CN107881779A - 一种刺绣用耐磨抗静电整理剂的制备方法 - Google Patents
一种刺绣用耐磨抗静电整理剂的制备方法 Download PDFInfo
- Publication number
- CN107881779A CN107881779A CN201711238706.1A CN201711238706A CN107881779A CN 107881779 A CN107881779 A CN 107881779A CN 201711238706 A CN201711238706 A CN 201711238706A CN 107881779 A CN107881779 A CN 107881779A
- Authority
- CN
- China
- Prior art keywords
- parts
- good
- wear
- finishing agent
- embroidery
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 238000002360 preparation method Methods 0.000 title claims abstract description 18
- NUVBSKCKDOMJSU-UHFFFAOYSA-N ethylparaben Chemical compound CCOC(=O)C1=CC=C(O)C=C1 NUVBSKCKDOMJSU-UHFFFAOYSA-N 0.000 claims abstract description 28
- FGIUAXJPYTZDNR-UHFFFAOYSA-N potassium nitrate Chemical compound [K+].[O-][N+]([O-])=O FGIUAXJPYTZDNR-UHFFFAOYSA-N 0.000 claims abstract description 24
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 19
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 claims abstract description 17
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 claims abstract description 17
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 17
- 239000000853 adhesive Substances 0.000 claims abstract description 15
- 230000001070 adhesive effect Effects 0.000 claims abstract description 15
- MQIUGAXCHLFZKX-UHFFFAOYSA-N Di-n-octyl phthalate Natural products CCCCCCCCOC(=O)C1=CC=CC=C1C(=O)OCCCCCCCC MQIUGAXCHLFZKX-UHFFFAOYSA-N 0.000 claims abstract description 14
- BJQHLKABXJIVAM-UHFFFAOYSA-N bis(2-ethylhexyl) phthalate Chemical compound CCCCC(CC)COC(=O)C1=CC=CC=C1C(=O)OCC(CC)CCCC BJQHLKABXJIVAM-UHFFFAOYSA-N 0.000 claims abstract description 14
- 235000010228 ethyl p-hydroxybenzoate Nutrition 0.000 claims abstract description 14
- 239000004403 ethyl p-hydroxybenzoate Substances 0.000 claims abstract description 14
- -1 dimethyl siloxane Chemical class 0.000 claims abstract description 13
- USDJGQLNFPZEON-UHFFFAOYSA-N [[4,6-bis(hydroxymethylamino)-1,3,5-triazin-2-yl]amino]methanol Chemical compound OCNC1=NC(NCO)=NC(NCO)=N1 USDJGQLNFPZEON-UHFFFAOYSA-N 0.000 claims abstract description 12
- 235000010333 potassium nitrate Nutrition 0.000 claims abstract description 12
- 239000004323 potassium nitrate Substances 0.000 claims abstract description 12
- 235000021355 Stearic acid Nutrition 0.000 claims abstract description 11
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims abstract description 11
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 claims abstract description 11
