CN107881465A - A kind of technique of glass physical vapour deposition color film - Google Patents

A kind of technique of glass physical vapour deposition color film Download PDF

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Publication number
CN107881465A
CN107881465A CN201711113442.7A CN201711113442A CN107881465A CN 107881465 A CN107881465 A CN 107881465A CN 201711113442 A CN201711113442 A CN 201711113442A CN 107881465 A CN107881465 A CN 107881465A
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China
Prior art keywords
glass
film
afterwards
coating equipment
vacuum coating
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Application number
CN201711113442.7A
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Chinese (zh)
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CN107881465B (en
Inventor
王春生
贾志江
张荣晋
孙爽
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Suzhou Anjie Technology Co Ltd
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Suzhou Anjie Technology Co Ltd
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Priority to CN201711113442.7A priority Critical patent/CN107881465B/en
Publication of CN107881465A publication Critical patent/CN107881465A/en
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    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C14/00Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
    • C23C14/04Coating on selected surface areas, e.g. using masks
    • C23C14/042Coating on selected surface areas, e.g. using masks using masks
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B41PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
    • B41MPRINTING, DUPLICATING, MARKING, OR COPYING PROCESSES; COLOUR PRINTING
    • B41M1/00Inking and printing with a printer's forme
    • B41M1/12Stencil printing; Silk-screen printing
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C17/00Surface treatment of glass, not in the form of fibres or filaments, by coating
    • C03C17/22Surface treatment of glass, not in the form of fibres or filaments, by coating with other inorganic material
    • C03C17/23Oxides
    • C03C17/25Oxides by deposition from the liquid phase
    • C03C17/256Coating containing TiO2
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C14/00Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
    • C23C14/06Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the coating material
    • C23C14/08Oxides
    • C23C14/083Oxides of refractory metals or yttrium

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Physical Vapour Deposition (AREA)
  • Surface Treatment Of Glass (AREA)

Abstract

The invention provides a kind of technique of glass physical vapour deposition color film, and it causes the easy to make, quick of color film, and the aberration for making the color film formed is small, can be suitably used for industrial production.Predefine the parameter of glass, corresponding parameter is inputted into vacuum coating equipment afterwards, film design software in vacuum coating equipment according to the parameter of glass and need plated film thickness calculate automatically required for deposition material inventory and quantitative value, corresponding deposition material is put into vacuum coating equipment, glass is put on the machine umbrella leaf of vacuum coating equipment afterwards, start vacuum coating equipment operation physical vapour deposition (PVD) program, afterwards physical vapour deposition (PVD) film exposed surface silk-screen corresponding color ink, exposure imaging is dried afterwards, value of chromatism is measured to glass afterwards, appropriate color is made further according to colour table requirement by silk-screen to adjust.

