CN107854510A - A kind of high-quality emblic cotyledon cream and preparation method thereof - Google Patents
A kind of high-quality emblic cotyledon cream and preparation method thereof Download PDFInfo
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- CN107854510A CN107854510A CN201711405368.6A CN201711405368A CN107854510A CN 107854510 A CN107854510 A CN 107854510A CN 201711405368 A CN201711405368 A CN 201711405368A CN 107854510 A CN107854510 A CN 107854510A
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- emblic cotyledon
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- 235000015489 Emblica officinalis Nutrition 0.000 title claims abstract description 122
- 244000119298 Emblica officinalis Species 0.000 title claims abstract description 106
- 239000006071 cream Substances 0.000 title claims abstract description 60
- 238000002360 preparation method Methods 0.000 title claims abstract description 18
- 238000002137 ultrasound extraction Methods 0.000 claims abstract description 21
- 238000005119 centrifugation Methods 0.000 claims abstract description 11
- 238000001914 filtration Methods 0.000 claims abstract description 11
- 239000002994 raw material Substances 0.000 claims abstract description 8
- 238000004140 cleaning Methods 0.000 claims abstract description 6
- 239000000843 powder Substances 0.000 claims description 31
- 238000000605 extraction Methods 0.000 claims description 19
- 240000009120 Phyllanthus emblica Species 0.000 claims description 16
- 238000005516 engineering process Methods 0.000 claims description 16
- 239000000706 filtrate Substances 0.000 claims description 15
- 239000000284 extract Substances 0.000 claims description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 12
- 238000004806 packaging method and process Methods 0.000 claims description 10
- 238000001035 drying Methods 0.000 claims description 8
- 238000007493 shaping process Methods 0.000 claims description 7
- 239000000047 product Substances 0.000 claims description 6
- 239000005030 aluminium foil Substances 0.000 claims description 5
- 238000007667 floating Methods 0.000 claims description 5
- 238000000227 grinding Methods 0.000 claims description 5
- 239000012535 impurity Substances 0.000 claims description 5
- 239000007788 liquid Substances 0.000 claims description 5
- 238000003801 milling Methods 0.000 claims description 5
- 239000002245 particle Substances 0.000 claims description 5
- 238000002390 rotary evaporation Methods 0.000 claims description 5
- 239000006228 supernatant Substances 0.000 claims description 5
- 238000009423 ventilation Methods 0.000 claims description 5
- 238000000465 moulding Methods 0.000 claims description 4
- 238000012856 packing Methods 0.000 claims description 3
- 235000009508 confectionery Nutrition 0.000 claims description 2
- 238000000746 purification Methods 0.000 claims description 2
- 238000002604 ultrasonography Methods 0.000 claims 1
- 235000016709 nutrition Nutrition 0.000 abstract description 8
- 239000000796 flavoring agent Substances 0.000 abstract description 6
- 235000019634 flavors Nutrition 0.000 abstract description 6
- 238000000034 method Methods 0.000 abstract description 6
- 206010030113 Oedema Diseases 0.000 abstract description 5
- 230000000844 anti-bacterial effect Effects 0.000 abstract description 5
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- 208000004880 Polyuria Diseases 0.000 abstract description 4
- 208000010668 atopic eczema Diseases 0.000 abstract description 4
- 230000035619 diuresis Effects 0.000 abstract description 4
- 239000004615 ingredient Substances 0.000 abstract description 4
- 206010006458 Bronchitis chronic Diseases 0.000 abstract description 3
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- 241000700605 Viruses Species 0.000 abstract description 3
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- 208000007451 chronic bronchitis Diseases 0.000 abstract description 3
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- 230000036039 immunity Effects 0.000 abstract description 3
- 206010014561 Emphysema Diseases 0.000 abstract description 2
- 206010036790 Productive cough Diseases 0.000 abstract description 2
