CN107882988A - A kind of elastane - Google Patents

A kind of elastane Download PDF

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Publication number
CN107882988A
CN107882988A CN201710961961.2A CN201710961961A CN107882988A CN 107882988 A CN107882988 A CN 107882988A CN 201710961961 A CN201710961961 A CN 201710961961A CN 107882988 A CN107882988 A CN 107882988A
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China
Prior art keywords
parts
holding plate
hole
elastane
oil
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CN201710961961.2A
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Chinese (zh)
Inventor
李燕
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Chengdu Jiushidu Industrial Product Design Co Ltd
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Chengdu Jiushidu Industrial Product Design Co Ltd
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Priority to CN201710961961.2A priority Critical patent/CN107882988A/en
Publication of CN107882988A publication Critical patent/CN107882988A/en
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    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F16ENGINEERING ELEMENTS AND UNITS; GENERAL MEASURES FOR PRODUCING AND MAINTAINING EFFECTIVE FUNCTIONING OF MACHINES OR INSTALLATIONS; THERMAL INSULATION IN GENERAL
    • F16JPISTONS; CYLINDERS; SEALINGS
    • F16J15/00Sealings
    • F16J15/02Sealings between relatively-stationary surfaces
    • F16J15/06Sealings between relatively-stationary surfaces with solid packing compressed between sealing surfaces
    • F16J15/10Sealings between relatively-stationary surfaces with solid packing compressed between sealing surfaces with non-metallic packing
    • F16J15/102Sealings between relatively-stationary surfaces with solid packing compressed between sealing surfaces with non-metallic packing characterised by material
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D35/00Filtering devices having features not specifically covered by groups B01D24/00 - B01D33/00, or for applications not specifically covered by groups B01D24/00 - B01D33/00; Auxiliary devices for filtration; Filter housing constructions
    • B01D35/30Filter housing constructions
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L75/00Compositions of polyureas or polyurethanes; Compositions of derivatives of such polymers
    • C08L75/04Polyurethanes
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F01MACHINES OR ENGINES IN GENERAL; ENGINE PLANTS IN GENERAL; STEAM ENGINES
    • F01MLUBRICATING OF MACHINES OR ENGINES IN GENERAL; LUBRICATING INTERNAL COMBUSTION ENGINES; CRANKCASE VENTILATING
    • F01M11/00Component parts, details or accessories, not provided for in, or of interest apart from, groups F01M1/00 - F01M9/00
    • F01M11/03Mounting or connecting of lubricant purifying means relative to the machine or engine; Details of lubricant purifying means
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F02COMBUSTION ENGINES; HOT-GAS OR COMBUSTION-PRODUCT ENGINE PLANTS
    • F02MSUPPLYING COMBUSTION ENGINES IN GENERAL WITH COMBUSTIBLE MIXTURES OR CONSTITUENTS THEREOF
    • F02M37/00Apparatus or systems for feeding liquid fuel from storage containers to carburettors or fuel-injection apparatus; Arrangements for purifying liquid fuel specially adapted for, or arranged on, internal-combustion engines
    • F02M37/22Arrangements for purifying liquid fuel specially adapted for, or arranged on, internal-combustion engines, e.g. arrangements in the feeding system
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/03Polymer mixtures characterised by other features containing three or more polymers in a blend
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/03Polymer mixtures characterised by other features containing three or more polymers in a blend
    • C08L2205/035Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/14Polymer mixtures characterised by other features containing polymeric additives characterised by shape
    • C08L2205/16Fibres; Fibrils

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  • Engineering & Computer Science (AREA)
  • General Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Mechanical Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Combustion & Propulsion (AREA)
  • Gasket Seals (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Sealing Material Composition (AREA)

Abstract

A kind of elastane, for the holding plate sealing structure of oil rectifier, the holding plate is sealedly and fixedly connected at the oil-out of support by nut member, and the through hole on holding plate is coaxially disposed and by the first seal ring seal contact gap with entering oil hole;Through hole edge on holding plate protrudes to form through hole boss, first seal ring set is on through hole boss, and first sealing ring thickness be not less than through hole boss height, polytetrafluoroethylene floor of first sealing ring by elastomeric polyurethane layer and coated on elastic polyurethane layer surface is formed, and elastane is made up of the material of following parts by weight:90 95 parts of TPU resins, 25 parts of wax powder, 12 15 parts of aerosil, 68 parts of cotton fiber, 12 parts of coupling agent, 0.5 1 parts of antioxidant, 0.5 1 parts of levelling agent, 0.5 1 parts of dispersant.A kind of elastane provided by the invention, it is mainly used in the holding plate sealing structure of oil rectifier, by compounding obtained elastane the first sealing ring can be made to be not susceptible to the sealing property that plastic deformation which thereby enhances holding plate in long-term extrusion process, even if making to be not easy to loosen under the long-term Vibration Condition of holding plate.

