CN107897220A - A kind of expelling parasite water of the component containing false indigo and preparation method thereof - Google Patents

A kind of expelling parasite water of the component containing false indigo and preparation method thereof Download PDF

Info

Publication number
CN107897220A
CN107897220A CN201711025889.9A CN201711025889A CN107897220A CN 107897220 A CN107897220 A CN 107897220A CN 201711025889 A CN201711025889 A CN 201711025889A CN 107897220 A CN107897220 A CN 107897220A
Authority
CN
China
Prior art keywords
false indigo
mosquito
extracting solution
extract
wormwood
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201711025889.9A
Other languages
Chinese (zh)
Inventor
宋小利
魏园园
王雪
高立国
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Yulin University
Original Assignee
Yulin University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Yulin University filed Critical Yulin University
Priority to CN201711025889.9A priority Critical patent/CN107897220A/en
Publication of CN107897220A publication Critical patent/CN107897220A/en
Pending legal-status Critical Current

Links

Classifications

    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08—Magnoliopsida [dicotyledons]
    • A01N65/12—Asteraceae or Compositae [Aster or Sunflower family], e.g. daisy, pyrethrum, artichoke, lettuce, sunflower, wormwood or tarragon
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08—Magnoliopsida [dicotyledons]
    • A01N65/20—Fabaceae or Leguminosae [Pea or Legume family], e.g. pea, lentil, soybean, clover, acacia, honey locust, derris or millettia
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08—Magnoliopsida [dicotyledons]
    • A01N65/22—Lamiaceae or Labiatae [Mint family], e.g. thyme, rosemary, skullcap, selfheal, lavender, perilla, pennyroyal, peppermint or spearmint
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08—Magnoliopsida [dicotyledons]
    • A01N65/28—Myrtaceae [Myrtle family], e.g. teatree or clove
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change

Landscapes

  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Microbiology (AREA)
  • Biotechnology (AREA)
  • Agronomy & Crop Science (AREA)
  • Mycology (AREA)
  • Plant Pathology (AREA)
  • Dentistry (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Botany (AREA)
  • Medicines Containing Plant Substances (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

Mosquito-repellent water the present invention provides a kind of component containing false indigo and preparation method thereof, including 6 8% false indigo extract, 1 4% Folium Artemisiae Argyi extract, 5 13% dried peppermint leaf leaching thing, 3 7% cloves sesame oil, 0.8 1.2% emulsifying agent, surplus are that the sum of the ethanol solution that mass fraction is 3 7%, above material volume fraction is 100%.The expelling parasite water uses pure natural substance, pollution-free, and significant effect is walked quickly and kept away to mosquitos and flies, worm ant.

