CN107881838B - 一种石头合成纸及其制备方法 - Google Patents

一种石头合成纸及其制备方法 Download PDF

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CN107881838B
CN107881838B CN201711167375.7A CN201711167375A CN107881838B CN 107881838 B CN107881838 B CN 107881838B CN 201711167375 A CN201711167375 A CN 201711167375A CN 107881838 B CN107881838 B CN 107881838B
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闫秋玲
赵化阵
轩海涵
轩伟
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Fujian Shixiang Environmental Protection Technology Co ltd
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Abstract

本发明公开了一种石头合成纸及其制备方法，它按照以下重量份的原料制成：CaCO360‑70，CaO5‑10，滑石粉3‑5，聚乙烯3‑5，聚乙烯蜡4‑6，硬脂酸锌3‑4，复合型偶联剂2.5‑4，分散剂1.5‑2，超微发泡剂1.5‑2，三氧化二锑1‑1.5，磷酸铵1.5‑2，氢氧化镁乳状悬浊液10‑15，十溴联苯酸1‑1.5，硫代硫酸钠1.5‑2，水合硼酸锌10‑15，改性氢氧化铝1‑2，过氧化二异丙苯0.5‑1；萜烯树脂1‑2，硬脂酸0.5‑0.8，云母颗粒18‑20，聚烯烃弹性体4‑6，玻璃纤维短纤2‑4，合成橡胶1‑2；采用上述结构，实现了抗压强度高，耐潮防水，耐腐蚀，不脱色，耐折并具有阻燃功能的效果。

