stabilized is distributed in lipstick, have it is anti-oxidant, eliminate or
Inhibit bacteria, promote normal cell growth, lipstick lubrication sense prepared by the present invention is good, has no adverse reaction, can carry out to skin
Moisturizing antibacterial is strong, moistens lip, can effectively avoid the generation of cheilitis.
Embodiment
A kind of preparation method of antibacterial moisturizing lactalbumin polysaccharide lipstick, it is characterised in that its by following steps prepare and
Into:
(1)Ilex Latifolia Thunb is processed
Killed successively by roller after the 40 fresh old leafs of parts by weight Ilex Latifolia Thunb are cleaned in the clear water containing 3 parts by weight of sucrose powder
In blue or green machine, after obtaining blank after microwave high-temperature water-removing, it is put into sterilizing, drying equipment, first 120 DEG C of high-temperature sterilizations 60s, Ran Houxun
Speed is cooled to less than 80 DEG C, and low temperature drying is stand-by;
(2)Digest Ilex Latifolia Thunb
By step(1)Add 20 times of water and 1.5 parts by weight of lemon acid sodium after the Ilex latifolia tea-leaf ultramicro grinding of gained, locate under the conditions of 45 DEG C
Manage 2.5 it is small when be cooled to room temperature, add 0.8 part by weight of cellulose enzyme, adjusting pH is 9-10, and processor for ultrasonic wave is placed at 40 DEG C
In, 40KHz ultrasonic wave extractions 30 minutes, after cooling, centrifuge filtrate, lower sediment are added in the water of same volume and is continued
Processing, is so repeated 2 times, merging filtrate is stand-by;
(3)Crystallization and mixture recombination reaction
By step(2)Gains are placed in ice-water bath, are stood still for crystals, low temperature drying, are carried out after freezing, and crush and 10 weight
Part lactalbumin, 15 parts by weight xanthans pour into 35 parts by weight water together, when magnetic agitation 3 is small at room temperature, 60 DEG C of microwaves
Processing 3 minutes after by mixed liquor carry out cryogenic freezing 10 it is small when, it is stand-by after defrosting;
(4)The preparation of lipstick
Under the conditions of 25 parts by weight of base oil and 3 parts by weight beeswaxs are blended in 85 DEG C after heating and melting, slowly and step(3)Gained
Thing is thoroughly mixed, and is persistently stirred 4 minutes, adds 12 parts by weight vitamin Cs, and 12 parts by weight honey and 2.5 weight fruits are fragrant
Essence, be dried after mixing de-bubbled 2 it is small when, it is filling after low temperature solidification both antibacterial moisturizing lactalbumin polysaccharide lipstick.
The water-removing is that Ilex Latifolia Thunb is put into 160 DEG C of water-removings in roller fixation machine to handle 3 minutes, and room temperature spreading for cooling 10 divides
Clock, is delivered to microwave de-enzyming machine and carries out secondary water-removing, 190 DEG C of fixation times 3 minutes.
The high-temperature sterilization temperature is 135 DEG C, and sterilization time is 60 seconds, and low temperature drying temperature is 55 DEG C, and the time is small for 5
When, freeze to be refrigerated to -15 DEG C, in 25Pa, 30 DEG C of heating is until distillation terminates.
Base oil used is the one or more in olive oil, wheat-germ oil, coconut oil, Sweet Almond Oil and shea butter
Mixture.
Claims (4)
1. a kind of preparation method of antibacterial moisturizing lactalbumin polysaccharide lipstick, it is characterised in that it is prepared by following steps:
(1)Ilex Latifolia Thunb is processed
Pass through successively after the fresh old leaf of 30-45 parts by weight Ilex Latifolia Thunbs is cleaned in the clear water of the powder of parts by weight of sucrose containing 2-5
In roller fixation machine, after obtaining blank after microwave high-temperature water-removing, it is put into sterilizing, drying equipment, first 115-125 DEG C of high-temperature sterilization
30-120s, is then cooled to rapidly less than 80 DEG C, low temperature drying is stand-by;
(2)Digest Ilex Latifolia Thunb
By step(1)Add 10-30 times of water and 1-2 parts by weight of lemon acid sodium, 40-50 DEG C of bar after the Ilex latifolia tea-leaf ultramicro grinding of gained
It is cooled to room temperature when processing 2-3 is small under part, adds 0.5-1 part by weight of cellulose enzymes, adjusting pH is 9-10, is placed at 20-60 DEG C
In processor for ultrasonic wave, 30-50KHz ultrasonic wave extractions 20-50 minutes, after cooling, centrifuge filtrate, lower sediment are added
Continue with the water of same volume, be so repeated 2 times, merging filtrate is stand-by;
(3)Crystallization and mixture recombination reaction
By step(2)Gains are placed in ice-water bath, are stood still for crystals, low temperature drying, are carried out after freezing, and crush and 5-15 is heavy
Part lactalbumin is measured, 10-20 parts by weight xanthans pours into 30-50 parts by weight water together, and magnetic agitation 2-4 is small at room temperature
When, 50-80 DEG C of microwave treatment after 2-5 minutes by mixed liquor carry out cryogenic freezing 6-12 it is small when, it is stand-by after defrosting;
(4)The preparation of lipstick
Under the conditions of 20-30 parts by weight of base oil and 2-5 parts by weight beeswaxs are blended in 80-90 DEG C after heating and melting, slowly with step
Suddenly(3)Gains are thoroughly mixed, and are persistently stirred 3-5 minutes, add 10-15 parts by weight vitamin Cs, 10-15 parts by weight honey
With 2-3 parts by weight fruit essences, be dried after mixing de-bubbled 1-3 it is small when, it is filling after low temperature solidification both antibacterial guarantor
Wet lactalbumin polysaccharide lipstick.
