CN107841190A - A kind of writing brush cleaning fluid and preparation method thereof - Google Patents
A kind of writing brush cleaning fluid and preparation method thereof Download PDFInfo
- Publication number
- CN107841190A CN107841190A CN201711289107.2A CN201711289107A CN107841190A CN 107841190 A CN107841190 A CN 107841190A CN 201711289107 A CN201711289107 A CN 201711289107A CN 107841190 A CN107841190 A CN 107841190A
- Authority
- CN
- China
- Prior art keywords
- parts
- sodium
- writing brush
- water
- styryl
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D9/00—Chemical paint or ink removers
- C09D9/04—Chemical paint or ink removers with surface-active agents
Abstract
The invention discloses a kind of writing brush cleaning fluid and preparation method thereof, is related to writing brush cleaning technique field, and the present invention includes the composition of following component：30~50 parts of sodium sulfonate hydrazinobenzene hydrochloride salt, styryl are to 20~35 parts of chlorobenzene ketone, 12~20 parts of laruyl alcohol polyoxy ether, 8~15 parts of cocoamidopropyl betaine, 2~10 parts of sodium citrate, 8~10 parts of tripolyphosphate, 4~10 parts of sodium phosphate, 10~30 parts of lactic acid sylvite, 30~40 parts of ethanol, 20~40 parts of acetone, 100~120 parts of water, the present invention forms the cleaning agent for being easy to clean stupid stain dirt, composition is simple, and cleaning performance is good.
Description
Technical field
The present invention relates to cleaning applications, more particularly to a kind of method of washing writing brush.
Background technology
For the people for the traditional Chinese Painting that practices calligraphy, paints, writing brush is a kind of painting tool that they have to use.But clean
Ink marks or pigment on writing brush is pretty troublesome, although because prepared Chinese ink, pigment can be watered down by water, but still be very easy to be attached to hair
On the fiber of pen nib, it is not easy to remove totally, substantial amounts of water resource will be expended by being rinsed using tap.Currently there are no can be easily
Remove prepared Chinese ink, the instrument of pigment on writing brush.
The content of the invention
It is an object of the invention to：To understand above-mentioned technical problem, the present invention provides a kind of writing brush cleaning fluid and its preparation
Method.
The present invention specifically uses following technical scheme to achieve these goals：
A kind of writing brush cleaning fluid, include the composition of following component：30~50 parts of sodium sulfonate hydrazinobenzene hydrochloride salt, styryl pair
20~35 parts of chlorobenzene ketone, 12~20 parts of laruyl alcohol polyoxy ether, 8~15 parts of cocoamidopropyl betaine, sodium citrate 2~
10 parts, 8~10 parts of tripolyphosphate, 4~10 parts of sodium phosphate, 10~30 parts of lactic acid sylvite, 30~40 parts of ethanol, acetone 20~40
Part, 100~120 parts of water.
Further, 31 parts of sodium sulfonate hydrazinobenzene hydrochloride salt, styryl are to 28 parts of chlorobenzene ketone, laruyl alcohol polyoxy ether 16
Part, 12 parts of cocoamidopropyl betaine, 8 parts of sodium citrate, 9 parts of tripolyphosphate, 8 parts of sodium phosphate, 22 parts of lactic acid sylvite, second
34 parts of alcohol, 32 parts of acetone, 116 parts of water.
Comprise the following steps：
It is prepared by step 1, sodium sulfonate hydrazinobenzene hydrochloride salt：Added in retort 50 parts of sodium sulfanilate, 500 parts of water with
20 parts of hydrochloric acid, is stirred, and is cooled to 2~3 DEG C, and 15 parts of solution of natrium nitrosum are further added dropwise, produce diazotising liquid, another water intaking
500 parts, the 45 parts of solution mixing of 30 parts of sodium hydrogensulfite and sodium hydroxide, temperature be 80~85 DEG C, pH value be 6.2~6.7
Under the conditions of, the diazotising liquid is added, continues 1.5~2.0h of stirring, adds 100 parts of tetrasodium ethylenediamine tetraacetate, zinc powder 20
Part, 55 parts of sulfonic acid, 10 parts of NPE, continue to stir, and stir 10~20min, are cooled to 15~25 DEG C, Ji Chenghuang
Sour sodium hydrazinobenzene hydrochloride salt；
Step 2, styryl are prepared to chlorobenzene ketone：50 parts of alchlor, 15 parts of chlorobenzene and two sulphur are added in reaction pot
Change 20 parts of solvents of carbon, be stirred, further add in 100 parts of water and be heated to reflux, 30 parts of acetic anhydride is added dropwise, continues 1~2h of stirring,
To obtain parachloroacetophenone, added in another 20 parts of Qu dioxanes 25 parts of benzaldehyde and described parachloroacetophenone mixing backflow 6~
7h, styryl to chlorobenzene ketone；
Step 3, the sodium sulfonate hydrazinobenzene hydrochloride salt being prepared into step 1 is taken the benzene second prepared in 30~50 parts and step 2
Alkenyl takes 20~35 parts to chlorobenzene ketone, then stirs into mixing, is adding 12~20 parts of laruyl alcohol polyoxy ether, coconut thereto
8~15 parts of oleamide CAB, 2~10 parts of sodium citrate, 8~10 parts of tripolyphosphate, 4~10 parts of sodium phosphate, potassium lactate
10~30 parts of salt, 30~40 parts of ethanol, 20~40 parts of acetone, 100~120 parts of water, are then uniformly mixed to obtain mixed liquor；
Step 4, the mixed liquor that step 4 is obtained are bottled or packed produce quick cleaning fluid for writing brush.