Description

A kind of elastane
The application is entitled:A kind of oil rectifier holding plate sealing structure, Application No.:2016108440579 The divisional application of patent of invention, parent application day are on 09 23rd, 2016.
Technical field
The present invention relates to gasoline filter seals technical field, more particularly to a kind of oil rectifier is sealed with holding plate The elastane of structure.
Background technology
Usual automobile using cleaner can all include a housing and support, and housing and support are detachably connected.On support often Oil inlet and oil-out are set, the lower end of housing is connected with being equipped with the cylinder thread seal of filter element, the other end of housing to Stretch to form end in center, end is provided with through hole, for the oil inlet on connection support, is provided with and keeps between end and cylinder Plate, through hole is again provided with holding plate, to connect the filter chamber in oil inlet and cylinder.Holding plate not only play connection housing and The effect of cylinder filter chamber, also play a part of sealing oil inlet and oil-out, therefore, the quality of holding plate performance and tightness Directly affect the job stability of cleaner.
In the existing oil rectifier used, the mechanical oscillation of engine drive oil rectifier vibration, due to holding plate with Support, housing, cylinder are to be rigidly connected, and mechanical oscillation can cause holding plate to loosen, and then joint gap occur, between connection The appearance of gap can be such that the through hole on the through hole and holding plate of the end of housing is not on same axis, and oil circuit is changed into bent from straight line Local permeability phenomenon can occur for line, holding plate junction, because steam turbine oil has corrosivity, particularly added with the vapour for saving finish Machine oil, these oil oozed out can corrode seal interface, and then cause sealing property to be greatly reduced, and when serious, then oil-feed can occur The oil of mouth is scurried into oil-out, have impact on the job stability of cleaner.Simultaneously as cleaner needs to change filter core often, Easily make to loosen in the holding plate that factory fixes through machine, it is this loosening also result in holding plate connection it is unstable, make guarantor Hold Board position to shift, during engine mechanical oscillation, after this deviation is constantly exaggerated, also results in oil circuit and lead to Road is obstructed, expands joint gap, causes tightness insufficient, and then Leakage occur.
The content of the invention
The goal of the invention of the present invention is:For above-mentioned problem, there is provided a kind of elastane, it is main to use In the holding plate sealing structure of oil rectifier, the first sealing ring can be made long-term by compounding obtained elastane It is not susceptible to be plastically deformed in extrusion process, enables the stability of the long-term holding structure of the first sealing ring and size, maintain The sealing function of itself, which thereby enhances the sealing property of holding plate, even if making to be not easy under the long-term Vibration Condition of holding plate Loosen.
The technical solution adopted by the present invention is as follows:A kind of elastane, the holding plate for oil rectifier seal Structure, the holding plate are sealedly and fixedly connected at the oil-out of support by nut member, it is characterised in that on holding plate Through hole is coaxially disposed and by the first seal ring seal contact gap with entering oil hole;Through hole edge on holding plate protrudes to be formed Through hole boss, the first seal ring set is on through hole boss, and the thickness of the first sealing ring is not less than the height of through hole boss, and first Polytetrafluoroethylene floor of the sealing ring by elastomeric polyurethane layer and coated on elastic polyurethane layer surface forms, elastane It is made up of the material of following parts by weight:TPU resin 90-95 parts, wax powder 2-5 parts, aerosil 12-15 parts, cotton fiber 6-8 Part, coupling agent 1-2 parts, antioxidant 0.5-1 parts, levelling agent 0.5-1 parts, dispersant 0.5-1 parts.