- 239000008117 stearic acid Substances 0.000 claims abstract description 11
- 238000002156 mixing Methods 0.000 claims description 17
- 238000010792 warming Methods 0.000 claims description 15
- 239000002994 raw material Substances 0.000 claims description 6
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 claims description 5
- 229920000877 Melamine resin Polymers 0.000 claims description 5
- 238000001914 filtration Methods 0.000 claims description 5
- 238000009413 insulation Methods 0.000 claims description 5
- JDSHMPZPIAZGSV-UHFFFAOYSA-N melamine Chemical compound NC1=NC(N)=NC(N)=N1 JDSHMPZPIAZGSV-UHFFFAOYSA-N 0.000 claims description 5
- 239000004576 sand Substances 0.000 claims description 5
- 125000002887 hydroxy group Chemical group [H]O* 0.000 claims description 4
- XNGIFLGASWRNHJ-UHFFFAOYSA-N phthalic acid Chemical compound OC(=O)C1=CC=CC=C1C(O)=O XNGIFLGASWRNHJ-UHFFFAOYSA-N 0.000 claims 6
- 150000002148 esters Chemical class 0.000 claims 3
- 239000007767 bonding agent Substances 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 14
- 241000588724 Escherichia coli Species 0.000 abstract description 5
- 238000005299 abrasion Methods 0.000 abstract description 5
- 238000005260 corrosion Methods 0.000 abstract description 5
- 230000007797 corrosion Effects 0.000 abstract description 5
- 238000001035 drying Methods 0.000 abstract description 5
- 238000005406 washing Methods 0.000 abstract description 5
- 230000000845 anti-microbial effect Effects 0.000 abstract description 4
- AYAUBWSUZRFVQO-UHFFFAOYSA-N 2-[2-(4-phenyl-5-sulfanylidene-1h-1,2,4-triazol-3-yl)ethyl]benzo[de]isoquinoline-1,3-dione Chemical compound O=C1C(C=23)=CC=CC3=CC=CC=2C(=O)N1CCC1=NNC(=S)N1C1=CC=CC=C1 AYAUBWSUZRFVQO-UHFFFAOYSA-N 0.000 abstract 1
- 239000004744 fabric Substances 0.000 description 9
- 239000000835 fiber Substances 0.000 description 9
- 125000003118 aryl group Chemical group 0.000 description 8
- 239000003205 fragrance Substances 0.000 description 6
- 239000000463 material Substances 0.000 description 5
- FJKROLUGYXJWQN-UHFFFAOYSA-N 4-hydroxybenzoic acid Chemical compound OC(=O)C1=CC=C(O)C=C1 FJKROLUGYXJWQN-UHFFFAOYSA-N 0.000 description 4
- 239000003094 microcapsule Substances 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 238000010417 needlework Methods 0.000 description 4
- 238000000034 method Methods 0.000 description 3
- 229920000728 polyester Polymers 0.000 description 3