- 230000001093 anti-cancer Effects 0.000 abstract description 2
- 208000035269 cancer or benign tumor Diseases 0.000 abstract description 2
- 230000012010 growth Effects 0.000 abstract description 2
- 238000010791 quenching Methods 0.000 abstract description 2
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- 230000000694 effects Effects 0.000 description 5
- 238000011156 evaluation Methods 0.000 description 4
- 239000000463 material Substances 0.000 description 3
- 230000035764 nutrition Effects 0.000 description 3
- 241000221017 Euphorbiaceae Species 0.000 description 2
- REFJWTPEDVJJIY-UHFFFAOYSA-N Quercetin Chemical compound C=1C(O)=CC(O)=C(C(C=2O)=O)C=1OC=2C1=CC=C(O)C(O)=C1 REFJWTPEDVJJIY-UHFFFAOYSA-N 0.000 description 2
- 241000191967 Staphylococcus aureus Species 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
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- 239000004744 fabric Substances 0.000 description 2
- 229930003935 flavonoid Natural products 0.000 description 2
- 235000017173 flavonoids Nutrition 0.000 description 2
- 150000002215 flavonoids Chemical class 0.000 description 2
- LNTHITQWFMADLM-UHFFFAOYSA-N gallic acid Chemical compound OC(=O)C1=CC(O)=C(O)C(O)=C1 LNTHITQWFMADLM-UHFFFAOYSA-N 0.000 description 2
- 150000004676 glycans Chemical class 0.000 description 2
- IYRMWMYZSQPJKC-UHFFFAOYSA-N kaempferol Chemical compound C1=CC(O)=CC=C1C1=C(O)C(=O)C2=C(O)C=C(O)C=C2O1 IYRMWMYZSQPJKC-UHFFFAOYSA-N 0.000 description 2
- MWDZOUNAPSSOEL-UHFFFAOYSA-N kaempferol Natural products OC1=C(C(=O)c2cc(O)cc(O)c2O1)c3ccc(O)cc3 MWDZOUNAPSSOEL-UHFFFAOYSA-N 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
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- 150000007965 phenolic acids Chemical class 0.000 description 2
- 229920001282 polysaccharide Polymers 0.000 description 2
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- 150000003648 triterpenes Chemical class 0.000 description 2
- 241000894006 Bacteria Species 0.000 description 1
- 208000034657 Convalescence Diseases 0.000 description 1
- UBSCDKPKWHYZNX-UHFFFAOYSA-N Demethoxycapillarisin Natural products C1=CC(O)=CC=C1OC1=CC(=O)C2=C(O)C=C(O)C=C2O1 UBSCDKPKWHYZNX-UHFFFAOYSA-N 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 206010017553 Furuncle Diseases 0.000 description 1
- 208000018522 Gastrointestinal disease Diseases 0.000 description 1
- 206010020772 Hypertension Diseases 0.000 description 1
- 206010061218 Inflammation Diseases 0.000 description 1
- 241000588747 Klebsiella pneumoniae Species 0.000 description 1
- 241000699670 Mus sp. Species 0.000 description 1
- 241001130943 Phyllanthus <Aves> Species 0.000 description 1
- ZVOLCUVKHLEPEV-UHFFFAOYSA-N Quercetagetin Natural products C1=C(O)C(O)=CC=C1C1=C(O)C(=O)C2=C(O)C(O)=C(O)C=C2O1 ZVOLCUVKHLEPEV-UHFFFAOYSA-N 0.000 description 1
- HWTZYBCRDDUBJY-UHFFFAOYSA-N Rhynchosin Natural products C1=C(O)C(O)=CC=C1C1=C(O)C(=O)C2=CC(O)=C(O)C=C2O1 HWTZYBCRDDUBJY-UHFFFAOYSA-N 0.000 description 1
- 208000004078 Snake Bites Diseases 0.000 description 1
- GAMYVSCDDLXAQW-AOIWZFSPSA-N Thermopsosid Natural products O(C)c1c(O)ccc(C=2Oc3c(c(O)cc(O[C@H]4[C@H](O)[C@@H](O)[C@H](O)[C@H](CO)O4)c3)C(=O)C=2)c1 GAMYVSCDDLXAQW-AOIWZFSPSA-N 0.000 description 1
- 241000607479 Yersinia pestis Species 0.000 description 1
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- 230000003110 anti-inflammatory effect Effects 0.000 description 1
- 208000002399 aphthous stomatitis Diseases 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 230000035613 defoliation Effects 0.000 description 1
- 238000004925 denaturation Methods 0.000 description 1
- 230000036425 denaturation Effects 0.000 description 1
- 235000005911 diet Nutrition 0.000 description 1
- 230000037213 diet Effects 0.000 description 1
- 208000010643 digestive system disease Diseases 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 229930003944 flavone Natural products 0.000 description 1
- 150000002212 flavone derivatives Chemical class 0.000 description 1
- 235000011949 flavones Nutrition 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 235000013376 functional food Nutrition 0.000 description 1
- 208000003512 furunculosis Diseases 0.000 description 1
- 229940074391 gallic acid Drugs 0.000 description 1
