CN1079643C - Preparation method for peatyfulvic acid somatotropic harmone of plant - Google Patents
Preparation method for peatyfulvic acid somatotropic harmone of plant Download PDFInfo
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- CN1079643C CN1079643C CN98117372A CN98117372A CN1079643C CN 1079643 C CN1079643 C CN 1079643C CN 98117372 A CN98117372 A CN 98117372A CN 98117372 A CN98117372 A CN 98117372A CN 1079643 C CN1079643 C CN 1079643C
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- acid
- peat
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- plant
- somatotropic
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A40/00—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
- Y02A40/10—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in agriculture
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Abstract
The present invention relates to a method for preparing peaty fulvic acid plant somatotropic hormones, which mainly comprises: preparing peaty fulvic acid by peat, deionized water, sodium hydrate, sulphuric acid, etc. through the processing steps of heating, cooling, separation, slag elimination, washing, precipitation, liquid combination, centrifugal separation, washing precipitation, evaporation, concentration, etc.; adding nitrogen, phosphorus, kalium and trace elements which are required by plant growth, and then processing through mixing, stirring and packaging to obtain a product of the peaty fulvic acid plant somatotropic hormones of the present invention. The product has the advantages of convenient use, low dosage, low cost, easy popularization and obvious effect of increasing yield.
Description
The present invention relates to a kind of preparation method of peatyfulvic acid somatotropic harmone of plant, relate to a kind of pure natural peat that utilizes specifically and be raw material, extract molecular weight little, be easy to by the fulvic acid of plant absorbing, add the peatyfulvic acid somatotropic harmone of plant that the essential nitrogen of plant growing, phosphorus, potassium and trace element form again.
At present, the plant growth regulator of development is of a great variety both at home and abroad, and effect of increasing production is different, exists raw material sources difficulty, the high deficiency of cost mostly.
The auximone of selling on the China market mostly is feedstock production with the weathered coal, and its method has one-step method and alkali-soluble acid analysis method, is used for the agrochemistry aspect more, and plant growth regulator is arranged, as Handilong, spray products such as treasured etc.But because of its molecular weight big, it is poor to hold hard water, exist market sale concentration differing greatly with working concentration, affect the credibility of its use, so far also there is not a kind of China's abundant peat resource in local native country of utilizing, preparation production molecular weight is little, and it is strong to hold hard water, the peatyfulvic acid somatotropic harmone of plant of physiologically active and the effect of promotion jarovize.
The object of the present invention is to provide a kind of is the raw material separation and Extraction with peat, has no stimulation physiologically active and promote the preparation method of the peatyfulvic acid somatotropic harmone of plant of jarovize effect.
The object of the present invention is achieved like this: it is mainly by peat, deionized water, sodium hydroxide, sulfuric acid etc., through heating, cool off, separate, remove slag, wash, precipitation, liquid merging, centrifugation, washing precipitation, evaporation, the peat fulvic acid that forms such as concentrating; Add the essential nitrogen of plant growing, phosphorus, potassium and trace element again, form peatyfulvic acid somatotropic harmone of plant product of the present invention through mixing, stir, packing.
The preparation method of peatyfulvic acid somatotropic harmone of plant is characterized in that:
One, the preparation of peat fulvic acid
(1) preparation of humic acid in peat solution
1. weigh and extract the following weight proportion raw material
Peat 1000-800.00 kilogram
Deionized water 6000-4800.00 kilogram
Sodium hydroxide 14-10.80 kilogram
Sulfuric acid 57-45.54 kilogram
2. the deionized water that adds 4 times in the peat adds sodium hydroxid while stirring, and mix and stir,
3. be heated to 85-95 ℃, reacted 45 minutes,
4. be cooled to room temperature,
5. centrifugation must precipitate and mother liquor,
6. use the deionized water washing precipitation of peat weight twice,
7. centrifugation again must precipitate and washing lotion,
8. precipitation is sent to the threshing ground, makes soil conditioner after drying,
(2) preparation of peat yellow humic acid solution
1. above-mentioned mother liquor and washing lotion are merged,
2. the sulfuric acid that adds said ratio, pH is 2-4, and keeps 20 minutes pH values constant,
3. centrifugation must precipitate and mother liquor,
4. use the deionized water washing precipitation of pH=4, consumption is 1/5 volume of mother liquor body,
5. centrifugation again must precipitate and washing lotion,
6. twice liquid is merged,
7. use the centrifugal-film evaporator heating evaporation, being concentrated into fulvic acid content is 4%, promptly gets the required fulvic acid product of auximone,
Two, the yellow humic acid solution processing and preparing is become auximone
1. press ethylene glycol, ammonium molybdate, potassium dihydrogen phosphate and boric acid that the every 1000g of yellow humic acid solution adds following weight (g),
Ethylene glycol 35.00-45.00
Ammonium molybdate 11.30-15.00
Potassium dihydrogen phosphate 75.25-86.83
Boric acid 12.35-12.94
2. after mixing, under 30 times/minute speed, constantly stir,
3. pack, check, promptly get peatyfulvic acid somatotropic harmone of plant concentrate of the present invention.
