CN107809102A - A kind of mass spectrometer detector high tension protection circuit - Google Patents

A kind of mass spectrometer detector high tension protection circuit Download PDF

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Publication number
CN107809102A
CN107809102A CN201711112487.2A CN201711112487A CN107809102A CN 107809102 A CN107809102 A CN 107809102A CN 201711112487 A CN201711112487 A CN 201711112487A CN 107809102 A CN107809102 A CN 107809102A
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CN
China
Prior art keywords
control unit
detector
voltage
high pressure
source module
Prior art date
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Pending
Application number
CN201711112487.2A
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Chinese (zh)
Inventor
应刚
刘建魁
游小燕
李林
周立
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Jiangsu Skyray Instrument Co Ltd
Original Assignee
Jiangsu Skyray Instrument Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Jiangsu Skyray Instrument Co Ltd filed Critical Jiangsu Skyray Instrument Co Ltd
Priority to CN201711112487.2A priority Critical patent/CN107809102A/en
Publication of CN107809102A publication Critical patent/CN107809102A/en
Pending legal-status Critical Current

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Classifications

    • HELECTRICITY
    • H02GENERATION; CONVERSION OR DISTRIBUTION OF ELECTRIC POWER
    • H02HEMERGENCY PROTECTIVE CIRCUIT ARRANGEMENTS
    • H02H3/00Emergency protective circuit arrangements for automatic disconnection directly responsive to an undesired change from normal electric working condition with or without subsequent reconnection ; integrated protection
    • H02H3/20Emergency protective circuit arrangements for automatic disconnection directly responsive to an undesired change from normal electric working condition with or without subsequent reconnection ; integrated protection responsive to excess voltage
    • H02H3/202Emergency protective circuit arrangements for automatic disconnection directly responsive to an undesired change from normal electric working condition with or without subsequent reconnection ; integrated protection responsive to excess voltage for dc systems

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  • Protection Of Static Devices (AREA)

Abstract

The invention discloses a kind of mass spectrometer detector high tension protection circuit, including:Control unit, HVDC source module, high pressure sets component, switch control assembly, and feedback component, the HVDC source module communications status is fed back to described control unit and is transferred to described control unit by the feedback component, carry out judging whether integrated circuit whether state is normal by described control unit, and and then control the switch control assembly to be powered to the HVDC source module, while the high pressure sets component that the HVDC source will be controlled to export predetermined high pressure value to be delivered to the HVDC source;The present invention is using the judgement to circuit working state; and detector is powered by controlling switch circuit and power operation; ensure that detector has voltage in the course of the work; avoid unrelated loss for a long time; meanwhile using setting highest to protect voltage, detector is avoided to carry too high voltages; detector is further protected, lifts service life.

