CN107905030A - Anti-mildew wallpaper and preparation method thereof - Google Patents
Anti-mildew wallpaper and preparation method thereof Download PDFInfo
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- CN107905030A CN107905030A CN201711000962.7A CN201711000962A CN107905030A CN 107905030 A CN107905030 A CN 107905030A CN 201711000962 A CN201711000962 A CN 201711000962A CN 107905030 A CN107905030 A CN 107905030A
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Classifications
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- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
- D21H21/14—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by function or properties in or on the paper
- D21H21/36—Biocidal agents, e.g. fungicidal, bactericidal, insecticidal agents
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H19/00—Coated paper; Coating material
- D21H19/36—Coatings with pigments
- D21H19/38—Coatings with pigments characterised by the pigments
- D21H19/385—Oxides, hydroxides or carbonates
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H19/00—Coated paper; Coating material
- D21H19/36—Coatings with pigments
- D21H19/44—Coatings with pigments characterised by the other ingredients, e.g. the binder or dispersing agent
- D21H19/46—Non-macromolecular organic compounds
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H19/00—Coated paper; Coating material
- D21H19/36—Coatings with pigments
- D21H19/44—Coatings with pigments characterised by the other ingredients, e.g. the binder or dispersing agent
- D21H19/56—Macromolecular organic compounds or oligomers thereof obtained by reactions only involving carbon-to-carbon unsaturated bonds
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H19/00—Coated paper; Coating material
- D21H19/36—Coatings with pigments
- D21H19/44—Coatings with pigments characterised by the other ingredients, e.g. the binder or dispersing agent
- D21H19/64—Inorganic compounds
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H27/00—Special paper not otherwise provided for, e.g. made by multi-step processes
- D21H27/18—Paper- or board-based structures for surface covering
- D21H27/20—Flexible structures being applied by the user, e.g. wallpaper
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Paper (AREA)
Abstract
The invention discloses a kind of anti-mildew wallpaper and preparation method thereof, wherein, the preparation method includes：1) drainage after mixing paper pulp and modified fibre, dries after compressing, wallpaper matrix is made；2) by polyvinyl chloride resin, dioctyl phthalate, nano-titanium dioxide, chlorinated paraffin, calcium carbonate, aluminium hydroxide and solvent mixed smelting, coating is made；3) obtained coating is coated on wallpaper matrix surface, anti-mildew wallpaper is made.Drainage after the present invention mixes paper pulp and modified fibre, drying after compressing, wallpaper matrix is made, again by polyvinyl chloride resin, dioctyl phthalate, nano-titanium dioxide, chlorinated paraffin, calcium carbonate, aluminium hydroxide and solvent mixed smelting, coating is made, above-mentioned coating is coated on wallpaper matrix surface, so that there is good anti-mildew energy by wallpaper made from above-mentioned material.
Description
Technical field
The present invention relates to wallpaper Material Field, and in particular, to anti-mildew wallpaper and preparation method thereof.
Background technology
Wallpaper is widely applied with its abundant pattern and good performance, and security of material etc.,
Thus, its usage amount is also increasing.And it is well known that the problems such as wallpaper often goes mouldy in use, so that significantly
Influence its performance and using effect.
Therefore it provides one kind can be effectively anti-mildew, and with the anti-mildew wallpaper of the performances such as good tensile load
And preparation method thereof the problem of being urgent need to resolve of the present invention.
The content of the invention
For the above-mentioned prior art, it is an object of the invention to overcome in the prior art wallpaper often occur in use
The problems such as going mouldy, so that the problem of largely effecting on its performance and using effect, can be effectively anti-mildew so as to provide one kind, and
Anti-mildew wallpaper with performances such as good tensile loads and preparation method thereof.