Beneficial effects of the present invention are as follows：
Each composition of the invention cooperates, and forms the cleaning agent for being easy to clean stupid stain dirt, composition is simple, cleaning performance
It is good, quickly the cleaning of writing brush, the prepared Chinese ink of oil painting brush or pigment can be siphoned away, writing brush, oil painting brush elasticity and gloss can be increased,
And easy to use, health etc..
Embodiment
In order to which those skilled in the art are better understood from the present invention, following examples are further retouched in detail to present invention work
State.
Embodiment 1
A kind of writing brush cleaning fluid, include the composition of following component：30 parts of sodium sulfonate hydrazinobenzene hydrochloride salt, styryl are to chlorobenzene
20 parts of ketone, 12 parts of laruyl alcohol polyoxy ether, 8 parts of cocoamidopropyl betaine, 2 parts of sodium citrate, 8 parts of tripolyphosphate, phosphorus
Sour 4 parts of sodium, 10 parts of lactic acid sylvite, 30 parts of ethanol, 20 parts of acetone, 100 parts of water.
Embodiment 2
A kind of writing brush cleaning fluid, include the composition of following component：50 parts of sodium sulfonate hydrazinobenzene hydrochloride salt, styryl are to chlorobenzene
35 parts of ketone, 20 parts of laruyl alcohol polyoxy ether, 15 parts of cocoamidopropyl betaine, 10 parts of sodium citrate, 10 parts of tripolyphosphate,
10 parts of sodium phosphate, 30 parts of lactic acid sylvite, 40 parts of ethanol, 40 parts of acetone, 120 parts of water.
Embodiment 3
A kind of writing brush cleaning fluid, include the composition of following component：31 parts of sodium sulfonate hydrazinobenzene hydrochloride salt, styryl are to chlorobenzene
28 parts of ketone, 16 parts of laruyl alcohol polyoxy ether, 12 parts of cocoamidopropyl betaine, 8 parts of sodium citrate, 9 parts of tripolyphosphate, phosphorus
Sour 8 parts of sodium, 22 parts of lactic acid sylvite, 34 parts of ethanol, 32 parts of acetone, 116 parts of water.
Embodiment 4
A kind of preparation method of writing brush cleaning fluid, it is characterised in that comprise the following steps：
It is prepared by step 1, sodium sulfonate hydrazinobenzene hydrochloride salt：Added in retort 50 parts of sodium sulfanilate, 500 parts of water with
20 parts of hydrochloric acid, is stirred, and is cooled to 2~3 DEG C, and 15 parts of solution of natrium nitrosum are further added dropwise, produce diazotising liquid, another water intaking
500 parts, the 45 parts of solution mixing of 30 parts of sodium hydrogensulfite and sodium hydroxide, temperature be 80~85 DEG C, pH value be 6.2~6.7
Under the conditions of, the diazotising liquid is added, continues 1.5~2.0h of stirring, adds 100 parts of tetrasodium ethylenediamine tetraacetate, zinc powder 20
Part, 55 parts of sulfonic acid, 10 parts of NPE, continue to stir, and stir 10~20min, are cooled to 15~25 DEG C, Ji Chenghuang
Sour sodium hydrazinobenzene hydrochloride salt；
Step 2, styryl are prepared to chlorobenzene ketone：50 parts of alchlor, 15 parts of chlorobenzene and two sulphur are added in reaction pot
Change 20 parts of solvents of carbon, be stirred, further add in 100 parts of water and be heated to reflux, 30 parts of acetic anhydride is added dropwise, continues 1~2h of stirring,
To obtain parachloroacetophenone, added in another 20 parts of Qu dioxanes 25 parts of benzaldehyde and described parachloroacetophenone mixing backflow 6~
7h, styryl to chlorobenzene ketone；
Step 3, the sodium sulfonate hydrazinobenzene hydrochloride salt being prepared into step 1 is taken the benzene second prepared in 30~50 parts and step 2
Alkenyl takes 20~35 parts to chlorobenzene ketone, then stirs into mixing, is adding 12~20 parts of laruyl alcohol polyoxy ether, coconut thereto
8~15 parts of oleamide CAB, 2~10 parts of sodium citrate, 8~10 parts of tripolyphosphate, 4~10 parts of sodium phosphate, potassium lactate
10~30 parts of salt, 30~40 parts of ethanol, 20~40 parts of acetone, 100~120 parts of water, are then uniformly mixed to obtain mixed liquor；
Step 4, the mixed liquor that step 4 is obtained are bottled or packed produce quick cleaning fluid for writing brush.