Description

A kind of expelling parasite water of the component containing false indigo and preparation method thereof
Technical field
The present invention relates to mosquito repellent technical field；It is related to a kind of expelling parasite water of component containing false indigo, further relates to above-mentioned expelling parasite water Preparation method.
Background technology
Stepped up with the living standard of people, the puzzlement of mosquito is most unpleasant thing in hot summer.Can With the development of modern science and technology, chemical agent spreads unchecked use so that the drug resistance of mosquito increases significantly, and common on the market Mosquito-repellent incense is habitual using insecticidal materials such as fluorine chlorine ether chrysanthemum esters, these chemical substances have human body a toxic, the increasing of dosage, Certainly the health of people is damaged.
The content of the invention
The present invention provides a kind of expelling parasite water of component containing false indigo, which uses pure natural substance, pollution-free, right Mosquitos and flies, worm ant walk quickly and keep away significant effect.
Present invention also offers the preparation method of above-mentioned mosquito-repellent water, by obtaining carrying for false indigo, folium artemisiae argyi and dried peppermint leaf Liquid is taken, then carries out the preparation of mosquito-repellent water.
The technical scheme is that：A kind of mosquito-repellent water of the component containing false indigo, including include 6-8%'s by volume fraction False indigo extract, the Folium Artemisiae Argyi extract of 1-4%, the dried peppermint leaf leaching thing of 5-13%, the cloves sesame oil of 3-7%, 0.8-1.2% Emulsifying agent, surplus be the sum of the ethanol solution that mass fraction is 3-7%, above material volume fraction be 100%.
Wherein by volume fraction include 7% false indigo extracting solution, 3% Folium Artemisiae Argyi extractive liquid, 15% peppermint leaching liquid, 5% cloves sesame oil, 1% emulsifying agent, 69% mass fraction are 5% ethanol solution.
Present invention also offers the preparation method of the mosquito-repellent water of the above-mentioned component containing false indigo, comprise the following steps：
Step S1, the false indigo extract of 6-8%, the Folium Artemisiae Argyi extract of 1-4%, the peppermint of 5-13% are taken by volume fraction Leaf leaches thing, and the cloves sesame oil of 3-7%, the emulsifying agent of 0.8-1.2%, surplus is the ethanol solution that mass fraction is 3-7%, with The sum of volume fraction of upper material is 100%；
Step S2, by the false indigo extract obtained in step 1, Folium Artemisiae Argyi extract, dried peppermint leaf leaching thing, cloves sesame oil, Emulsifying agent is dissolved in ethanol solution, obtains mosquito-repellent water.
Further, the features of the present invention also resides in：
7% false indigo extracting solution, 3% Folium Artemisiae Argyi extractive liquid, 15% peppermint are taken by volume fraction in wherein step S1 Leaching liquid, 5% cloves sesame oil, 1% emulsifying agent, 69% mass fraction are 5% ethanol solution.
The preparation process of wherein false indigo extract is：The amorpha fruticosa leaf powder 20-30g to dry in the shade is taken, then using anhydrous After alcohol steep takes 2-3h, extracting solution is filtered, obtains filtrate, then filtrate is evaporated to obtain false indigo extract.
The preparation process of wherein wormwood extracting solution is：Take the wormwood leaf powder 20-30g to dry in the shade, then using petroleum ether- Extraction takes 1-2h at 20 DEG C, then filters extracting solution, obtains wormwood leaf filtrate, then adds second into wormwood leaf filtrate The mass ratio of acetoacetic ester, wormwood leaf filtrate and ethyl acetate is 2:(4-6), soaks 15-20min under conditions of 0-5 DEG C, into Row multi-reflow extracts, and then recycling obtains wormwood extracting solution.
The preparation process of wherein peppermint leaf extract is：The dried peppermint leaf powder 20-30g to dry in the shade is taken, then adds quality point Number takes 1-2h for 5% ethanol solution extraction, and peppermint extracting solution is obtained after filtering.
