CN107828292A - Electronic jacquard machine toughened paint and preparation method thereof - Google Patents
Electronic jacquard machine toughened paint and preparation method thereof Download PDFInfo
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- CN107828292A CN107828292A CN201711235970.XA CN201711235970A CN107828292A CN 107828292 A CN107828292 A CN 107828292A CN 201711235970 A CN201711235970 A CN 201711235970A CN 107828292 A CN107828292 A CN 107828292A
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- preparation
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- jacquard machine
- electronic jacquard
- toughened paint
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D129/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an alcohol, ether, aldehydo, ketonic, acetal, or ketal radical; Coating compositions based on hydrolysed polymers of esters of unsaturated alcohols with saturated carboxylic acids; Coating compositions based on derivatives of such polymers
- C09D129/02—Homopolymers or copolymers of unsaturated alcohols
- C09D129/04—Polyvinyl alcohol; Partially hydrolysed homopolymers or copolymers of esters of unsaturated alcohols with saturated carboxylic acids
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2227—Oxides; Hydroxides of metals of aluminium
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2237—Oxides; Hydroxides of metals of titanium
- C08K2003/2241—Titanium dioxide
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Adhesives Or Adhesive Processes (AREA)
- Paints Or Removers (AREA)
Abstract
The invention discloses a kind of electronic jacquard machine toughened paint and preparation method thereof, the preparation method includes：1) cyclodextrin, Peracetic acid, nanometer silica gel, water are subjected to haptoreaction so that gelatinization thing is made；2) carboxymethyl cellulose and water is blended so that jelly is made；3) Ludox, nano aluminium oxide, water is mixed so that mixture is made；4) polyvinyl alcohol, urea, titanium dioxide, wollastonite powder, tributyl phosphate and water are heat-treated, then sequentially add gelatinization thing, jelly, mixture and stir so that electronic jacquard machine toughened paint is made.There is excellent adhesive force, and the preparation method has process simple and the advantages of raw material is easy to get between the toughened paint and metal.
Description
Technical field
The present invention relates to electronic jacquard machine, in particular it relates to a kind of electronic jacquard machine toughened paint and preparation method thereof.
Background technology
Electronic jacquard loom is a kind of electronic equipment, and its main effect is that decorative pattern is being woven on fabric.Existing electricity
The agent structure of sub- jacquard loom is metallic magnetism, and metallic magnetism has the big energy advantage of Stability Analysis of Structures, mechanical strength, and then causes
Electronic jacquard machine has more excellent performance in the course of the work.
But because the surface of metallic magnetism needs to carry out antirust treatment, corrosion protection method the most frequently used at present is i.e. in metal machine
The surface spraying coating of structure and then play a part of protection, but the adhesive force between current coating and metal is often poor,
And then after causing electronic jacquard loom to use a period of time, just there is the situation to come off in coating, and then has severely impacted electricity
The quality of sub- jacquard loom.
The content of the invention
It is an object of the invention to provide a kind of electronic jacquard machine toughened paint and preparation method thereof, the toughened paint and gold
There is excellent adhesive force, and the preparation method has process simple and the advantages of raw material is easy to get between category.
To achieve these goals, the invention provides a kind of preparation method of electronic jacquard machine toughened paint, including：
1) cyclodextrin, Peracetic acid, nanometer silica gel, water are subjected to haptoreaction so that gelatinization thing is made；
2) carboxymethyl cellulose and water is blended so that jelly is made；
3) Ludox, nano aluminium oxide, water is mixed so that mixture is made；
4) polyvinyl alcohol, urea, titanium dioxide, wollastonite powder, tributyl phosphate and water are heat-treated, then sequentially added
It is gelatinized thing, jelly, mixture and stirs so that electronic jacquard machine toughened paint is made.
Present invention also offers a kind of electronic jacquard machine toughened paint, the electronic jacquard machine toughened paint passes through above-mentioned
Preparation method be prepared.
In the above-mentioned technical solutions, the obtained tempering of collective effect that the present invention passes through above steps and raw material
There is excellent adhesive force, and the preparation method has process simple and the advantages of raw material is easy to get between coating and metal.