Description

一种石头合成纸及其制备方法
技术领域
本发明涉及一种石头合成纸及其制备方法。
背景技术
目前，但随着人们环保观念的日益增强，再加上全球森林资源的日益匮乏和水土资源的日益短缺，生产纸箱用纸所需木材的采伐在许多国家都越来越受到限制，致使瓦楞纸箱业木材纤维的来源受到严重影响。且传统的纸箱纸板不宜在湿度较大的环境中长期使用，这会影响其强度，遇水会出现褪色现象，污染箱内货物。
上世纪五十年代，出现了以塑料、碳酸钙及多种助剂为原料，用吹膜法、流延法生产的环保合成纸，其特点是各项物理机械性能优于传统纸，耐潮湿、防水，耐腐蚀，尺寸稳定性好，满足了不同领域的多种要求，取代了传统纸的部分领域，合成纸生产过程中无三废排放，对环境无污染，并可将合成纸重复循环利用，是优良的环保型材料。新型的环保合成纸—石头纸，继承了合成纸的优点，并加以创新实现了3R原则（Reduce，Reuse，Recycle），即节约，重复利用，循环使用原则，这是造纸工业的一次变革，新型的环保型石头纸，石头纸做成的纸板后作成纸箱，将具有传统纸板所不具有的优点：抗压强度大，耐潮防水，耐腐蚀，不脱色等。但石头纸无法适用于传统的纸箱制作工艺。
发明内容
本发明的目的是一种结构简单，使用方便，抗压强度大，耐潮防水，耐腐蚀，不脱色，耐折并具有阻燃功能的石头合成纸。
1、为实现上述目的，本发明的技术方案是一种石头合成纸，其特征在于：它按照以下重量份的原料制成：CaCO360-70，CaO5-10，滑石粉3-5，聚乙烯3-5，聚乙烯蜡4-6，硬脂酸锌3-4，复合型偶联剂2.5-4，分散剂1.5-2，超微发泡剂1.5-2，三氧化二锑1-1.5，磷酸铵1.5-2，氢氧化镁乳状悬浊液10-15，十溴联苯酸1-1.5，硫代硫酸钠1.5-2，水合硼酸锌10-15，改性氢氧化铝1-2，过氧化二异丙苯0.5-1；萜烯树脂1-2，硬脂酸0.5-0.8，云母颗粒18-20，聚烯烃弹性体4-6，玻璃纤维短纤2-4，合成橡胶1-2。
本发明的技术方案还可以是它按照以下重量份的原料制成：CaCO370，CaO8，滑石粉3，聚乙烯3，聚乙烯蜡6，硬脂酸锌4，复合型偶联剂2.5，分散剂1.5，超微发泡剂2，三氧化二锑1，磷酸铵2，氢氧化镁乳状悬浊液10，十溴联苯酸1，硫代硫酸钠2，水合硼酸锌10，改性氢氧化铝2，过氧化二异丙苯0.5；萜烯树脂2，硬脂酸0.8，云母颗粒20，聚烯烃弹性体5，玻璃纤维短纤3，合成橡胶1.5。
本发明的技术方案还可以是它按照以下重量份的原料制成：CaCO365，CaO5，滑石粉3，聚乙烯5，聚乙烯蜡6，硬脂酸锌3，复合型偶联剂4，分散剂2，超微发泡剂1.5，三氧化二锑1.5，磷酸铵1.5，氢氧化镁乳状悬浊液15，十溴联苯酸1，硫代硫酸钠1.5，水合硼酸锌15，改性氢氧化铝1，过氧化二异丙苯1；萜烯树脂1，硬脂酸0.5，云母颗粒18，聚烯烃弹性体4，玻璃纤维短纤2，合成橡胶1，锰粉0.9，钛白粉0.8。
本发明的第二目的是提供一种制造上述石头合成纸的制备方法。
为实现上述第二目的，本发明的技术方案是一种石头合成纸的制备方法，它包括以下步骤：
它包括以下步骤：
步骤①:将CaCO3，CaO，滑石粉，聚乙烯，聚乙烯蜡，硬脂酸锌，复合型偶联剂，分散剂，超微发泡剂，三氧化二锑，磷酸铵，氢氧化镁乳状悬浊液，十溴联苯酸，硫代硫酸钠，水合硼酸锌，改性氢氧化铝，过氧化二异丙苯；萜烯树脂，硬脂酸，云母颗粒，聚烯烃弹性体，玻璃纤维短纤，合成橡胶通过搅拌机均匀混合然后进行真空烘干处理至含水量小于2%；
步骤②:分别将上述干燥后的混料经造粒机加热至100-110℃进行挤出造粒；
步骤③:将上述步骤②挤出的造粒分别通过螺旋推进装置输送至带挤出头的加热装置中，所述造粒在200-210℃温度下形成熔融流体，且此温度下所述熔融流体在所述超微发泡剂作用下会发泡，经发泡后挤出的所述熔融流体进入各自的真空定型平台，且该真空定型平台在真空压力0.6MPa下，经各自的第一牵引机构牵引定形至厚度为2-6mm，获得石头纸粗纸；
