CN107980775A - It is a kind of to utilize method of the bamboo vinegar extraction with disease-preventing and yield-increasing functional preparation - Google Patents
It is a kind of to utilize method of the bamboo vinegar extraction with disease-preventing and yield-increasing functional preparation Download PDFInfo
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- CN107980775A CN107980775A CN201711326678.9A CN201711326678A CN107980775A CN 107980775 A CN107980775 A CN 107980775A CN 201711326678 A CN201711326678 A CN 201711326678A CN 107980775 A CN107980775 A CN 107980775A
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- bamboo vinegar
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/02—Saturated carboxylic acids or thio analogues thereof; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N29/00—Biocides, pest repellants or attractants, or plant growth regulators containing halogenated hydrocarbons
- A01N29/04—Halogen directly attached to a carbocyclic ring system
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N31/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic oxygen or sulfur compounds
- A01N31/08—Oxygen or sulfur directly attached to an aromatic ring system
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N31/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic oxygen or sulfur compounds
- A01N31/08—Oxygen or sulfur directly attached to an aromatic ring system
- A01N31/16—Oxygen or sulfur directly attached to an aromatic ring system with two or more oxygen or sulfur atoms directly attached to the same aromatic ring system
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N35/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having two bonds to hetero atoms with at the most one bond to halogen, e.g. aldehyde radical
- A01N35/04—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having two bonds to hetero atoms with at the most one bond to halogen, e.g. aldehyde radical containing aldehyde or keto groups, or thio analogues thereof, directly attached to an aromatic ring system, e.g. acetophenone; Derivatives thereof, e.g. acetals
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- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- Agronomy & Crop Science (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Plant Pathology (AREA)
- Pest Control & Pesticides (AREA)
- Medicines Containing Plant Substances (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
Abstract
A kind of method using bamboo vinegar extraction with disease-preventing and yield-increasing functional preparation, the bamboo vinegar is by three-stage filtration, distillation and refines；Component content and proportioning in solution of the bamboo vinegar after three-stage filtration are 10 15 parts of 10 20 parts of butyric acid, 56 parts of metacresol, 8 15 parts of guaiacol, 5 10 parts of xylenol, 6 12 parts of M-and P-cresols, 10 15 parts of ethyl -phenol, 8 15 parts of xylenol, 15 20 parts of 2 methoxyl group, 5 methylphenol, 10 15 part, chlorobenzyl chloride, 15 20 parts of vanillic aldehyde, 10 15 parts of trimethoxytoluene, 10 20 parts of catechol and 2 methoxyl group, 4 methylphenol；Therefore, the present invention has the advantages that preventing disease production-increasing effect is good, extraction facilitates, fungistatic effect is notable, pure natural extraction, ecological, environmental protective, green and healthy.
Description
Technical field
The invention belongs to bamboo vinegar technical field, and in particular to one kind has the function of disease-preventing and yield-increasing system using bamboo vinegar extraction
The method of agent.
Background technology
Bamboo vinegar is to collect the gas that bamboo wood produces in pyrolytic during being made charcoal with bamboo wood, and by this gas
The body liquid substance that high pressure cools down at normal temperatures, bamboo vinegar contain nearly 300 kinds of natural polymer organic compounds, containing having
Machine acids, alcohols, ketone, aldehydes, phenols, esters and micro alkaline components etc., part phenols, acids and ketone in bamboo vinegar
Class has the function that to sterilize and promote plant growth；The present invention is to provide a kind of liquid mixing to plant with disease-preventing and yield-increasing
Thing, and the source of this liquid mixture is bamboo vinegar, is the extracting liq mixture from bamboo vinegar, meets the new agriculture of China
The trend of industry sustainable development；Therefore, develop that a kind of preventing disease production-increasing effect is good, extraction is convenient, fungistatic effect is notable, pure natural carries
Take, ecological, environmental protective, it is green and healthy using bamboo vinegar extract the method with disease-preventing and yield-increasing functional preparation with highly important
Strategic importance.