Other features and advantages of the present invention will be described in detail in subsequent specific embodiment part.
Embodiment
The embodiment of the present invention is described in detail below.It is it should be appreciated that described herein specific
Embodiment is merely to illustrate and explain the present invention, and is not intended to limit the invention.
The invention provides a kind of preparation method of electronic jacquard machine toughened paint, including：
1) cyclodextrin, Peracetic acid, nanometer silica gel, water are subjected to haptoreaction so that gelatinization thing is made；
2) carboxymethyl cellulose and water is blended so that jelly is made；
3) Ludox, nano aluminium oxide, water is mixed so that mixture is made；
4) polyvinyl alcohol, urea, titanium dioxide, wollastonite powder, tributyl phosphate and water are heat-treated, then sequentially added
It is gelatinized thing, jelly, mixture and stirs so that electronic jacquard machine toughened paint is made.
In the step 1) of the present invention, the dosage of each material can select in wide scope, but in order that obtained
There is more excellent adhesive force between toughened paint and metal；Preferably, in step 1), cyclodextrin, Peracetic acid, nano-silicon
Glue, the weight ratio of water are 10：1-3：0.8-1.6：30-50.
In the step 1) of the present invention, catalytic condition can select in wide scope, but in order that be made
Toughened paint and metal between there is more excellent adhesive force；Preferably, in step 1), haptoreaction meets following bar
Part：Reaction temperature is 70-80 DEG C, reaction time 4-6h.
In the step 2) of the present invention, the dosage of each material can select in wide scope, but in order that obtained
There is more excellent adhesive force between toughened paint and metal；Preferably, in step 2), the weight of carboxymethyl cellulose and water
Than for 10：60-100.
In the step 2) of the present invention, the condition of blending can select in wide scope, but in order that obtained steel
Changing between coating and metal has more excellent adhesive force；Preferably, in step 2), blending meets following condition：Blending temperature
Spend for 45-55 DEG C, the blending time is 2-4h.
In the step 3) of the present invention, the dosage of each material can select in wide scope, but in order that obtained
There is more excellent adhesive force between toughened paint and metal；Preferably, in step 3), Ludox, nano aluminium oxide, water
Weight ratio is 10：0.5-1：30-45.
In the step 3) of the present invention, the condition of mixing can select in wide scope, but in order that obtained steel
Changing between coating and metal has more excellent adhesive force；Preferably, in step 3), mixing meets following condition：Mixing temperature
Spend for 20-30 DEG C, incorporation time 2-4h.
In the step 4) of the present invention, the dosage of each material can select in wide scope, but in order that obtained
There is more excellent adhesive force between toughened paint and metal；Preferably, in step 4), polyvinyl alcohol, urea, titanium dioxide,
Wollastonite powder, tributyl phosphate, water, gelatinization thing, jelly, the weight ratio of mixture are 10：2-3：1-1.5：0.4-0.8：5-8：
30-40：6-9：4-8：10-13.
In the step 4) of the present invention, the condition of heat treatment and stirring can select in wide scope, but in order to
Made from making there is more excellent adhesive force between toughened paint and metal；Preferably, in step 4), heat treatment meets following
Condition：Heat treatment temperature is 110-120 DEG C, heat treatment time 3-5h；Stirring meets following condition：Whipping temp is 25-35
DEG C, mixing time 0.5-1h, stir speed (S.S.) 800-1200rpm.
Present invention also offers a kind of electronic jacquard machine toughened paint, the electronic jacquard machine toughened paint passes through above-mentioned
Preparation method be prepared.
The present invention will be described in detail by way of examples below.
