CN107827245A - A kind of efficiently Shui nationality water purification effervescent tablet and preparation method thereof - Google Patents

A kind of efficiently Shui nationality water purification effervescent tablet and preparation method thereof Download PDF

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Publication number
CN107827245A
CN107827245A CN201711024379.XA CN201711024379A CN107827245A CN 107827245 A CN107827245 A CN 107827245A CN 201711024379 A CN201711024379 A CN 201711024379A CN 107827245 A CN107827245 A CN 107827245A
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China
Prior art keywords
parts
agent
effervescent
water purification
shui nationality
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CN201711024379.XA
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Chinese (zh)
Inventor
宋小飞
蔡文婷
施召才
高权
陈婷玉
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South China University of Technology SCUT
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South China University of Technology SCUT
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Priority to CN201711024379.XA priority Critical patent/CN107827245A/en
Publication of CN107827245A publication Critical patent/CN107827245A/en
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    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F3/00Biological treatment of water, waste water, or sewage
    • C02F3/34Biological treatment of water, waste water, or sewage characterised by the microorganisms used
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N25/00Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
    • A01N25/34Shaped forms, e.g. sheets, not provided for in any other sub-group of this main group
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N63/00Biocides, pest repellants or attractants, or plant growth regulators containing microorganisms, viruses, microbial fungi, animals or substances produced by, or obtained from, microorganisms, viruses, microbial fungi or animals, e.g. enzymes or fermentates
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/50Treatment of water, waste water, or sewage by addition or application of a germicide or by oligodynamic treatment

Abstract

The invention discloses a kind of efficiently Shui nationality water purification effervescent tablet and preparation method thereof.The efficient Shui nationality water purification effervescent tablet of the present invention is counted in parts by weight, including following component:1 10 parts of potassium hydrogen persulfate, 1 10 parts of alum, zeolite powder 10 50,1 10 parts of EDTA, compound 10 40 parts of hay bacillus, 1 10 parts of compound vitamin, waterproofing agent is more than 0 less than or equal to 40 parts, 3 30 parts of acidic effervescent agent, 3 30 parts of basic effervescent agent, filler is more than 0 less than or equal to 40 parts, 15 parts of 15 parts of binding agent and glidant.Again prepared by tabletting method using direct compressing dry granulation method or wet granulation for the efficient Shui nationality water purification effervescent tablet of the present invention.The efficient Shui nationality water purification effervescent tablet of the present invention has the advantages of disintegration is rapid, active ingredient dissolution is abundant, purifying water effect is good, and can effectively purify water environment, reduces aquatic-organism and is susceptible to suffer from the disease problems such as enteritis, body surface ulcer.

Description

A kind of efficiently Shui nationality water purification effervescent tablet and preparation method thereof
Technical field
The present invention relates to effervescent tablet and its preparing technical field, and in particular to it is a kind of efficiently Shui nationality water purification effervescent tablet and Its preparation method.
Background technology
At present due to ecologic structure and the traditional breeding way of aquaculture itself the defects of so that most of cultivation is present Many problems:Culture benefit declines, and aquatic product quality reduces;The use for cultivating the outer row, chemicals of nutrients causes water Body self-pollution, environmental degradation;Main breed variety is in a bad way and break out and spread etc..
Water purification agent has very important effect in being cultivated in the modern times, and market water purification class product is seen everywhere, many substrates Improved products also contain water purification agent composition, or even some products are exactly water purification agent at all.Compared with other type water transfer products:Only Aqua has the characteristics that quick acting, positive effect stabilization, not by extraneous eco-environmental impact.
Compound hay bacillus can produce hydrogen peroxide, bacteriocin, establish microecological balance, promote beneficial to anaerobe Breeding, suppress harmful bacteria(Escherichia coli, Salmonella)Growth, so as to prevent the stomach tract disease such as diarrhea;It is and compound Multidimensional can ensure healthy fish, fast-growth, the generation of aquatic products disease be reduced while efficient water purification, improve aquatic products quality Amount;Thus, study and add compound hay bacillus and compound vitamin in effervescent tablet, be advantageous to obtain the effervescent tablet of efficient water purification Agent.