4. add 66 times water dilution, can use.
Its feature is that also described peat water content is 50%.
Its feature is that also the concentration of described sulfuric acid is 98%.
Its feature is that also the temperature of described centrifugal-film evaporator steam raising is below 40 ℃.
The present invention compared with prior art, it has no stimulation, physiologically active and promote the effect of jarovize, be better than the blade face treasured that sprays other same period, it all shows quite stable to any water quality, has guaranteed result of use, and it is to cereal crops and vegetables and other green plants increase yield significantlies such as economic crops, the economic benefit height, easy to use, consumption is little, and cost is low, easily promote obvious effect of increasing production.
Further specify the present invention below in conjunction with embodiment
Embodiment
Get moisture 50% peat 800Kg, add deionized water 3200Kg, sodium hydroxide 10.8Kg, be heated to 85-95 ℃, reacted 45 minutes, be cooled to room temperature, centrifugation must precipitate and mother liquor, with 1.6 tons deionized water washing precipitation, centrifugation again, must precipitate and washing lotion, precipitation is sent to the threshing ground, can make soil conditioner after drying;
Above-mentioned mother liquor and washing lotion are merged, and adding concentration is 98% sulfuric acid 45.54Kg, and this moment, pH was 3-4, and keeping 20 minutes pH values constant, centrifugation must precipitate and mother liquor, with the deionized water washing precipitation of pH=4, consumption is 1/5 volume of mother liquor body, centrifugation again, must precipitate and wash, twice liquid is merged, and at heating evaporation below 40 ℃, the content that is concentrated into fulvic acid is 4% with the centrifugal-film evaporator temperature, promptly get the required fulvic acid product of auximone
Get 4% fulvic acid solution 1000g, add ethylene glycol 40g, ammonium molybdate 13.00g, potassium dihydrogen phosphate 80.00g, boric acid 12.50g, mix the back and constantly stir under 30 times/minute speed, bag distribution packaging then is by the weight of every bag of splendid attire 50g, in the packing plastic sack, promptly get the concentrate of packed peatyfulvic acid somatotropic harmone of plant, add 66 times water dilution during use, can spray usefulness for 0.07 hectare.
In addition, spend the precipitation after the deionised water, can make the raw material of organic or inorganic compound fertilizer, produce Remixed humic acid fertilizer.
Claims (2)
1, the preparation method of peatyfulvic acid somatotropic harmone of plant is characterized in that:
One, the preparation of peat fulvic acid
(1), the preparation of humic acid in peat solution
1., weigh and extract the following weight proportion raw material
Moisture 50% peat 1000-800.00 kilogram
Deionized water 6000-4800.00 kilogram
Sodium hydroxide 14-10.80 kilogram
Sulfuric acid 57-45.54 kilogram
2., add 4 times deionized water in the peat, add sodium hydroxid while stirring, mix and stir,
3., be heated to 85-95 ℃, reacted 45 minutes,
4., be cooled to room temperature,
5., centrifugation, must precipitate and mother liquor,
6., with the deionized water washing precipitation of peat weight twice,
7., centrifugation again, must precipitate and washing lotion,
8., precipitation is sent to the threshing ground, make soil conditioner after drying,
(2), the preparation of peat yellow humic acid solution
1., and also, with above-mentioned mother liquor and washing lotion
2., add the sulfuric acid of said ratio, pH is 2-4, and keeps 20 minutes pH values constant,
3., centrifugation, must precipitate and mother liquor,
4., with the deionized water washing precipitation of pH=4, consumption is 1/5 volume of mother liquor body,
5., centrifugation again, must precipitate and washing lotion,
6., twice liquid is merged,
7., with centrifugal-film evaporator heating, in evaporation below 40 ℃, being concentrated into fulvic acid content is 4%, promptly gets the required fulvic acid product of auximone,
Two, the yellow humic acid solution processing and preparing is become auximone
1., press ethylene glycol, ammonium molybdate, potassium dihydrogen phosphate and boric acid that the every 1000g of yellow humic acid solution adds following weight g,
Ethylene glycol 35.00-45.00
Ammonium molybdate 11.30-15.00
Potassium dihydrogen phosphate 75.25-86.83
Boric acid 12.35-12.94
2., mix after, under 30 times/minute speed, constantly stir,
3., the packing, the check, promptly get peatyfulvic acid somatotropic harmone of plant product of the present invention.