Embodiment 1
1) by cyclodextrin, Peracetic acid, nanometer silica gel, water according to 10：2：1：40 weight is than carrying out haptoreaction (reaction
Temperature is 75 DEG C, reaction time 5h) it is gelatinized thing to be made；
2) by carboxymethyl cellulose and water according to 10：80 weight ratio is blended, and (blending temperature is 50 DEG C, and the time is blended
For 3h) with obtained jelly；
3) by Ludox, nano aluminium oxide, water according to 10：0.8：35 weight ratio mixed (mixing temperature be 25 DEG C,
Incorporation time is 3h) with obtained mixture；
4) polyvinyl alcohol, urea, titanium dioxide, wollastonite powder, tributyl phosphate and water is heat-treated to (heat treatment temperature is
115 DEG C, heat treatment time 4h), then sequentially add gelatinization thing, jelly, mixture and stir (whipping temp is 30 DEG C,
Mixing time is 0.8h, stir speed (S.S.) 1000rpm) be made electronic jacquard machine with toughened paint A1 (polyvinyl alcohol, urea,
Titanium dioxide, wollastonite powder, tributyl phosphate, water, gelatinization thing, jelly, the weight ratio of mixture are 10：2.5：1.3：0.6：7：
35：7：5：12).
Embodiment 2
1) by cyclodextrin, Peracetic acid, nanometer silica gel, water according to 10：1：0.8：30 weight is (more anti-than carrying out haptoreaction
It is 70 DEG C to answer temperature, reaction time 4h) it is gelatinized thing to be made；
2) by carboxymethyl cellulose and water according to 10：60 weight ratio is blended, and (blending temperature is 45 DEG C, and the time is blended
For 2h) with obtained jelly；
3) by Ludox, nano aluminium oxide, water according to 10：0.5：30 weight ratio mixed (mixing temperature be 20 DEG C,
Incorporation time is 2h) with obtained mixture；
4) polyvinyl alcohol, urea, titanium dioxide, wollastonite powder, tributyl phosphate and water is heat-treated to (heat treatment temperature is
110 DEG C, heat treatment time 3h), then sequentially add gelatinization thing, jelly, mixture and stir (whipping temp is 25 DEG C,
Mixing time is 0.5h, stir speed (S.S.) 800rpm) with obtained electronic jacquard machine toughened paint A2 (polyvinyl alcohol, urea, titanium
White powder, wollastonite powder, tributyl phosphate, water, gelatinization thing, jelly, the weight ratio of mixture are 10：2：1：0.4：5：30：6：4：
10)。
Embodiment 3
1) by cyclodextrin, Peracetic acid, nanometer silica gel, water according to 10：3：1.6：50 weight is (more anti-than carrying out haptoreaction
It is 80 DEG C to answer temperature, reaction time 6h) it is gelatinized thing to be made；
2) by carboxymethyl cellulose and water according to 10：100 weight ratio is blended, and (blending temperature is 55 DEG C, during blending
Between be 4h) be made jelly；
3) by Ludox, nano aluminium oxide, water according to 10：1：45 weight ratio is mixed, and (mixing temperature is 30 DEG C, is mixed
The conjunction time is 4h) with obtained mixture；
4) polyvinyl alcohol, urea, titanium dioxide, wollastonite powder, tributyl phosphate and water is heat-treated to (heat treatment temperature is
120 DEG C, heat treatment time 5h), then sequentially add gelatinization thing, jelly, mixture and stir (whipping temp is 35 DEG C,
Mixing time is 1h, stir speed (S.S.) 1200rpm) with obtained electronic jacquard machine toughened paint A3 (polyvinyl alcohol, urea, titanium
White powder, wollastonite powder, tributyl phosphate, water, gelatinization thing, jelly, the weight ratio of mixture are 10：3：1.5：0.8：8：40：9：
8：13).
Comparative example 1
Method according to embodiment 1 carries out that toughened paint B1 is made, unlike, gelatinization thing is not used in step 3).
Comparative example 2
Method according to embodiment 1 carries out that toughened paint B2 is made, unlike, jelly is not used in step 3).
Comparative example 3
Method according to embodiment 1 carries out that toughened paint B3 is made, unlike, mixture is not used in step 3).
Detect example 1
According to the adhesive force of the GB 1720-1979 method detection above-mentioned coatings recorded, concrete outcome is shown in Table 1.
Table 1
| A | A | A | B | B | B | |
| Adhesive force grade | One-level | One-level | One-level | Seven grades | Six grades | Seven grades |
Wherein, one-level is optimal in adhesive force grade, and seven grades are worst.