In above-mentioned, scurried into prevent the through hole on holding plate and enter the oil of oil hole in installation gap, it is close by first The sealing function of seal ring, make oil stream can only be via entering oil hole and through hole flows through;In order to prevent in vibration processes, the first sealing Ring occur relative displacement and influence tightness, the through hole edge on holding plate, which protrudes, to form through hole boss, the first seal ring set in On through hole boss, and the thickness of the first sealing ring is not less than the height of through hole boss.Through hole and enter oil hole on the same axis When relative skew occurs, the first sealing ring can be close to through hole and enter the wall of oil hole, and oil inlet passage is placed in all the time In one sealing ring, and then it ensure that tightness;In order that the first sealing ring has good elasticity and wearability, prevent that first is close Plastic deformation and bonding corrosion contact surface occurs to early in seal ring, and the first sealing ring is by elastomeric polyurethane layer and coated on the poly- ammonia of elasticity The polytetrafluoroethylene floor composition on ester layer surface, it is contemplated that the weatherability of elastic polyurethane, while in view of in long-term extrusion process In easily occur plastic deformation and influence sealing property, elastomeric polyurethane layer employs above-mentioned elastane, in above-mentioned bullet In property polyurethane material, the addition of organic siliconresin can make TPU resins have the excellent characteristic such as heat-resisting, cold-resistant, make first close Seal ring can adapt to the working environment of oil rectifier, add the stability of TPU resin matrixes, TPU resin matrixes anti-aging effect Fruit is good, can greatly improve the combination property using TPU resins as the elastic polyurethane of matrix;Talcum powder can improve TPU resins The hardness of matrix, the skin-friction coefficient of TPU resins is reduced, makes elastane that there is excellent toughness and stability; The use of cotton fiber can not only greatly improve the toughness, wearability and tear resistance of elastane, moreover it is possible to make poly- ammonia Ester body keeps good elasticity in long-term use, and the rate of plastic deformation of polyurethane is greatly reduced, enables polyurethane body The stability of long-term holding structure and size.
Preferably, the white cotton linter fiber that cotton fiber is obtained by white cotton after roller gin preliminary working is made after disperseing .
Preferably, TPU resins is the TPU resins after improvement, the TPU resins after the improvement are made by following steps:
Step 1, dimethicone that mass ratio is 26%, 38.5% TPR and 6% linseed oil be placed in turbine stirrer and stirred Mix well mixed, and mixed liquor be heated to 100 DEG C, the organic siliconresin that mass ratio is 7% is heated to 160 DEG C to after melting, It is added in mixed liquor, keeps the temperature of mixed liquor at 100 DEG C, stirs 3h with 600rad/min mixing speed, mixed Liquid;
Step 2, the talcum powder by mass ratio is 10.8%, 3.2% zinc stearate, 1.5% triethylamine nertralizer, 0.5% have Machine tin catalyst and 4.3% erucyl amide are added in the mixed liquor of step 1 after being uniformly mixed in agitator and are stirred Uniformly, the mixed liquor after then will be well mixed delivers to banburying 8h in banbury, is eventually adding the boric acid that mass ratio is 2.2% and allows Its coagulation forming.
Preferably, the preparation technology of elastane comprises the following steps:
Step 1, cotton fiber and TPU resins are placed under 50 DEG C of hot blasts and fully dried, contain cotton fiber and the water of TPU resins Amount is in below 0.06wt%;
Step 2, according to proportioning each component is weighed, TPU resins, wax powder, aerosil, cotton fiber, coupling agent is anti-oxidant Agent and levelling agent are placed in agitator, are uniformly mixed at 90 DEG C under 600rad/min mixing speed, are then added Cotton fiber is uniformly dispersed with dispersion machine, reduces the temperature of batch mixing to 80 DEG C, be incubated 2min, then by batch mixing throw into banbury in Banburying 4-5h at 110-120 DEG C;
It is step 3, the batch mixing tablet press machine obtained after step 2 banburying is compressing.