To achieve these goals, the present invention provides a kind of preparation method of anti-mildew wallpaper, it is characterised in that described
Preparation method includes：
1) drainage after mixing paper pulp and modified fibre, dries after compressing, wallpaper matrix is made；
2) by polyvinyl chloride resin, dioctyl phthalate, nano-titanium dioxide, chlorinated paraffin, calcium carbonate, aluminium hydroxide and
Solvent mixed smelting, is made coating；
3) obtained coating is coated on wallpaper matrix surface, anti-mildew wallpaper is made.
Present invention also offers a kind of wallpaper anti-mildew according to made from preparation method described above.
Through the above technical solutions, the present invention is obtained by drainage after paper pulp and modified fibre mixing, compressing rear drying
Wallpaper matrix, then by polyvinyl chloride resin, dioctyl phthalate, nano-titanium dioxide, chlorinated paraffin, calcium carbonate, aluminium hydroxide and
Solvent mixed smelting, is made coating, above-mentioned coating is coated on wallpaper matrix surface, so that by made from above-mentioned material
Wallpaper has good anti-mildew energy.
Other features and advantages of the present invention will be described in detail in subsequent specific embodiment part.
Embodiment
The embodiment of the present invention is described in detail below.It is it should be appreciated that described herein specific
Embodiment is merely to illustrate and explain the present invention, and is not intended to limit the invention.
The endpoint of disclosed scope and any value are not limited to the accurate scope or value herein, these scopes or
Value should be understood to comprising the value close to these scopes or value.For number range, between the endpoint value of each scope, respectively
It can be combined with each other between the endpoint value of a scope and single point value, and individually between point value and obtain one or more
New number range, these number ranges should be considered as specific open herein.
The present invention provides a kind of preparation method of anti-mildew wallpaper, wherein, the preparation method includes：
1) drainage after mixing paper pulp and modified fibre, dries after compressing, wallpaper matrix is made；
2) by polyvinyl chloride resin, dioctyl phthalate, nano-titanium dioxide, chlorinated paraffin, calcium carbonate, aluminium hydroxide and
Solvent mixed smelting, is made coating；
3) obtained coating is coated on wallpaper matrix surface, anti-mildew wallpaper is made.
Drainage after the present invention mixes paper pulp and modified fibre, it is compressing after drying, be made wallpaper matrix, then by PVC
Resin, dioctyl phthalate, nano-titanium dioxide, chlorinated paraffin, calcium carbonate, aluminium hydroxide and solvent mixed smelting, system
Coating is obtained, above-mentioned coating is coated on wallpaper matrix surface, so that having well by wallpaper made from above-mentioned material
Anti-mildew energy.
In a kind of preferred embodiment, the preparation method of modified fibre described in step 1) includes：
A) in the presence of a solvent, temperature will after sodium metasilicate and dispersant, be placed in as under conditions of 35-45 DEG C
Heating water bath, obtains mixture M 1；
B) in the case where temperature is 35-45 DEG C of condition of water bath heating, to step A) in chlorination is added dropwise in obtained mixture M 1
After the aqueous solution of ammonium, supernatant is abandoned, takes precipitation；
C) by above-mentioned precipitation dry roasting, particulate matter is made；
D step C) is added into the water slurry containing fiber) in after obtained particulate matter and coupling agent, it is 60- to be placed in temperature
1-3h is stirred under conditions of 80 DEG C, modified fibre is made.
In the embodiment being more highly preferred to, in step 1), relative to the paper pulp of 100 parts by weight, the modified fibre
Dosage be 30-60 parts by weight.
In another preferred embodiment of the present invention, in step 2), relative to the polyvinyl chloride resin of 100 parts by weight, institute
The dosage for stating dioctyl phthalate is 10-30 parts by weight, and the dosage of the nano-titanium dioxide is 5-10 parts by weight, described
The dosage of chlorinated paraffin is 10-20 parts by weight, and the dosage of the calcium carbonate is 10-30 parts by weight, the dosage of the aluminium hydroxide
For 1-5 parts by weight, the dosage of the solvent is 30-70 parts by weight.