- 238000009941 weaving Methods 0.000 description 3
- 229940090248 4-hydroxybenzoic acid Drugs 0.000 description 2
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 2
- 238000009956 embroidering Methods 0.000 description 2
- 125000004494 ethyl ester group Chemical group 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000004753 textile Substances 0.000 description 2
- DCXXMTOCNZCJGO-UHFFFAOYSA-N tristearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCCCCCCCCCC)COC(=O)CCCCCCCCCCCCCCCCC DCXXMTOCNZCJGO-UHFFFAOYSA-N 0.000 description 2
- 229920000742 Cotton Polymers 0.000 description 1
- 241000099774 Cuscuta salina Species 0.000 description 1
- 244000062175 Fittonia argyroneura Species 0.000 description 1
- 239000004900 Hydrophilic Finishing Agent Substances 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000010242 baoji Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000003115 biocidal effect Effects 0.000 description 1
- 238000005202 decontamination Methods 0.000 description 1
- 230000003588 decontaminative effect Effects 0.000 description 1
- 238000005034 decoration Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- XYIBRDXRRQCHLP-UHFFFAOYSA-N ethyl acetoacetate Chemical compound CCOC(=O)CC(C)=O XYIBRDXRRQCHLP-UHFFFAOYSA-N 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 230000002209 hydrophobic effect Effects 0.000 description 1
- 230000000147 hypnotic effect Effects 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 239000007937 lozenge Substances 0.000 description 1
- 238000010428 oil painting Methods 0.000 description 1
- 238000010422 painting Methods 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 229960003742 phenol Drugs 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000009988 textile finishing Methods 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/50—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with organometallic compounds; with organic compounds containing boron, silicon, selenium or tellurium atoms
- D06M13/51—Compounds with at least one carbon-metal or carbon-boron, carbon-silicon, carbon-selenium, or carbon-tellurium bond
- D06M13/513—Compounds with at least one carbon-metal or carbon-boron, carbon-silicon, carbon-selenium, or carbon-tellurium bond with at least one carbon-silicon bond
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
- D06M11/45—Oxides or hydroxides of elements of Groups 3 or 13 of the Periodic Table; Aluminates