- 235000004515 gallic acid Nutrition 0.000 description 1
- 208000018685 gastrointestinal system disease Diseases 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 238000000338 in vitro Methods 0.000 description 1
- 238000001727 in vivo Methods 0.000 description 1
- 230000002779 inactivation Effects 0.000 description 1
- 230000001939 inductive effect Effects 0.000 description 1
- 230000004054 inflammatory process Effects 0.000 description 1
- 208000014674 injury Diseases 0.000 description 1
- 235000008777 kaempferol Nutrition 0.000 description 1
- 210000004072 lung Anatomy 0.000 description 1
- 239000002932 luster Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- UXOUKMQIEVGVLY-UHFFFAOYSA-N morin Natural products OC1=CC(O)=CC(C2=C(C(=O)C3=C(O)C=C(O)C=C3O2)O)=C1 UXOUKMQIEVGVLY-UHFFFAOYSA-N 0.000 description 1
- 230000000050 nutritive effect Effects 0.000 description 1
- 230000000144 pharmacologic effect Effects 0.000 description 1
- 239000000419 plant extract Substances 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 235000005875 quercetin Nutrition 0.000 description 1
- 229960001285 quercetin Drugs 0.000 description 1
- 235000014347 soups Nutrition 0.000 description 1
- 235000018553 tannin Nutrition 0.000 description 1
- 239000001648 tannin Substances 0.000 description 1
- 229920001864 tannin Polymers 0.000 description 1
- 235000012976 tarts Nutrition 0.000 description 1
- 230000008542 thermal sensitivity Effects 0.000 description 1
- 230000008736 traumatic injury Effects 0.000 description 1
- 230000004614 tumor growth Effects 0.000 description 1
- 231100000611 venom Toxicity 0.000 description 1
- VHBFFQKBGNRLFZ-UHFFFAOYSA-N vitamin p Natural products O1C2=CC=CC=C2C(=O)C=C1C1=CC=CC=C1 VHBFFQKBGNRLFZ-UHFFFAOYSA-N 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/47—Euphorbiaceae (Spurge family), e.g. Ricinus (castorbean)
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/15—Preparation or pretreatment of starting material involving mechanical treatment, e.g. chopping up, cutting or grinding
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/331—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation or decoction
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/39—Complex extraction schemes, e.g. fractionation or repeated extraction steps
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/50—Methods involving additional extraction steps
- A61K2236/51—Concentration or drying of the extract, e.g. Lyophilisation, freeze-drying or spray-drying
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Botany (AREA)
- Mycology (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Alternative & Traditional Medicine (AREA)
- Microbiology (AREA)
- Food Science & Technology (AREA)
- Nutrition Science (AREA)
- Biotechnology (AREA)
- Medical Informatics (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Pharmacology & Pharmacy (AREA)
- Epidemiology (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The present invention relates to a kind of high-quality emblic cotyledon cream and preparation method thereof, the high-quality emblic cotyledon cream using emblic cotyledon as raw material, pass sequentially through cleaning, dry, be milled, ultrasound extraction, centrifugation, filtering, concentration, forming step is made.The present invention is made by special technique to be enriched with the nutritional ingredient of emblic cotyledon to form high-quality emblic cotyledon cream, with the distinctive fresh scent of emblic cotyledon, taste is soft, flavour is certainly but strong, the high-quality emblic cotyledon cream can effectively antibacterial, neoplasm growth, anticancer, effectively strengthen body immunity, heat-clearing and quench one's thirst fall fire, clearing damp resolving sputum, clearing damp diuresis, special efficacy with treatment oedema, skin eczema, being capable of antitumor, anti-hepatitis virus, antibacterial and preventing and treating chronic bronchitis merging pulmonary emphysema.
Description
Technical field
The invention belongs to plant extract cream technical field, and in particular to a kind of high-quality emblic cotyledon cream and preparation method thereof.