Compared with prior art, the beneficial effects of the invention are as follows：Using pure plant extracting solution, the false indigo of use, which has, to be touched Kill, stomach toxicity, the agricultural active such as food refusal, by equal existing with gas chromatography and mass spectromentry joint technology, column chromatography, high pressure preparation solution For isolation technics and the spectroscopic technique such as infrared, ultraviolet, mass spectrum, nuclear magnetic resonance spectroscopy, Dui Zi Miho Chinese scholartrees fruit essential oils and flavonoids kill Worm active ingredient is identified that determine Zi Miho Chinese scholartrees essential oils has certain bioactivity to different harmful organisms.
Further, there is provided the preparation method of false indigo extracting solution, Folium Artemisiae Argyi extractive liquid and peppermint leaching liquid.
Embodiment
Technical scheme is further illustrated with reference to specific embodiment.
The present invention provides a kind of mosquito-repellent water of component containing false indigo, includes following material, the purple of 6-8% by volume fraction Fringe Chinese scholartree extract, the Folium Artemisiae Argyi extract of 1-4%, the dried peppermint leaf leaching thing of 5-13%, the cloves sesame oil of 3-7%, 0.8-1.2%'s Emulsifying agent, surplus are that the sum of the ethanol solution that mass fraction is 3-7%, the volume fraction of above material is 100%.
Preferably, 7% false indigo extracting solution, 3% Folium Artemisiae Argyi extractive liquid, 15% peppermint leaching are included by volume fraction Liquid, 5% cloves sesame oil, 1% emulsifying agent, 69% mass fraction are 5% ethanol solution.
Present invention also offers the preparation method of above-mentioned mosquito-repellent water, comprise the following steps：
Step S1, the false indigo extract of 6-8%, the Folium Artemisiae Argyi extract of 1-4%, the peppermint of 5-13% are taken by volume fraction Leaf leaches thing, and the cloves sesame oil of 3-7%, the emulsifying agent of 0.8-1.2%, surplus is the ethanol solution that mass fraction is 3-7%, with The sum of volume fraction of upper material is 100%.
The preparation process of wherein false indigo extract is：The amorpha fruticosa leaf powder 20-30g to dry in the shade is taken, then using anhydrous After alcohol steep takes 2-3h, extracting solution is filtered, obtains filtrate, then filtrate is evaporated to obtain false indigo extract.
The preparation process of wherein wormwood extracting solution is：Take the wormwood leaf powder 20-30g to dry in the shade, then using petroleum ether- Extraction takes 1-2h at 20 DEG C, then filters extracting solution, obtains wormwood leaf filtrate, then adds second into wormwood leaf filtrate The mass ratio of acetoacetic ester, wormwood leaf filtrate and ethyl acetate is 2:(4-6), soaks 15-20min under conditions of 0-5 DEG C, into Row multi-reflow extracts, and then recycling obtains wormwood extracting solution.
The preparation process of wherein peppermint leaf extract is：The dried peppermint leaf powder 20-30g to dry in the shade is taken, then adds quality point Number takes 1-2h for 5% ethanol solution extraction, and peppermint extracting solution is obtained after filtering.
Then by the false indigo extract obtained in step 1, Folium Artemisiae Argyi extract, dried peppermint leaf leaching thing, cloves sesame oil, emulsification Agent is dissolved in ethanol solution, obtains mosquito-repellent water.
The specific embodiment of the present invention includes：
Embodiment 1
The mosquito-repellent water containing false indigo component is produced, its detailed process is：The amorpha fruticosa leaf powder 20g to dry in the shade is taken, then After taking 2h using absolute ethyl alcohol extraction, extracting solution is filtered, obtains filtrate, then filtrate is evaporated to obtain false indigo extraction Thing；The wormwood leaf powder 20g to dry in the shade is taken, is then extracted using petroleum ether at -20 DEG C and takes 1h, then extracting solution is filtered, is obtained To wormwood leaf filtrate, the quality of ethyl acetate, wormwood leaf filtrate and ethyl acetate is then added into wormwood leaf filtrate Than for 2:5,20min is soaked under conditions of 0 DEG C, carries out 3 refluxing extractions, then recycling obtains wormwood extracting solution；Take and dry in the shade Dried peppermint leaf powder 20g, then add mass fraction be 5% ethanol solution extraction takes 1h, peppermint extracting solution is obtained after filtering.
Then above-mentioned false indigo extract 7ml, wormwood extracting solution 3ml, peppermint extracting solution 15ml, and cloves sesame oil are taken The mass fraction of 5ml, emulsifying agent 1ml, 69ml are 5% ethanol solution, obtain mosquito-repellent water after mixing.