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/58—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with nitrogen or compounds thereof, e.g. with nitrides
- D06M11/64—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with nitrogen or compounds thereof, e.g. with nitrides with nitrogen oxides; with oxyacids of nitrogen or their salts
- D06M11/65—Salts of oxyacids of nitrogen
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
- D06M13/188—Monocarboxylic acids; Anhydrides, halides or salts thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
- D06M13/2246—Esters of unsaturated carboxylic acids
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/35—Heterocyclic compounds
- D06M13/355—Heterocyclic compounds having six-membered heterocyclic rings
- D06M13/358—Triazines
- D06M13/364—Cyanuric acid; Isocyanuric acid; Derivatives thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/53—Polyethers
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/30—Flame or heat resistance, fire retardancy properties
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/35—Abrasion, pilling or fibrillation resistance
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/50—Modified hand or grip properties; Softening compositions
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Microbiology (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
本申请公开了一种刺绣用耐磨抗静电整理剂的制备方法，称取RO纯水、邻苯二甲酸二辛酯、粘合剂、硬脂酸、醋酸酯、氧化铝、二甲基硅氧烷、三羟甲基三聚氰胺、对羟基苯甲酸乙酯、硝酸钾和脂肪醇聚氧乙烯醚；制备方法简单，耐候性好，防霉效果好，抗拉强度2‑4MPa，抗潮气性优良，耐磨性好；增加光泽，附着力高，附着力1级，耐腐蚀性好，耐洗刷性200‑400次，平滑亲水性好；洗涤40‑80次后，收缩率0.02‑0.04%，耐水洗性50‑90次螨虫趋避率96‑98%，柔韧性1mm，光泽度好；抗静电性好，延长刺绣使用寿命，干燥快，阻燃性能好，抗菌性能好，对大肠杆菌抑菌率99‑99.8%。
Description
技术领域
本申请属于刺绣材料领域，尤其涉及一种刺绣用耐磨抗静电整理剂的制备方法。
背景技术
手工刺绣的主要艺术特点是图案工整绢秀，色彩清新高雅，针法丰富，雅艳相宜，绣工精巧细腻绝伦。就刺绣的针法而言，极其丰富而变化无穷，共有9 大类43种，主要有齐针、抡针、套针、施针、乱针、滚针、切针、平金、打点、打子、结子、网绣、冰纹针、挑花、纳锦、刻鳞针、施毛针、穿珠针等等，采用不同的针法可以生产不同的线条组织和独特的手工刺绣艺术表现效果。例如，运用施针、滚针绣的珍禽异兽，毛丝颂顺，活灵活现，栩栩如生；采用散套针绣的花卉，活色生香，香味朴鼻，尽态尽妍；使用乱针绣的人像和风景，绒条组织多变，装饰味浓，艺术效果强，富有浓郁的民间、民族特色；刺绣是中国优秀的传统工艺，有着悠久的历史。刺绣是一种在织物上用各种线料织出种种不同图案的工艺。根据各种古墓出土的帛画和刺绣等实物可知，远在3000多年前的殷周时代，中国就已有华美的暗花绸和多彩刺绣。在河南发现的商代刺绣实物，是中国最早的刺绣工艺品。这种刺绣花纹为菱形纹和折角波浪纹，在花纹线条的边缘使用加绞拈的丝线，工艺达到了相当高的水平。西周(公元前1100~前771年)的刺绣印痕发现于陕西省宝鸡茹家庄的西周墓中。这种刺绣采用今天还在使用的辫子股绣的针法，运用了双线条，线条舒卷自如，针脚也相当均匀齐整，说明刺绣技巧是很熟练的。
这种丝织刺绣工艺品的生产，不仅对中国社会起了很大的作用，而且在国际文化生活中也产生了很大的作用与影响。到了秦汉时期(公元前221~公元220年)刺绣已发展到了较高的水平，绣品也成为对外输出的主要商品。由于中国是丝绸的故乡，自古以来，富者以“闺房绣楼”为贞，北京的京绣、温州的瓯绣、上海的顾绣、苗族的苗绣等，产地不同，风格烔异。刺绣的针法有错针绣、乱针绣、网绣、满地绣等。刺绣的花卉不闻犹香，飞禽栩栩如生。走兽神态逼真。解放后，中国将油画、中国画、照片等艺术形式运用于刺绣，使之达到远看是画、近看地绣的绝妙效果。刺绣品的用途也进一步扩大，从戏剧服装到日常生活中的枕套、台布、屏风、壁挂及生活服装等等。此外，刺绣品还是中国传统的外贸产品，经济价值很高。