Description

A kind of technique of glass physical vapour deposition color film
Technical field
The present invention relates to the technical field of glass surface treatment, specially a kind of work of glass physical vapour deposition color film Skill.
Background technology
When the surface of existing glass needs to set color film, it needs the technique by complexity to make to form corresponding face Color film, and the aberration for making the color film formed is relatively large so that it is not applied for field of industrial production.
The content of the invention
In view of the above-mentioned problems, the invention provides a kind of technique of glass physical vapour deposition color film, it causes color Film it is easy to make, quick, and make formed color film aberration it is small, can be suitably used for industrial production.
A kind of technique of glass physical vapour deposition color film, it is characterised in that:The parameter of glass is predefined, afterwards will Corresponding parameter inputs vacuum coating equipment, and the film design software in vacuum coating equipment is according to the parameter of glass and needs the thickness of plated film Degree is automatic to calculate required deposition material inventory and quantitative value, and corresponding deposition material is put into vacuum coating equipment, it Glass is put on the machine umbrella leaf of vacuum coating equipment afterwards, starts vacuum coating equipment operation physical vapour deposition (PVD) program, Zhi Hou The ink of the exposed surface silk-screen corresponding color of physical vapour deposition (PVD) film, dries exposure imaging, glass is surveyed afterwards afterwards Value of chromatism is measured, making appropriate color by silk-screen further according to colour table requirement adjusts.
It is further characterized by:
The glass is AG glass or light glass, when the glass is AG glass, the AG parameters input according to corresponding to it Vacuum coating equipment;
In the silk-screen printing process, printing screen plate selects 250 mesh polyester half tones, and printing screen plate tension force is 25N ± 1N;
When needing to carry out yellow plated film, the TiO that thickness is 90nm is plated respectively by vacuum coating equipment2Film, thickness are 71nm SiO2Film, the TiO that thickness is 85nm2Film, wherein vacuum are 3.0 × 10-5T, temperature is 60 DEG C, is sunk in physical vapor The exposed surface silk-screen of integrated membrane corresponds to the ink of yellow, dries exposure imaging afterwards, measures value of chromatism to glass afterwards, then Appropriate color is made according to colour table requirement to adjust;
The thickness is 90nm TiO2Plating film pressure when film carries out plated film is 1.2 × 10-4T;
The thickness is 85nm TiO2Plating film pressure when film carries out plated film is 1.2 × 10-4T。
After technique using the present invention, due to the parameter and the thickness of film according to glass, set by the film of vacuum coating equipment Meter software calculates required deposition material inventory and quantitative value automatically, is completed afterwards by vacuum coating equipment for glass The coating process of physical vapour deposition (PVD) film, it is corresponding in the exposed surface silk-screen of physical vapour deposition (PVD) film after then glass is taken out The ink of color, exposure imaging is dried afterwards, value of chromatism is measured to glass afterwards, made further according to colour table requirement by silk-screen Go out appropriate color adjustment so that color film it is easy to make, quick, and the aberration for making the color film formed is small, can be applicable In industrial production.
Embodiment
A kind of technique of glass physical vapour deposition color film:The parameter of glass is predefined, afterwards by corresponding parameter Vacuum coating equipment is inputted, the film design software in vacuum coating equipment is according to the parameter of glass and needs the thickness of plated film to calculate automatically Deposition material inventory and quantitative value required for going out, corresponding deposition material is put into vacuum coating equipment, afterwards put glass Enter on the machine umbrella leaf of vacuum coating equipment, start vacuum coating equipment operation physical vapour deposition (PVD) program, sunk afterwards in physical vapor The ink of the exposed surface silk-screen corresponding color of integrated membrane, dries exposure imaging afterwards, measures value of chromatism to glass afterwards, then Appropriate color is made according to colour table requirement by silk-screen to adjust.
Glass is AG glass or light glass, when glass is AG glass, the AG parameters input vacuum coating according to corresponding to it Machine.
Specific embodiment:Yellow film is plated on light glass, the film design software in vacuum coating equipment is according to the parameter of glass Deposition material inventory and quantitative value required for being calculated automatically with the thickness for needing plated film, corresponding deposition material is put into very In empty coating machine, glass is put on the machine umbrella leaf of vacuum coating equipment afterwards, plating thickness respectively by vacuum coating equipment is 90nm TiO2Film, the SiO that thickness is 71nm2Film, the TiO that thickness is 85nm2Film, wherein vacuum are 3.0 × 10-5T, temperature For 60 DEG C, the ink of yellow is corresponded in the exposed surface silk-screen of physical vapour deposition (PVD) film, exposure imaging is dried afterwards, afterwards to glass Glass measures value of chromatism, and making appropriate color further according to colour table requirement adjusts;
Thickness is 90nm TiO2Plating film pressure when film carries out plated film is 1.2 × 10-4T;
Thickness is 85nm TiO2Plating film pressure when film carries out plated film is 1.2 × 10-4T。
The specific embodiment of the present invention is described in detail above, but content is only the preferable implementation of the invention Example, it is impossible to be considered as the practical range for limiting the invention.All impartial changes made according to the invention application range Change and improvement etc., all should still be belonged within this patent covering scope.

Claims (6)

  1. A kind of 1. technique of glass physical vapour deposition color film, it is characterised in that:The parameter of glass is predefined, afterwards will be right The parameter input vacuum coating equipment answered, film design software in vacuum coating equipment is according to the parameter of glass and needs the thickness of plated film It is automatic to calculate required deposition material inventory and quantitative value, corresponding deposition material is put into vacuum coating equipment, afterwards Glass is put on the machine umbrella leaf of vacuum coating equipment, starts vacuum coating equipment operation physical vapour deposition (PVD) program, afterwards in thing The ink of the exposed surface silk-screen corresponding color of physical vapor deposition film, dries exposure imaging, glass is measured afterwards afterwards Value of chromatism, appropriate color is made by silk-screen further according to colour table requirement and adjusted.
  2. A kind of 2. technique of glass physical vapour deposition color film as claimed in claim 1, it is characterised in that:The glass is AG glass or light glass, when the glass is AG glass, the AG parameters input vacuum coating equipment according to corresponding to it.
  3. A kind of 3. technique of glass physical vapour deposition color film as claimed in claim 1, it is characterised in that:The silk-screen mistake Cheng Zhong, printing screen plate select 250 mesh polyester half tones, and printing screen plate tension force is 25N ± 1N.
  4. A kind of 4. technique of glass physical vapour deposition color film as claimed in claim 1, it is characterised in that:When needing to carry out During yellow plated film, the TiO that thickness is 90nm is plated respectively by vacuum coating equipment2Film, the SiO that thickness is 71nm2Film, thickness are 85nm TiO2Film, wherein vacuum are 3.0 × 10-5T, temperature is 60 DEG C, in the exposed surface silk-screen of physical vapour deposition (PVD) film The ink of corresponding yellow, dries exposure imaging, measures value of chromatism to glass afterwards afterwards, is made further according to colour table requirement suitable When color adjustment.
  5. A kind of 5. technique of glass physical vapour deposition color film as claimed in claim 4, it is characterised in that:The thickness is 90nm TiO2Plating film pressure when film carries out plated film is 1.2 × 10-4T。
  6. A kind of 6. technique of glass physical vapour deposition color film as claimed in claim 4, it is characterised in that:The thickness is 85nm TiO2Plating film pressure when film carries out plated film is 1.2 × 10-4T。
CN201711113442.7A 2017-11-13 2017-11-13 Method for physically vapor depositing color film on glass Active CN107881465B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201711113442.7A CN107881465B (en) 2017-11-13 2017-11-13 Method for physically vapor depositing color film on glass