Embodiment 2
The mosquito-repellent water containing false indigo component is produced, its detailed process is：The amorpha fruticosa leaf powder 30g to dry in the shade is taken, then After taking 3h using absolute ethyl alcohol extraction, extracting solution is filtered, obtains filtrate, then filtrate is evaporated to obtain false indigo extraction Thing；The wormwood leaf powder 30g to dry in the shade is taken, is then extracted using petroleum ether at -20 DEG C and takes 2h, then extracting solution is filtered, is obtained To wormwood leaf filtrate, the quality of ethyl acetate, wormwood leaf filtrate and ethyl acetate is then added into wormwood leaf filtrate Than for 2:4,15min is soaked under conditions of 5 DEG C, carries out 4 refluxing extractions, then recycling obtains wormwood extracting solution；Take and dry in the shade Dried peppermint leaf powder 30g, then add mass fraction be 5% ethanol solution extraction takes 2h, peppermint extracting solution is obtained after filtering.
Then above-mentioned false indigo extract 6ml, wormwood extracting solution 4ml, peppermint extracting solution 13ml, and cloves sesame oil are taken The mass fraction of 7ml, emulsifying agent 1.2ml, 68.8ml are 3% ethanol solution, obtain mosquito-repellent water after mixing.
Embodiment 3
The mosquito-repellent water containing false indigo component is produced, its detailed process is：The amorpha fruticosa leaf powder 25g to dry in the shade is taken, then After taking 2.5h using absolute ethyl alcohol extraction, extracting solution is filtered, obtains filtrate, then filtrate is evaporated to obtain false indigo and carry Take thing；The wormwood leaf powder 25g to dry in the shade is taken, is then extracted using petroleum ether at -20 DEG C and takes 1.5h, then by extracting solution mistake Filter, obtains wormwood leaf filtrate, then adds ethyl acetate into wormwood leaf filtrate, wormwood leaf filtrate and ethyl acetate Mass ratio is 2:6,18min is soaked under conditions of 2 DEG C, carries out multi-reflow extraction, then recycling obtains wormwood extracting solution；Take The dried peppermint leaf powder 26g to dry in the shade, then adds the ethanol solution extraction that mass fraction is 5% and takes 1.8h, peppermint is obtained after filtering Extracting solution.
Then above-mentioned false indigo extract 8ml, wormwood extracting solution 4ml, peppermint extracting solution 5ml, and cloves sesame oil are taken The mass fraction of 3ml, emulsifying agent 0.8ml, 79.2ml are 3% ethanol solution, obtain mosquito-repellent water after mixing.
Embodiment 4
The mosquito-repellent water containing false indigo component is produced, its detailed process is：The amorpha fruticosa leaf powder 28g to dry in the shade is taken, then After taking 2.8h using absolute ethyl alcohol extraction, extracting solution is filtered, obtains filtrate, then filtrate is evaporated to obtain false indigo and carry Take thing；The wormwood leaf powder 22g to dry in the shade is taken, is then extracted using petroleum ether at -20 DEG C and takes 1.2h, then by extracting solution mistake Filter, obtains wormwood leaf filtrate, then adds ethyl acetate into wormwood leaf filtrate, wormwood leaf filtrate and ethyl acetate Mass ratio is 2:4,17min is soaked under conditions of 4 DEG C, carries out multi-reflow extraction, then recycling obtains wormwood extracting solution；Take The dried peppermint leaf powder 24g to dry in the shade, then adds the ethanol solution extraction that mass fraction is 5% and takes 1h, obtaining peppermint after filtering carries Take liquid.
Then above-mentioned false indigo extract 6ml, wormwood extracting solution 1ml, peppermint extracting solution 13ml, and cloves sesame oil are taken The mass fraction of 3ml, emulsifying agent 1ml, 76ml are 6% ethanol solution, obtain mosquito-repellent water after mixing.
Embodiment 5
The mosquito-repellent water containing false indigo component is produced, its detailed process is：The amorpha fruticosa leaf powder 20g to dry in the shade is taken, then After taking 2h using absolute ethyl alcohol extraction, extracting solution is filtered, obtains filtrate, then filtrate is evaporated to obtain false indigo extraction Thing；The wormwood leaf powder 30g to dry in the shade is taken, is then extracted using petroleum ether at -20 DEG C and takes 1h, then extracting solution is filtered, is obtained To wormwood leaf filtrate, the quality of ethyl acetate, wormwood leaf filtrate and ethyl acetate is then added into wormwood leaf filtrate Than for 2:6,20min is soaked under conditions of 5 DEG C, carries out multi-reflow extraction, then recycling obtains wormwood extracting solution；Take and dry in the shade Dried peppermint leaf powder 22g, then add mass fraction be 5% ethanol solution extraction takes 2h, peppermint extracting solution is obtained after filtering.