In a kind of preferred embodiment, the solvent is selected from formaldehyde and/or acetone.
In the embodiment being more highly preferred to, the temperature of mixed smelting is 180-230 DEG C in step 2).
In another preferred embodiment of the present invention, step A) in, the solvent is the aqueous solution of ethanol, and described
The concentration of ethanol is 10-20 weight % in the aqueous solution of ethanol；The dispersant is selected from polyvinylpyrrolidone and/or carboxymethyl
Cellulose；Step A) in, relative to the sodium metasilicate of 100 parts by weight, the dosage of the dispersant is 1-5 parts by weight, described
The dosage of solvent is 80-120 parts by weight.
In a more preferred embodiment, step B) in, relative to the mixture M 1 of 100 parts by weight, the chlorination
The dosage of ammonium is 20-50 parts by weight；Step B) in, the content of ammonium chloride is 30-40 weight % in the aqueous solution of ammonium chloride；It is preferred that
Ground, step C) in drying temperature be 80-100 DEG C, drying time 3-5h；Calcination temperature is 400-500 DEG C, and roasting time is
0.5-2h。
In a kind of preferred embodiment, step D) in, the water slurry containing fiber beats system by water and waste paper mixing
；Preferably, the content of the waste paper in water slurry is 40-50 weight %；It is further preferred that relative to described in 100 parts by weight
Water slurry, the dosage of the particulate matter is 40-80 parts by weight, and the dosage of the coupling agent is 5-30 parts by weight；It is further preferable that institute
State coupling agent and be selected from KH550 silane coupling agents.
Present invention also offers a kind of wallpaper anti-mildew according to made from preparation method described above.
The present invention will be described in detail by way of examples below.Modified fibre is made by following methods：1) in 100 weights
Under the conditions of measuring existing for the aqueous solution (concentration be 15 weight %) of the ethanol of part, by the sodium metasilicate of 100 parts by weight and 3 parts by weight
After polyvinylpyrrolidone mixing, it is heating water bath under conditions of 40 DEG C to be placed in temperature, obtains mixture M 1；2) it is 40 in temperature
DEG C condition of water bath heating under, be added dropwise into step 1) in the mixture M 1 of obtained 100 parts by weight with the speed of 100 drops/min
After the ammonium chloride (aqueous solution by concentration for the ammonium chloride of 35 weight %) of 40 parts by weight, supernatant is abandoned, takes precipitation；3) will be above-mentioned
After being deposited in 90 DEG C of dry 4h, then at 450 DEG C of roasting 1h, particulate matter is made；
4) to the water slurry (waste paper containing fiber of 100 parts by weight：Water=45：55) obtained 60 weights in step 3) are added in
After measuring the particulate matter of part and the KH550 silane coupling agents of 20 parts by weight, it is placed under conditions of temperature is 70 DEG C and is stirred 2h, make
Obtain modified fibre.
Embodiment 1
1) drainage after mixing the paper pulp of 100 parts by weight and the modified fibre of 30 parts by weight, dries after compressing, is made
Wallpaper matrix；
2) by the polyvinyl chloride resin of 100 parts by weight, the dioctyl phthalate of 10 parts by weight, 5 parts by weight nanometer titanium dioxide
Titanium, the chlorinated paraffin of 10 parts by weight, the calcium carbonate of 10 parts by weight, the acetone of the aluminium hydroxide of 1 parts by weight and 30 parts by weight are placed in
Temperature is mixed smelting under conditions of 180 DEG C, and coating is made；
3) obtained coating is coated on wallpaper matrix surface, anti-mildew wallpaper A1 is made.