2, the preparation method of peatyfulvic acid somatotropic harmone of plant according to claim 1, the concentration that it is characterized in that described sulfuric acid is 98%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN98117372A CN1079643C (en) | 1998-08-25 | 1998-08-25 | Preparation method for peatyfulvic acid somatotropic harmone of plant |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN98117372A CN1079643C (en) | 1998-08-25 | 1998-08-25 | Preparation method for peatyfulvic acid somatotropic harmone of plant |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1211392A CN1211392A (en) | 1999-03-24 |
| CN1079643C true CN1079643C (en) | 2002-02-27 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN98117372A Expired - Fee Related CN1079643C (en) | 1998-08-25 | 1998-08-25 | Preparation method for peatyfulvic acid somatotropic harmone of plant |
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Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1304463C (en) * | 2005-02-06 | 2007-03-14 | 方宁 | Technology for producing yellow humic acid by using coal |
| CN102584906A (en) * | 2012-01-15 | 2012-07-18 | 山西大学 | Extracting method of fulvic acid |
| CN103708855B (en) * | 2013-12-27 | 2016-03-23 | 云南中电新能源有限公司 | The preparation method of microbial fertilizer or agricultural chemicals and obtained microbial fertilizer or agricultural chemicals |
| CN105130551A (en) * | 2015-08-04 | 2015-12-09 | 宁夏共享生物化工有限公司 | Method of preparing humic acid containing powdery water-soluble fertilizer from furfural residues |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1031997A (en) * | 1988-10-20 | 1989-03-29 | 喜文 | Multifunctional agricultural chemical fertilizer amd and production method thereof |
| CN1047190A (en) * | 1990-04-17 | 1990-11-28 | 梅国培 | The extraction method of xanthohumic acid kind auximone |
| CN1094387A (en) * | 1993-04-29 | 1994-11-02 | 中国科学院沈阳应用生态研究所 | A kind of long-effect plant compoiste fertilizer |
| CN1122650A (en) * | 1995-07-04 | 1996-05-22 | 河南省科学院化学研究所 | Xanthohumate |
-
1998
- 1998-08-25 CN CN98117372A patent/CN1079643C/en not_active Expired - Fee Related
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1031997A (en) * | 1988-10-20 | 1989-03-29 | 喜文 | Multifunctional agricultural chemical fertilizer amd and production method thereof |
| CN1047190A (en) * | 1990-04-17 | 1990-11-28 | 梅国培 | The extraction method of xanthohumic acid kind auximone |
| CN1094387A (en) * | 1993-04-29 | 1994-11-02 | 中国科学院沈阳应用生态研究所 | A kind of long-effect plant compoiste fertilizer |
| CN1122650A (en) * | 1995-07-04 | 1996-05-22 | 河南省科学院化学研究所 | Xanthohumate |
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| Publication number | Publication date |
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| CN1211392A (en) | 1999-03-24 |
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Inventor after: Xu Chuanzhong Inventor after: Zhu Yaqin Inventor before: Zhu Yaqin Inventor before: Xu Chuanzhong |
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Free format text: CORRECT: INVENTOR; FROM: ZHU YAQIN; XU ZHUANZHONG TO: XU ZHUANZHONG; ZHU YAQIN |
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