Background technology
Emblic cotyledon is Euphorbiaceae（Euphorbiaceae）Leafflower（Phyllan-thus）Defoliation small arbor or filling
The leaf of wood, also known as emblic leafflower leaf, silk leaf are its acrid flavour, mild-natured, have the effect of clearing damp diuresis, for oedema, skin eczema.
Emblic cotyledon is medicinal material among the people conventional simply, on the books both at home and abroad.Such as Indonesia, often as antidiarrheic, use
In treatment gastrointestinal disease.
Emblic cotyledon is conventional natural plant among the people, and there are some researches show have in Extracts from Leaves of Phyllanthus emblica L containing a variety of
Composition is imitated, there are a variety of effects such as antibacterial anti-inflammatory, antitumor, Immune-enhancing effect, is a kind of medicinal material with exploitation potential.At present,
Emblic cultivation is semi-wild or wild mostly, and pest and disease damage is few, is that qualified pollution-free food adds hardly by industrial pollution
Work raw material, develop into remedy diet and functional food, wide market.
The content of the invention
It is an object of the invention to provide a kind of high-quality emblic cotyledon cream and preparation method thereof.
To achieve the above object, the technical scheme that uses of the present invention is：A kind of high-quality emblic cotyledon cream, with emblic cotyledon
For raw material, pass sequentially through cleaning, dry, be milled, ultrasound extraction, centrifugation, filtering, concentration, forming step are made.
To achieve the above object, another technical scheme for using of the present invention is：A kind of preparation side of high-quality emblic cotyledon cream
Method, comprise the following steps：
（1）Select：Select complete, immaculate, the fresh emblic cotyledon without worm hole；
（2）Milling：Emblic cotyledon is fully cleaned, ventilation is placed in and dries, is then entered the emblic cotyledon after drying
Row crushes, and obtains emblic cotyledon powder；
（3）Ultrasound extraction：By emblic cotyledon powder and pure water with solid-liquid ratio 1:(15-25) is mixed, and utilizes ultrasonic extraction
Technology is extracted, time 25-35min, 35-45 DEG C of temperature, is filtered after extraction, obtains filtrate and filter residue；By filter residue with it is pure
Water purification is with 1:The ratio of (15-25) is mixed, and extraction 2-4 times, each extraction time 25- are repeated using ultrasonic extraction technology
35min, 35-45 DEG C of temperature, filtered every time after extraction, respectively obtain filtrate；Merge all filtrates, obtain mixed liquor；
（4）Filtering：Mixed liquor is subjected to centrifugation 5-10min under 4000-4500rpm rotating speeds, takes its supernatant to be filtered, goes
Fall the impurity of floating, obtain clarifying the extract solution of no layering；
（5）Concentration：Extract solution is subjected to rotary evaporation in vacuo concentration, temperature is 45-55 DEG C, rotating speed 60-70r/min, concentration
It is 30-40% to dry matter content, obtains condensed cream；
（6）Shaping：Condensed cream is poured into mould, dried using vacuum dehydrating at lower temperature technology, temperature is 40-50 DEG C, is dried to
Dry matter content is 90-93%, that is, obtains high-quality emblic cotyledon cream.
Preferably, can also comprise the following steps：（7）Packaging：High-quality emblic cotyledon cream is cooled to room temperature, after packaged
As product.
Preferably, in step（7）In, packed using aluminium foil bag, manner of packing is one piece of one bag.
Preferably, in step（1）In, selected again after emblic cotyledon transport reaches, reject and go out in transportation
Existing bad leaf.
Preferably, in step（2）In, the emblic cotyledon powder be by emblic cotyledon ultramicro grinding to particle diameter below 20 μm
Broken wall emblic cotyledon powder.
Preferably, in step（2）In, the emblic cotyledon powder is that progress low-temperature submicron powder is broken below 65 DEG C.
Preferably, in step（3）In, the power of ultrasonic wave is 400-500W, frequency 20-25KHz.
Preferably, in step（5）In, vacuum is -0.068Mpa.
Preferably, in step（6）In, vacuum is -0.092MPa.
Preferably, in step（6）In, the emblic cotyledon cream in mould is suppressed again after drying moulding.