A kind of 2. preparation method of antibacterial moisturizing lactalbumin polysaccharide lipstick according to claim 1, it is characterised in that institute
The water-removing stated is that Ilex Latifolia Thunb is put into 155-175 DEG C of water-removing in roller fixation machine to handle 2-5 minutes, room temperature spreading for cooling 5-15 minutes,
It is delivered to microwave de-enzyming machine and carries out secondary water-removing, 180-200 DEG C of fixation time 2-5 minutes.
A kind of 3. preparation method of antibacterial moisturizing lactalbumin polysaccharide lipstick according to claim 1, it is characterised in that institute
The high-temperature sterilization temperature stated is 130-140 DEG C, and sterilization time is 30-90 seconds, and low temperature drying temperature is 50-60 DEG C, time 4-6
Hour, freeze to be refrigerated to -10--20 DEG C, in 20-30Pa, 20-40 DEG C of heating is until distillation terminates.
A kind of 4. preparation method of antibacterial moisturizing lactalbumin polysaccharide lipstick according to claim 1, it is characterised in that institute
It is one or more of mixtures in olive oil, wheat-germ oil, coconut oil, Sweet Almond Oil and shea butter with base oil.
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CN201711274438.9A CN107998057A (en) | 2017-12-06 | 2017-12-06 | A kind of preparation method of antibacterial moisturizing lactalbumin polysaccharide lipstick |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109010117A (en) * | 2018-07-10 | 2018-12-18 | 山西医科大学 | A kind of micro emulsion gel lip care gel and preparation method thereof with moist moisture-keeping function |
CN111961226A (en) * | 2019-05-20 | 2020-11-20 | 财团法人食品工业发展研究所 | Process for preparing whey protein gels |
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CN103040699A (en) * | 2012-12-14 | 2013-04-17 | 吴江市德佐日用化学品有限公司 | Moisturizing antibacterial lipstick |
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CN106491420A (en) * | 2016-10-26 | 2017-03-15 | 华南农业大学 | Lipstick rich in oil tea main component and preparation method thereof |
JP2017101006A (en) * | 2015-12-04 | 2017-06-08 | 一丸ファルコス株式会社 | Glycerol production enhancer derived from staphylococcus-epidermidis, antimicrobial peptide production enhancer derived from skin epidermal keratinocyte, and their application to external preparations for skin protection |
CN107125372A (en) * | 2017-07-10 | 2017-09-05 | 柴华 | The preparation method of Ilex Latifolia Thunb leaf of Moringa composite instant tea powder |
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CN102458139A (en) * | 2009-04-30 | 2012-05-16 | 奥普蒂森斯有限公司 | Concentrated, creamy to solid and dry compositions of oil-in-water emulsion, method for production thereof and use thereof for producing improved foods in terms of sensory aspects and nutrition physiology |
CN103169626A (en) * | 2011-12-26 | 2013-06-26 | 日本乐敦制药株式会社 | Stabilizing method for external composition |
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CN106491420A (en) * | 2016-10-26 | 2017-03-15 | 华南农业大学 | Lipstick rich in oil tea main component and preparation method thereof |
CN107125372A (en) * | 2017-07-10 | 2017-09-05 | 柴华 | The preparation method of Ilex Latifolia Thunb leaf of Moringa composite instant tea powder |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
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CN109010117A (en) * | 2018-07-10 | 2018-12-18 | 山西医科大学 | A kind of micro emulsion gel lip care gel and preparation method thereof with moist moisture-keeping function |
CN109010117B (en) * | 2018-07-10 | 2021-05-25 | 山西医科大学 | Micro-emulsion gel lip-protecting gel with moisturizing and moisturizing effects and preparation method thereof |
CN111961226A (en) * | 2019-05-20 | 2020-11-20 | 财团法人食品工业发展研究所 | Process for preparing whey protein gels |
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