The content of the invention
It is an object of the invention to provide a kind of efficiently Shui nationality water purification effervescent tablet.The water purification effervescent tablet can be purified effectively Water environment, reduce aquatic-organism and be susceptible to suffer from the diseases such as enteritis, body surface ulcer.
The present invention also aims to provide a kind of preparation method of described efficiently Shui nationality water purification effervescent tablet.
The purpose of the present invention is achieved through the following technical solutions.
A kind of efficiently Shui nationality water purification effervescent tablet, is counted in parts by weight, including following component:
Potassium hydrogen persulfate 1-10 parts, alum 1-10 parts, zeolite powder 10-50, ethylenediamine tetra-acetic acid(EDTA)1-10 parts, it is multiple Hay bacillus 10-40 parts, compound vitamin 1-10 parts are closed, waterproofing agent is more than 0 less than or equal to 40 parts, acidic effervescent agent 3-30 parts, alkali Property effervescent agent 3-30 parts, binding agent 1-5 parts and glidant 1-5 parts.
The waterproofing agent is selected from one or more of calcium monohydrogen phosphate, calcium carbonate, bentonite, diatomite and alundum (Al2O3), The waterproofing agent preferably is selected from one or more of diatomite and calcium monohydrogen phosphate;The introducing of waterproofing agent solves active ingredient solid system The sucting wet problem of agent, the product for enabling subsequently to prepare effectively keep tablet state;
The acidic effervescent agent is selected from one or more of citric acid, tartaric acid and oxalic acid, and the acidic effervescent agent preferably is selected from lemon One or more of lemon acid and tartaric acid;
The basic effervescent agent is selected from one or more of sodium carbonate, sodium acid carbonate, potassium carbonate and saleratus, the alkalescence bubble Rise agent and preferably be selected from one or more of sodium acid carbonate and saleratus;
The binding agent is selected from one or more of polyethylene glycol and carboxymethyl cellulose, and the mean molecule of the polyethylene glycol Measure as 5000-15000;
The glidant is selected from one or more of stearic acid, calcium stearate, magnesium stearate and talcum powder, and the glidant is preferred From one or more of talcum powder and magnesium stearate.
It is further preferred that the efficiently Shui nationality water purification effervescent tablet is counted in parts by weight, including following component:
5 parts of potassium hydrogen persulfate, 5 parts of alum, 25 parts of zeolite powder, 5 parts of EDTA, compound 20 parts of hay bacillus, compound vitamin 5 1 part of part, 10 parts of waterproofing agent, 7 parts of acidic effervescent agent, 10 parts of basic effervescent agent, 2 parts of binding agent and glidant.
Further, the efficiently Shui nationality water purification effervescent tablet also includes filler, and the mass parts of the filler are small more than 0 In equal to 40 parts.
It is further preferred that the filler is selected from one or more of starch, kaolin, lactose and white carbon, it is described to fill out Material is still more preferably from one or more of lactose and kaolin.
Still more preferably, the efficiently Shui nationality water purification effervescent tablet is counted in parts by weight, including following component:
5 parts of potassium hydrogen persulfate, 5 parts of alum, 10 parts of zeolite powder, 5 parts of EDTA, compound 20 parts of hay bacillus, compound vitamin 5 18 parts of part, 10 parts of waterproofing agent, 8 parts of acidic effervescent agent, 10 parts of basic effervescent agent, 2 parts of binding agent, 2 parts of glidant and filler.
Still more preferably, the efficiently Shui nationality water purification effervescent tablet is counted in parts by weight, including following component:
5 parts of potassium hydrogen persulfate, 5 parts of alum, 10 parts of zeolite powder, 5 parts of EDTA, compound 20 parts of hay bacillus, compound vitamin 5 27 parts of part, 2 parts of waterproofing agent, 8 parts of acidic effervescent agent, 10 parts of basic effervescent agent, 2 parts of binding agent, 1 part of glidant and filler.
The method for preparing a kind of efficiently Shui nationality water purification effervescent agent described in any of the above-described, including direct compressing dry granulation method Or wet granulation tabletting method again.