步骤④:将上述步骤③获得石头纸粗纸进入经第二加温装置进行加热，加热温度设置为130-140℃，通过对辊进行滚压，再经过第二牵引装置牵引定形后，通过55-60℃低温烘烤将第二次牵引后的石头纸箱纸板中应力消除，随后进入风冷装置，再通过对辊进行滚压3-8次达到设计厚度，将石头纸板冷却形成设定厚度为的石头合成纸，将上述石头合成纸卷轴打包。
与现有技术相比，本发明的有益效果是：生产过程中，不使用水源，不排放污水，不产生废物垃圾，不烧煤碳，不排放烟雾，石头合成纸的边角料可循环利用，防止了环境污染，由于其主要成分为CaCO3和助剂生产出的石头合成纸实现了抗压强度高，耐潮防水，耐腐蚀，不脱色，耐折并具有阻燃功能的效果。
具体实施方式
本发明涉及一种石头合成纸，其特征在于：它按照以下重量份的原料制成：CaCO360-70，CaO5-10，滑石粉3-5，聚乙烯3-5，聚乙烯蜡4-6，硬脂酸锌3-4，复合型偶联剂2.5-4，分散剂1.5-2，超微发泡剂1.5-2，三氧化二锑1-1.5，磷酸铵1.5-2，氢氧化镁乳状悬浊液10-15，十溴联苯酸1-1.5，硫代硫酸钠1.5-2，水合硼酸锌10-15，改性氢氧化铝1-2，过氧化二异丙苯0.5-1；萜烯树脂1-2，硬脂酸0.5-0.8，云母颗粒18-20，聚烯烃弹性体4-6，玻璃纤维短纤2-4，合成橡胶1-2。
本发明的技术方案还优选为它按照以下重量份的原料制成：CaCO370，CaO8，滑石粉3，聚乙烯3，聚乙烯蜡6，硬脂酸锌4，复合型偶联剂2.5，分散剂1.5，超微发泡剂2，三氧化二锑1，磷酸铵2，氢氧化镁乳状悬浊液10，十溴联苯酸1，硫代硫酸钠2，水合硼酸锌10，改性氢氧化铝2，过氧化二异丙苯0.5；萜烯树脂2，硬脂酸0.8，云母颗粒20，聚烯烃弹性体5，玻璃纤维短纤3，合成橡胶1.5。
本发明的技术方案还优选为它按照以下重量份的原料制成：CaCO365，CaO5，滑石粉3，聚乙烯5，聚乙烯蜡6，硬脂酸锌3，复合型偶联剂4，分散剂2，超微发泡剂1.5，三氧化二锑1.5，磷酸铵1.5，氢氧化镁乳状悬浊液15，十溴联苯酸1，硫代硫酸钠1.5，水合硼酸锌15，改性氢氧化铝1，过氧化二异丙苯1；萜烯树脂1，硬脂酸0.5，云母颗粒18，聚烯烃弹性体4，玻璃纤维短纤2，合成橡胶1，锰粉0.9，钛白粉0.8。
一种石头合成纸的制备方法，它包括以下步骤：
步骤①:将CaCO3，CaO，滑石粉，聚乙烯，聚乙烯蜡，硬脂酸锌，复合型偶联剂，分散剂，超微发泡剂，三氧化二锑，磷酸铵，氢氧化镁乳状悬浊液，十溴联苯酸，硫代硫酸钠，水合硼酸锌，改性氢氧化铝，过氧化二异丙苯；萜烯树脂，硬脂酸，云母颗粒，聚烯烃弹性体，玻璃纤维短纤，合成橡胶通过搅拌机均匀混合然后进行真空烘干处理至含水量小于2%；
步骤②:分别将上述干燥后的混料经造粒机加热至100-110℃进行挤出造粒；
步骤③:将上述步骤②挤出的造粒分别通过螺旋推进装置输送至带挤出头的加热装置中，所述造粒在200-210℃温度下形成熔融流体，且此温度下所述熔融流体在所述超微发泡剂作用下会发泡，经发泡后挤出的所述熔融流体进入各自的真空定型平台，且该真空定型平台在真空压力0.6MPa下，经各自的第一牵引机构牵引定形至厚度为2-6mm，获得石头纸粗纸；
步骤④:将上述步骤③获得石头纸粗纸进入经第二加温装置进行加热，加热温度设置为130-140℃，通过对辊进行滚压，再经过第二牵引装置牵引定形后，通过55-60℃低温烘烤将第二次牵引后的石头纸箱纸板中应力消除，随后进入风冷装置，再通过对辊进行滚压3-8次达到设计厚度，将石头纸板冷却形成设定厚度为的石头合成纸，将上述石头合成纸卷轴打包。
制作的上述结构的石头合成纸能够大大降低了生产成本，使石头合成纸在生产过程中，不使用水源，不排放污水，不产生废物垃圾，不烧煤碳，不排放烟雾，石头合成纸的边角料可循环利用，防止了环境污染，由于其主要成分为CaCO3和助剂生产出的纸箱纸板实现了抗压强度高，耐潮防水，耐腐蚀，不脱色，耐折并具有阻燃功能的效果。