The content of the invention
The purpose of the invention is to overcome the deficiencies in the prior art, and provide that a kind of preventing disease production-increasing effect is good, extraction side
Just, fungistatic effect is notable, pure natural extraction, ecological, environmental protective, green and healthy has the function of disease-preventing and yield-increasing using bamboo vinegar extraction
The method of preparation.
The object of the present invention is achieved like this：It is a kind of to utilize side of the bamboo vinegar extraction with disease-preventing and yield-increasing functional preparation
Method, the bamboo vinegar is by three-stage filtration, distillation and refines.
Component content and proportioning in solution of the bamboo vinegar after three-stage filtration are 10-20 parts of butyric acid, metacresol
5-6 parts, 8-15 parts of guaiacol, 5-10 parts of xylenol, 6-12 parts of M-and P-cresols, 10-15 parts of ethyl -phenol, xylenol 8-
15 parts, 10-15 parts of 2- methoxyl group -5- methylphenols, 15-20 parts of a chlorobenzyl chloride, 15-20 parts of vanillic aldehyde, trimethoxytoluene 10-
10-15 parts of 15 parts, 10-20 parts of catechol and 2- methoxyl groups -4- methylphenols.
The xylenol is divided into 40-60 parts of 30-60 parts of 2,5- xylenols and 2,6 xylenol.
The ethyl -phenol is 30-50 parts of 4- ethyl -phenols, xylenol 2,40-60 parts of 3- xylenols.
Solution after the three-stage filtration contains 5-10 parts of cyclopentanone, 15-20 parts of 2- cyclopentenones, chaff after distillation
15-25 parts of aldehyde, 10-15 parts of furancarbinol, 8-15 parts of butyric acid, 8-15 parts of isobutyric acid, 10-20 parts of vanillic aldehyde, trimethoxytoluene
10-15 parts, 10-15 parts of xylenol.
The furancarbinol is 3- furancarbinols.
Solution after the distillation contains 8-15 parts of vanillic aldehyde, 8-15 parts of trimethoxytoluene, butyric acid 8- after refined
20 parts, 8-15 parts of 2- cyclopentenones, 10-25 parts of guaiacol, 10-25 parts of xylenol.
10 parts of vanillic aldehyde in solution after refined, 10 parts of trimethoxytoluene, 10 parts of butyric acid, 10 parts of 2- cyclopentenones, more
Wooden 20 parts of the phenol of wound, 20 parts of xylenol, remaining component is water, is mixed to form liquid mixture.
The three-stage filtration is using the 0.1mol/ml2,2- diphenyl -1- picryl hydrazines that 50ml is added in 500ml solution
The standard reagent of base is extracted.
The peroxidating with being calculated as 0.1~20% by liquid to be treated weight or volume is added in solution after the distillation
Aqueous solution of hydrogen obtains refined liquid.
Beneficial effects of the present invention：Principle in the present invention is after bamboo vinegar passes through three-stage filtration, distillation and refines, to obtain
To the liquid mixture for being conducive to plant production and diseases prevention, 10 parts of vanillic aldehyde, trimethoxy first in the solution after refined
10 parts of benzene, 10 parts of butyric acid, 10 parts of 2- cyclopentenones, 20 parts of guaiacol, 20 parts of xylenol, remaining component are water, mixing
Form liquid mixture；The vanillic aldehyde high purity 9% so drawn, the purity of trimethoxytoluene reach the purity of 9%, butyric acid
Reach the 9%, purity of 2- cyclopentenones and reach the purity of 9%, guaiacol and reach the purity of 18%, xylenol and reach 18%；
And vanillic aldehyde, trimethoxytoluene, butyric acid, 2- cyclopentenones, guaiacol, the stability of xylenol are stronger, mutually
Between compatibility it is also very strong；Wherein, the effect of vanillic aldehyde is to promote plant growth, and has certain bactericidal effect；Three
The effect of methoxy toluene is to be conducive to the antibacterial synergy of plant；The effect of guaiacol is bactericidal yield-increase, is given birth to available for pesticide
The intermediate of production；The effect of xylenol is to be used for pesticide aspect, disease-resistant beneficial to plant yield-increasing；The effect of butyric acid is favorably
It is active in liquid mixture, it is a kind of activating agent；Therefore, the present invention is with preventing disease production-increasing effect is good, extraction is convenient, antibacterial
Significant effect, pure natural extraction, ecological, environmental protective, it is green and healthy the advantages of.
