CN107815358A - 一种油茶籽洗衣粉的制备方法 - Google Patents
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Abstract
本发明公开了一种油茶籽洗衣粉的制备方法，涉及日化洗涤产品技术领域，洗衣粉的制备，包括以下步骤：S1.将油茶籽粕干燥；S2.将干燥后的油茶籽粕粉碎成末；S3.将油茶籽粉末、十二烷基苯磺酸钠、水混合搅拌；S4.再加入无水碳酸钠、硅酸钠、羧甲基纤维素混合搅拌；S5.最后加入蛋白酶搅拌混合；S6.将混合物干燥；S7.将干燥后的混合物粉碎、过筛，得到洗衣粉成品；本发明采用纯天然油茶籽，不仅增加了油茶籽的利用率，而且天然环保健康，不会对环境造成污染也不会损害人体。
Description
技术领域
本发明涉及日化洗涤产品技术领域，具体是一种油茶籽洗衣粉的制备方法。
背景技术
洗衣粉是人们日常生活的必需品，随着生活水平质量的提高以及科技的快速发展，人们也开始由单一的注重洗衣效果到注重洗衣效果与环保结合起来。传统的洗衣粉中含有大量的磷，在洗衣的过程中，磷会随洗衣水流入到各种水域造成水质营养化，使得水草大量繁殖，消耗水中的氧气造成水中生物大量死亡，最终导致水质恶化不能使用，严重污染了环境以及危及人们的用水健康。
油茶，(拉丁文名Camellia oleifera Abel.)，茶科属常绿小乔木；因其种子可榨油供食用，故名。油茶籽油即从油茶籽中提取的油脂，其养分含量丰富不饱和脂肪酸93％(油酸83％，亚油酸10％)、山茶苷、磷脂质和皂苷、维生素E和鞣质，被誉为“中国橄榄油”。而油茶籽经过油茶籽油提取后剩余的油茶籽粕中同样含有丰富养分其含有茶皂素20％～25％，茶多糖18％～20％，茶蛋白15％～20％，具有很高的经济价值。
油茶中的茶皂素是一种天然功能性活性成分，其去油、去污能力非常强，能迅速去除油污；可用于碗筷、盘子、锅子、蔬菜、水果等的清洗。中国是茶籽油生产的大国，每年产生大量的副产品茶籽饼粕，很少用来做进一步的深加工，价值很低，没有得到充分利用。
发明内容
本发明的目的在于：为了解决由传统洗衣粉中的磷对环境及人们饮用水健康污染的问题，提供了一种油茶籽洗衣粉的制备方法。
本发明采用的技术方案如下：
一种油茶籽洗衣粉的制备方法，具体包括以下步骤：
S1.将脱油后的油茶籽粕用干燥机干燥；
S2.将干燥后的油茶籽粕，用粉碎机粉碎成粉末；
粉碎后的油茶籽粕粉碎所需时间更少，粉碎效果更好；
S3.将S2步骤制得的油茶籽粉40～55份、十二烷基苯磺酸钠10～15份、水2～3份混合搅拌，搅拌速度为200～400r/min，搅拌5～8min，形成混合溶液；
S4.将无水碳酸钠20～30份、硅酸钠3～6份、羧甲基纤维素1～2.5份、水1～2份加入到步骤S3制得的混合溶液中搅拌，搅拌速度为300～500r/min，搅拌5～10min，形成糊状混合物，备用；
S5.将蛋白酶2～3份加入到步骤S4制得的糊状混合物中搅拌，搅拌速度为100～300r/min，搅拌5～8min，形成糊状混合物，备用；
S6.将步骤S5中制得的糊状混合物，用干燥机干燥，得到大颗粒的洗衣粉固体，备用；
S7.将步骤S6制得的洗衣粉固体粉碎，得到洗衣粉成品，包装完成。
优选的，所述步骤S1中油茶籽粕中茶皂素含量为20％～25％。
优选的，所述步骤S2中油茶籽粉末过200～500目筛。
优选的，所述步骤S1和S6中所述的干燥机为微波干燥机，其功率为2～4w、温度为40～50℃、时间为5～15min。
优选的，所述步骤S7中洗衣粉成品颗粒的粒径为过30～80目筛。
优选的，所述步骤S7中所述洗衣粉成品水分为0.1％～0.5％。
综上所述，由于采用了上述技术方案，本发明的有益效果是：
