CN107868701A - The preparation method of apricot extract - Google Patents
The preparation method of apricot extract Download PDFInfo
- Publication number
- CN107868701A CN107868701A CN201711096383.7A CN201711096383A CN107868701A CN 107868701 A CN107868701 A CN 107868701A CN 201711096383 A CN201711096383 A CN 201711096383A CN 107868701 A CN107868701 A CN 107868701A
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- CN
- China
- Prior art keywords
- apricot
- extraction
- preparation
- raw material
- apricot extract
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
Abstract
The present invention relates to a kind of preparation method of apricot extract, comprise the following steps that：（1）Pretreatment of raw material, by raw material cleaning removal of impurities, remove fruit stone；（2）Flash extracter rapid extraction；（3）Filter off the removal of impurity；（4）Macroporous resin adsorption；（5）Ethanol elution；（6）Eluent is concentrated under reduced pressure, and obtains apricot extract.The aroma of pure for the apricot extract that the present invention obtains has natural apricot odor characteristic true to nature, can be widely used in the perfumed products such as daily use chemicals, tobacco, improve the quality of perfumed products, beautify the life of people naturally, stability is good.
Description
Technical field
The present invention relates to a kind of preparation method of apricot extract, belong to active ingredients of plants extraction and separation technology field.
Background technology
Apricot sweet mouthfeel, fragrance is tempting, is a kind of fruit that people enjoy a lot, and apricot often makes achievement by people
The food such as dried meat, fruit juice.Research in recent years finds that high-quality apricot contains alpha, beta-lonone, linalool, hexyl acetate, γ-decalactone
It is the quality raw materials for preparing high-grade natural fruit fragrance essence Deng multiple fragrance material.At present to apricot Studies on Analysis of Flavor Constituents
Study more, but using apricot as raw material, the technical study for preparing apricot extract has not found.
As people pay close attention to health, back to nature, natural product enjoys people to pursue, and apricot essence on the market at present
All be to be formed with synthesizing perfume material allotment, in order to meet the needs of people are to natural product, this patent provide it is a kind of using apricot as
The method that raw material prepares apricot extract, to meet the needs of people, beautify the life of people.
The content of the invention
The purpose of the present invention is to overcome the deficiencies in the prior art, there is provided a kind of preparation method of apricot extract,
Using apricot as raw material, using homogenate extraction, macroreticular resin isolation technics, apricot extract, the apricot extract tool of preparation are prepared
There is the graceful tempting fruit aroma style of apricot.
According to technical scheme provided by the invention, the preparation method of the apricot extract, it is characterized in that, including following work
Skill step, component ratio by mass number meter：
（1）Pretreatment of raw material：Apricot is cleaned and cleaned, the fruit stone of apricot is removed, obtains raw material；
（2）Homogenate extraction：1 part of raw material after processing is fitted into flash extracter, adds 20 ~ 25 parts of deionized waters, opens and dodges
Formula extractor carries out homogenate extraction, 30 ~ 50 seconds extraction times；
（3）Filtering：The material filtering that homogenate extraction is obtained removes pulp impurity, then miscellaneous with organic membrane filter, retention macromolecular
Matter；
（4）Absorption：It will be adsorbed by the extraction clear liquid being filtrated to get twice through large pore resin absorption column；
（5）Elution：With the macroporous absorbent resin after the ethanol elution absorption of material quality 88 ~ 95%, elution speed is：30~
40ml/min；
（6）Concentration：Obtained eluent is transferred in rotary evaporator and is concentrated under reduced pressure, vacuum is during concentration：0.092~
0.098Mpa, temperature of charge are：55 ~ 60 DEG C, concentrate is concentrated into put into 25 ~ the 30 ‰ of material quality, obtains apricot extraction
Thing.
Further, the step（3）The material that the middle strainer filtering homogenate extraction using 300 ~ 400 mesh obtains.
Further, the step（3）The specification of middle organic film is：The maximum molecular weight of retention is 2000 ~ 4000,
UF membrane is carried out under 0.1 ~ 0.4MPa pressure conditions.
Further, the step（4）The model of middle polymeric adsorbent：DA-201 type macroporous absorbent resins, adsorption rate
For：20~30ml/min.
The advantage of the invention is that：The extraction of advanced flash extracter, macroreticular resin isolation technics are combined, for original
The extraction separation of material and purifying, both technologies have the advantages of operation temperature is low（Operate at room temperature）, effectively prevent
Flavor matter easily oxidized, so as to preferably retain the fragrance of apricot script, is improved apricot extraction by thermal oxide in apricot
The value of thing, while the extraction time of homogenate extraction is only tens seconds, relative to traditional extracting method extraction of several hours
Time, extraction time is substantially reduced, improve efficiency.The apricot extract that this patent obtains not only maintains apricot fruit head
Fragrant original appearance, fragrance is especially naturally pure and fresh, stable lasting, has apricot fruit odor characteristic true to nature, and preparation method is not
Complexity, raw material availability is high, and easily operation, pollution-free.
Embodiment
With reference to specific embodiment, the invention will be further described.
Rotary evaporator used in the present invention is the RE-52AA type rotary evaporations of Shanghai Yarong Biochemical Instrument Plant's production
Device；
Embodiment one：A kind of preparation method of apricot extract, is comprised the following steps that：
（1）Pretreatment of raw material：Raw material is cleaned and cleaned, removes the fruit stone of apricot；
（2）Homogenate extraction：1 part of raw material after processing is loaded into homogenate extraction wherein, adds 20 parts of deionized waters, opens flash carry
Device is taken to carry out homogenate extraction, 50 seconds extraction times；
（3）Filtering：After homogenate extraction terminates, material is released, first with the strainer filtering of 300 mesh, removes the impurity such as tiny pulp,
It is being with the specification of organic membrane filter, film：The maximum molecular weight of retention is 2000, and film is carried out under the conditions of 0.1MPa operating pressures
Separation, removes big molecular impurity；
（4）Absorption：Large pore resin absorption column on the extraction clear liquid being filtrated to get twice will be passed through to be adsorbed, the type of polymeric adsorbent
Number it is：DA-201 type macroporous absorbent resins, adsorption rate are：20ml/min；
（5）Elution：With the macroporous absorbent resin after the ethanol elution absorption of input material quality 88%, elution speed is：30ml/
min；
（6）Concentration：Obtained eluent is transferred in rotary evaporator and is concentrated under reduced pressure, vacuum is during concentration：0.092Mpa,
Temperature of charge is：60 DEG C, concentrate is concentrated into put into the 25 ‰ of material quality, obtains apricot extract.
Embodiment two：The preparation method of one seed extract, is comprised the following steps that：
（1）Pretreatment of raw material：Raw material is cleaned and cleaned, removes the fruit stone of apricot；
（2）Homogenate extraction：1 part of raw material after processing is loaded into homogenate extraction wherein, adds 25 parts of deionized waters, opens flash carry
Device is taken to carry out homogenate extraction, 30 seconds extraction times；
（3）Filtering：After homogenate extraction terminates, material is released, first with the strainer filtering of 400 mesh, removes the impurity such as tiny pulp,
It is being with the specification of organic membrane filter, film：The maximum molecular weight of retention is 4000, and film is carried out under the conditions of 0.4MPa operating pressures
Separation, removes big molecular impurity；
（4）Absorption：Large pore resin absorption column on the extraction clear liquid being filtrated to get twice will be passed through to be adsorbed, the type of polymeric adsorbent
Number it is：DA-201 type macroporous absorbent resins, adsorption rate 30ml/min；
（5）Elution：With the macroporous absorbent resin after the ethanol elution absorption of input material quality 92%, elution speed is：40ml/
min；
（6）Concentration：Obtained eluent is transferred in rotary evaporator and is concentrated under reduced pressure, vacuum is during concentration：0.098Mpa,
Temperature of charge is：55 DEG C, concentrate is concentrated into put into the 30 ‰ of material quality, obtains apricot extract.
Embodiment three：A kind of preparation method of apricot extract, is comprised the following steps that：
（1）Pretreatment of raw material：Raw material is cleaned and cleaned, removes the fruit stone of apricot；
（2）Homogenate extraction：1 part of raw material after processing is loaded into homogenate extraction wherein, adds 23 parts of deionized waters, opens flash carry
Device is taken to carry out homogenate extraction, 40 seconds extraction times；
（3）Filtering：After homogenate extraction terminates, material is released, first with the strainer filtering of 350 mesh, removes the impurity such as tiny pulp,
It is being with the specification of organic membrane filter, film：The maximum molecular weight of retention is 3000, is carried out under the conditions of 0.25MPa operating pressures
UF membrane, remove big molecular impurity；
（4）Absorption：Large pore resin absorption column on the extraction clear liquid being filtrated to get twice will be passed through to be adsorbed, the type of polymeric adsorbent
Number it is：DA-201 type macroporous absorbent resins, adsorption rate are：25ml/min；
（5）Elution：With the macroporous absorbent resin after the ethanol elution absorption of input material quality 94%, elution speed is：35ml/
min；
（6）Concentration：Obtained eluent is transferred in rotary evaporator and is concentrated under reduced pressure, vacuum is during concentration：0.096Mpa,
Temperature of charge is：58 DEG C, concentrate is concentrated into put into the 28 ‰ of material quality, obtains apricot extract.
Claims (4)
1. a kind of preparation method of apricot extract, it is characterized in that, comprise the following steps that, component ratio by mass number
Meter：
（1）Pretreatment of raw material：Apricot is cleaned and cleaned, the fruit stone of apricot is removed, obtains raw material；
（2）Homogenate extraction：1 part of raw material after processing is fitted into flash extracter, adds 20 ~ 25 parts of deionized waters, opens and dodges
Formula extractor carries out homogenate extraction, 30 ~ 50 seconds extraction times；
（3）Filtering：The material filtering that homogenate extraction is obtained removes pulp impurity, then miscellaneous with organic membrane filter, retention macromolecular
Matter；
（4）Absorption：It will be adsorbed by the extraction clear liquid being filtrated to get twice through large pore resin absorption column；
（5）Elution：With the macroporous absorbent resin after the ethanol elution absorption of material quality 88 ~ 95%, elution speed is：30~
40ml/min；
（6）Concentration：Obtained eluent is transferred in rotary evaporator and is concentrated under reduced pressure, vacuum is during concentration：0.092~
0.098Mpa, temperature of charge are：55 ~ 60 DEG C, concentrate is concentrated into put into 25 ~ the 30 ‰ of material quality, obtains apricot extraction
Thing.
2. the preparation method of apricot extract as claimed in claim 1, it is characterized in that：The step（3）It is middle to use 300 ~ 400
The material that purpose strainer filtering homogenate extraction obtains.
3. the preparation method of apricot extract as claimed in claim 1, it is characterized in that：The step（3）The rule of middle organic film
Lattice are：The maximum molecular weight of retention is 2000 ~ 4000, and UF membrane is carried out under 0.1 ~ 0.4MPa pressure conditions.
4. the preparation method of apricot extract as claimed in claim 1, it is characterized in that：The step（4）Middle polymeric adsorbent
Model：DA-201 type macroporous absorbent resins, adsorption rate are：20~30ml/min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711096383.7A CN107868701A (en) | 2017-11-09 | 2017-11-09 | The preparation method of apricot extract |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711096383.7A CN107868701A (en) | 2017-11-09 | 2017-11-09 | The preparation method of apricot extract |
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| Publication Number | Publication Date |
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| CN107868701A true CN107868701A (en) | 2018-04-03 |
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| CN201711096383.7A Pending CN107868701A (en) | 2017-11-09 | 2017-11-09 | The preparation method of apricot extract |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109393409A (en) * | 2018-11-12 | 2019-03-01 | 高永腾 | A kind of compound nectar of moistening lung to arrest cough and preparation method thereof |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2000345186A (en) * | 1999-06-02 | 2000-12-12 | Kishibe Keori Kk | Natural flavoring agent, its production and bedding provided with the same |
| CN1316494A (en) * | 2000-04-06 | 2001-10-10 | 张高 | Process for extracting antioxidizing agent and perfume from rosemary |
| CN104531353A (en) * | 2014-12-19 | 2015-04-22 | 湖北中烟工业有限责任公司 | Casing flavor for light flavor-style cigarettes |
| CN104830537A (en) * | 2015-04-30 | 2015-08-12 | 东莞波顿香料有限公司 | Preparation method and application of aquilaria wood hydrolat |
| CN105831792A (en) * | 2016-04-27 | 2016-08-10 | 中国烟草总公司郑州烟草研究院 | Method for preparing roasted fragrant and sweet components of red dates and application of roasted fragrant and sweet components of red dates to pipe tobacco |
| CN107235949A (en) * | 2017-06-16 | 2017-10-10 | 湖南华诚生物资源股份有限公司 | A kind of extracting method without plasticiser cyanidin extract |
-
2017
- 2017-11-09 CN CN201711096383.7A patent/CN107868701A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2000345186A (en) * | 1999-06-02 | 2000-12-12 | Kishibe Keori Kk | Natural flavoring agent, its production and bedding provided with the same |
| CN1316494A (en) * | 2000-04-06 | 2001-10-10 | 张高 | Process for extracting antioxidizing agent and perfume from rosemary |
| CN104531353A (en) * | 2014-12-19 | 2015-04-22 | 湖北中烟工业有限责任公司 | Casing flavor for light flavor-style cigarettes |
| CN104830537A (en) * | 2015-04-30 | 2015-08-12 | 东莞波顿香料有限公司 | Preparation method and application of aquilaria wood hydrolat |
| CN105831792A (en) * | 2016-04-27 | 2016-08-10 | 中国烟草总公司郑州烟草研究院 | Method for preparing roasted fragrant and sweet components of red dates and application of roasted fragrant and sweet components of red dates to pipe tobacco |
| CN107235949A (en) * | 2017-06-16 | 2017-10-10 | 湖南华诚生物资源股份有限公司 | A kind of extracting method without plasticiser cyanidin extract |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109393409A (en) * | 2018-11-12 | 2019-03-01 | 高永腾 | A kind of compound nectar of moistening lung to arrest cough and preparation method thereof |
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Application publication date: 20180403 |
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