The invention has the advantages that：
It the latest study proves, emblic cotyledon contains the Multiple components such as organic phenolic acid class, reduced sugar, polysaccharide, flavonoids, triterpene.And
Research is found：It is quick that emblic cotyledon extract solution can suppress klebsiella pneumoniae, staphylococcus aureus to some extent in vitro
Feel strain, staphylococcus aureus resistance strain etc.；Extracts from Leaves of Phyllanthus emblica L can suppress tumor-bearing mice tumour growth, show emblic cotyledon
Extract also has antitumor action in vivo, also has the function that strengthen immunity.
The present invention is made by special technique to be enriched with the nutritional ingredient of emblic cotyledon to form high-quality emblic cotyledon cream, is had
There is the distinctive fresh scent of emblic cotyledon, taste is soft, and flavour is certainly but strong, and the high-quality emblic cotyledon cream can effectively press down
Bacterium, neoplasm growth, anticancer, effectively strengthen body immunity, heat-clearing and quench one's thirst fall fire, clearing damp resolving sputum, clearing damp diuresis, there is treatment
The special efficacy of oedema, skin eczema, being capable of antitumor, anti-hepatitis virus, antibacterial and preventing and treating chronic bronchitis merging lung qi
It is swollen.
Brief description of the drawings
Fig. 1 is a kind of process chart that the present invention prepares high-quality emblic cotyledon cream.
Embodiment
In order to allow features described above of the invention and advantage to become apparent, below especially exemplified by embodiment, and coordinate accompanying drawing, make detailed
Carefully it is described as follows.
Embodiment one：A kind of high-quality emblic cotyledon cream, using emblic cotyledon as raw material, pass sequentially through cleaning, dry, be milled,
Ultrasound extraction, centrifugation, filtering, concentration, forming step are made.
Fig. 1 is refer to, a kind of preparation method of high-quality emblic cotyledon cream, is comprised the following steps：
（1）Select：Select complete, immaculate, the fresh emblic cotyledon without worm hole；
（2）Milling：Emblic cotyledon is fully cleaned, ventilation is placed in and dries, is then entered the emblic cotyledon after drying
Row crushes, and obtains emblic cotyledon powder；
（3）Ultrasound extraction：By emblic cotyledon powder and pure water with solid-liquid ratio 1:15 are mixed, and are carried using ultrasonic extraction technology
Take, time 25min, 35 DEG C of temperature, filtered after extraction, obtain filtrate and filter residue；By filter residue and pure water with 1:15
Ratio is mixed, and is repeated extraction 4 times using ultrasonic extraction technology, each extraction time 25min, 35 DEG C of temperature, is carried every time
Filtered after taking, respectively obtain filtrate；Merge all filtrates, obtain mixed liquor；
（4）Filtering：Mixed liquor is subjected to centrifugation 10min under 4000rpm rotating speeds, takes its supernatant to be filtered, removes floating
Impurity, obtain clarifying the extract solution of no layering；
（5）Concentration：Extract solution is subjected to rotary evaporation in vacuo concentration, temperature is 55 DEG C, rotating speed 60r/min, is concentrated to dry
Matter content is 30%, obtains condensed cream；
（6）Shaping：Condensed cream is poured into mould, dried using vacuum dehydrating at lower temperature technology, temperature is 40 DEG C, is dried to dry
Matter content is 90%, that is, obtains high-quality emblic cotyledon cream.
In step（2）In, the emblic cotyledon powder is the broken wall by emblic cotyledon ultramicro grinding to particle diameter below 20 μm
Emblic cotyledon powder.
In step（2）In, the emblic cotyledon powder is that progress low-temperature submicron powder is broken below 65 DEG C.
In step（3）In, the power of ultrasonic wave is 400W, frequency 20KHz.
Embodiment two：A kind of high-quality emblic cotyledon cream, using emblic cotyledon as raw material, pass sequentially through cleaning, dry, be milled,
Ultrasound extraction, centrifugation, filtering, concentration, shaping, packaging step are made.