Description

A kind of mass spectrometer detector high tension protection circuit
Technical field
The invention belongs to mass spectrometry art, more particularly to a kind of mass spectrometer detector high tension protection circuit therein.
Background technology
Mass spectrograph is mainly made up of sampling system, ion gun, electro-ionic osmosis and ion transmission, mass analyzer, detector, It is aided with electricity system simultaneously and vacuum system ensures the normal operation of instrument.In inductivity coupled plasma mass spectrometry analytical instrument In, the species and content of element micro in sample are detected, sample enters after sampling system imports is in Gao Zhen The ionizing system of dummy status is ionized, and conventional ionization method is electron ionization i.e. electron bombardment method.It is profit Thermoelectron interacts with the organic molecule in gas phase caused by filament heating, molecule is lost valence electron, ionization turns into Positively charged molecular ion.If the interior energy of molecular ion is larger, it is possible to chemical bond rupture occurs, generation m/Z is less Fragment ion.These ions and fragment enter mass analyzer under the guiding of electromagnetic field, using ion in magnetic field or electric field Kinetic property, the ion of different mass-to-charge ratioes can be separated, then measure the intensity of ion stream respectively by detector, obtained specific Mass spectrogram, and molecular structure is different, and mass spectrogram is also different, and qualitative and structural analysis can be carried out according to the position at peak, and peak Intensity be directly proportional with number of ions, obtain the quantitative information of sample according to this.
After mass analyzer filters out the ion signal of needs, these ions enter detector, the band in detector at a high speed The signal ion of positive charge is converted to electron stream, and the pulse signal exported after testing after device amplification is put by detector signal acquisition Big circuit receives amplification, and is converted into the square-wave pulse signal easily detected by MCU, and a pulse is exactly a count value, meter The size of number numerical value and the charged ion quantity that mass analyzer exports are proportional, have a charged ion theoretically just There is a count value, but due to the ion stream speed into detector quickly, detector has the limitation in dead time, institute in itself It is not many times one-to-one relationship with detected charged ion and count value, but multiple ion pairs answer a pulsimeter Count, after the count value that MCU module is needed, these data are transmitted to host computer, spectrogram is shown for host computer, and it is upper Machine carries out appropriate buckle back scape and set as needed.
In actually detected, there can be certain signal to noise ratio, it crosses the presentation that senior general directly affects signal collection of illustrative plates, Er Qiezhi Connect detector is applied with kilovolt high pressure will acceleration detection device loss, the maximum voltage more than detector will to detect Device is directly scrapped, it is therefore desirable to finds a kind of technical scheme or method that can solve the problem that above mentioned problem.
The content of the invention
In view of this, it is necessary to overcome at least one in drawbacks described above of the prior art.The invention provides a germplasm Spectrometer detector high tension protection circuit, including control unit, HVDC source module, for controlling the HVDC source to export Predetermined high pressure and the high pressure setting component being connected with described control unit, for controlling to HVDC source module power supply Control assembly is switched, and the HVDC source module communications status is fed back to the feedback component of described control unit, institute State feedback component the HVDC source module communications status is fed back into described control unit and be transferred to described control unit, by Described control unit carries out judging whether integrated circuit whether state is normal, and and then controls the switch control assembly to described HVDC source module is powered, while the high pressure sets component to control the HVDC source output predetermined high pressure value The HVDC source is delivered to, if described control unit judges that the integrated circuit is normal, inputs the electricity of the detector Press as normal value, if described control unit judges that the integrated circuit is abnormal or does not work, then input the detector Voltage is 0.
According in this patent background technology to that described in prior art, in actually detected, can there is certain signal to noise ratio, its Cross the presentation that senior general directly affects signal collection of illustrative plates, and directly detector is applied with kilovolt high pressure will acceleration detection device damage Consumption, the maximum voltage more than detector will cause detector directly to scrap;And mass spectrometer detector high pressure disclosed by the invention Protection circuit, using the judgement to circuit working state, and behaviour is powered and powered off to detector by controlling switch circuit Make, ensure that detector only there can be voltage in the course of the work, avoid prolonged unrelated loss, meanwhile, utilize setting Highest protects voltage, and detector can be avoided to carry too high voltage, further protects detector, lifts service life.
In addition, following additional technical feature is also had according to the rotational structure disclosed by the invention for more collimaters:
Further, the HVDC source module includes positive high voltage direct current source module and negative high voltage direct current source module;
The positive high voltage DC source module status:
The HVDC source is exported predetermined positive high voltage and is conveyed to the high pressure by described control unit sets component and further Be conveyed to the positive high voltage direct current source module be used for export positive supply binding post predeterminated voltage to the detector;Meanwhile institute Control unit is stated by sentencing to the working state signal transmitted by the positive high voltage DC source from the feedback component It is disconnected, if normally, controlling the switch control assembly to start and being powered to the positive high voltage DC source, if abnormal or do not work, Then power off;
The negative high voltage DC source module status:
The HVDC source is exported predetermined negative high-pressure delivery and sets component and further to the high pressure by described control unit Be conveyed to the negative high voltage direct current source module be used for export negative supply binding post predeterminated voltage to the detector;Meanwhile institute Control unit is stated by sentencing to the working state signal transmitted by the negative high voltage DC source from the feedback component It is disconnected, if normally, controlling the switch control assembly to start and being powered to the negative high voltage DC source, if abnormal or do not work, Then power off.