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201711113442.7A CN107881465B (en) 2017-11-13 2017-11-13 Method for physically vapor depositing color film on glass

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CN107881465A true CN107881465A (en) 2018-04-06
CN107881465B CN107881465B (en) 2020-04-21

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108914067A (en) * 2018-08-14 2018-11-30 苏州安洁科技股份有限公司 A kind of cell phone rear cover PVD gradient color coating process
CN108973373A (en) * 2018-08-01 2018-12-11 苏州安洁科技股份有限公司 Be cracked after plated film membrane stress removal technique on a kind of ink layer
CN110643946A (en) * 2019-11-12 2020-01-03 安徽安合鑫光电科技有限公司 PVD (physical vapor deposition) gradient-color coating process for mobile phone rear cover
CN111549315A (en) * 2020-06-23 2020-08-18 中建材蚌埠玻璃工业设计研究院有限公司 Rapid prefabrication method for multiple colors of single-layer structure colored glass
CN115626780A (en) * 2022-10-31 2023-01-20 四川虹基光玻新材料科技有限公司 Manufacturing method of glass cover plate, glass cover plate and display device

Citations (9)

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CN1622981A (en) * 2001-07-12 2005-06-01 默克专利股份有限公司 Multilayer pigments based on glass flakes
CN102615875A (en) * 2012-03-22 2012-08-01 东莞劲胜精密组件股份有限公司 Discontinuous metallic silver membrane and membrane coating method for same
CN102877024A (en) * 2012-09-27 2013-01-16 厦门建霖工业有限公司 Pearl-like film coating method
CN103243301A (en) * 2013-04-26 2013-08-14 东莞华清光学科技有限公司 Method for displaying three-dimensional pattern through vacuum coating
CN103395310A (en) * 2013-07-04 2013-11-20 广东星星光电科技有限公司 Composite printing technology of mobile phone glass with 3D effect
CN204066067U (en) * 2014-06-19 2014-12-31 南昌欧菲光学技术有限公司 Infrared composite transparent sheet and there is the touch-screen of described infrared composite transparent sheet
CN105459656A (en) * 2015-11-30 2016-04-06 广东星弛光电科技有限公司 Printing process for fluorescent display mobile phone protection screen
CN105739789A (en) * 2016-03-14 2016-07-06 东莞劲胜精密组件股份有限公司 Electronic touch control screen and coated film preparation technology
CN206584057U (en) * 2016-12-05 2017-10-24 福建省辉锐电子技术有限公司 A kind of coated cover-plate and touch-screen

Patent Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1622981A (en) * 2001-07-12 2005-06-01 默克专利股份有限公司 Multilayer pigments based on glass flakes
CN102615875A (en) * 2012-03-22 2012-08-01 东莞劲胜精密组件股份有限公司 Discontinuous metallic silver membrane and membrane coating method for same
CN102877024A (en) * 2012-09-27 2013-01-16 厦门建霖工业有限公司 Pearl-like film coating method
CN103243301A (en) * 2013-04-26 2013-08-14 东莞华清光学科技有限公司 Method for displaying three-dimensional pattern through vacuum coating
CN103395310A (en) * 2013-07-04 2013-11-20 广东星星光电科技有限公司 Composite printing technology of mobile phone glass with 3D effect
CN204066067U (en) * 2014-06-19 2014-12-31 南昌欧菲光学技术有限公司 Infrared composite transparent sheet and there is the touch-screen of described infrared composite transparent sheet
CN105459656A (en) * 2015-11-30 2016-04-06 广东星弛光电科技有限公司 Printing process for fluorescent display mobile phone protection screen
CN105739789A (en) * 2016-03-14 2016-07-06 东莞劲胜精密组件股份有限公司 Electronic touch control screen and coated film preparation technology
CN206584057U (en) * 2016-12-05 2017-10-24 福建省辉锐电子技术有限公司 A kind of coated cover-plate and touch-screen

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108973373A (en) * 2018-08-01 2018-12-11 苏州安洁科技股份有限公司 Be cracked after plated film membrane stress removal technique on a kind of ink layer
CN108914067A (en) * 2018-08-14 2018-11-30 苏州安洁科技股份有限公司 A kind of cell phone rear cover PVD gradient color coating process
CN110643946A (en) * 2019-11-12 2020-01-03 安徽安合鑫光电科技有限公司 PVD (physical vapor deposition) gradient-color coating process for mobile phone rear cover
CN111549315A (en) * 2020-06-23 2020-08-18 中建材蚌埠玻璃工业设计研究院有限公司 Rapid prefabrication method for multiple colors of single-layer structure colored glass
CN115626780A (en) * 2022-10-31 2023-01-20 四川虹基光玻新材料科技有限公司 Manufacturing method of glass cover plate, glass cover plate and display device

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