Embodiment 2
1) drainage after mixing the paper pulp of 100 parts by weight and the modified fibre of 60 parts by weight, dries after compressing, is made
Wallpaper matrix；
2) by the polyvinyl chloride resin of 100 parts by weight, the dioctyl phthalate of 30 parts by weight, 10 parts by weight nano-silica
The acetone for changing titanium, the chlorinated paraffin of 20 parts by weight, the calcium carbonate of 30 parts by weight, the aluminium hydroxide of 5 parts by weight and 70 parts by weight is put
Mixed smelting under conditions of being 230 DEG C in temperature, is made coating；
3) obtained coating is coated on wallpaper matrix surface, anti-mildew wallpaper A2 is made.
Embodiment 3
1) drainage after mixing the paper pulp of 100 parts by weight and the modified fibre of 50 parts by weight, dries after compressing, is made
Wallpaper matrix；
2) by the polyvinyl chloride resin of 100 parts by weight, the dioctyl phthalate of 20 parts by weight, 8 parts by weight nanometer titanium dioxide
Titanium, the chlorinated paraffin of 15 parts by weight, the calcium carbonate of 20 parts by weight, the acetone of the aluminium hydroxide of 3 parts by weight and 50 parts by weight are placed in
Temperature is mixed smelting under conditions of 200 DEG C, and coating is made；
3) obtained coating is coated on wallpaper matrix surface, anti-mildew wallpaper A3 is made.
Embodiment 4
It is prepared by the preparation method according to embodiment 1, unlike, the dosage of the dioctyl phthalate is 5
Parts by weight, the dosage of the nano-titanium dioxide are 2 parts by weight, and the dosage of the chlorinated paraffin is 5 parts by weight, the calcium carbonate
Dosage be 5 parts by weight, the dosage of the aluminium hydroxide is 0.5 parts by weight, and the dosage of the solvent is 20 parts by weight, is made anti-
Go mouldy wallpaper A4.
Comparative example 1
It is prepared by the preparation method according to embodiment 1, unlike, modified fibre is added without, wallpaper D1 is made.
Comparative example 2
It is prepared by the preparation method according to embodiment 2, unlike, it is added without dioctyl phthalate, nanometer two
Titanium oxide, chlorinated paraffin, are made wallpaper D2.
Comparative example 3
It is prepared by the preparation method according to embodiment 3, unlike, calcium carbonate, aluminium hydroxide are added without, wallpaper is made
D3。
Test case
Above-mentioned A1-A4 and D1-D3 are respectively placed in the environment of wetness is more than 80% and place 30d, detects feelings of going mouldy
Condition, while detect its laterally moistening tensile load and longitudinal direction moistening tensile load, the obtained result such as institute of table 1 according to QB/T4034
Show.D4 is the standard of high-class product.
The preferred embodiment of the present invention described in detail above, still, during present invention is not limited to the embodiments described above
Detail, in the range of the technology design of the present invention, a variety of simple variants can be carried out to technical scheme, this
A little simple variants belong to protection scope of the present invention.
It is further to note that each particular technique feature described in above-mentioned embodiment, in not lance
In the case of shield, can be combined by any suitable means, in order to avoid unnecessary repetition, the present invention to it is various can
The combination of energy no longer separately illustrates.
In addition, various embodiments of the present invention can be combined randomly, as long as it is without prejudice to originally
The thought of invention, it should equally be considered as content disclosed in this invention.
Claims (10)
1. a kind of preparation method of anti-mildew wallpaper, it is characterised in that the preparation method includes：
1) drainage after mixing paper pulp and modified fibre, dries after compressing, wallpaper matrix is made；
2) by polyvinyl chloride resin, dioctyl phthalate, nano-titanium dioxide, chlorinated paraffin, calcium carbonate, aluminium hydroxide and solvent
Mixed smelting, is made coating；
3) obtained coating is coated on wallpaper matrix surface, anti-mildew wallpaper is made.