许多芳香剂具有镇静、杀菌、催眠、保健等作用,但是,把芳香剂简单地喷洒在纺织品上,其留香期很短,用芳香剂作囊芯制备的芳香微胶囊弥补了这一缺陷。芳香剂微胶囊化后,芯材与外界环境隔绝,使其性质基本不变,开始时在微胶囊外层的香精散发香味,在穿着过程中,由于摩擦、受热等外力作用,微胶囊内部的香精缓缓地释放香味,起到长效缓释的作用,从而使纺织品具有相当持久的芳香功能。芳香微胶囊具有缓释性,香味的释放速率能得到有效地控制,使得整理过的纺织品能够长期释放出香味,满足了人们对芳香纺织品的需求。
织物整理是在织物上施加一种整理剂，它能改变织物的表面性能，从而赋予织物特殊的功能。有机硅聚酯纤维整理剂含有多种活性基团,经它处理过的三维中空和中空纤维具有滑爽、蓬松、手感柔软、弹性足等特点,同时也提高了纤维了耐搓性。
聚酯纤维具有许多天然纤维无法比拟的优良性能,如弹性好、强度高、耐磨性好等,但由于其是典型的疏水性纤维,在服用或装饰用过程中存在易带静电、易吸污、难去污及手感差等缺点。其中的改善方法之一就是用亲水整理剂对聚酯纤维进行后整理加工,赋予织物亲水性、抗静电性和柔软性。用于纯棉、毛、丝、麻、化纤、各种棍纺织物.使织物手感柔软、厚实猾爽、弹性好、耐洗、耐磨。
发明内容
解决的技术问题：
本申请针对上述技术问题，提供一种刺绣用耐磨抗静电整理剂的制备方法，解决现有刺绣用耐磨抗静电整理剂防霉效果差、光泽度低和耐磨性差等技术问题。
技术方案：
一种刺绣用耐磨抗静电整理剂的制备方法，包括如下步骤：
第一步：按照重量份数配比称取RO纯水100份、邻苯二甲酸二辛酯10-50份、粘合剂0.5-10.5份、硬脂酸0.5-4.5份、醋酸酯1-20份、氧化铝10-30份、二甲基硅氧烷15-35份、三羟甲基三聚氰胺1-5份、对羟基苯甲酸乙酯5-9份、硝酸钾3-7份和脂肪醇聚氧乙烯醚2-8份；
第二步：将氧化铝、三羟甲基三聚氰胺和对羟基苯甲酸乙酯投入带有温度计、搅拌机和加热装置的反应釜中，打开搅拌机混合，升温至45-65℃，混合速度为250-350r/min，混合20-30min；
第三步：依次加入醋酸酯、RO纯水和邻苯二甲酸二辛酯，升温至70-90℃，调节混合速度至400-600 r/min，保温反应40-60min，加入剩余原料，升温至95-105℃，混合80-120min，溶解完全后将混合均匀的产物投入砂磨机中，砂磨2次，过滤后冷却至20-40℃即得。
作为本发明的一种优选技术方案：所述第一步中刺绣用耐磨抗静电整理剂的原料按重量份数配比如下：RO纯水100份、邻苯二甲酸二辛酯10份、粘合剂0.5份、硬脂酸0.5份、醋酸酯1份、氧化铝10份、二甲基硅氧烷15份、三羟甲基三聚氰胺1份、对羟基苯甲酸乙酯5份、硝酸钾3份和脂肪醇聚氧乙烯醚2份。
作为本发明的一种优选技术方案：所述第一步中刺绣用耐磨抗静电整理剂的原料按重量份数配比如下：RO纯水100份、邻苯二甲酸二辛酯50份、粘合剂10.5份、硬脂酸4.5份、醋酸酯20份、氧化铝30份、二甲基硅氧烷35份、三羟甲基三聚氰胺5份、对羟基苯甲酸乙酯9份、硝酸钾7份和脂肪醇聚氧乙烯醚8份。
作为本发明的一种优选技术方案：所述第一步中刺绣用耐磨抗静电整理剂的原料按重量份数配比如下：RO纯水100份、邻苯二甲酸二辛酯30份、粘合剂5.5份、硬脂酸2.5份、醋酸酯10份、氧化铝20份、二甲基硅氧烷25份、三羟甲基三聚氰胺3份、对羟基苯甲酸乙酯7份、硝酸钾5份和脂肪醇聚氧乙烯醚5份。
作为本发明的一种优选技术方案：所述粘合剂采用丙烯酸酯。
有益效果：
本发明所述一种刺绣用耐磨抗静电整理剂的制备方法采用以上技术方案与现有技术相比，具有以下技术效果：1、制备方法简单，耐候性好，防霉效果好，抗拉强度2-4MPa，抗潮气性优良，耐磨性好；2、增加光泽，附着力高，附着力1级，耐腐蚀性好，耐洗刷性200-400次，平滑亲水性好；3、洗涤40-80次后，收缩率0.02-0.04%，耐水洗性50-90次螨虫趋避率96-98%，柔韧性1mm，光泽度好；4、抗静电性好，延长刺绣使用寿命，干燥快，阻燃性能好，抗菌性能好，对大肠杆菌抑菌率99-99.8%，可以广泛生产并不断代替现有材料。
具体实施方式
实施例1:
按照重量份数配比称取RO纯水100份、邻苯二甲酸二辛酯10份、丙烯酸酯0.5份、硬脂酸0.5份、醋酸酯1份、氧化铝10份、二甲基硅氧烷15份、三羟甲基三聚氰胺1份、对羟基苯甲酸乙酯5份、硝酸钾3份和脂肪醇聚氧乙烯醚2份。
将氧化铝、三羟甲基三聚氰胺和对羟基苯甲酸乙酯投入带有温度计、搅拌机和加热装置的反应釜中，打开搅拌机混合，升温至45℃，混合速度为250r/min，混合20min。
依次加入醋酸酯、RO纯水和邻苯二甲酸二辛酯，升温至70℃，调节混合速度至400r/min，保温反应40min，加入剩余原料，升温至95℃，混合80min，溶解完全后将混合均匀的产物投入砂磨机中，砂磨2次，过滤后冷却至20℃即得。
制备方法简单，耐候性好，防霉效果好，抗拉强度2MPa，抗潮气性优良，耐磨性好；增加光泽，附着力高，附着力1级，耐腐蚀性好，耐洗刷性200次，平滑亲水性好；洗涤40次后，收缩率0.04%，耐水洗性50次螨虫趋避率96%，柔韧性1mm，光泽度好；抗静电性好，延长刺绣使用寿命，干燥快，阻燃性能好，抗菌性能好，对大肠杆菌抑菌率99%，可以广泛生产并不断代替现有材料。
实施例2:
按照重量份数配比称取RO纯水100份、邻苯二甲酸二辛酯50份、丙烯酸酯10.5份、硬脂酸4.5份、醋酸酯20份、氧化铝30份、二甲基硅氧烷35份、三羟甲基三聚氰胺5份、对羟基苯甲酸乙酯9份、硝酸钾7份和脂肪醇聚氧乙烯醚8份。