Further, the directly compressing dry granulation method comprises the following steps:
(1)By the mass parts, by potassium hydrogen persulfate, alum, zeolite powder, EDTA, compound hay bacillus and compound vitamin It is dried, remaining component is crushed respectively;
(2)Step will be passed through(1)After all raw material components of processing are well mixed, direct compressing dry granulation, the High-efficient Water is obtained Race's water purification effervescent agent.
Further, it is mechanical crushing to the breaking method of acidic effervescent agent and basic effervescent agent, the particle diameter after crushing It is 80-100 mesh;Breaking method to remaining component to be comminuted is comminution by gas stream, and the particle diameter after crushing is 800-1000 Mesh.
Further, the wet granulation again tabletting method be applied to the efficient Shui nationality water purification effervescent tablet containing filler system It is standby, comprise the following steps:
(1)Prepare acid particles and alkali grain
(1-1)Filler is divided into two parts, respectively acidic effervescent agent pair according to the mass ratio of acidic effervescent agent and basic effervescent agent The filler answered filler corresponding with basic effervescent agent;After binding agent is crushed, according to the matter of acidic effervescent agent and basic effervescent agent It is two parts, the respectively binding agent corresponding with basic effervescent agent of binding agent corresponding to acidic effervescent agent to measure score;
(1-2)Mix, obtain acid with EDTA, compound vitamin and compound hay bacillus after filler corresponding to acidic effervescent agent is crushed Material;Will filler corresponding to basic effervescent agent and waterproofing agent mix after crush, then with the zeolite powder of drying, potassium hydrogen persulfate and Alum mixes, and obtains alkaline material;
(1-3)After acidic effervescent agent and basic effervescent agent are crushed, corresponding acid material and alkaline material, mixing are separately added into Corresponding binding agent is separately added into again after uniformly, is well mixed, and acid softwood and alkaline softwood are made respectively;
(1-4)Acid softwood and alkaline softwood are pelletized respectively, dried, whole grain, respectively obtains acid particles and alkali grain;
(2)After acid particles and alkali grain are well mixed, the glidant after addition crushing, mix, tabletting, obtain the height Imitate Shui nationality water purification effervescent tablet.
Further, it is mechanical crushing to the breaking method of acidic effervescent agent and basic effervescent agent, the particle diameter after crushing It is 80-100 mesh;Waterproofing agent, binding agent, glidant and filler are crushed using comminution by gas stream, the particle diameter after crushing It is 800-1000 mesh.
By direct compressing dry granulation or wet granulation again tabletting tabletting method prepare efficient Shui nationality water purification effervescent tablet Be shaped as circular or irregular shape, including ellipse or rhombus, and the weight of every efficient Shui nationality water purification effervescent tablet is 0.5 gram -3.0 grams.
Compared with prior art, the invention has the advantages that and beneficial effect:
(1)The water purification composition including zeolite powder and EDTA is introduced in the efficient Shui nationality water purification effervescent tablet of the present invention, is drawn simultaneously Compound hay bacillus and compound vitamin are entered, can effectively purify water environment, reduced aquatic-organism and be susceptible to suffer from the diseases such as enteritis, body surface ulcer Sick problem, ensure the health of aquatic-organism;
(2)The efficient Shui nationality water purification effervescent tablet of the present invention is with disintegration is rapid, active ingredient dissolution is abundant, purifying water effect is good The advantages of, compared with traditional water purification agent, the various diseases of aquatic-organism can be effectively reduced in aquaculture;
(3)Preparation method of the present invention is simple and easy, it is easy to accomplish industrialization.
Brief description of the drawings
Fig. 1 is the production technology for preparing efficient Shui nationality water purification effervescent tablet in embodiment 1 using direct compressing dry granulation method Flow chart;
Fig. 2 is that using wet granulation, tabletting method prepares the production technology stream of efficient Shui nationality water purification effervescent tablet again in embodiment 2 Cheng Tu.
Embodiment
Technical solution of the present invention is described in further detail below in conjunction with specific embodiment and accompanying drawing, but present invention protection Scope not limited to this.
