CN107903843A - A kind of covering of the fan water-fast adhesive and preparation method - Google Patents
A kind of covering of the fan water-fast adhesive and preparation method Download PDFInfo
- Publication number
- CN107903843A CN107903843A CN201711182722.3A CN201711182722A CN107903843A CN 107903843 A CN107903843 A CN 107903843A CN 201711182722 A CN201711182722 A CN 201711182722A CN 107903843 A CN107903843 A CN 107903843A
- Authority
- CN
- China
- Prior art keywords
- parts
- fan
- water
- covering
- starch
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J103/00—Adhesives based on starch, amylose or amylopectin or on their derivatives or degradation products
- C09J103/04—Starch derivatives
- C09J103/08—Ethers
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/04—Non-macromolecular additives inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/08—Macromolecular additives
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
Abstract
A kind of water-fast adhesive of covering of the fan of the invention, is prepared by the raw material of following parts by weight：10~20 parts of Heveatex, 20~30 parts of etherification starch, 20~30 parts of carboxy starch, 0.5~0.7 part of 44 epoxy resin of E, 0.3~0.5 part of attapulgite powder, 10~15 parts of ethyl acetate, 13~16 parts of flake asbestos, 0.5~0.7 part of chitosan, 2~5 parts of ε polylysines and excess water, the product have that bonding force is strong, water resistance is stable, storage period is long, rate of drying is fast, permeability and good fluidity；And have the advantages that Preparation equipment is simple, operating condition is easy to control, non-secondary pollution and Environmental Safety, for the connection of covering of the fan and ribs of the fan, the fan rate of drying after bonding significantly improves.
Description
Technical field
The present invention relates to fan making technical field, specifically, is related to a kind of covering of the fan water-fast adhesive and preparation side
Method.
Background technology
The fan of Chinese tradition, ribs of the fan generally make of bamboo and wood, and rare also has ivory, beast bone, ox horn, carved lacquerware etc..Bamboo
The ribs of the fan of system also has the rare kinds such as the bamboo palm, the bamboo of the Ladies of the Xiang, Bambusa ventricosa except common radix polygonati officinalis, Bai Zhu.Wooden has red sandalwood, Asiatic sweet leaf
(santal), Chinese littleleaf box, peach silk, chicken wings, nanmu etc..In traditional Chinese culture, in antique historical relic handed down from ancient times, covering of the fan painting and calligraphy are except exquisite
Outside famous expert drives quill, also extremely luxury, red sandalwood, ebony, hawksbill turtle, ivory, mottled bamboo, beast bone contend in beauty bucket very to the greatest extent for the making of ribs of the fan；Sun is carved, is micro-
Carve, inlay, coating with lacquer paint, bronze designs or patterns on fans, wooden furniture, etc., Freehandhand-drawing are made something perfect even more perfect, in fan making technique, producer usually needs to consolidate covering of the fan and ribs of the fan
The decorative suspension member of fixed or stickup, used adhesive water resistance and moisture-proof are poor, the moisture absorption easily in humid air, adhesive strength
It is not high；Use can produce creep at high temperature, decline glue-joint strength, below -5 DEG C store easy freezing, make lotion by
To destruction, therefore cause its application significantly limited.
The content of the invention
The present invention proposes a kind of covering of the fan water-fast adhesive and preparation method, to solve existing fan glue in the prior art
Glutinous agent glues that glutinous effect is undesirable, and the deficiency that harmful material is more.
The technical proposal of the invention is realized in this way：
A kind of water-fast adhesive of covering of the fan, is prepared by the raw material of following parts by weight：10~20 parts of Heveatex, ether
Change 20~30 parts of starch, 20~30 parts of carboxy starch, 0.5~0.7 part of E-44 epoxy resin, 0.3~0.5 part of attapulgite powder,
10~15 parts of ethyl acetate, 13~16 parts of flake asbestos, 0.5~0.7 part of chitosan, 2~5 parts of ε polylysines and excess water.
Further, the water-fast adhesive of a kind of covering of the fan, is prepared by the raw material of following parts by weight：Heveatex 15
Part, 25 parts of etherification starch, 20 parts of carboxy starch, 0.5 part of E-44 epoxy resin, 0.5 part of attapulgite powder, 10 parts of ethyl acetate,
13 parts of flake asbestos, chitosan 0.5, ε polylysines 2 and excess water.