Embodiment
It is a kind of using bamboo vinegar extraction with disease-preventing and yield-increasing functional preparation method, the bamboo vinegar by three-stage filtration,
Distill and refined；Component content and proportioning in solution of the bamboo vinegar after three-stage filtration are 10-20 parts of butyric acid, a first
5-6 parts of phenol, 8-15 parts of guaiacol, 5-10 parts of xylenol, 6-12 parts of M-and P-cresols, 10-15 parts of ethyl -phenol, xylenol
8-15 parts, 10-15 parts of 2- methoxyl group -5- methylphenols, 15-20 parts of a chlorobenzyl chloride, 15-20 parts of vanillic aldehyde, trimethoxytoluene
10-15 parts of 10-15 parts, 10-20 parts of catechol and 2- methoxyl groups -4- methylphenols；The xylenol is divided into 2,5- bis-
Methylphenol and 2,6 xylenols；The ethyl -phenol is 4- ethyl -phenols, xylenol 2,3- xylenols；The three-level
Solution after filtering contains 5-10 parts of cyclopentanone, 15-20 parts of 2- cyclopentenones, 15-25 parts of furfural, furans first after distillation
10-15 parts of alcohol, 8-15 parts of butyric acid, 8-15 parts of isobutyric acid, 10-20 parts of vanillic aldehyde, 10-15 parts of trimethoxytoluene, dimethyl benzene
10-15 parts of phenol；The furancarbinol is 3- furancarbinols；Solution after the distillation contains vanillic aldehyde 8-15 after refined
Part, 8-15 parts of trimethoxytoluene, 8-20 parts of butyric acid, 8-15 parts of 2- cyclopentenones, 10-25 parts of guaiacol, xylenol
10-25 parts；10 parts of vanillic aldehyde in solution after refined, 10 parts of trimethoxytoluene, 10 parts of butyric acid, 10 parts of 2- cyclopentenones, more
Wooden 20 parts of the phenol of wound, 20 parts of xylenol, remaining component is water, is mixed to form liquid mixture；What the three-stage filtration used
It is that the standard reagent of 0.1mol/ml2,2- diphenyl -1- picrylhydrazyls that 50ml is added in 500ml solution is extracted；It is described
Add in solution after distillation and obtained with being calculated as 0.1~20% aqueous hydrogen peroxide solution by liquid to be treated weight or volume
Refined liquid.
Purpose in the present invention is to produce the liquid mixture for being conducive to plant yield-increasing and diseases prevention, the liquid mixture
There is sterilization, volume increase and diseases prevention, specific inventive principle be bamboo vinegar by three-stage filtration, distillation and it is refined after,
Obtain being conducive to plant growth and the liquid mixture of diseases prevention, vanillic aldehyde, trimethoxy are contained in the solution by being refining to obtain
Base toluene, butyric acid, 2- cyclopentenones, guaiacol, xylenol, wherein, the effect of vanillic aldehyde is to promote plant growth, and
And there is certain bactericidal effect；The effect of trimethoxytoluene is to be conducive to the antibacterial synergy of plant；The effect of guaiacol is
Bactericidal yield-increase, the intermediate available for pesticide producing；The effect of xylenol is in terms of being used for pesticide, to resist beneficial to plant yield-increasing
Disease；The effect of butyric acid is to be conducive to liquid mixture active, is a kind of activating agent；Specifically it act as：To plant and
The tissue of animal has good permeability and absorbability；Bamboo vinegar can also play the role of in terms of adjusting growth, to crop
A certain amount of bamboo vinegar is added, then can play and promote plant establishment, germination, growth, the effect for making the taste of fruit improve；Cause
This, the present invention has that preventing disease production-increasing effect is good, extraction is convenient, fungistatic effect is notable, pure natural extraction, ecological, environmental protective, green are good for
The advantages of health.
Embodiment is unrestricted to further explanation of the invention, is existed for those of ordinary skills
Further conversion is done in the case of not departing from substantive content of the present invention to structure, and all these conversion should all belong to institute of the present invention
Attached scope of the claims.