As shown in figure 1, a kind of preparation method of high-quality emblic cotyledon cream, comprises the following steps：
（1）Select：Fresh emblic cotyledon is plucked, selects complete, immaculate, the emblic cotyledon without worm hole；
（2）Milling：Emblic cotyledon is fully cleaned, ventilation is placed in and dries, is then entered the emblic cotyledon after drying
Row crushes, and obtains emblic cotyledon powder；
（3）Ultrasound extraction：By emblic cotyledon powder and pure water with solid-liquid ratio 1:20 are mixed, and are carried using ultrasonic extraction technology
Take, time 30min, 40 DEG C of temperature, filter cloth can be passed through after extraction（Such as its mesh number is not less than 800 mesh）Filtered, obtained
Filtrate and filter residue；By filter residue and pure water with 1:20 ratio is mixed, and extraction 3 times is repeated using ultrasonic extraction technology,
Each extraction time 30min, 40 DEG C of temperature, it can be filtered every time after extraction by filter cloth, respectively obtain filtrate；Merge institute
There is filtrate, obtain mixed liquor；
（4）Filtering：Mixed liquor is subjected to centrifugation 8min under 4200rpm rotating speeds, takes its supernatant to be filtered, removes floating
Impurity, obtain clarifying the extract solution of no layering；
（5）Concentration：Extract solution is subjected to rotary evaporation in vacuo concentration, temperature is 50 DEG C, rotating speed 65r/min, is concentrated to dry
Matter content is 35%, obtains condensed cream；
（6）Shaping：Condensed cream is poured into mould, dried using vacuum dehydrating at lower temperature technology, temperature is 45 DEG C, is dried to dry
Matter content is 91-92%, that is, obtains high-quality emblic cotyledon cream；
（7）Packaging：High-quality emblic cotyledon cream is cooled to room temperature, is product after packaged.
In step（1）In, selected, occurred in rejecting transportation bad again after emblic cotyledon transport reaches
Leaf.
In step（2）In, the emblic cotyledon powder is the broken wall by emblic cotyledon ultramicro grinding to particle diameter below 20 μm
Emblic cotyledon powder.Powder diameter reaches broken wall requirement, nutrition is fully discharged below 20 μm, soluble in water.
In step（2）In, the emblic cotyledon powder is that progress low-temperature submicron powder is broken below 65 DEG C.Less than 65 DEG C of low temperature
Under the conditions of crush, keep nutritional ingredient not to be denatured or lost by high temperature, nutrition caused by producing high temperature when having prevented crushing into
Divide rotten denaturation；If crushed under the high temperature conditions, volume can be caused to diminish, quality is hardened, volatile component loss, some
The material of thermal sensitivity（Such as protein, tannin）It is denatured, inactivation even aoxidizes, while nutritional utilization is insufficient and loses tight
Weight.
In step（3）In, the power of ultrasonic wave is 500W, frequency 22KHz.
In step（5）In, vacuum is -0.068Mpa.
In step（6）In, vacuum is -0.092MPa.
In step（6）In, the emblic cotyledon cream in mould is suppressed again moulding after drying, product is more stepped up
Cause.
In step（7）In, the characteristics of for the easy moisture absorption and to peculiar smell sensitivity, packed using aluminium foil bag, packaging side
Formula is one piece of one bag.
Embodiment three：A kind of high-quality emblic cotyledon cream, using emblic cotyledon as raw material, pass sequentially through cleaning, dry, be milled,
Ultrasound extraction, centrifugation, filtering, concentration, shaping, packaging step are made.
As shown in figure 1, a kind of preparation method of high-quality emblic cotyledon cream, comprises the following steps：
（1）Select：Fresh emblic cotyledon is bought, selects complete, immaculate, the emblic cotyledon without worm hole；
（2）Milling：Emblic cotyledon is fully cleaned, ventilation is placed in and dries, is then entered the emblic cotyledon after drying
Row crushes, and obtains emblic cotyledon powder；
（3）Ultrasound extraction：By emblic cotyledon powder and pure water with solid-liquid ratio 1:25 are mixed, and are carried using ultrasonic extraction technology
Take, time 35min, temperature 45 C, filtered after extraction, obtain filtrate and filter residue；By filter residue and pure water with 1:(15-
25) ratio is mixed, and repeats to extract 2 times, each extraction time 35min using ultrasonic extraction technology, temperature 45 C, often
Filtered after secondary extraction, respectively obtain filtrate；Merge all filtrates, obtain mixed liquor；
（4）Filtering：Mixed liquor is subjected to centrifugation 5min under 4500rpm rotating speeds, takes its supernatant to be filtered, removes floating
Impurity, obtain clarifying the extract solution of no layering；
（5）Concentration：Extract solution is subjected to rotary evaporation in vacuo concentration, temperature is 45 DEG C, rotating speed 70r/min, is concentrated to dry
Matter content is 40%, obtains condensed cream；
（6）Shaping：Condensed cream is poured into mould, dried using vacuum dehydrating at lower temperature technology, temperature is 50 DEG C, is dried to dry
Matter content is 93%, that is, obtains high-quality emblic cotyledon cream；
（7）Packaging：High-quality emblic cotyledon cream is cooled to room temperature, is product after packaged.