In summary, by adopting the above-described technical solution, the beneficial effects of the invention are as follows:The elastic polyurethane of the present invention Material is mainly used in the holding plate sealing structure of oil rectifier, by compound obtained elastane can make it is first close Seal ring is not susceptible to be plastically deformed in long-term extrusion process, enables the stabilization of the long-term holding structure of the first sealing ring and size Performance, the sealing function of itself is maintained, which thereby enhance the sealing property of holding plate, even if making the long-term Vibration Condition of holding plate Under be not easy to loosen.
Brief description of the drawings
Fig. 1 is a kind of oil rectifier holding plate sealed structural representation of the present invention;
Fig. 2 is the mplifying structure schematic diagram of part A in Fig. 1;
Fig. 3 is another situation of Fig. 2 structures;
Fig. 4 is the elastic sealing gasket cross-sectional view of the present invention;
Fig. 5 is the sealing ring cross-sectional view of the present invention.
Marked in figure:1 is housing, and 2 be support, and 201 be oil inlet, and 202 be oil-out, and 3 be filter element, and 4 be oil-feed Through hole, 5 be holding plate, and 501 be through hole, and 6 be nut member, and 7 be annular boss, and 8 be open-ended, and 9 be depressed part, and 10 be close Component is sealed, 11 be elastic sealing gasket, and 1101 be elastomeric polyurethane layer, and 1102 be polytetrafluoroethylene floor, and 12 be the first sealing ring, 13 It is the collar for through hole boss, 14,1401 be shirt rim, and 15 be gap.
Embodiment
Below in conjunction with the accompanying drawings, the present invention is described in detail.
In order to make the purpose , technical scheme and advantage of the present invention be clearer, it is right below in conjunction with drawings and Examples The present invention is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, and It is not used in the restriction present invention.
As shown in Figures 1 to 5, a kind of oil rectifier holding plate sealing structure, including housing 1 and support 2, housing 1 Round barrel cover of the lower seal connection with filter element 3, support 2 are provided with oil inlet 201 and oil-out 202, oil inlet 201 Bottom, the end on the top of housing 1 are provided with into oil hole 4, enter the bottom of oil hole 4, and the top of filter element 3 is provided with holding plate 5, Holding plate 5 is sealedly and fixedly connected at the oil-out 202 of support 2 by nut member 6, and the middle part of holding plate 5 is provided with threaded The annular boss 7 of through hole, annular boss 7 are provided with depressed part 9, the energy of depressed part 9 with open-ended 8 sides contacted of housing 1 Enough containment members 10 ordinatedly received for blocking the oil stream between open-ended the 8 of housing 1 and annular boss 7, it is preferable that Containment member 10 is O-ring seal, and the end face that holding plate 5 contacts with the inner wall of end of housing 1 is provided with elastic sealing gasket 11.
As an improvement ground embodiment, in order to prevent the through hole 501 on holding plate 5 from being scurried into entering the oil of oil hole 4 Install in gap, as shown in Figures 2 and 3, the through hole 501 on holding plate 5 is coaxially disposed and by the first sealing with entering oil hole 4 12 gap in sealing contact of ring.By the sealing function of the first sealing ring 12, make oil stream can only be via entering oil hole 4 and through hole 501 Flow through.
As an improvement ground embodiment, in order to prevent in vibration processes, relative displacement occurs for the first sealing ring 12 And tightness is influenceed, as shown in Fig. 2 the edge of through hole 501 on holding plate 5 protrudes and to form through hole boss 13, the first sealing ring 12 It is placed on through hole boss 13, and the thickness of the first sealing ring 12 is not less than the height of through hole boss 13.Through hole 501 and enter oil hole 4 when occurring relative skew on the same axis, and the first sealing ring 12 can be close to through hole 501 and enter the wall of oil hole 4, and begin Oil inlet passage is placed in the first sealing ring 12 eventually, and then ensure that tightness.