Claims (10)
1. a kind of utilize method of the bamboo vinegar extraction with disease-preventing and yield-increasing functional preparation, it is characterised in that：The bamboo vinegar passes through
Three-stage filtration, distillation and refined.
2. according to a kind of method using bamboo vinegar extraction with disease-preventing and yield-increasing functional preparation in claim 1, its feature exists
In：Component content in solution of the bamboo vinegar after three-stage filtration and proportioning are 10-20 parts of butyric acid, 5-6 parts of metacresol,
8-15 parts of guaiacol, 5-10 parts of xylenol, 6-12 parts of M-and P-cresols, 10-15 parts of ethyl -phenol, 8-15 parts of xylenol,
10-15 parts of 2- methoxyl group -5- methylphenols, 15-20 parts of a chlorobenzyl chloride, 15-20 parts of vanillic aldehyde, 10-15 parts of trimethoxytoluene,
10-15 parts of 10-20 parts of catechol and 2- methoxyl groups -4- methylphenols.
3. according to a kind of method using bamboo vinegar extraction with disease-preventing and yield-increasing functional preparation in claim 2, its feature exists
In：The xylenol is divided into 40-60 parts of 30-60 parts of 2,5- xylenols and 2,6 xylenol.
4. according to a kind of method using bamboo vinegar extraction with disease-preventing and yield-increasing functional preparation in claim 2, its feature exists
In：The ethyl -phenol is 30-50 parts of 4- ethyl -phenols, xylenol 2,40-60 parts of 3- xylenols.
5. according to a kind of method using bamboo vinegar extraction with disease-preventing and yield-increasing functional preparation in claim 2, its feature exists
In：Solution after the three-stage filtration contains 5-10 parts of cyclopentanone, 15-20 parts of 2- cyclopentenones, furfural 15- after distillation
25 parts, 10-15 parts of furancarbinol, 8-15 parts of butyric acid, 8-15 parts of isobutyric acid, 10-20 parts of vanillic aldehyde, trimethoxytoluene 10-15
Part, 10-15 parts of xylenol.
6. according to a kind of method using bamboo vinegar extraction with disease-preventing and yield-increasing functional preparation in claim 5, its feature exists
In：The furancarbinol is 3- furancarbinols.
7. according to a kind of method using bamboo vinegar extraction with disease-preventing and yield-increasing functional preparation in claim 1, its feature exists
In：Solution after the distillation after refined containing 8-15 parts of vanillic aldehyde, 8-15 parts of trimethoxytoluene, 8-20 parts of butyric acid,
8-15 parts of 2- cyclopentenones, 10-25 parts of guaiacol, 10-25 parts of xylenol.
8. according to a kind of method using bamboo vinegar extraction with disease-preventing and yield-increasing functional preparation in claim 7, its feature exists
In：10 parts of vanillic aldehyde, 10 parts of trimethoxytoluene, 10 parts of butyric acid, 10 parts of 2- cyclopentenones, guaiacol in solution after refined
20 parts, 20 parts of xylenol, remaining component are water, are mixed to form liquid mixture.
9. according to a kind of method using bamboo vinegar extraction with disease-preventing and yield-increasing functional preparation in claim 2, its feature exists
In：The three-stage filtration is using the 0.1mol/ml2,2- diphenyl -1- picrylhydrazyls that 50ml is added in 500ml solution
Standard reagent is extracted.