Experimental method described in following examples, it is conventional method unless otherwise specified;The reagent and material, such as Without specified otherwise, commercially obtain.
Embodiment 1
A kind of efficiently Shui nationality water purification effervescent tablet, by weight, including following component:
5.0 parts of potassium hydrogen persulfate, 5.0 parts of alum, 20.0 parts of compound hay bacillus, 5.0 parts of compound vitamin, EDTA 5.0 Part, 10.0 parts of zeolite powder, diatomite(Waterproofing agent)10.0 parts, citric acid(Acidic effervescent agent)8.0 parts, sodium acid carbonate(Alkalescence bubble Rise agent)10.0 parts, polyethylene glycol(Binding agent)2.0 parts, magnesium stearate(Glidant)2.0 parts, lactose(Filler)18 parts.
A kind of described efficiently Shui nationality water purification effervescent tablet is prepared using direct compressing dry granulation method(10 kg sample meters), Process chart is as shown in figure 1, specifically comprise the following steps:
(1)By 0.5 kg potassium hydrogen persulfates, 0.5 kg alums and 0.5 kg compound vitamins 43 DEG C dry 2 hours, 0.5 Kg EDTA and 1.0 kg zeolite powders pack respectively after 105 DEG C dry 2 hours;
(2)By 0.80 kg citric acids and 1.00 kg sodium acid carbonates mechanical crushings to 100 mesh, 1 kg diatomite, the poly- second of 0.2 kg Rear air-flow crushing is mixed evenly to 800 mesh in glycol, 0.2 kg magnesium stearates and 1.8 kg lactose;
(3)Step will be passed through(1)And step(2)All compound hay bacilluses of raw material components and 2.0kg of processing stir in mixing Mix in machine stirring 10 minutes it is well mixed after, be pressed into effervescent tablet, pack, obtain finished product, be the efficient Shui nationality of round sheet Water purification effervescent tablet, and the weight average of every efficient Shui nationality water purification effervescent tablet is 1g.
Embodiment 2
A kind of efficiently Shui nationality water purification effervescent tablet, by weight, including following component:
5.0 parts of potassium hydrogen persulfate, 5.0 parts of alum, 20.0 parts of compound hay bacillus, 5.0 parts of compound vitamin, EDTA 5.0 Part, 10.0 parts of zeolite powder, diatomite(Waterproofing agent)2.0 parts, citric acid(Acidic effervescent agent)8.0 parts, sodium acid carbonate(Alkaline effervesce Agent)10.0 parts, polyethylene glycol(Binding agent)2.0 parts, magnesium stearate(Glidant)1.0 parts, lactose(Filler)27 parts.
Using wet granulation, tabletting method prepares a kind of described efficiently Shui nationality water purification effervescent tablet again(10 kg samples Meter), process chart is as shown in Fig. 2 specifically comprise the following steps:
(1)By 0.5 kg potassium hydrogen persulfates, 0.5 kg alums and 0.5 kg compound vitamins 43 DEG C dry 2 hours, 0.5 Kg EDTA and 1.0 kg zeolite powders pack respectively after 105 C are dried 2 hours;
(2)It is compound withered with dried EDTA, compound vitamin and 2.0 kg by 1.35 kg lactose air-flow crushings to 1000 mesh After careless bacillus stirs 10 minutes in mixing and blending machine, pack, obtain material A;By 0.2 kg diatomite and 1.35 kg lactose It is mixed evenly, air-flow crushing to 1000 mesh, is being mixed with dried zeolite powder, potassium hydrogen persulfate and alum Stirring 10 minutes, pack, obtain material B in machine;
(3)By 0.8 kg citric acids and 1.0 kg sodium acid carbonates mechanical crushings to 100 mesh, 0.1 kg magnesium stearate air-flow crushings arrive 1000 mesh, are individually packed;
(4)Citric acid after crushing is added into step(2)In the material A of preparation, add after being stirred 10 minutes in mixing and blending machine Enter 0.1 kg polyethylene glycol, remix 10 minutes, acid softwood is made;Sodium acid carbonate after crushing is added into step(2)Prepare Material B in, add 0.1 kg polyethylene glycol after being stirred 10 minutes in mixing and blending machine, remix 10 minutes, be made alkalescence Softwood;
(5)Respectively by step(4)In obtained acid softwood and alkaline softwood be placed in granulator and pelletize, dried at 45 DEG C to water Divide after being less than 2%, obtain acid particles and alkali grain through 20 mesh sieve whole grains, pack respectively;
(6)By step(5)In the obtained kg of acid particles 5.25, the kg of alkali grain 4.65 add mixer in, addition 0.1 Kg magnesium stearates, tabletting after mixing 10 minutes, tabletting are made effervescent tablet, packed, and obtain finished product, are the height of round sheet Shui nationality water purification effervescent tablet is imitated, and the weight average of every efficient Shui nationality water purification effervescent tablet is 1.2g.