Further, the water-fast adhesive of a kind of covering of the fan, is prepared by the raw material of following parts by weight：Heveatex 10
Part, 30 parts of etherification starch, 20 parts of carboxy starch, 0.5 part of E-44 epoxy resin, 0.4 part of attapulgite powder, 12 parts of ethyl acetate,
15 parts of flake asbestos, 0.6 part of chitosan, 4 parts of ε polylysines and excess water.
A kind of covering of the fan preparation method of water-fast adhesive, includes the following steps：
S1：In the reaction kettle with blender, deionized water and Heveatex and E-44 epoxy resin are added, is warming up to
88-92 DEG C, temperature 30min is kept, Heveatex is diluted, is cooled to 60-70 DEG C；
S2：Etherification starch and carboxy starch are added in step S1, ethyl acetate is stirring evenly and then adding into, in the case where being stirred continuously
React 60-80min；；
S3：Chitosan and ε polylysines are added, stirs 30-40min；
S4：Flake asbestos, attapulgite powder are added, after stirring 30-40min, that is, product is made.
The beneficial aspects of the present invention are：The product is with bonding force is strong, water resistance is stable, storage period is long, rate of drying
It hurry up, permeability and good fluidity；And with Preparation equipment is simple, operating condition is easy to control, non-secondary pollution and environmental protection are pacified
Congruent advantage, for the connection of covering of the fan and ribs of the fan, the fan rate of drying after bonding significantly improves.
Embodiment
The technical solution in the embodiment of the present invention is clearly and completely described below, it is clear that described embodiment
Only part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, the common skill in this area
Art personnel all other embodiments obtained without creative efforts, belong to the model that the present invention protects
Enclose.
Embodiment：
A kind of water-fast adhesive of covering of the fan, is prepared by the raw material of following parts by weight：10~20 parts of Heveatex, ether
Change 20~30 parts of starch, 20~30 parts of carboxy starch, 0.5~0.7 part of E-44 epoxy resin, 0.3~0.5 part of attapulgite powder,
10~15 parts of ethyl acetate, 13~16 parts of flake asbestos, 0.5~0.7 part of chitosan, 2~5 parts of ε polylysines and excess water.
A kind of water-fast adhesive of covering of the fan, is prepared by the raw material of following parts by weight：15 parts of Heveatex, etherificate are formed sediment
25 parts of powder, 20 parts of carboxy starch, 0.5 part of E-44 epoxy resin, 0.5 part of attapulgite powder, 10 parts of ethyl acetate, flake asbestos 13
Part, chitosan 0.5, ε polylysines 2 and excess water.
A kind of water-fast adhesive of covering of the fan, is prepared by the raw material of following parts by weight：10 parts of Heveatex, etherificate are formed sediment
30 parts of powder, 20 parts of carboxy starch, 0.5 part of E-44 epoxy resin, 0.4 part of attapulgite powder, 12 parts of ethyl acetate, flake asbestos 15
Part, 0.6 part of chitosan, 4 parts of ε polylysines and excess water.
A kind of covering of the fan preparation method of water-fast adhesive, includes the following steps：
S1：In the reaction kettle with blender, deionized water and Heveatex and E-44 epoxy resin are added, is warming up to
88-92 DEG C, temperature 30min is kept, Heveatex is diluted, is cooled to 60-70 DEG C；
S2：Etherification starch and carboxy starch are added in step S1, ethyl acetate is stirring evenly and then adding into, in the case where being stirred continuously
React 60-80min；；
S3：Chitosan and ε polylysines are added, stirs 30-40min；
S4：Flake asbestos, attapulgite powder are added, after stirring 30-40min, that is, product is made.
The product has that bonding force is strong, water resistance is stable, storage period is long, rate of drying is fast, permeability and good fluidity；
And have the advantages that Preparation equipment is simple, operating condition is easy to control, non-secondary pollution and Environmental Safety, for covering of the fan and ribs of the fan
Connection, the fan rate of drying after bonding significantly improves.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all essences in the present invention
With within principle, any modification, equivalent replacement, improvement and so on, should all be included in the protection scope of the present invention god.
Claims (4)
- A kind of 1. water-fast adhesive of covering of the fan, it is characterised in that：It is prepared by the raw material of following parts by weight：Heveatex 10 ~20 parts, 20~30 parts of etherification starch, 20~30 parts of carboxy starch, 0.5~0.7 part of E-44 epoxy resin, attapulgite powder 0.3 ~0.5 part, 10~15 parts of ethyl acetate, 13~16 parts of flake asbestos, 0.5~0.7 part of chitosan, 2~5 parts of ε polylysines and remaining Measure water.