Then above-mentioned false indigo extract 6ml, wormwood extracting solution 1ml, peppermint extracting solution 5ml, and cloves sesame oil are taken The mass fraction of 3ml, emulsifying agent 1.2ml, 83.8ml are 7% ethanol solution, obtain mosquito-repellent water after mixing.
Embodiment 6
The mosquito-repellent water containing false indigo component is produced, its detailed process is：The amorpha fruticosa leaf powder 24g to dry in the shade is taken, then After taking 3h using absolute ethyl alcohol extraction, extracting solution is filtered, obtains filtrate, then filtrate is evaporated to obtain false indigo extraction Thing；The wormwood leaf powder 29g to dry in the shade is taken, is then extracted using petroleum ether at -20 DEG C and takes 2h, then extracting solution is filtered, is obtained To wormwood leaf filtrate, the quality of ethyl acetate, wormwood leaf filtrate and ethyl acetate is then added into wormwood leaf filtrate Than for 2:6,17min is soaked under conditions of 1 DEG C, carries out multi-reflow extraction, then recycling obtains wormwood extracting solution；Take and dry in the shade Dried peppermint leaf powder 24g, then add mass fraction be 5% ethanol solution extraction takes 1h, peppermint extracting solution is obtained after filtering.
Then above-mentioned false indigo extract 8ml, wormwood extracting solution 2ml, peppermint extracting solution 6ml, and cloves sesame oil are taken The mass fraction of 4ml, emulsifying agent 1ml, 79ml are 4% ethanol solution, obtain mosquito-repellent water after mixing.
Embodiment 7
The mosquito-repellent water containing false indigo component is produced, its detailed process is：The amorpha fruticosa leaf powder 24g to dry in the shade is taken, then After taking 2.5h using absolute ethyl alcohol extraction, extracting solution is filtered, obtains filtrate, then filtrate is evaporated to obtain false indigo and carry Take thing；The wormwood leaf powder 23g to dry in the shade is taken, is then extracted using petroleum ether at -20 DEG C and takes 2h, then filter extracting solution, Wormwood leaf filtrate is obtained, the matter of ethyl acetate, wormwood leaf filtrate and ethyl acetate is then added into wormwood leaf filtrate Amount is than being 2:4.6,16min is soaked under conditions of 2 DEG C, carries out multi-reflow extraction, then recycling obtains wormwood extracting solution；Take The dried peppermint leaf powder 26g to dry in the shade, then adds the ethanol solution extraction that mass fraction is 5% and takes 1h, obtaining peppermint after filtering carries Take liquid.
Then above-mentioned false indigo extract 8ml, wormwood extracting solution 1ml, peppermint extracting solution 10ml, and cloves sesame oil are taken The mass fraction of 3ml, emulsifying agent 0.9ml, 77.1ml are 3% ethanol solution, obtain mosquito-repellent water after mixing.
Embodiment 8
The mosquito-repellent water containing false indigo component is produced, its detailed process is：The amorpha fruticosa leaf powder 26g to dry in the shade is taken, then After taking 2.5h using absolute ethyl alcohol extraction, extracting solution is filtered, obtains filtrate, then filtrate is evaporated to obtain false indigo and carry Take thing；The wormwood leaf powder 20g to dry in the shade is taken, is then extracted using petroleum ether at -20 DEG C and takes 1h, then filter extracting solution, Wormwood leaf filtrate is obtained, the matter of ethyl acetate, wormwood leaf filtrate and ethyl acetate is then added into wormwood leaf filtrate Amount is than being 2:5.5,18min is soaked under conditions of 3 DEG C, carries out multi-reflow extraction, then recycling obtains wormwood extracting solution；Take The dried peppermint leaf powder 25g to dry in the shade, then adds the ethanol solution extraction that mass fraction is 5% and takes 1h, obtaining peppermint after filtering carries Take liquid.
Then above-mentioned false indigo extract 8ml, wormwood extracting solution 1ml, peppermint extracting solution 12ml, and cloves sesame oil are taken The mass fraction of 4ml, emulsifying agent 1ml, 74ml are 5% ethanol solution, obtain mosquito-repellent water after mixing.