1、本发明中采用纯天然油茶籽，天然环保健康，所有成分均为天然可降解的有机成分，不会对环境造成污染也不会损害人体。所含有效成分茶皂素又名茶皂甙，是由茶树种子中提取出来的一类醣甙化合物，是一种性能良好的天然表面活性剂。经检测，茶皂素具有良好的乳化、分散、发泡、湿润等功能，并且具有消炎、镇痛，抗渗透等药理作用，具有极强的去油污能力。所含有效成分茶多酚是水溶性物质，具有消毒、灭菌、抗皮肤老化，减少日光中的紫外线辐射对皮肤的损伤等功效。
2、本发明采用微波干燥，由于微波干燥能够深入到物料的内部，内外同时加热，而不是依靠物料本身的热传导，脱水速度更快，避免常规加热过程中容易引起材料的表面硬化几不均匀等现象。
3、将油茶籽粕干燥后粉碎，粉碎效果更好；粉碎后的油茶籽粕在使用过程中，其反应面积增加，其活性效果更好。
4、洗衣粉颗粒不宜太细或太粗，太细易成粉尘，流动性就差；颗粒太大，会影响粒子的溶解度；经过30～80目筛大小的颗粒大小最佳。
具体实施方式
下面结合具体实施例对本发明作进一步说明：
实施例1
一种油茶籽洗衣粉的制备方法，具体包括以下步骤：
S1.将脱油后的油茶籽粕用干燥机干燥；
S2.将干燥后的油茶籽粕，用粉碎机粉碎成粉末；
粉碎后的油茶籽粕粉碎所需时间更少，粉碎效果更好；
S3.将S2步骤制得的油茶籽粉40份、十二烷基苯磺酸钠10份、水2份混合搅拌，搅拌速度为300r/min，搅拌6min，形成混合溶液；
S4.将无水碳酸钠20份、硅酸钠3份、羧甲基纤维素1份、水1份加入到步骤S3制得的混合溶液中搅拌，搅拌速度为400r/min，搅拌10min，形成糊状混合物，备用；
S5.将蛋白酶2份加入到步骤S4制得的糊状混合物中搅拌，搅拌速度为200r/min，搅拌7min，形成糊状混合物，备用；
S6.将步骤S5中制得的糊状混合物，用干燥机干燥，得到大颗粒的洗衣粉固体，备用；
S7.将步骤S6制得的洗衣粉固体粉碎，得到洗衣粉成品，包装完成。
所述步骤S1中油茶籽粕中茶皂素含量为20％～25％。
所述步骤S2中油茶籽粉末过200目筛。
所述步骤S1和S6中所述的干燥机为微波干燥机，其功率为4w、温度为45℃、时间为10min。
所述步骤S7中洗衣粉成品颗粒的粒径为过30目筛。
所述步骤S7中所述洗衣粉成品水分为0.1％～0.5％。
实施例2
一种油茶籽洗衣粉的制备方法，具体包括以下步骤：
S1.将脱油后的油茶籽粕用干燥机干燥；
S2.将干燥后的油茶籽粕，用粉碎机粉碎成粉末；
粉碎后的油茶籽粕粉碎所需时间更少，粉碎效果更好；
S3.将S2步骤制得的油茶籽粉50份、十二烷基苯磺酸钠12份、水2份混合搅拌，搅拌速度为300r/min，搅拌6min，形成混合溶液；
S4.将无水碳酸钠25份、硅酸钠4.5份、羧甲基纤维素1.5份、水1.5份加入到步骤S3制得的混合溶液中搅拌，搅拌速度为400r/min，搅拌10min，形成糊状混合物，备用；
S5.将蛋白酶2.5份加入到步骤S4制得的糊状混合物中搅拌，搅拌速度为200r/min，搅拌7min，形成糊状混合物，备用；
S6.将步骤S5中制得的糊状混合物，用干燥机干燥，得到大颗粒的洗衣粉固体，备用；
S7.将步骤S6制得的洗衣粉固体粉碎，得到洗衣粉成品，包装完成。
所述步骤S1中油茶籽粕中茶皂素含量为20％～25％。
所述步骤S2中油茶籽粉末过400目筛。
所述步骤S1和S6中所述的干燥机为微波干燥机，其功率为4w、温度为45℃、时间为10min。
所述步骤S7中洗衣粉成品颗粒的粒径为过500目筛。
所述步骤S7中所述洗衣粉成品水分为0.1％～0.5％。
实施例3
一种油茶籽洗衣粉的制备方法，具体包括以下步骤：
S1.将脱油后的油茶籽粕用干燥机干燥；
S2.将干燥后的油茶籽粕，用粉碎机粉碎成粉末；