将氧化铝、三羟甲基三聚氰胺和对羟基苯甲酸乙酯投入带有温度计、搅拌机和加热装置的反应釜中，打开搅拌机混合，升温至65℃，混合速度为350r/min，混合30min。
依次加入醋酸酯、RO纯水和邻苯二甲酸二辛酯，升温至90℃，调节混合速度至600r/min，保温反应60min，加入剩余原料，升温至105℃，混合120min，溶解完全后将混合均匀的产物投入砂磨机中，砂磨2次，过滤后冷却至40℃即得。
制备方法简单，耐候性好，防霉效果好，抗拉强度3MPa，抗潮气性优良，耐磨性好；增加光泽，附着力高，附着力1级，耐腐蚀性好，耐洗刷性300次，平滑亲水性好；洗涤60次后，收缩率0.03%，耐水洗性70次螨虫趋避率97%，柔韧性1mm，光泽度好；抗静电性好，延长刺绣使用寿命，干燥快，阻燃性能好，抗菌性能好，对大肠杆菌抑菌率99.4%，可以广泛生产并不断代替现有材料。
实施例3:
按照重量份数配比称取RO纯水100份、邻苯二甲酸二辛酯30份、丙烯酸酯5.5份、硬脂酸2.5份、醋酸酯10份、氧化铝20份、二甲基硅氧烷25份、三羟甲基三聚氰胺3份、对羟基苯甲酸乙酯7份、硝酸钾5份和脂肪醇聚氧乙烯醚5份。
将氧化铝、三羟甲基三聚氰胺和对羟基苯甲酸乙酯投入带有温度计、搅拌机和加热装置的反应釜中，打开搅拌机混合，升温至55℃，混合速度为300r/min，混合25min。
依次加入醋酸酯、RO纯水和邻苯二甲酸二辛酯，升温至80℃，调节混合速度至500r/min，保温反应50min，加入剩余原料，升温至100℃，混合100min，溶解完全后将混合均匀的产物投入砂磨机中，砂磨2次，过滤后冷却至30℃即得。
制备方法简单，耐候性好，防霉效果好，抗拉强度4MPa，抗潮气性优良，耐磨性好；增加光泽，附着力高，附着力1级，耐腐蚀性好，耐洗刷性400次，平滑亲水性好；洗涤80次后，收缩率0.02%，耐水洗性90次螨虫趋避率98%，柔韧性1mm，光泽度好；抗静电性好，延长刺绣使用寿命，干燥快，阻燃性能好，抗菌性能好，对大肠杆菌抑菌率99.8%，可以广泛生产并不断代替现有材料。
以上实施例中的组合物所有组分均可以商业购买。
上述实施例只是用于对本发明的内容进行阐述，而不是限制，因此在与本发明的权利要求书相当的含义和范围内的任何改变，都应该认为是包括在权利要求书的范围内。
Claims (5)
1.一种刺绣用耐磨抗静电整理剂的制备方法，其特征在于，包括如下步骤：
第一步：按照重量份数配比称取RO纯水100份、邻苯二甲酸二辛酯10-50份、粘合剂0.5-10.5份、硬脂酸0.5-4.5份、醋酸酯1-20份、氧化铝10-30份、二甲基硅氧烷15-35份、三羟甲基三聚氰胺1-5份、对羟基苯甲酸乙酯5-9份、硝酸钾3-7份和脂肪醇聚氧乙烯醚2-8份；
第二步：将氧化铝、三羟甲基三聚氰胺和对羟基苯甲酸乙酯投入带有温度计、搅拌机和加热装置的反应釜中，打开搅拌机混合，升温至45-65℃，混合速度为250-350r/min，混合20-30min；
第三步：依次加入醋酸酯、RO纯水和邻苯二甲酸二辛酯，升温至70-90℃，调节混合速度至400-600 r/min，保温反应40-60min，加入剩余原料，升温至95-105℃，混合80-120min，溶解完全后将混合均匀的产物投入砂磨机中，砂磨2次，过滤后冷却至20-40℃即得。
2.根据权利要求1所述的刺绣用耐磨抗静电整理剂的制备方法，其特征在于：所述第一步中刺绣用耐磨抗静电整理剂的原料按重量份数配比如下：RO纯水100份、邻苯二甲酸二辛酯10份、粘合剂0.5份、硬脂酸0.5份、醋酸酯1份、氧化铝10份、二甲基硅氧烷15份、三羟甲基三聚氰胺1份、对羟基苯甲酸乙酯5份、硝酸钾3份和脂肪醇聚氧乙烯醚2份。
3.根据权利要求1所述的刺绣用耐磨抗静电整理剂的制备方法，其特征在于：所述第一步中刺绣用耐磨抗静电整理剂的原料按重量份数配比如下：RO纯水100份、邻苯二甲酸二辛酯50份、粘合剂10.5份、硬脂酸4.5份、醋酸酯20份、氧化铝30份、二甲基硅氧烷35份、三羟甲基三聚氰胺5份、对羟基苯甲酸乙酯9份、硝酸钾7份和脂肪醇聚氧乙烯醚8份。
4.根据权利要求1所述的刺绣用耐磨抗静电整理剂的制备方法，其特征在于：所述第一步中刺绣用耐磨抗静电整理剂的原料按重量份数配比如下：RO纯水100份、邻苯二甲酸二辛酯30份、粘合剂5.5份、硬脂酸2.5份、醋酸酯10份、氧化铝20份、二甲基硅氧烷25份、三羟甲基三聚氰胺3份、对羟基苯甲酸乙酯7份、硝酸钾5份和脂肪醇聚氧乙烯醚5份。
5.根据权利要求1所述的刺绣用耐磨抗静电整理剂的制备方法，其特征在于：所述粘合剂采用丙烯酸酯。
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711238706.1A CN107881779A (zh) | 2017-11-30 | 2017-11-30 | 一种刺绣用耐磨抗静电整理剂的制备方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711238706.1A CN107881779A (zh) | 2017-11-30 | 2017-11-30 | 一种刺绣用耐磨抗静电整理剂的制备方法 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107881779A true CN107881779A (zh) | 2018-04-06 |
Family
ID=61776219