Claims (7)

  1. A kind of 1. mosquito-repellent water of component containing false indigo, it is characterised in that include the false indigo extract of 6-8% by volume fraction, The Folium Artemisiae Argyi extract of 1-4%, the dried peppermint leaf leaching thing of 5-13%, the cloves sesame oil of 3-7%, the emulsifying agent of 0.8-1.2%, surplus The sum of the ethanol solution for being 3-7% for mass fraction, above material volume fraction is 100%.
  2. 2. the mosquito-repellent water of the component according to claim 1 containing false indigo, it is characterised in that include 7% by volume fraction False indigo extracting solution, 3% Folium Artemisiae Argyi extractive liquid, 15% peppermint leaching liquid, 5% cloves sesame oil, 1% emulsifying agent, 69% Mass fraction be 5% ethanol solution.
  3. 3. the preparation method of the mosquito-repellent water of a kind of component containing false indigo, it is characterised in that comprise the following steps：
    Step S1, the false indigo extract of 6-8%, the Folium Artemisiae Argyi extract of 1-4%, the dried peppermint leaf leaching of 5-13% are taken by volume fraction Take thing, the cloves sesame oil of 3-7%, the emulsifying agent of 0.8-1.2%, surplus is the ethanol solution that mass fraction is 3-7%, above material The sum of volume fraction of material is 100%；
    Step S2, by the false indigo extract obtained in step 1, Folium Artemisiae Argyi extract, dried peppermint leaf leaching thing, cloves sesame oil, emulsification Agent is dissolved in ethanol solution, obtains mosquito-repellent water.
  4. 4. the preparation method of the mosquito-repellent water of the component according to claim 3 containing false indigo, it is characterised in that the step S1 In taken by volume fraction 7% false indigo extracting solution, 3% Folium Artemisiae Argyi extractive liquid, 15% peppermint leaching liquid, 5% cloves is fragrant Oil, 1% emulsifying agent, 69% mass fraction are 5% ethanol solution.
  5. 5. the preparation method of the mosquito-repellent water of the component containing false indigo according to 3 or 4 any one of claim, its feature exist In the preparation process of the false indigo extract is：The amorpha fruticosa leaf powder 20-30g to dry in the shade is taken, is then soaked using absolute ethyl alcohol After extracting 2-3h, extracting solution is filtered, obtains filtrate, then filtrate is evaporated to obtain false indigo extract.
  6. 6. the preparation method of the mosquito-repellent water of the component containing false indigo according to 3 or 4 any one of claim, its feature exist In the preparation process of the wormwood extracting solution is：The wormwood leaf powder 20-30g to dry in the shade is taken, then using petroleum ether at -20 DEG C Lower extraction takes 1-2h, then filters extracting solution, obtains wormwood leaf filtrate, and acetic acid second is then added into wormwood leaf filtrate The mass ratio of ester, wormwood leaf filtrate and ethyl acetate is 2:(4-6), soaks 15-20min under conditions of 0-5 DEG C, carries out more Secondary refluxing extraction, then recycling obtain wormwood extracting solution.
  7. 7. the preparation method of the mosquito-repellent water of the component containing false indigo according to 3 or 4 any one of claim, its feature exist In the preparation process of the peppermint leaf extract is：The dried peppermint leaf powder 20-30g to dry in the shade is taken, then adding mass fraction is 5% ethanol solution extraction takes 1-2h, and peppermint extracting solution is obtained after filtering.
CN201711025889.9A 2017-10-27 2017-10-27 A kind of expelling parasite water of the component containing false indigo and preparation method thereof Pending CN107897220A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201711025889.9A CN107897220A (en) 2017-10-27 2017-10-27 A kind of expelling parasite water of the component containing false indigo and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201711025889.9A CN107897220A (en) 2017-10-27 2017-10-27 A kind of expelling parasite water of the component containing false indigo and preparation method thereof