粉碎后的油茶籽粕粉碎所需时间更少，粉碎效果更好；
S3.将S2步骤制得的油茶籽粉55份、十二烷基苯磺酸钠15份、水3份混合搅拌，搅拌速度为300r/min，搅拌6min，形成混合溶液；
S4.将无水碳酸钠30份、硅酸钠6份、羧甲基纤维素2.5份、水2份加入到步骤S3制得的混合溶液中搅拌，搅拌速度为400r/min，搅拌10min，形成糊状混合物，备用；
S5.将蛋白酶3份加入到步骤S4制得的糊状混合物中搅拌，搅拌速度为200r/min，搅拌7min，形成糊状混合物，备用；
S6.将步骤S5中制得的糊状混合物，用干燥机干燥，得到大颗粒的洗衣粉固体，备用；
S7.将步骤S6制得的洗衣粉固体粉碎，得到洗衣粉成品，包装完成。
所述步骤S1中油茶籽粕中茶皂素含量为20％～25％。
所述步骤S2中油茶籽粉末过500目筛。
所述步骤S1和S6中所述的干燥机为微波干燥机，其功率为2～4w、温度为45℃、时间为10min。
所述步骤S7中洗衣粉成品颗粒的粒径为过80目筛。
所述步骤S7中所述洗衣粉成品水分为0.1％～0.5％。
以上所述仅为本发明的较佳实施例而已，并不用以限制本发明，凡在本发明的精神和原则之内所作的任何修改、等同替换和改进等，均应包含在本发明的保护范围之内。
Claims (7)
1.一种油茶籽洗衣粉的制备方法，其特征在于，所述洗衣粉的制备，包括以下步骤：
S1.将油茶籽粕用干燥机干燥，备用；
S2.将干燥的油茶籽粕用粉碎机粉碎成粉末，备用；
S3.将S2中制得的油茶籽粉末与十二烷基苯磺酸钠、水混合搅拌，形成混合溶液，备用；
S4.然后加入无水碳酸钠、硅酸钠、羧甲基纤维素混合搅拌，备用；
S5.再加入蛋白酶搅拌混合，得到糊状混合物，备用；
S6.用干燥机将步骤S5中制得的糊状混合物干燥，得到洗衣粉固体，备用；
S7.步骤S6制得的洗衣粉固体粉碎、过筛，得到成大小均匀的颗粒即洗衣粉成品。
2.根据权利要求1所述的油茶籽洗衣粉的制备方法，其特征在于，洗衣粉由下述组分(按质量份数)组成：十二烷基苯磺酸钠10～15份；羧甲基纤维素1～2.5份；无水碳酸钠20～30份；油茶籽粉40～55份；硅酸钠3～6份；蛋白酶2～3份；水3～5份。
3.根据权利要求1所述的油茶籽洗衣粉的制备方法，其特征在于，所述步骤S1中油茶籽粕中茶皂素含量为20％～25％。
4.根据权利要求1所述的油茶籽洗衣粉的制备方法，其特征在于，所述步骤S1与S6中的干燥机为微波干燥机。
5.根据权利要求1所述的油茶籽洗衣粉的制备方法，其特征在于，所述步骤S2中油茶籽粉末过200～500目筛。
6.根据权利要求1所述的油茶籽洗衣粉的制备方法，其特征在于，所述步骤S7中洗衣粉成品颗粒过30～80目筛。
7.根据权利要求1所述的油茶籽洗衣粉的制备方法，其特征在于，所述步骤S7中所述洗衣粉成品水分含量为0.1％～0.5％。
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| CN110184138A (zh) * | 2019-06-27 | 2019-08-30 | 湖南淳湘农林科技有限公司 | 一种油茶粕生物新型表面活性洗涤粉 |
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| CN109266465A (zh) * | 2018-11-23 | 2019-01-25 | 谢岳贤 | 一种粉状洗洁精配方 |
| CN110184138A (zh) * | 2019-06-27 | 2019-08-30 | 湖南淳湘农林科技有限公司 | 一种油茶粕生物新型表面活性洗涤粉 |
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