Embodiment 3
A kind of efficiently Shui nationality water purification effervescent tablet, by weight, including following component:
10.0 parts of potassium hydrogen persulfate, 10.0 parts of alum, 10.0 parts of compound hay bacillus, 1.0 parts of compound vitamin, EDTA 1.0 Part, 12.0 parts of zeolite powder, diatomite(Waterproofing agent)1.0 parts, citric acid(Acidic effervescent agent)30.0 parts, sodium acid carbonate(Alkalescence bubble Rise agent)20.0 parts, polyethylene glycol(Binding agent)1.0 parts, magnesium stearate(Glidant)1.0 parts, lactose(Filler)3.0 part.
Prepare a kind of described efficiently Shui nationality water purification effervescent tablet(10 kg sample meters), proportioning calculates each respectively more than Amounts of components, weigh, prepared by direct compressing dry granulation method, detailed process is the same as embodiment 1.
Obtained product is the efficient Shui nationality water purification effervescent tablet of round sheet, and every efficient Shui nationality water purification effervescent tablet Weight average be 1.5g.
Embodiment 4
A kind of efficiently Shui nationality water purification effervescent tablet, by weight, including following component:
1.0 parts of potassium hydrogen persulfate, 1.0 parts of alum, 10.0 parts of compound hay bacillus, 10.0 parts of compound vitamin, EDTA 10.0 Part, 50.0 parts of zeolite powder, diatomite(Waterproofing agent)1.0 parts, citric acid(Acidic effervescent agent)3.0 parts, sodium acid carbonate(Alkaline effervesce Agent)3.0 parts, polyethylene glycol(Binding agent)5.0 parts, magnesium stearate(Glidant)5.0 parts, lactose(Filler)1.0 part.
Prepare a kind of described efficiently Shui nationality water purification effervescent tablet(10 kg sample meters), proportioning calculates each respectively more than Amounts of components, weigh, prepared by direct compressing dry granulation method, detailed process is the same as embodiment 1.
Obtained product is the efficient Shui nationality water purification effervescent tablet of round sheet, and every efficient Shui nationality water purification effervescent tablet Weight average be 0.5g.
Embodiment 5
A kind of efficiently Shui nationality water purification effervescent tablet, by weight, including following component:
1.0 parts of potassium hydrogen persulfate, 1.0 parts of alum, 40.0 parts of compound hay bacillus, 2.0 parts of compound vitamin, EDTA 1.0 Part, 10.0 parts of zeolite powder, diatomite(Waterproofing agent)2.0 parts, citric acid(Acidic effervescent agent)10.0 parts, sodium acid carbonate(Alkalescence bubble Rise agent)30.0 parts, polyethylene glycol(Binding agent)1.0 parts, magnesium stearate(Glidant)1.0 parts, lactose(Filler)1.0 part.
Prepare a kind of described efficiently Shui nationality water purification effervescent tablet(10 kg sample meters), proportioning calculates each respectively more than Amounts of components, weigh, by wet granulation, again prepared by pressed disc method, and detailed process is the same as embodiment 2.
Obtained product is the efficient Shui nationality water purification effervescent tablet of round sheet, and every efficient Shui nationality water purification effervescent tablet Weight average be 3g.