As an improvement ground embodiment, as shown in figure 3, being provided with the collar 14, the edge of the one end of the collar 14 in through hole 501 Outward flanging forms shirt rim 1401, and shirt rim 1401 is pressed on the end face of through hole boss 13 by the inwall of the end of housing 1.Pass through pressure The mode of tight set ring 14, even if making through hole wall and entering the wall of oil hole 4 in the case of vibrations, sealing state can be also in, And then it ensure that tightness.
As an improvement ground embodiment, in order that elastic sealing gasket 11 has good elasticity and wearability, is prevented Plastic deformation and bonding corrosion contact surface occurs to early in elastic sealing gasket 11, as shown in figure 4, elastic sealing gasket 11 is by the poly- ammonia of elasticity Ester layer 1101 and polytetrafluoroethylene floor 1102 coated on the surface of elastomeric polyurethane layer 1101 form.
As an improvement ground embodiment, in order that sealing ring 12 has good elasticity and wearability, prevents first Plastic deformation and bonding corrosion contact surface occurs to early in sealing ring 12, as shown in figure 5, the first sealing ring 12 is by elastomeric polyurethane layer 1101 and the polytetrafluoroethylene floor 1102 coated on the surface of elastomeric polyurethane layer 1101 form.
As an improvement ground embodiment, in order to prevent upper end of the oil stream through holding plate 5 and the sky of nut mating connection To threaded connection place oil leak occurs for the following current of gap part 15, and the gap 15 that the upper end of holding plate 5 is connected with nut is set There are the second sealing ring, the gap 15 that upper end of second sealing ring full of holding plate 5 is connected with nut, with sealed airspace Part 15.
As an improvement ground embodiment, it is contemplated that the weatherability of elastic polyurethane, while in view of being extruded for a long time During plastic deformation easily occurs and influences sealing property, elastomeric polyurethane layer 1101 use elastane, and elasticity is gathered Urethane material is made up of the material of following parts by weight:TPU resin 90-95 parts, wax powder 2-5 parts, aerosil 12-15 parts, Cotton fiber 6-8 parts, coupling agent 1-2 parts, antioxidant 0.5-1 parts, levelling agent 0.5-1 parts, dispersant 0.5-1 parts, cotton fiber by The white cotton linter fiber obtained after Bai Mianjing roller gin preliminary working is made after disperseing, and TPU resins are the TPU trees after improvement Fat, the TPU resins after the improvement are made by following steps:
Step 1, dimethicone that mass ratio is 26%, 38.5% TPR and 6% linseed oil be placed in turbine stirrer and stirred Mix well mixed, and mixed liquor be heated to 100 DEG C, the organic siliconresin that mass ratio is 7% is heated to 160 DEG C to after melting, It is added in mixed liquor, keeps the temperature of mixed liquor at 100 DEG C, stirs 3h with 600rad/min mixing speed, mixed Liquid;
Step 2, the talcum powder by mass ratio is 10.8%, 3.2% zinc stearate, 1.5% triethylamine nertralizer, 0.5% have Machine tin catalyst and 4.3% erucyl amide are added in the mixed liquor of step 1 after being uniformly mixed in agitator and are stirred Uniformly, the mixed liquor after then will be well mixed delivers to banburying 8h in banbury, is eventually adding the boric acid that mass ratio is 2.2% and allows Its coagulation forming.
Furthermore, it is below the present invention in order to preferably explain and implement the elastane of the present invention The specific several embodiments of elastane, what deserves to be explained is, following examples are only to explain the present invention, and are not In order to limit the present invention.