- A kind of 2. water-fast adhesive of covering of the fan according to claim 1, it is characterised in that：By the raw material of following parts by weight It is prepared：15 parts of Heveatex, 25 parts of etherification starch, 20 parts of carboxy starch, 0.5 part of E-44 epoxy resin, attapulgite powder 0.5 part, 10 parts of ethyl acetate, 13 parts of flake asbestos, chitosan 0.5, ε polylysines 2 and excess water.
- A kind of 3. water-fast adhesive of covering of the fan according to claim 1, it is characterised in that：By the raw material of following parts by weight It is prepared：10 parts of Heveatex, 30 parts of etherification starch, 20 parts of carboxy starch, 0.5 part of E-44 epoxy resin, attapulgite powder 0.4 part, 12 parts of ethyl acetate, 15 parts of flake asbestos, 0.6 part of chitosan, 4 parts of ε polylysines and excess water.
- A kind of 4. covering of the fan preparation method of water-fast adhesive, it is characterised in that：Include the following steps：S1：In the reaction kettle with blender, deionized water and Heveatex and E-44 epoxy resin are added, is warming up to 88- 92 DEG C, temperature 30min is kept, Heveatex is diluted, is cooled to 60-70 DEG C；S2：Etherification starch and carboxy starch are added in step S1, ethyl acetate is stirring evenly and then adding into, is being stirred continuously lower reaction 60-80min；；S3：Chitosan and ε polylysines are added, stirs 30-40min；S4：Flake asbestos, attapulgite powder are added, after stirring 30-40min, that is, product is made.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711182722.3A CN107903843A (en) | 2017-11-23 | 2017-11-23 | A kind of covering of the fan water-fast adhesive and preparation method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711182722.3A CN107903843A (en) | 2017-11-23 | 2017-11-23 | A kind of covering of the fan water-fast adhesive and preparation method |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107903843A true CN107903843A (en) | 2018-04-13 |
Family
ID=61847585
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711182722.3A Pending CN107903843A (en) | 2017-11-23 | 2017-11-23 | A kind of covering of the fan water-fast adhesive and preparation method |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107903843A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109577088A (en) * | 2018-11-29 | 2019-04-05 | 苏州盛风文化创意发展有限公司 | A kind of set alum method improving covering of the fan paper performance |
| WO2022137861A1 (en) * | 2020-12-23 | 2022-06-30 | 株式会社ブリヂストン | Adhesive composition, and resin material, rubber article, organic fiber-rubber composite, and tire using same |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1055942A (en) * | 1990-04-20 | 1991-11-06 | 透平穆里株式会社 | The binder composition of the temporary adhesion scraps of paper |
| CN106381109A (en) * | 2016-08-31 | 2017-02-08 | 苏州市凌云工艺扇厂 | Adhesive for gluing of fan and preparation method thereof |
| CN106400473A (en) * | 2016-08-31 | 2017-02-15 | 苏州市凌云工艺扇厂 | Fan covering manufacturing process |
-
2017
- 2017-11-23 CN CN201711182722.3A patent/CN107903843A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1055942A (en) * | 1990-04-20 | 1991-11-06 | 透平穆里株式会社 | The binder composition of the temporary adhesion scraps of paper |
| CN106381109A (en) * | 2016-08-31 | 2017-02-08 | 苏州市凌云工艺扇厂 | Adhesive for gluing of fan and preparation method thereof |
| CN106400473A (en) * | 2016-08-31 | 2017-02-15 | 苏州市凌云工艺扇厂 | Fan covering manufacturing process |
Non-Patent Citations (3)
| Title |
|---|
| 于新等: "《天然食品添加剂》", 31 March 2014, 中国轻工业出版社 * |
| 王丁等: ""淀粉黄原酸酯—天然橡胶胶乳粘合剂的研制"", 《江西科学》 * |
| 黎厚斌，张萍主编: "《包装应用化学》", 31 January 2014, 北京印刷工业出版社 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109577088A (en) * | 2018-11-29 | 2019-04-05 | 苏州盛风文化创意发展有限公司 | A kind of set alum method improving covering of the fan paper performance |
| CN109577088B (en) * | 2018-11-29 | 2021-05-25 | 苏州盛风文化创意发展有限公司 | Alum covering method for improving fan-shaped paper performance |
| WO2022137861A1 (en) * | 2020-12-23 | 2022-06-30 | 株式会社ブリヂストン | Adhesive composition, and resin material, rubber article, organic fiber-rubber composite, and tire using same |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180413 |