Described above, only presently preferred embodiments of the present invention is not intended to limit the invention, patent protection model of the invention
Enclose and be defined by claims, the equivalent structure that the content of every specification with the present invention is made changes, and all should similarly wrap
Containing within the scope of the present invention.
Claims (3)
1. a kind of writing brush cleaning fluid, it is characterised in that include the composition of following component：30~50 parts of sodium sulfonate hydrazinobenzene hydrochloride salt,
Styryl to 20~35 parts of chlorobenzene ketone, 12~20 parts of laruyl alcohol polyoxy ether, 8~15 parts of cocoamidopropyl betaine,
2~10 parts of sodium citrate, 8~10 parts of tripolyphosphate, 4~10 parts of sodium phosphate, 10~30 parts of lactic acid sylvite, 30~40 parts of ethanol,
20~40 parts of acetone, 100~120 parts of water.
2. writing brush cleaning fluid according to claim 1, it is characterised in that 31 parts of sodium sulfonate hydrazinobenzene hydrochloride salt, styryl
To 28 parts of chlorobenzene ketone, 16 parts of laruyl alcohol polyoxy ether, 12 parts of cocoamidopropyl betaine, 8 parts of sodium citrate, tripolyphosphate
9 parts, 8 parts of sodium phosphate, 22 parts of lactic acid sylvite, 34 parts of ethanol, 32 parts of acetone, 116 parts of water.
3. the preparation method of writing brush cleaning fluid according to claim 1, it is characterised in that comprise the following steps：
It is prepared by step 1, sodium sulfonate hydrazinobenzene hydrochloride salt：50 parts of sodium sulfanilate, 500 parts of water and hydrochloric acid are added in retort
20 parts, it is stirred, is cooled to 2~3 DEG C, 15 parts of solution of natrium nitrosum is further added dropwise, produce diazotising liquid, separately fetch water 500
45 parts of part, 30 parts of sodium hydrogensulfite and sodium hydroxide solution mixing, in the condition that temperature is 80~85 DEG C, pH value is 6.2~6.7
Under, the diazotising liquid is added, continues 1.5~2.0h of stirring, adds 100 parts of tetrasodium ethylenediamine tetraacetate, 20 parts of zinc powder, sulphur
Sour 55 parts, 10 parts of NPE, continue to stir, and stir 10~20min, are cooled to 15~25 DEG C, sodium sulfonate
Hydrazinobenzene hydrochloride salt；
Step 2, styryl are prepared to chlorobenzene ketone：50 parts of alchlor, 15 parts of chlorobenzene and carbon disulfide are added in reaction pot
20 parts of solvents, are stirred, and further add in 100 parts of water and are heated to reflux, 30 parts of acetic anhydride is added dropwise, continue 1~2h of stirring, will
25 parts of benzaldehyde and described parachloroacetophenone mixing 6~7h of backflow are added to parachloroacetophenone, in another 20 parts of Qu dioxanes, i.e.,
Into styryl to chlorobenzene ketone；
Step 3, the sodium sulfonate hydrazinobenzene hydrochloride salt being prepared into step 1 is taken the styryl prepared in 30~50 parts and step 2
20~35 parts are taken to chlorobenzene ketone, then stirs into mixing, is adding 12~20 parts of laruyl alcohol polyoxy ether, coconut oleoyl thereto
8~15 parts of amine CAB, 2~10 parts of sodium citrate, 8~10 parts of tripolyphosphate, 4~10 parts of sodium phosphate, lactic acid sylvite 10
~30 parts, 30~40 parts of ethanol, 20~40 parts of acetone, 100~120 parts of water, be then uniformly mixed to obtain mixed liquor；
Step 4, the mixed liquor that step 4 is obtained are bottled or packed produce quick cleaning fluid for writing brush.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711289107.2A CN107841190A (en) | 2017-12-07 | 2017-12-07 | A kind of writing brush cleaning fluid and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711289107.2A CN107841190A (en) | 2017-12-07 | 2017-12-07 | A kind of writing brush cleaning fluid and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107841190A true CN107841190A (en) | 2018-03-27 |