Embodiment one
A kind of elastane, its preparation technology comprise the following steps:
Step 1, manufacture improvement after TPU resins, by mass ratio be 26% dimethicone, 38.5% TPR and 6% flax Oil is placed in turbine stirrer and is uniformly mixed, and mixed liquor is heated into 100 DEG C, by the organic siliconresin that mass ratio is 7% 160 DEG C are heated to after melting, is added in mixed liquor, the temperature of mixed liquor is kept at 100 DEG C, with 600rad/min stirring Speed stirs 3h, obtains mixed liquor;
Step 2, the talcum powder by mass ratio is 10.8%, 3.2% zinc stearate, 1.5% triethylamine nertralizer, 0.5% have Machine tin catalyst and 4.3% erucyl amide are added in the mixed liquor of step 1 after being uniformly mixed in agitator and are stirred Uniformly, the mixed liquor after then will be well mixed delivers to banburying 8h in banbury, is eventually adding the boric acid that mass ratio is 2.2% and allows Its coagulation forming, it is then the TPU resins after being improved by Twin screw extruder extruding pelletization, storage is standby;
Step 3, length is placed under 50 DEG C of hot blasts for the TPU resins after 3-7mm white cotton fiber and improvement and fully dried, Make the water content of the TPU resins after white cotton fiber and improvement in below 0.06wt%, it is standby;
Step 4, each component is weighed, by the TPU resins after 90 parts of improvement, 5 parts of wax powder, 15 parts of aerosils, 2 parts VTES coupling agent, 1 part of antioxidant 168 and 1 part of organic-silicon-modified polysiloxane leveling agents are placed in In agitator, it is uniformly mixed under 600rad/min mixing speed in 90 DEG C, then adds 8 parts of white cotton fibers and 1 part BYK-ATU dispersants are uniformly dispersed with dispersion machine, reduce the temperature of batch mixing to 80 DEG C, are incubated 2min, then batch mixing is thrown to banburying In machine at 110 DEG C banburying 4h;
Step 5, by the batch mixing tablet press machine obtained after step 4 banburying it is compressing after, obtain elastic polyurethane product.
Embodiment two
A kind of elastane, its preparation technology comprise the following steps:
Step 1, manufacture improvement after TPU resins, by mass ratio be 26% dimethicone, 38.5% TPR and 6% flax Oil is placed in turbine stirrer and is uniformly mixed, and mixed liquor is heated into 100 DEG C, by the organic siliconresin that mass ratio is 7% 160 DEG C are heated to after melting, is added in mixed liquor, the temperature of mixed liquor is kept at 100 DEG C, with 600rad/min stirring Speed stirs 3h, obtains mixed liquor;
Step 2, the talcum powder by mass ratio is 10.8%, 3.2% zinc stearate, 1.5% triethylamine nertralizer, 0.5% have Machine tin catalyst and 4.3% erucyl amide are added in the mixed liquor of step 1 after being uniformly mixed in agitator and are stirred Uniformly, the mixed liquor after then will be well mixed delivers to banburying 8h in banbury, is eventually adding the boric acid that mass ratio is 2.2% and allows Its coagulation forming, it is then the TPU resins after being improved by Twin screw extruder extruding pelletization, storage is standby;
Step 3, length is placed under 50 DEG C of hot blasts for the TPU resins after 3-7mm white cotton fiber and improvement and fully dried, Make the water content of the TPU resins after white cotton fiber and improvement in below 0.06wt%, it is standby;
Step 4, each component is weighed, by the TPU resins after 90 parts of improvement, 5 parts of wax powder, 12 parts of aerosils, 1 part VTES coupling agent, 0.5 part of antioxidant 168 and 1 part of organic-silicon-modified polysiloxane leveling agents are put In agitator, be uniformly mixed under 600rad/min mixing speed in 90 DEG C, then add 8 parts of white cotton fibers and 0.5 part of BYK-ATU dispersant is uniformly dispersed with dispersion machine, reduces the temperature of batch mixing to 80 DEG C, be incubated 2min, then by batch mixing throw to In banbury at 115 DEG C banburying 4h;
Step 5, by the batch mixing tablet press machine obtained after step 4 banburying it is compressing after, obtain elastic polyurethane product.