Claims (3)

1.一种石头合成纸，由以下重量份的原料制成：CaCO3 60-70，CaO 5-10，滑石粉3-5，聚乙烯3-5，聚乙烯蜡4-6，硬脂酸锌3-4，复合型偶联剂2.5-4，分散剂1.5-2，超微发泡剂1.5-2，三氧化二锑1-1.5，磷酸铵1.5-2，氢氧化镁乳状悬浊液10-15，十溴联苯酸1-1.5，硫代硫酸钠1.5-2，水合硼酸锌10-15，改性氢氧化铝1-2，过氧化二异丙苯0.5-1；萜烯树脂1-2，硬脂酸0.5-0.8，云母颗粒18-20，聚烯烃弹性体4-6，玻璃纤维短纤2-4，合成橡胶1-2；
其特征在于，其通过如下步骤制备得到：
步骤①:将CaCO3，CaO，滑石粉，聚乙烯，聚乙烯蜡，硬脂酸锌，复合型偶联剂，分散剂，超微发泡剂，三氧化二锑，磷酸铵，氢氧化镁乳状悬浊液，十溴联苯酸，硫代硫酸钠，水合硼酸锌，改性氢氧化铝，过氧化二异丙苯；萜烯树脂，硬脂酸，云母颗粒，聚烯烃弹性体，玻璃纤维短纤，合成橡胶通过搅拌机均匀混合然后进行真空烘干处理至含水量小于2％；
步骤②:分别将上述干燥后的混料经造粒机加热至100-110℃进行挤出造粒；
步骤③:将上述步骤②挤出的造粒分别通过螺旋推进装置输送至带挤出头的加热装置中，所述造粒在200-210℃温度下形成熔融流体，且此温度下所述熔融流体在所述超微发泡剂作用下会发泡，经发泡后挤出的所述熔融流体进入各自的真空定型平台，且该真空定型平台在真空压力0.6MPa下，经各自的第一牵引机构牵引定形至厚度为2-6mm，获得石头纸粗纸；
步骤④:将上述步骤③获得石头纸粗纸进入经第二加温装置进行加热，加热温度设置为130-140℃，通过对辊进行滚压，再经过第二牵引装置牵引定形后，通过55-60℃低温烘烤将第二次牵引后的石头纸箱纸板中应力消除，随后进入风冷装置，再通过对辊进行滚压3-8次达到设计厚度，将石头纸板冷却形成设定厚度为的石头合成纸，将上述石头合成纸卷轴打包。
2.根据权利要求1所述的石头合成纸，其特征在于：由以下重量份的原料制成：CaCO370，CaO 8，滑石粉3，聚乙烯3，聚乙烯蜡6，硬脂酸锌4，复合型偶联剂2.5，分散剂1.5，超微发泡剂2，三氧化二锑1，磷酸铵2，氢氧化镁乳状悬浊液10，十溴联苯酸1，硫代硫酸钠2，水合硼酸锌10，改性氢氧化铝2，过氧化二异丙苯0.5；萜烯树脂2，硬脂酸0.8，云母颗粒20，聚烯烃弹性体5，玻璃纤维短纤3，合成橡胶1.5。
3.根据权利要求1所述的石头合成纸，其特征在于：由以下重量份的原料制成：CaCO365，CaO 5，滑石粉3，聚乙烯5，聚乙烯蜡6，硬脂酸锌3，复合型偶联剂4，分散剂2，超微发泡剂1.5，三氧化二锑1.5，磷酸铵1.5，氢氧化镁乳状悬浊液15，十溴联苯酸1，硫代硫酸钠1.5，水合硼酸锌15，改性氢氧化铝1，过氧化二异丙苯1；萜烯树脂1，硬脂酸0.5，云母颗粒18，聚烯烃弹性体4，玻璃纤维短纤2，合成橡胶1，锰粉0.9，钛白粉0.8。
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