Family
ID=61664684
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711289107.2A Pending CN107841190A (en) | 2017-12-07 | 2017-12-07 | A kind of writing brush cleaning fluid and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107841190A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109384657A (en) * | 2018-12-18 | 2019-02-26 | 苏州开元民生科技股份有限公司 | A kind of parahydroxyacet-ophenone synthetic method |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103756400A (en) * | 2014-01-10 | 2014-04-30 | 戴新育 | Quick cleaning fluid for writing brush |
| CN104946431A (en) * | 2015-06-05 | 2015-09-30 | 柳州立洁科技有限公司 | Cleaning agent |
| CN106566707A (en) * | 2015-10-08 | 2017-04-19 | 邹贝尔 | Writing brush cleaning agent and preparation method |
-
2017
- 2017-12-07 CN CN201711289107.2A patent/CN107841190A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103756400A (en) * | 2014-01-10 | 2014-04-30 | 戴新育 | Quick cleaning fluid for writing brush |
| CN104946431A (en) * | 2015-06-05 | 2015-09-30 | 柳州立洁科技有限公司 | Cleaning agent |
| CN106566707A (en) * | 2015-10-08 | 2017-04-19 | 邹贝尔 | Writing brush cleaning agent and preparation method |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109384657A (en) * | 2018-12-18 | 2019-02-26 | 苏州开元民生科技股份有限公司 | A kind of parahydroxyacet-ophenone synthetic method |
| CN109384657B (en) * | 2018-12-18 | 2021-08-31 | 苏州开元民生科技股份有限公司 | Synthetic method of p-hydroxyacetophenone |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN106756942A (en) | A kind of stainless steel chromium-free passivation liquid | |
| CN107841190A (en) | A kind of writing brush cleaning fluid and preparation method thereof | |
| JP2017529406A (en) | BORONIC ALKALI BODY SURFACTANT COMPOSITION dominating water cluster and use thereof | |
| CN106010122A (en) | Hydrophobic corrosion-resistant ceramic paint and preparing method thereof | |
| CN105315838A (en) | Cathode electrophoretic paint liquid and preparation method therefor | |
| CN104387219B (en) | A kind of butter inhibitor for ethylene unit alkaline washing tower and preparation method thereof | |
| CN108277100A (en) | A kind of daily use chemicals compound liquid detergent of more effects | |
| CN105754411A (en) | Whiteboard pen ink and making method thereof | |
| CN103756400B (en) | Quick cleaning fluid for writing brush | |
| CN106280700A (en) | Gravure water-based metal ink and production method thereof | |
| CN104372319B (en) | Special corrosion-resistant passivator of galvanized steel plain sheet and preparation method thereof | |
| CN109267067A (en) | A kind of environmental-protecting chemical polishing fluid polished for aluminium and aluminium alloy high gloss | |
| CN105603436B (en) | A kind of composite corrosion inhibitor and preparation method thereof | |
| CN108191028A (en) | A kind of paint sewage agglomeration process agent and its application | |
| JP2020033497A (en) | Cleaning fluid for writing instrument | |
| CN101961301B (en) | Straight hair dye | |
| CN205323604U (en) | Dissolve material formula of throwing blending tank | |
| CN204712770U (en) | An a kind of art painting equipment for quick washing | |
| JP2017525830A (en) | Alkaline surfactant composition dominated by water clusters and use thereof | |
| CN108977034A (en) | A kind of environmental protection heat-conductive coating and its preparation method and application | |
| CN105542575B (en) | A kind of aqueous wax crayon of solid propylene and preparation method thereof | |
| CN103643568A (en) | Preparation technology of denim discharge printing paste | |
| CN103589242B (en) | Children watercolor pen dedicated ink capable of being scrubbed | |
| CN108441023A (en) | A kind of Writing brush calligraphy ink marks correction fluid and preparation method thereof | |
| JP7419129B2 (en) | Writing instrument cleaning liquid and writing instrument cleaning liquid package containing the same |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180327 |