Embodiment three
A kind of elastane, its preparation technology comprise the following steps:
Step 1, manufacture improvement after TPU resins, by mass ratio be 26% dimethicone, 38.5% TPR and 6% flax Oil is placed in turbine stirrer and is uniformly mixed, and mixed liquor is heated into 100 DEG C, by the organic siliconresin that mass ratio is 7% 160 DEG C are heated to after melting, is added in mixed liquor, the temperature of mixed liquor is kept at 100 DEG C, with 600rad/min stirring Speed stirs 3h, obtains mixed liquor;
Step 2, the talcum powder by mass ratio is 10.8%, 3.2% zinc stearate, 1.5% triethylamine nertralizer, 0.5% have Machine tin catalyst and 4.3% erucyl amide are added in the mixed liquor of step 1 after being uniformly mixed in agitator and are stirred Uniformly, the mixed liquor after then will be well mixed delivers to banburying 8h in banbury, is eventually adding the boric acid that mass ratio is 2.2% and allows Its coagulation forming, it is then the TPU resins after being improved by Twin screw extruder extruding pelletization, storage is standby;
Step 3, length is placed under 50 DEG C of hot blasts for the TPU resins after 3-7mm white cotton fiber and improvement and fully dried, Make the water content of the TPU resins after white cotton fiber and improvement in below 0.06wt%, it is standby;
Step 4, each component is weighed, by the TPU resins after 92 parts of improvement, 5 parts of wax powder, 13 parts of aerosils, 1 part VTES coupling agent, 0.5 part of antioxidant 168 and 1 part of organic-silicon-modified polysiloxane leveling agents are put In agitator, it is uniformly mixed under 600rad/min mixing speed in 90 DEG C, then adds 7 parts of white cotton fibers and 1 Part BYK-ATU dispersants are uniformly dispersed with dispersion machine, reduce the temperature of batch mixing to 80 DEG C, are incubated 2min, then batch mixing is thrown to close In mill at 110 DEG C banburying 5h;
Step 5, by the batch mixing tablet press machine obtained after step 4 banburying it is compressing after, obtain elastic polyurethane product.
Example IV
A kind of elastane, its preparation technology comprise the following steps:
Step 1, manufacture improvement after TPU resins, by mass ratio be 26% dimethicone, 38.5% TPR and 6% flax Oil is placed in turbine stirrer and is uniformly mixed, and mixed liquor is heated into 100 DEG C, by the organic siliconresin that mass ratio is 7% 160 DEG C are heated to after melting, is added in mixed liquor, the temperature of mixed liquor is kept at 100 DEG C, with 600rad/min stirring Speed stirs 3h, obtains mixed liquor;
Step 2, the talcum powder by mass ratio is 10.8%, 3.2% zinc stearate, 1.5% triethylamine nertralizer, 0.5% have Machine tin catalyst and 4.3% erucyl amide are added in the mixed liquor of step 1 after being uniformly mixed in agitator and are stirred Uniformly, the mixed liquor after then will be well mixed delivers to banburying 8h in banbury, is eventually adding the boric acid that mass ratio is 2.2% and allows Its coagulation forming, it is then the TPU resins after being improved by Twin screw extruder extruding pelletization, storage is standby;
Step 3, length is placed under 50 DEG C of hot blasts for the TPU resins after 3-7mm white cotton fiber and improvement and fully dried, Make the water content of the TPU resins after white cotton fiber and improvement in below 0.06wt%, it is standby;
Step 4, each component is weighed, by the TPU resins after 95 parts of improvement, 2 parts of wax powder, 12 parts of aerosils, 1 part VTES coupling agent, 0.5 part of antioxidant 168 and 0.5 part of organic-silicon-modified polysiloxane leveling agents Be placed in agitator, be uniformly mixed under 600rad/min mixing speed in 90 DEG C, then add 6 parts of white cotton fibers and 0.5 part of BYK-ATU dispersant is uniformly dispersed with dispersion machine, reduces the temperature of batch mixing to 80 DEG C, be incubated 2min, then by batch mixing throw to In banbury at 120 DEG C banburying 4h;
Step 5, by the batch mixing tablet press machine obtained after step 4 banburying it is compressing after, obtain elastic polyurethane product.