In step（2）In, the emblic cotyledon powder is the broken wall by emblic cotyledon ultramicro grinding to particle diameter below 20 μm
Emblic cotyledon powder.
In step（2）In, the emblic cotyledon powder is that progress low-temperature submicron powder is broken below 65 DEG C.
In step（3）In, the power of ultrasonic wave is 500W, frequency 25KHz.
In step（6）In, the emblic cotyledon cream in mould is suppressed again moulding after drying, product is more stepped up
Cause.
In step（7）In, the characteristics of for the easy moisture absorption and to peculiar smell sensitivity, packed using aluminium foil bag, packaging side
Formula is one piece of one bag, that is, the high-quality emblic cotyledon cream of each piece of packaging of aluminium foil bag is respectively adopted；Finally, predetermined quantity is can use loaded on bag
In vanning, packing box or packaging bag.
The nutriment very abundant that emblic cotyledon contains, contains organic phenolic acid class, reduced sugar, polysaccharide, flavonoids, triterpene
Deng Multiple components, but it is often wasted in process of production；The present invention can give full play to the nutrition of emblic cotyledon
Effect, there is unique nutritive value or health convalescence value.
The high-quality emblic cotyledon cream has the effect of clearing heat and detoxicating, inducing diuresis and reducing edema, is usually used in aphtha, furunculosis, eczema, skin
The treatment of inflammation, oedema, hypertension, venomous snake bite, traumatic injury；And it has antitumor, anti-hepatitis virus, antibacterial and preventing and treating
Chronic bronchitis merges the pharmacological action of pulmonary emphysema.The high-quality emblic cotyledon cream is dissolved in after water color and luster in uniformly light brown,
Even tissue is transparent, fine and smooth and without layering, has a distinctive fresh scent of emblic cotyledon, fresh and clean, free from extraneous odour, and taste is soft
With, sweet agreeable to the taste more slightly tart flavour, flavour oneself however it is strong.
The present invention each embodiment using emblic cotyledon as raw material, using gallic acid, Quercetin, Kaempferol and general flavone as
Evaluation index, optimize the extraction process of high-quality emblic cotyledon cream；Simultaneously using sensory evaluation scores as evaluation index, optimize high-quality emblic
The technique of leaf cream.The high-quality important nutritional ingredient of emblic cotyledon cream is shown in Table 1.
Using profile, soup look, fragrance, flavour as the index of subjective appreciation, high-quality emblic cotyledon cream sensory evaluation is shown in Table 2.
It is described above, only presently preferred embodiments of the present invention, any formal limitation not is done to the present invention, it is any ripe
Those skilled in the art is known in every case without departing from the content of technical solution of the present invention, and the technical spirit according to the present invention is real to more than
Apply example and make any simple modification, equivalent changes and modifications, should all belong to the covering scope of the present invention.
Claims (10)
- A kind of 1. high-quality emblic cotyledon cream, it is characterised in that using emblic cotyledon as raw material, pass sequentially through cleaning, dry, be milled, Ultrasound extraction, centrifugation, filtering, concentration, forming step are made.