Embodiment 6
A kind of efficiently Shui nationality water purification effervescent tablet, by weight, including following component:
2.0 parts of potassium hydrogen persulfate, 2.0 parts of alum, 15.0 parts of compound hay bacillus, 3.0 parts of compound vitamin, EDTA 3.0 Part, 15.0 parts of zeolite powder, diatomite(Waterproofing agent)8.0 parts, citric acid(Acidic effervescent agent)5.0 parts, sodium acid carbonate(Alkaline effervesce Agent)5.0 parts, polyethylene glycol(Binding agent)1.0 parts, magnesium stearate(Glidant)1.0 parts, lactose(Filler)40.0 parts.
Prepare a kind of described efficiently Shui nationality water purification effervescent tablet(10 kg sample meters), proportioning calculates each respectively more than Amounts of components, weigh, by wet granulation, again prepared by pressed disc method, and detailed process is the same as embodiment 2.
Obtained product is the efficient Shui nationality water purification effervescent tablet of round sheet, and every efficient Shui nationality water purification effervescent tablet Weight average be 2.1g.
Above example is only preferrred embodiment of the present invention, is only used for explaining the present invention, is not intended to limit the present invention, this Change that art personnel are made under without departing from spirit of the invention, replacement, modification etc. all should belong to the guarantor of the present invention Protect scope.

Claims (10)

  1. A kind of 1. efficiently Shui nationality water purification effervescent tablet, it is characterised in that count in parts by weight, including following component:
    Potassium hydrogen persulfate 1-10 parts, alum 1-10 parts, zeolite powder 10-50, EDTA 1-10 parts, compound hay bacillus 10-40 Part, compound vitamin 1-10 parts, waterproofing agent is more than 0 less than or equal to 40 parts, acidic effervescent agent 3-30 parts, basic effervescent agent 3-30 parts, Binding agent 1-5 parts and glidant 1-5 parts;
    The waterproofing agent is selected from one or more of calcium monohydrogen phosphate, calcium carbonate, bentonite, diatomite and alundum (Al2O3);It is described Acidic effervescent agent is selected from one or more of citric acid, tartaric acid and oxalic acid;The basic effervescent agent is selected from sodium carbonate, bicarbonate One or more of sodium, potassium carbonate and saleratus;The one kind of the binding agent in polyethylene glycol and carboxymethyl cellulose More than, and the mean molecule quantity of the polyethylene glycol is 5000-15000;The glidant is selected from stearic acid, calcium stearate, hard One or more of fatty acid magnesium and talcum powder.
  2. 2. a kind of efficiently Shui nationality water purification effervescent tablet according to claim 1, it is characterised in that count, wrap in parts by weight Include following component:
    5 parts of potassium hydrogen persulfate, 5 parts of alum, 25 parts of zeolite powder, 5 parts of EDTA, compound 20 parts of hay bacillus, compound vitamin 5 1 part of part, 10 parts of waterproofing agent, 7 parts of acidic effervescent agent, 10 parts of basic effervescent agent, 2 parts of binding agent and glidant.
  3. 3. a kind of efficiently Shui nationality water purification effervescent tablet according to claim any one of 1-2, it is characterised in that described to block water Agent is selected from one or more of diatomite and calcium monohydrogen phosphate;The acidic effervescent agent in citric acid and tartaric acid it is a kind of with On;The basic effervescent agent is selected from one or more of sodium acid carbonate and saleratus;The glidant is selected from talcum powder and firmly One or more of fatty acid magnesium.
  4. A kind of 4. efficiently Shui nationality water purification effervescent tablet according to claim 1, it is characterised in that the efficiently Shui nationality water purification Effervescent tablet also includes filler;The mass parts of the filler are to be less than or equal to 40 parts more than 0;The filler is selected from starch, kaolinite One or more of soil, lactose and white carbon.
  5. 5. a kind of efficiently Shui nationality water purification effervescent tablet according to claim 4, it is characterised in that count, wrap in parts by weight Include following component:
    5 parts of potassium hydrogen persulfate, 5 parts of alum, 10 parts of zeolite powder, 5 parts of EDTA, compound 20 parts of hay bacillus, compound vitamin 5 18 parts of part, 10 parts of waterproofing agent, 8 parts of acidic effervescent agent, 10 parts of basic effervescent agent, 2 parts of binding agent, 2 parts of glidant and filler.