If elastic polyurethane product obtained above is respectively taken into dry sample, tested with testing equipments such as universal testing machines The main performance of elastane obtains, and the tensile strength of elastane reaches 13MPa, and tearing toughness reaches 23KN/m, ageing resistance reach 8%, and the rate of plastic deformation is minimum to reach 0.27%, have outstanding combination property.(Note:Ageing resistance It is that the decline percentage for surveying its performance after aging for a week in artificial accelerated aging case obtains, the test of plastic deformation is 1000 Measured after secondary Quick bending)
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, it is all the present invention spirit and All any modification, equivalent and improvement made within principle etc., should be included in the scope of the protection.

Claims (4)

1. a kind of elastane, for the holding plate sealing structure of oil rectifier, the holding plate passes through nut member It is sealedly and fixedly connected at the oil-out of support, it is characterised in that through hole on holding plate is coaxially disposed and led to entering oil hole Cross the first seal ring seal contact gap;Through hole edge on holding plate protrudes to form through hole boss, and the first seal ring set is in logical On the boss of hole, and the thickness of the first sealing ring is not less than the height of through hole boss, and the first sealing ring is by elastomeric polyurethane layer and painting The polytetrafluoroethylene floor composition of elastic polyurethane layer surface is overlying on, elastane is made up of the material of following parts by weight: TPU resin 90-95 parts, wax powder 2-5 parts, aerosil 12-15 parts, cotton fiber 6-8 parts, coupling agent 1-2 parts, antioxidant 0.5-1 parts, levelling agent 0.5-1 parts, dispersant 0.5-1 parts.
2. elastane as claimed in claim 1, it is characterised in that cotton fiber is just added by white cotton through roller gin The white cotton linter fiber obtained after work is made after disperseing.
3. elastane as claimed in claim 1, it is characterised in that TPU resins for improvement after TPU resins, institute The TPU resins after improvement are stated to be made by following steps:
Step 1, dimethicone that mass ratio is 26%, 38.5% TPR and 6% linseed oil be placed in turbine stirrer and stirred Mix well mixed, and mixed liquor be heated to 100 DEG C, the organic siliconresin that mass ratio is 7% is heated to 160 DEG C to after melting, It is added in mixed liquor, keeps the temperature of mixed liquor at 100 DEG C, stirs 3h with 600rad/min mixing speed, mixed Liquid;
Step 2, the talcum powder by mass ratio is 10.8%, 3.2% zinc stearate, 1.5% triethylamine nertralizer, 0.5% have Machine tin catalyst and 4.3% erucyl amide are added in the mixed liquor of step 1 after being uniformly mixed in agitator and are stirred Uniformly, the mixed liquor after then will be well mixed delivers to banburying 8h in banbury, is eventually adding the boric acid that mass ratio is 2.2% and allows Its coagulation forming.
4. elastane as claimed in claim 1, it is characterised in that the preparation technology of elastane includes Following steps:
Step 1, cotton fiber and TPU resins are placed under 50 DEG C of hot blasts and fully dried, contain cotton fiber and the water of TPU resins Amount is in below 0.06wt%;
Step 2, according to proportioning each component is weighed, TPU resins, wax powder, aerosil, cotton fiber, coupling agent is anti-oxidant Agent and levelling agent are placed in agitator, are uniformly mixed at 90 DEG C under 600rad/min mixing speed, are then added Cotton fiber is uniformly dispersed with dispersion machine, reduces the temperature of batch mixing to 80 DEG C, be incubated 2min, then by batch mixing throw into banbury in Banburying 4-5h at 110-120 DEG C;
It is step 3, the batch mixing tablet press machine obtained after step 2 banburying is compressing.
CN201710961961.2A 2016-09-23 2016-09-23 A kind of elastane Pending CN107882988A (en)

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