- 2. a kind of preparation method of high-quality emblic cotyledon cream, it is characterised in that comprise the following steps：（1）Select：Select complete, immaculate, the fresh emblic cotyledon without worm hole；（2）Milling：Emblic cotyledon is fully cleaned, ventilation is placed in and dries, is then entered the emblic cotyledon after drying Row crushes, and obtains emblic cotyledon powder；（3）Ultrasound extraction：By emblic cotyledon powder and pure water with solid-liquid ratio 1:(15-25) is mixed, and utilizes ultrasonic extraction Technology is extracted, time 25-35min, 35-45 DEG C of temperature, is filtered after extraction, obtains filtrate and filter residue；By filter residue with it is pure Water purification is with 1:The ratio of (15-25) is mixed, and extraction 2-4 times, each extraction time 25- are repeated using ultrasonic extraction technology 35min, 35-45 DEG C of temperature, filtered every time after extraction, respectively obtain filtrate；Merge all filtrates, obtain mixed liquor；（4）Filtering：Mixed liquor is subjected to centrifugation 5-10min under 4000-4500rpm rotating speeds, takes its supernatant to be filtered, goes Fall the impurity of floating, obtain clarifying the extract solution of no layering；（5）Concentration：Extract solution is subjected to rotary evaporation in vacuo concentration, temperature is 45-55 DEG C, rotating speed 60-70r/min, concentration It is 30-40% to dry matter content, obtains condensed cream；（6）Shaping：Condensed cream is poured into mould, dried using vacuum dehydrating at lower temperature technology, temperature is 40-50 DEG C, is dried to Dry matter content is 90-93%, that is, obtains high-quality emblic cotyledon cream.
- 3. the preparation method of high-quality emblic cotyledon cream according to claim 2, it is characterised in that：It is further comprising the steps of：（7）Packaging：High-quality emblic cotyledon cream is cooled to room temperature, is product after packaged.
- 4. the preparation method of high-quality emblic cotyledon cream according to claim 3, it is characterised in that：In step（7）In, use Aluminium foil bag is packed, and manner of packing is one piece of one bag.
- 5. the preparation method of high-quality emblic cotyledon cream according to claim 2, it is characterised in that：In step（1）In, treat remaining Sweet cotyledon transport is selected again after reaching, and rejects the bad leaf occurred in transportation.
- 6. the preparation method of high-quality emblic cotyledon cream according to claim 2, it is characterised in that：In step（2）In, it is described Emblic cotyledon powder is the broken wall emblic cotyledon powder below 20 μm by emblic cotyledon ultramicro grinding to particle diameter.
- 7. the preparation method of the high-quality emblic cotyledon cream according to claim 2 or 6, it is characterised in that：In step（2）In, The emblic cotyledon powder is that progress low-temperature submicron powder is broken below 65 DEG C.
- 8. the preparation method of high-quality emblic cotyledon cream according to claim 2, it is characterised in that：In step（3）In, ultrasound The power of ripple is 400-500W, frequency 20-25KHz.
- 9. the preparation method of high-quality emblic cotyledon cream according to claim 2, it is characterised in that：In step（5）In, vacuum Spend for -0.068MPa；In step（6）In, vacuum is -0.092MPa.
- 10. the preparation method of high-quality emblic cotyledon cream according to claim 2, it is characterised in that：In step（6）In, do Emblic cotyledon cream in mould suppressed again after dry moulding.
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Citations (3)
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|---|---|---|---|---|
| CN101156887A (en) * | 2007-09-26 | 2008-04-09 | 广西中医学院 | Emblic cotyledon preparation with pulmonary emphysema against function |
| CN101912432A (en) * | 2010-08-16 | 2010-12-15 | 西北农林科技大学 | Antioxidant substance extracted from branches, barks and leaves of eucommia bark leaved forest and extraction method thereof |
| CN102273575A (en) * | 2011-08-26 | 2011-12-14 | 吉林紫鑫药业股份有限公司 | Ginseng and tuckahoe cream and production process thereof |
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2017
- 2017-12-22 CN CN201711405368.6A patent/CN107854510A/en active Pending
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101156887A (en) * | 2007-09-26 | 2008-04-09 | 广西中医学院 | Emblic cotyledon preparation with pulmonary emphysema against function |
| CN101912432A (en) * | 2010-08-16 | 2010-12-15 | 西北农林科技大学 | Antioxidant substance extracted from branches, barks and leaves of eucommia bark leaved forest and extraction method thereof |
| CN102273575A (en) * | 2011-08-26 | 2011-12-14 | 吉林紫鑫药业股份有限公司 | Ginseng and tuckahoe cream and production process thereof |
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| 刘成伦主编: "《天然药物化学》", 31 December 2011, 中央广播电视大学出版社 * |
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