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711238706.1A Withdrawn CN107881779A (zh) | 2017-11-30 | 2017-11-30 | 一种刺绣用耐磨抗静电整理剂的制备方法 |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107881779A (zh) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20210162489A1 (en) * | 2018-07-27 | 2021-06-03 | HÜTTENES-ALBERTUS Chemische Werke Gesellschaft mit beschränkter Haftung | Wash composition for reducing formaldehyde emissions |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103496209A (zh) * | 2013-10-21 | 2014-01-08 | 田艳 | 一种抗菌防静电耐磨布料 |
| CN103665645A (zh) * | 2013-11-29 | 2014-03-26 | 青岛科创塑料机械有限公司 | 一种环保耐磨抗静电塑料 |
| CN105780470A (zh) * | 2016-04-29 | 2016-07-20 | 江苏苏扬服帽有限公司 | 一种用于针织物的高效抗静电剂、其制备方法及其应用 |
-
2017
- 2017-11-30 CN CN201711238706.1A patent/CN107881779A/zh not_active Withdrawn
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103496209A (zh) * | 2013-10-21 | 2014-01-08 | 田艳 | 一种抗菌防静电耐磨布料 |
| CN103665645A (zh) * | 2013-11-29 | 2014-03-26 | 青岛科创塑料机械有限公司 | 一种环保耐磨抗静电塑料 |
| CN105780470A (zh) * | 2016-04-29 | 2016-07-20 | 江苏苏扬服帽有限公司 | 一种用于针织物的高效抗静电剂、其制备方法及其应用 |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20210162489A1 (en) * | 2018-07-27 | 2021-06-03 | HÜTTENES-ALBERTUS Chemische Werke Gesellschaft mit beschränkter Haftung | Wash composition for reducing formaldehyde emissions |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102312342B (zh) | 多功能保暖内衣面料及其加工方法 | |
| CN107794621A (zh) | 一种隐藏提字松紧织带的制造方法 | |
| CN100365183C (zh) | 一种织物的生产方法 | |
| CN101949075A (zh) | 一种含竹炭纤维的毛衫原料 | |
| CN104947261A (zh) | 一种优质绣花线及其加工方法 | |
| Arifovna et al. | CHARACTERISTICS-OF-UZBEK-EMBROIDERY | |
| CN102644142A (zh) | 一种抗菌防霉服装面料 | |
| CN103924395B (zh) | 粗纺绒线双面机绣的方法和应用 | |
| CN203792824U (zh) | 一种四层结构的透气针织花边面料 | |
| CN105442165A (zh) | 一种天丝棉丝光面料及其生产方法 | |
| CN103046218B (zh) | 抗菌耐磨罗布麻纤维的蕾丝花边的制备工艺 | |
| CN107881779A (zh) | 一种刺绣用耐磨抗静电整理剂的制备方法 | |
| CN1563559A (zh) | 成衣染色图形一体化艺术染整工艺 | |
| CN104846569A (zh) | 一种双面三异绣法 | |
| CN105908498A (zh) | 一种高速数码印花以及真丝金银丝交织工艺 | |
| CN101058929A (zh) | 新型绣花工艺 | |
| CN1851079A (zh) | 机织仿传统手工地毯的生产方法 | |
| CN1045733A (zh) | 绒绣壁挂 | |
| CN107956113A (zh) | 一种刺绣用防霉整理剂的制备方法 | |
| CN107794758A (zh) | 一种刺绣用整理剂的制备方法 | |
| CN105256437A (zh) | 镂空蕾丝面料 | |
| CN207277061U (zh) | 一种幻彩针织衫面料 | |
| CN107938350A (zh) | 一种刺绣用柔软整理剂的制备方法 | |
| CN108589092A (zh) | 一种双面刺绣工艺 | |
| Akinrujomu | Embroidery as a form of decorative stitches in art |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WW01 | Invention patent application withdrawn after publication | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20180406 |