2. preparation method according to claim 1, wherein, the preparation method of modified fibre described in step 1) includes：
A) in the presence of a solvent, after sodium metasilicate and dispersant, will be placed in temperature is water-bath under conditions of 35-45 DEG C
Heating, obtains mixture M 1；
B) in the case where temperature is 35-45 DEG C of condition of water bath heating, to step A) in ammonium chloride is added dropwise in obtained mixture M 1
After aqueous solution, supernatant is abandoned, takes precipitation；
C) by above-mentioned precipitation dry roasting, particulate matter is made；
D step C) is added into the water slurry containing fiber) in after obtained particulate matter and coupling agent, be placed in temperature as 60-80 DEG C
Under conditions of be stirred 1-3h, be made modified fibre.
3. preparation method according to claim 1 or 2, wherein, in step 1), relative to the paper pulp of 100 parts by weight,
The dosage of the modified fibre is 30-60 parts by weight.
4. preparation method according to claim 1 or 2, wherein, in step 2), relative to the PVC trees of 100 parts by weight
Fat, the dosage of the dioctyl phthalate is 10-30 parts by weight, and the dosage of the nano-titanium dioxide is 5-10 weight
Part, the dosage of the chlorinated paraffin is 10-20 parts by weight, and the dosage of the calcium carbonate is 10-30 parts by weight, the aluminium hydroxide
Dosage be 1-5 parts by weight, the dosage of the solvent is 30-70 parts by weight.
5. preparation method according to claim 1 or 2, wherein, the solvent is selected from formaldehyde and/or acetone.
6. preparation method according to claim 1 or 2, wherein, the temperature of mixed smelting is 180-230 DEG C in step 2).
7. preparation method according to claim 2, wherein, step A) in, the solvent is the aqueous solution of ethanol, and described
The concentration of ethanol is 10-20 weight % in the aqueous solution of ethanol；
The dispersant is selected from polyvinylpyrrolidone and/or carboxymethyl cellulose；
Step A) in, relative to the sodium metasilicate of 100 parts by weight, the dosage of the dispersant is 1-5 parts by weight, the solvent
Dosage be 80-120 parts by weight.
8. preparation method according to claim 2, wherein, step B) in, relative to the mixture M 1 of 100 parts by weight, institute
The dosage for stating ammonium chloride is 20-50 parts by weight；
Step B) in, the content of ammonium chloride is 30-40 weight % in the aqueous solution of ammonium chloride；
Preferably, step C) in drying temperature be 80-100 DEG C, drying time 3-5h；
Calcination temperature is 400-500 DEG C, roasting time 0.5-2h.
9. preparation method according to claim 2, wherein, step D) in, the water slurry containing fiber is by water and waste paper
Mixing, which is beaten, to be made；
Preferably, the content of the waste paper in water slurry is 40-50 weight %；
It is further preferred that relative to the water slurry of 100 parts by weight, the dosage of the particulate matter is 40-80 parts by weight, described
The dosage of coupling agent is 5-30 parts by weight；
It is further preferable that the coupling agent is selected from KH550 silane coupling agents.
10. anti-mildew wallpaper made from the preparation method in a kind of 1-9 according to claim described in any one.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201711000962.7A CN107905030A (en) | 2017-10-24 | 2017-10-24 | Anti-mildew wallpaper and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201711000962.7A CN107905030A (en) | 2017-10-24 | 2017-10-24 | Anti-mildew wallpaper and preparation method thereof |
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| CN107905030A true CN107905030A (en) | 2018-04-13 |
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| CN201711000962.7A Pending CN107905030A (en) | 2017-10-24 | 2017-10-24 | Anti-mildew wallpaper and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108517722A (en) * | 2018-05-07 | 2018-09-11 | 合肥市晨雷思建筑材料科技有限公司 | A kind of novel anticracking wallpaper and preparation method thereof |
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2017
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN108517722A (en) * | 2018-05-07 | 2018-09-11 | 合肥市晨雷思建筑材料科技有限公司 | A kind of novel anticracking wallpaper and preparation method thereof |
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Application publication date: 20180413 |