Publications (1)

Publication Number Publication Date
CN107897220A true CN107897220A (en) 2018-04-13

Family

ID=61841899

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201711025889.9A Pending CN107897220A (en) 2017-10-27 2017-10-27 A kind of expelling parasite water of the component containing false indigo and preparation method thereof

Country Status (1)

Country Link
CN (1) CN107897220A (en)

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102939998A (en) * 2012-11-28 2013-02-27 滨州职业学院 Mosquito repellent liquid and preparation method thereof
KR20150044017A (en) * 2015-03-26 2015-04-23 대한민국(환경부 국립생물자원관장) Methods of Preventing Plant Diseases by Using Composition Comprising the Extract of Amorpha fruticosa
CN105767028A (en) * 2016-04-08 2016-07-20 泰山医学院 Fly fumigating killing incense containing amorpha fruticosa ingredients and production method thereof
CN106212560A (en) * 2016-08-05 2016-12-14 太仓张根木生物科技有限公司 A kind of Chinese medicine infant mosquito-driving liquid

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102939998A (en) * 2012-11-28 2013-02-27 滨州职业学院 Mosquito repellent liquid and preparation method thereof
KR20150044017A (en) * 2015-03-26 2015-04-23 대한민국(환경부 국립생물자원관장) Methods of Preventing Plant Diseases by Using Composition Comprising the Extract of Amorpha fruticosa
CN105767028A (en) * 2016-04-08 2016-07-20 泰山医学院 Fly fumigating killing incense containing amorpha fruticosa ingredients and production method thereof
CN106212560A (en) * 2016-08-05 2016-12-14 太仓张根木生物科技有限公司 A kind of Chinese medicine infant mosquito-driving liquid

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
罗永明: "《中药化学成分提取分离技术与方法》", 31 January 2016, 上海科学技术出版社 *
肖子英: "《中国药物化妆品》", 31 March 1992, 中国医药科技出版社 *

Similar Documents

Publication Publication Date Title
CN106266685B (en) A kind of compound essential oil and preparation method thereof
AU2018314123A1 (en) Phytochemical extraction system and methods to extract phytochemicals from plants including plants of the family cannabaceae sensu stricto
CN104055705B (en) A kind of plant anophelifuge
CN105342887A (en) Peppermint perfume and preparation method thereof
CN101632391A (en) Development of novel indoor acaricide
CN107484784A (en) A kind of application of opopanax alkane type sesquiterpene compound in anti-eliminate aphis
CN105248489B (en) A kind of biological agent for tea place preventing and treating pest and disease damage and preparation method thereof
CN106265148B (en) A kind of perfume and preparation method thereof containing natural plant essential oils
CN107232187A (en) Careless plant mosquito-repellent spray liquid of one kind hundred and preparation method thereof
CN107743985A (en) Plant composition with disinfecting mite-removing function
CN100527962C (en) An insecticide with Artemisia argyi leaves and Atractylodes lancea extract as active components
JP4647991B2 (en) SCF expression inhibitor
George et al. Ethno-botanical verification and phytochemical profile of ethanolic leaves extract of two medicinal plants (Phragmenthera capitata and Lantana camara) used in Nigeria using GC-MS Technique
CN106614827A (en) Mosquito-repelling combination and preparation method thereof and application
CN107897220A (en) A kind of expelling parasite water of the component containing false indigo and preparation method thereof
CN104224925B (en) A kind of mosquito-expelling and antipruritic Chinese medicine composition and application thereof
CN109090147A (en) A kind of fragrant pearl of lasting fragrance and preparation method thereof
CN102846493A (en) Long-acting repellent liquid and preparation method thereof
Stevovic et al. Environmental adaptibility of tansy (Tanacetum vulgare L.)
CN110269071A (en) A kind of mosquito repellent composition and preparation method thereof
KR20130057742A (en) Acaricidal component
El-Naggar et al. Chemical composition of essential oil of Haplophyllum tuberculatum (Rutaceae) grow wild in different habitats of Egypt
CN107753349A (en) A kind of feminine care wet tissue for preventing and treating menstruation infection
CN106365969A (en) Preparation method and application of carvone
CN107711910A (en) A kind of mosquito-repellent incense of the composition containing false indigo and preparation method thereof

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination