CN107868133A - A kind of immersion process in processing of farm products production - Google Patents

A kind of immersion process in processing of farm products production Download PDF

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Publication number
CN107868133A
CN107868133A CN201711191755.4A CN201711191755A CN107868133A CN 107868133 A CN107868133 A CN 107868133A CN 201711191755 A CN201711191755 A CN 201711191755A CN 107868133 A CN107868133 A CN 107868133A
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China
Prior art keywords
soak
corn
immersion
immersion process
agricultural product
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CN201711191755.4A
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Chinese (zh)
Inventor
李荣杰
纪传侠
尚海涛
穆晓玲
孙杨静
李文
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Anhui Bbca Group Co ltd
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Anhui BBCA Fermentation Technology Engineering Research Co Ltd
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Priority to CN201711191755.4A priority Critical patent/CN107868133A/en
Publication of CN107868133A publication Critical patent/CN107868133A/en
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    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08BPOLYSACCHARIDES; DERIVATIVES THEREOF
    • C08B30/00Preparation of starch, degraded or non-chemically modified starch, amylose, or amylopectin
    • C08B30/04Extraction or purification
    • C08B30/042Extraction or purification from cereals or grains
    • C08B30/044Extraction or purification from cereals or grains from corn or maize
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08HDERIVATIVES OF NATURAL MACROMOLECULAR COMPOUNDS
    • C08H1/00Macromolecular products derived from proteins
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21BFIBROUS RAW MATERIALS OR THEIR MECHANICAL TREATMENT
    • D21B1/00Fibrous raw materials or their mechanical treatment
    • D21B1/04Fibrous raw materials or their mechanical treatment by dividing raw materials into small particles, e.g. fibres
    • D21B1/12Fibrous raw materials or their mechanical treatment by dividing raw materials into small particles, e.g. fibres by wet methods, by the use of steam
    • D21B1/30Defibrating by other means
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21BFIBROUS RAW MATERIALS OR THEIR MECHANICAL TREATMENT
    • D21B1/00Fibrous raw materials or their mechanical treatment
    • D21B1/04Fibrous raw materials or their mechanical treatment by dividing raw materials into small particles, e.g. fibres
    • D21B1/12Fibrous raw materials or their mechanical treatment by dividing raw materials into small particles, e.g. fibres by wet methods, by the use of steam
    • D21B1/30Defibrating by other means
    • D21B1/34Kneading or mixing; Pulpers

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Wood Science & Technology (AREA)
  • Mechanical Engineering (AREA)
  • Coloring Foods And Improving Nutritive Qualities (AREA)

Abstract

The present invention relates to processing of farm products field, specifically discloses the immersion process in a kind of processing of farm products production.The present invention utilizes the SO in the substitution of vitamin C whole or part substitution traditional handicraft2The agricultural product such as soaking corn, reach the immersion effect suitable with traditional soaking technology, and the SO in using vitamin C all substitution traditional handicraft2, will be without SO in all products when being soaked2Residual, can reach international food standards.Maize germ, zein fiber, cornstarch and the zein of corn reprocessing gained after immersion are directly edible, without carrying out desulfurization process, simplify production process.Moreover, immersion terminates nutritious in the soak that is obtained afterwards, can be developed into nourishing beverage or as food auxiliary material etc..

Description

A kind of immersion process in processing of farm products production
Technical field
The present invention relates to processing of farm products field, in particular it relates to the immersion process in a kind of processing of farm products production.
Background technology
Corn belongs to one of world's Three major grain crops, and its product cornstarch, zein, maize germ, corn are fine Dimension etc. is widely used in the fields such as food, beverage, medicine, feed.How the relatively high yield pulp1 of above-mentioned product is obtained in production, The severe challenge that always every country and area are faced.
At present, starch is extracted from corn typically has two methods of dry and wet, and wherein wet underwater welding cornstarch is Many countries and regions obtain the main method of cornstarch.But in wet underwater welding cornstarch technique, immersion process is it In a mostly important step process, the degree of corn soaking, decide the progress of subsequent technique.Sulfurous is used in traditional handicraft Acid or solution of sodium bisulfite carry out corn soaking, and the starch release for making to wrap up in protein comes out.
For example, Publication No. CN103265639A Chinese patent discloses the corn soaking in a kind of production of corn starch Technique, using 7 tank infusion methods, including enter No. 7 tank of broken mill and add No. 1 tank of new corn, into before broken mill No. 6 tank add new relieving haperacidity, the sulfurous acid concentration of new relieving haperacidity is 0.15~0.17%;Before adding new relieving haperacidity, using tank switching method, i.e., It is in opposite direction with feeding intake for corn, the soak of the 6th to No. 1 each tank of tank is poured into small sequence number tank from big sequence number tank adverse current successively In, after tank switching terminates, for the liquid level of each tank soak untill corn is soaked and do not revealed, the liquid level of each tank soak is identical;Heating Heating, after heating terminates, the 6th to No. 2 tank soak temperature is incremented by step by step successively by tank switching direction, and its thermograde difference is 1 DEG C, the sulfurous acid concentration of soak successively decreases step by step by tank switching direction, and its concentration difference is 0.02%, wherein after No. 6 tank heating Temperature is 48 DEG C, and the sulfurous acid concentration of soak is 0.10%.
For another example Publication No. CN104558213A Chinese patent application discloses a kind of immersion work for preparing cornstarch Skill, comprise the following steps:(1) once soak:Iblet is squeezed into steeping tank, sulfurous acid solution is then added into steeping tank, The mass percentage concentration of the steeping tank sulfite is 0.08~0.1%, in the steeping tank temperature of soak for 50~ 52 DEG C, soak 5~6 hours, a soak is made;(2) inoculating lactic acid bacterium:To a soak made from the step (1) The middle lactic acid bacteria for adding corn total amount 4-6%, fermentation time are 4~6 hours, and fermentation temperature is 33~38 DEG C, obtains zymotic fluid; (3) coarse crushing:Secondary soak is filtered off into zymotic fluid by gravity curved screen, two then are carried out to hominy grits by crushing system It is secondary broken, keep corn particle to be broken into 6~8 valves, (4) secondary immersion:Added into zymotic fluid made from the step (2) beautiful The cellulase and 0.2~0.5% acid protease of rice total amount 0.1~0.3%, are kept for 4~6 hours at 48~52 DEG C, Into the production process of starch.
However, the above method, in process is soaked, added with sulfurous acid, it decomposes the SO of generation2Environmental pollution pole Greatly, and the health of people can be caused to seriously endanger.Moreover, due to SO in the product of its production gained2Residual It is higher, it is impossible to meet international food standards requirement, can not directly eat so that products obtained therefrom also needs to carry out at follow-up desulfurization Reason, causes technique cumbersome, complicated, adds production cost.
Therefore, a kind of dosage for reducing soaking technology sulfite of exploitation is needed badly, or directly without using the leaching of sulfurous acid Bubble method, produced for the deep processing of corn or other agricultural product.
The content of the invention
In order to solve problems of the prior art, in being produced it is an object of the invention to provide a kind of processing of farm products Immersion process.
In order to realize the object of the invention, technical scheme is as follows:
Firstth, the immersion process in being produced the invention provides a kind of processing of farm products, by the agricultural product by pretreatment It is placed in containing being soaked in ascorbic soak.
Immersion process of the present invention realizes the destruction to protein net using vitamin C, so as to reach release starch, Protein isolate matter etc. soaks purpose.
Present contribution to the art is to be found that ascorbic above-mentioned effect, develops vitamin C in agricultural production New opplication in terms of product deep processing.
In order to reduce SO in traditional soaking technology2, sulfurous acid or its derive salt usage amount, and then reduce immersion after produce The SO of product2Residual, the present invention provide a kind of immersion process, substitute the SO in traditional soaking technology using Vitamin C fraction2(or it is sub- The derivative salt of sulfuric acid or sulfurous acid).The present invention pass through experimental studies have found that, after being soaked using vitamin C, separation prepare form sediment The yield of the products such as powder is with using traditional soaking technology (SO2) obtained by yield it is suitable, therefore, vitamin C proposed by the present invention It is a kind of good replacement composition.
Preferably, in order to cost-effective, the desulfurization process to agricultural product after immersion or its reprocessing product, this hair are saved It is bright that a kind of preferable immersion process is provided, the SO in traditional soaking technology is all substituted using vitamin C2(or sulfurous acid or Asia The derivative salt of sulfuric acid), i.e., SO is not contained in the soak used in described immersion process2, sulfurous acid or its derive salt.
Further, the dip operation meets the conventional immersion requirement in this area, does not usually have soak Soak.
Further, ascorbic mass concentration is 0.01~5% in soak of the present invention.
Preferably, ascorbic mass concentration is 0.2~0.8% in the soak.When ascorbic concentration expires During the foot condition, preferably immersion centrifugation can be played on the basis of control cost.
Further, the pretreatment of foregoing agricultural product includes:Agricultural product are screened, impurity is removed and goes mouldy Agricultural product;And the agricultural product after screening are cleaned.Its concrete operations meets the custom requirements of this area, the present invention Preprocess method is not construed as limiting separately.
Further, in order to improve immersion efficiency, the soaking conditionses are put to be closed in 30~65 DEG C of water bath with thermostatic control 36~72h is put, the condition of preferably described immersion is 45~60h of closed placement in 40~55 DEG C of water bath with thermostatic control, more preferably The closed placement 48h in 50 DEG C of water bath with thermostatic control.
Further, after being terminated using immersion process of the present invention immersion, the agricultural product is separated with soak, can be obtained Agricultural product after to immersion and containing nutritious soak.
The soak is recyclable to be continuing with, and avoids ascorbic waste, can also be directly entered downstream production technology, Prepare reprocessing product.
Agricultural product of the present invention can be corn, wheat, soybean, paddy etc..
In the specific embodiment of the present invention, select the agricultural product as corn, immersion terminate after, by corn with Soak separates, corn after being soaked and containing nutritious soak;Corn after the immersion can be further Processing, production zein fiber, plumule, starch or protein product;And then can further it be prepared as containing nutritious soak The food such as beverage, flavouring, or health products, or medicine etc..
Secondth, the preceding solution based on the present invention, present invention also offers one kind using foregoing immersion process to agriculture Contain nutritious soak obtained by after product immersion, and the gained soak is preparing food, health products or medicine The application of aspect.
The present invention relates to raw material or reagent be ordinary commercial products, the operation being related to is unless otherwise specified This area routine operation.
On the basis of common sense in the field is met, above-mentioned each optimum condition, it can be mutually combined, obtain specific embodiment party Formula.
The beneficial effects of the present invention are:
The present invention utilizes the SO in the substitution of vitamin C whole or part substitution traditional handicraft2The agricultural product such as soaking corn, reach To the immersion effect suitable with traditional soaking technology, and the SO in using vitamin C all substitution traditional handicraft2Soaked , will be without SO in all products during bubble2Residual, can reach international food standards.The maize of corn reprocessing gained after immersion Bud, zein fiber, cornstarch and zein are directly edible, without carrying out desulfurization process, simplify production process.Not only such as This, immersion terminates nutritious in the soak that is obtained afterwards, can be developed into nourishing beverage or as food auxiliary material etc..
Embodiment
The preferred embodiment of the present invention is described in detail below in conjunction with embodiment.It is it will be appreciated that following real Providing merely to play the purpose of explanation for example is applied, is not used to limit the scope of the present invention.The skill of this area Art personnel can carry out various modifications and replacement in the case of without departing substantially from spirit of the invention and spirit to the present invention.
Experimental method used in following embodiments is conventional method unless otherwise specified.
Material used, reagent etc., unless otherwise specified, are commercially obtained in following embodiments.
Embodiment 1
The present embodiment is used to illustrate that immersion process provided by the present invention is applied to maize germ, fiber, starch and albumen Preparation, comprise the following steps that:
Step (1):The corn purchased is screened, impurity and the corn that goes mouldy is removed, weighs corn 1000g;
Step (2):By the corn after weighing in beaker, while 1000mL running water is added, shake about 2min, cleaning Terminate, remove wash water, by same procedure repeated washing 3 times;
Step (3):Corn after cleaning is transferred in 2500mL port grinding bottles;
Step (4):0.4% vitamin C soak 1800g is added in port grinding bottle, it is close in 55 DEG C of water bath with thermostatic control Close and place 48h;
Step (5):The corn soaked after terminating is filtered, obtains corn and corn steep liquor;
Step (6):Corn obtained by step (5) is poured into wall-breaking machine, about 2000mL running water is added, is crushed, Obtain corn slurries;
Step (7):Corn slurries obtained by step (6) are placed in 5000mL beaker, the jade on top is taken out with strainer Rice plumule, then stir the corn slurries to plumule and suspend, then plumule is fished for strainer.Repeatedly the operation into slurries without plumule Untill.The thick plumule of taking-up is repeatedly washed with running water, 12h is bakeed in 105 DEG C of baking oven, obtains maize germ;
Step (8):Step (7) is taken off to the corn slurries after embryo and obtains crude fibre, further powder by the bent sieve of fiber separation Repeatedly washed with running water after broken, centrifuge separating and dehydrating, dry, obtain fibrous finished product;
Step (9):Corn slurries of the step (8) after the bent sieve of fiber are separated with disk plate centrifuge, obtain jade Rice Crude starch and The Corn Protein slurries;
Step (10):By corn Crude starch obtained by step (9), carry out multi-stage countercurrent with running water and wash, remove residual Insoluble protein, drying, cornstarch finished product is made;
Step (11):By The Corn Protein slurries obtained by step (9), repeatedly washed, be concentrated in vacuo with running water, from The heart is dehydrated, and finally obtains The Corn Protein by drying, crushing.
While above step is carried out, one group of 0.2%SO is carried out2The parallel control experiment of immersion.
Result of the test:The plumule yield that 0.4% vitamin C soaks in the present embodiment is 3.73%, and 0.2%SO2Immersion Plumule yield be 3.75%;The former protein yield 4.71%, the latter 4.69%;The former starch recoveries are 68.72%, The latter is 68.33%;The former fiber yield is 11.35%, and the latter 11.26%.
Data show that it is suitable that both soak products obtained therefrom yield;But all products of gained of the invention are follow-up without carrying out Desulfurized step.
Embodiment 2
The present embodiment is used to illustrate that immersion process provided by the present invention is applied to maize germ, fiber, starch and albumen Preparation, comprise the following steps that:
Step (1):The corn purchased is screened, impurity and the corn that goes mouldy is removed, weighs corn 1500g;
Step (2):By the corn after weighing in beaker, while 1500mL running water is added, shake about 3min, cleaning Terminate, remove wash water, by same procedure repeated washing 3 times;
Step (3):Corn after cleaning is transferred in 2500mL port grinding bottles;
Step (4):0.6% vitamin C soak 2700g is added in port grinding bottle, it is close in 50 DEG C of water bath with thermostatic control Close and place 48h;
Step (5):The corn soaked after terminating is filtered, obtains corn and corn steep liquor;
Step (6):Corn obtained by step (5) is poured into wall-breaking machine, about 2500mL running water is added, is crushed, Obtain corn slurries;
Step (7):Corn slurries obtained by step (6) are placed in 5000mL beaker, the jade on top is taken out with strainer Rice plumule, then stir the corn slurries to plumule and suspend, then plumule is fished for strainer.Repeatedly the operation into slurries without plumule Untill.The thick plumule of taking-up is repeatedly washed with running water, 12h is bakeed in 105 DEG C of baking oven, obtains maize germ;
Step (8):Step (7) is taken off to the corn slurries after embryo and obtains top crude fibre by the bent sieve of fiber separation, enters one Step is repeatedly washed after crushing with running water, centrifuge separating and dehydrating, drying, obtains fibrous finished product;
Step (9):The corn slurries of the bent sieve rear lower of step (8) fiber are separated with supercentrifuge, obtained down Portion's corn Crude starch and top The Corn Protein slurries;
Step (10):By corn Crude starch obtained by step (9), multiple countercurrent washing is carried out with running water, removes residual Insoluble protein, drying, cornstarch finished product is made;
Step (11):By The Corn Protein slurries obtained by step (9), repeatedly washed, be concentrated in vacuo with running water, from Gains in depth of comprehension finally obtain crude protein to wet albumen by drying, crushing.
While above step is carried out, one group of 0.2%SO is carried out2The parallel control experiment of immersion.
The plumule yield that 0.6% vitamin C soaks in the present embodiment is 4.11%, and 0.2%SO2The plumule yield of immersion For 4.08%;The former protein yield 4.96%, the latter 4.98%;The former starch recoveries are 71%, and the latter 70.3%; The former fiber yield is 12.73%, and the latter 12.85%.
Data show that it is suitable that both soak products obtained therefrom yield;But all products of gained of the invention are follow-up without carrying out Desulfurized step.
Embodiment 3
The present embodiment is used to illustrate that immersion process provided by the present invention is applied to maize germ, fiber, starch and albumen Preparation, comprise the following steps that:
Step (1):The corn purchased is screened, impurity and the corn that goes mouldy is removed, weighs corn 1700g;
Step (2):By the corn after weighing in beaker, while 1700mL running water is added, shake about 2min, cleaning Terminate, remove wash water, by same procedure repeated washing 3 times;
Step (3):Corn after cleaning is transferred in 2500mL port grinding bottles;
Step (4):0.8% vitamin C soak 3060g is added in port grinding bottle, it is close in 50 DEG C of water bath with thermostatic control Close and place 50h;
Step (5):The corn soaked after terminating is filtered, obtains corn and corn steep liquor;
Step (6):Corn obtained by step (5) is poured into wall-breaking machine, about 3400mL running water is added, is crushed, Obtain corn slurries;
Step (7):Corn slurries obtained by step (6) are placed in 5000mL beaker, the jade on top is taken out with strainer Rice plumule, then stir the corn slurries to plumule and suspend, then plumule is fished for strainer.Repeatedly the operation into slurries without plumule Untill.The thick plumule of taking-up is repeatedly washed with running water, 12h is bakeed in 105 DEG C of baking oven, obtains maize germ;
Step (8):Step (7) is taken off to the corn slurries after embryo and obtains crude fibre, further powder by the bent sieve of fiber separation Repeatedly washed with running water after broken, centrifuge separating and dehydrating, dry, obtain fibrous finished product;
Step (9):Corn slurries of the step (8) after the bent sieve of fiber are separated with supercentrifuge, obtain jade Rice Crude starch and The Corn Protein slurries;
Step (10):By corn Crude starch obtained by step (9), multiple countercurrent washing is carried out with running water, removes residual Insoluble protein, drying, cornstarch finished product is made;
Step (11):By The Corn Protein slurries obtained by step (9), repeatedly washed, be concentrated in vacuo with running water, from Gains in depth of comprehension finally obtain crude protein to wet albumen by drying, crushing.
While above step is carried out, one group of 0.2%SO is carried out2The parallel control experiment of immersion.
The germ recovery rate that 0.8% vitamin C soaks in the present embodiment is 3.15%, and 0.2%SO2The plumule of immersion returns Yield is 3.12%;The former protein yield 4.92%, the latter 4.78%;The former starch recoveries are 69%, Hou Zhewei 69.3%;The former fiber yield is 12.50%, and the latter 12.27%.
Data show that it is suitable that both soak products obtained therefrom yield;But all products of gained of the invention are follow-up without carrying out Desulfurized step.
Embodiment 4
The present embodiment and the difference of embodiment 2 are:The dimension that 0.6% vitamin C soak is replaced with to 0.01% is given birth to Plain C soaks.
While above step is carried out, one group of 0.2%SO is carried out2The parallel control experiment of immersion.
The germ recovery rate that 0.01% vitamin C soaks in the present embodiment is 2.53%, and 0.2%SO2The plumule of immersion Yield is 4.08%;The former protein yield 2.87%, the latter 4.98%;The former starch recoveries are 51%, Hou Zhewei 70.3%;The former fiber yield is 8.19%, and the latter 12.85%.
Embodiment 5
The present embodiment and the difference of embodiment 2 are:0.6% vitamin C soak is replaced with into 5% vitamin C Soak.
While above step is carried out, one group of 0.2%SO is carried out2The parallel control experiment of immersion.
The germ recovery rate that 0.5% vitamin C soaks in the present embodiment is 4.11%, and 0.2%SO2The plumule of immersion is received Rate is 4.08%;The former protein yield 5.01%, the latter 4.98%;The former starch recoveries are 70.18%, Hou Zhewei 70.3%;The former fiber yield is 12.47%, and the latter 12.85%.
It should be appreciated that after equal proportion expansion is carried out to the dosage of above-described embodiment agents useful for same or raw material or is reduced Technical scheme, it is substantially identical with above-described embodiment.
Although above the present invention is described in detail with a general description of the specific embodiments, On the basis of the present invention, it can be made some modifications or improvements, this will be apparent to those skilled in the art.Cause This, these modifications or improvements, belong to the scope of protection of present invention without departing from theon the basis of the spirit of the present invention.

Claims (10)

1. the immersion process in a kind of processing of farm products production, it is characterised in that by the agricultural product by pretreatment be placed in containing Soaked in ascorbic soak.
2. immersion process according to claim 1, it is characterised in that do not contain SO in the soak2, sulfurous acid or its Derivative salt.
3. immersion process according to claim 1 or 2, it is characterised in that ascorbic mass concentration in the soak For 0.01~5%.
4. immersion process according to claim 3, it is characterised in that ascorbic mass concentration is in the soak 0.2~0.8%.
5. according to the immersion process described in any one of Claims 1 to 4, it is characterised in that the soaking conditionses are 30~65 DEG C water bath with thermostatic control in 36~72h of closed placement.
6. according to the immersion process described in any one of Claims 1 to 5, it is characterised in that after immersion terminates, by the agricultural product Separated with soak, agricultural product after being soaked and containing nutritious soak.
7. according to the immersion process described in any one of claim 1~6, it is characterised in that the agricultural product be corn, wheat, Soybean, paddy etc..
8. immersion process according to claim 7, it is characterised in that the agricultural product are corn, after immersion terminates, by jade Rice separates with soak, corn after being soaked and containing nutritious soak;
Corn after the immersion can be processed further, production zein fiber, plumule, starch or protein product.
9. a kind of agricultural product soak, it is characterised in that it is the immersion process pair described in using any one of claim 1~8 After agricultural product are soaked, isolated contains nutritious soak.
10. the agricultural product soak described in claim 9 is preparing the application of food, health products or pharmaceutical preparations.
CN201711191755.4A 2017-11-24 2017-11-24 A kind of immersion process in processing of farm products production Pending CN107868133A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113278664A (en) * 2021-05-17 2021-08-20 齐齐哈尔龙江阜丰生物科技有限公司 Process for degrading corn epidermal fibers by cellulase
CN114698822A (en) * 2022-03-07 2022-07-05 江苏海洋大学 Method for brewing soy sauce by using corn steep liquor

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CN101665541A (en) * 2008-09-05 2010-03-10 甘肃雪晶生化有限责任公司 Method for producing waxy corn starch

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113278664A (en) * 2021-05-17 2021-08-20 齐齐哈尔龙江阜丰生物科技有限公司 Process for degrading corn epidermal fibers by cellulase
CN114698822A (en) * 2022-03-07 2022-07-05 江苏海洋大学 Method for brewing soy sauce by using corn steep liquor

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