The preferred embodiment of the present invention described in detail above, still, the present invention are not limited in above-mentioned embodiment
Detail, in the range of the technology design of the present invention, a variety of simple variants can be carried out to technical scheme, this
A little simple variants belong to protection scope of the present invention.
It is further to note that each particular technique feature described in above-mentioned embodiment, in not lance
In the case of shield, can be combined by any suitable means, in order to avoid unnecessary repetition, the present invention to it is various can
The combination of energy no longer separately illustrates.
In addition, various embodiments of the present invention can be combined randomly, as long as it is without prejudice to originally
The thought of invention, it should equally be considered as content disclosed in this invention.
Claims (10)
- A kind of 1. preparation method of electronic jacquard machine toughened paint, it is characterised in that including：1) cyclodextrin, Peracetic acid, nanometer silica gel, water are subjected to haptoreaction so that gelatinization thing is made；2) carboxymethyl cellulose and water is blended so that jelly is made；3) Ludox, nano aluminium oxide, water is mixed so that mixture is made；4) polyvinyl alcohol, urea, titanium dioxide, wollastonite powder, tributyl phosphate and water are heat-treated, then sequentially added described It is gelatinized thing, jelly, mixture and stirs so that the electronic jacquard machine toughened paint is made.
- 2. preparation method according to claim 1, wherein, in step 1), the cyclodextrin, Peracetic acid, nano-silicon Glue, the weight ratio of water are 10：1-3：0.8-1.6：30-50.
- 3. preparation method according to claim 1, wherein, in step 1), the haptoreaction meets following condition：Instead It is 70-80 DEG C to answer temperature, reaction time 4-6h.
- 4. preparation method according to claim 1, wherein, in step 2), the weight of the carboxymethyl cellulose and water Than for 10：60-100.
- 5. preparation method according to claim 1, wherein, in step 2), the blending meets following condition：Blending temperature Spend for 45-55 DEG C, the blending time is 2-4h.
- 6. preparation method according to claim 1, wherein, in step 3), the Ludox, nano aluminium oxide, water Weight ratio is 10：0.5-1：30-45.
- 7. preparation method according to claim 1, wherein, in step 3), the mixing meets following condition：Mixing temperature Spend for 20-30 DEG C, incorporation time 2-4h.
- 8. according to the preparation method described in any one in claim 1-7, wherein, in step 4), the polyvinyl alcohol, urine Element, titanium dioxide, wollastonite powder, tributyl phosphate, water, gelatinization thing, jelly, the weight ratio of mixture are 10：2-3：1-1.5： 0.4-0.8：5-8：30-40：6-9：4-8：10-13.
- 9. preparation method according to claim 8, wherein, in step 4), the heat treatment meets following condition：At heat It is 110-120 DEG C to manage temperature, heat treatment time 3-5h；The stirring meets following condition：Whipping temp is 25-35 DEG C, mixing time 0.5-1h, stir speed (S.S.) 800- 1200rpm。
- 10. a kind of electronic jacquard machine toughened paint, it is characterised in that the electronic jacquard machine toughened paint will by right The preparation method in 1-9 described in any one is asked to be prepared.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711235970.XA CN107828292A (en) | 2017-11-30 | 2017-11-30 | Electronic jacquard machine toughened paint and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711235970.XA CN107828292A (en) | 2017-11-30 | 2017-11-30 | Electronic jacquard machine toughened paint and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107828292A true CN107828292A (en) | 2018-03-23 |
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ID=61647178
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711235970.XA Pending CN107828292A (en) | 2017-11-30 | 2017-11-30 | Electronic jacquard machine toughened paint and preparation method thereof |
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Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106243850A (en) * | 2016-08-04 | 2016-12-21 | 安徽罗伯特科技股份有限公司 | High temperature resistant spark gap and preparation method thereof |
-
2017
- 2017-11-30 CN CN201711235970.XA patent/CN107828292A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106243850A (en) * | 2016-08-04 | 2016-12-21 | 安徽罗伯特科技股份有限公司 | High temperature resistant spark gap and preparation method thereof |
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Application publication date: 20180323 |
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