  6. 6. a kind of efficiently Shui nationality water purification effervescent tablet according to claim 4, it is characterised in that count, wrap in parts by weight Include following component:
    5 parts of potassium hydrogen persulfate, 5 parts of alum, 10 parts of zeolite powder, 5 parts of EDTA, compound 20 parts of hay bacillus, compound vitamin 5 27 parts of part, 2 parts of waterproofing agent, 8 parts of acidic effervescent agent, 10 parts of basic effervescent agent, 2 parts of binding agent, 1 part of glidant and filler.
  7. 7. a kind of efficiently Shui nationality water purification effervescent tablet according to claim any one of 4-6, it is characterised in that described to block water Agent is selected from one or more of diatomite and calcium monohydrogen phosphate;The acidic effervescent agent in citric acid and tartaric acid it is a kind of with On;The basic effervescent agent is selected from one or more of sodium acid carbonate and saleratus;The glidant is selected from talcum powder and firmly One or more of fatty acid magnesium.
  8. A kind of 8. efficiently Shui nationality water purification effervescent tablet according to claim any one of 4-6, it is characterised in that the filler Selected from one or more of lactose and kaolin.
  9. 9. prepare a kind of method of efficiently Shui nationality water purification effervescent tablet described in claim any one of 1-8, it is characterised in that be Direct compressing dry granulation method, comprises the following steps:
    (1)By the mass parts, by potassium hydrogen persulfate, alum, zeolite powder, EDTA, compound hay bacillus and compound vitamin It is dried, remaining component is crushed respectively;
    It is mechanical crushing to the breaking method of acidic effervescent agent and basic effervescent agent, the particle diameter after crushing is 80-100 mesh;It is right The breaking method of remaining component to be comminuted is comminution by gas stream, and the particle diameter after crushing is 800-1000 mesh;
    (2)Step will be passed through(1)After all raw material components of processing are well mixed, direct compressing dry granulation, the High-efficient Water is obtained Race's water purification effervescent agent.
  10. 10. prepare a kind of method of efficiently Shui nationality water purification effervescent tablet described in claim any one of 4-8, it is characterised in that For wet granulation tabletting method again, comprise the following steps:
    (1)Prepare acid particles and alkali grain
    (1-1)Filler is divided into two parts, respectively acidic effervescent agent pair according to the mass ratio of acidic effervescent agent and basic effervescent agent The filler answered filler corresponding with basic effervescent agent;After binding agent is crushed, according to the matter of acidic effervescent agent and basic effervescent agent It is two parts, the respectively binding agent corresponding with basic effervescent agent of binding agent corresponding to acidic effervescent agent to measure score;
    (1-2)Mix, obtain acid with EDTA, compound vitamin and compound hay bacillus after filler corresponding to acidic effervescent agent is crushed Material;Will filler corresponding to basic effervescent agent and waterproofing agent mix after crush, then with the zeolite powder of drying, potassium hydrogen persulfate and Alum mixes, and obtains alkaline material;
    (1-3)After acidic effervescent agent and basic effervescent agent are crushed, corresponding acid material and alkaline material, mixing are separately added into Corresponding binding agent is separately added into again after uniformly, is well mixed, and acid softwood and alkaline softwood are made respectively;
    (1-4)Acid softwood and alkaline softwood are pelletized respectively, dried, whole grain, respectively obtains acid particles and alkali grain;
    (2)After acid particles and alkali grain are well mixed, the glidant after addition crushing, mix, tabletting, obtain the height Imitate Shui nationality water purification effervescent tablet;
    It is mechanical crushing to the breaking method of acidic effervescent agent and basic effervescent agent, the particle diameter after crushing is 80-100 mesh;It is right Waterproofing agent, binding agent, glidant and filler are crushed using comminution by gas stream, and the particle diameter after crushing is 800-1000 mesh.
CN201711024379.XA 2017-10-27 2017-10-27 A kind of efficiently Shui nationality water purification effervescent tablet and preparation method thereof Pending CN107827245A (en)

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