10. according to a kind of method using bamboo vinegar extraction with disease-preventing and yield-increasing functional preparation in claim 5, its feature exists
In：Addition is water-soluble with being calculated as 0.1~20% hydrogen peroxide by liquid to be treated weight or volume in solution after the distillation
Liquid obtains refined liquid.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711326678.9A CN107980775A (en) | 2017-12-13 | 2017-12-13 | It is a kind of to utilize method of the bamboo vinegar extraction with disease-preventing and yield-increasing functional preparation |
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| CN201711326678.9A CN107980775A (en) | 2017-12-13 | 2017-12-13 | It is a kind of to utilize method of the bamboo vinegar extraction with disease-preventing and yield-increasing functional preparation |
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| CN201711326678.9A Pending CN107980775A (en) | 2017-12-13 | 2017-12-13 | It is a kind of to utilize method of the bamboo vinegar extraction with disease-preventing and yield-increasing functional preparation |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113057162A (en) * | 2021-03-29 | 2021-07-02 | 山东农业大学 | Application of 4-ethylphenol in prevention and treatment of tobacco black shank |
| CN114062528A (en) * | 2020-07-29 | 2022-02-18 | 丘比株式会社 | Vinegar, food and drink, method for imparting smoke aroma, and method for masking unpleasant odor |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1616600A (en) * | 2003-11-13 | 2005-05-18 | 丽水市森得立生物农业研发有限公司 | Method for highly refining wood and bamboo vinegar liquid |
| CN1687311A (en) * | 2005-04-10 | 2005-10-26 | 张江兴 | Method for preparing bamboo vinegar |
| CN1715367A (en) * | 2004-06-28 | 2006-01-04 | 刘远胜 | Process for producing pyroligneous liquor |
| CN101130103A (en) * | 2007-08-03 | 2008-02-27 | 浙江省林业科学研究院 | Highly effective composite type foreign smell eliminating agent containing wood, bamboo vinegar liquid extractive |
| CN101538474A (en) * | 2009-03-20 | 2009-09-23 | 西北农林科技大学 | Method for preparing pyroligneous by utilizing apricot shells |
| CN102021012A (en) * | 2010-12-15 | 2011-04-20 | 安徽省石台县牯牛降竹炭制品有限责任公司 | Preparation method of bamboo vinegar |
-
2017
- 2017-12-13 CN CN201711326678.9A patent/CN107980775A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1616600A (en) * | 2003-11-13 | 2005-05-18 | 丽水市森得立生物农业研发有限公司 | Method for highly refining wood and bamboo vinegar liquid |
| CN1715367A (en) * | 2004-06-28 | 2006-01-04 | 刘远胜 | Process for producing pyroligneous liquor |
| CN1687311A (en) * | 2005-04-10 | 2005-10-26 | 张江兴 | Method for preparing bamboo vinegar |
| CN101130103A (en) * | 2007-08-03 | 2008-02-27 | 浙江省林业科学研究院 | Highly effective composite type foreign smell eliminating agent containing wood, bamboo vinegar liquid extractive |
| CN101538474A (en) * | 2009-03-20 | 2009-09-23 | 西北农林科技大学 | Method for preparing pyroligneous by utilizing apricot shells |
| CN102021012A (en) * | 2010-12-15 | 2011-04-20 | 安徽省石台县牯牛降竹炭制品有限责任公司 | Preparation method of bamboo vinegar |
Non-Patent Citations (6)
| Title |
|---|
| 吴哲洙等: "木醋液精制方法的探讨", 《延边大学学报（自然科学版）》 * |
| 庄晓伟等: "精制处理前后竹醋液组分及其含量的分析", 《林产化工通讯》 * |
| 张宏等: "2种精制竹醋液组分及含量的分析比较", 《竹子研究汇刊》 * |
| 张文标 等: "不同收集温度的竹醋液组分及其形成过程分析", 《竹子研究汇刊》 * |
| 张文标 等: "不同竹种竹醋液组分分析", 《世界竹藤通讯》 * |
| 张文标等: "竹醋液的组分分析", 《竹子研究汇刊》 * |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114062528A (en) * | 2020-07-29 | 2022-02-18 | 丘比株式会社 | Vinegar, food and drink, method for imparting smoke aroma, and method for masking unpleasant odor |
| CN114062528B (en) * | 2020-07-29 | 2023-10-20 | 丘比株式会社 | Vinegar, food and drink, method for giving fumigated aroma, and method for masking unpleasant odor |
| CN113057162A (en) * | 2021-03-29 | 2021-07-02 | 山东农业大学 | Application of 4-ethylphenol in prevention and treatment of tobacco black shank |
| CN113057162B (en) * | 2021-03-29 | 2022-02-08 | 山东农业大学 | Application of 4-ethylphenol in prevention and treatment of tobacco black shank |
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