Further, the high pressure sets component to include high pressure and sets D/A conversion unit and the conditioning of high pressure setting signal Unit, the high pressure set D/A conversion unit to be coupled described control unit and will turned from goal-selling voltage value signal Change and be transmitted to the high pressure setting signal conditioning unit, it is conditioned after magnitude of voltage be conveyed to the HVDC source and exported Give detector voltage binding post;
Further, the switch control assembly includes being coupled the switch for being used to control solid-state relay of described control unit Circuit, and solid-state relay and the power supply part of the control solid-state relay by on-off circuit control.
Further, the feedback component includes being used to nurse one's health the feedback signal tune from the HVDC source signal Reason unit and the feedback signal is subjected to analog-to-digital conversion and is transmitted to described control unit and thus circuitry operating conditions are entered The feedback modulus converting unit that row judges.
Further, the protection circuit also includes host computer and between described control unit and the host computer The communication unit to be communicated.
Preferably, it is highest protection voltage that the host computer, which is provided with, and it is defeated that the highest protects the setting of voltage to allow The voltage entered onto detector is no more than this protection voltage, further ensure that the protection to detector.
The HVDC source being related in this case includes feedback pin (FB), sets pin(VREF), feeder ear(VIN), it is high Pressure side(HV), the feedback pin is connected with the feedback component, described to set pin to set component to be connected with the high pressure, institute State feeder ear to be connected with the switch control assembly, the high tension terminal of the high-pressure side and the detector is connected, if described HVDC source is positive high voltage DC source, then high-pressure side is positive high voltage end, is connected with the detector positive high voltage binding post, if institute It is negative high voltage DC source to state HVDC source, then high-pressure side is negative high-voltage end, is connected with the detector negative high voltage binding post.
The additional aspect of the present invention and advantage will be set forth in part in the description, and will partly become from the following description Obtain substantially, or recognized by the practice of the present invention.
Brief description of the drawings
The above-mentioned and/or additional aspect and advantage of the present invention will become from the following description of the accompanying drawings of embodiments Substantially and it is readily appreciated that, wherein:
Fig. 1 is the positive high voltage protection circuit theory diagram according to the present invention;
Fig. 2 is the negative high-voltage protection circuit theory diagram according to the present invention;
In Fig. 1,1 host computer, 2 high pressures set component, and 21 high pressures set D/A conversion unit, 22 high pressure setting signals conditioning list Member, 3 feedback components, 31 feedback modulus converting units, 32 feedback signal conditioning units, 4 communication units, 5 HVDC sources, 51 just HVDC source, 52 negative high voltage DC sources, 6 detector binding posts, 61 detector positive voltage binding posts, the crimping of 62 detector negative electricity Terminal, 7 switch control assemblies, 71 on-off circuits, 72 solid-state relays.
Embodiment
Embodiments of the invention are described below in detail, the example of the embodiment is shown in the drawings, wherein from beginning to end Same or similar label represents same or similar element or the element with same or like function.Below with reference to attached The embodiment of figure description is exemplary, is only used for explaining the present invention, and is not construed as limiting the claims.
In the description of the invention, it is to be understood that term " on ", " under ", " bottom ", " top ", "front", "rear", The orientation or position relationship of the instruction such as " interior ", " outer ", " horizontal stroke ", " perpendicular ", " inner side ", " outside " be based on orientation shown in the drawings or Position relationship, it is for only for ease of and describes the present invention and simplify description, rather than indicates or imply that signified device or element must There must be specific orientation, with specific azimuth configuration and operation, therefore be not considered as limiting the invention.
In the description of the invention, it is necessary to which explanation, unless otherwise clearly defined and limited, term " connection ", " connects It is logical ", " connected ", " connection ", " cooperation " should be interpreted broadly, for example, it may be fixedly connected, be integrally connected or It is detachably connected;It can be the connection of two element internals;Can be joined directly together, the indirect phase of intermediary can also be passed through Even;" cooperation " can be the cooperation in face and face or the cooperation in point and face or line and face, and the also cooperation including hole axle is right For one of ordinary skill in the art, the concrete meaning of above-mentioned term in the present invention can be understood with concrete condition.
The inventive concept of the present invention is as follows, using the judgement to circuit working state, and by controlling switch circuit to inspection Survey device is powered and power operation, ensures that detector only can have voltage in the course of the work, avoids prolonged nothing Loss is closed, meanwhile, using setting highest to protect voltage, detector can be avoided to carry too high voltage, further protect inspection Device is surveyed, lifts service life.
Below with reference to accompanying drawings come describe the present invention steel bonding piece alignment device, wherein Fig. 1 be according to the present invention just High voltage protection circuit theory diagram;Fig. 2 is the negative high-voltage protection circuit theory diagram according to the present invention.
According to an embodiment of the invention, as shown in Figure 1, 2, high tension protection circuit disclosed by the invention, including control unit, HVDC source module, the high pressure for controlling the HVDC source output predetermined high pressure and being connected with described control unit are set Component is put, for controlling the switch control assembly to HVDC source module power supply, and by HVDC source mould Block communications status feeds back to the feedback component of described control unit, and the feedback component communicates the HVDC source module shape State feeds back to described control unit and is transferred to described control unit, carries out whether judging whether integrated circuit by described control unit State is normal, and and then control the switch control assembly to be powered to the HVDC source module, while the high pressure Set component that the HVDC source output predetermined high pressure value will be controlled to be delivered to the HVDC source, if described control unit Judge that the integrated circuit is normal, then the voltage for inputting the detector is normal value, if described control unit judge it is described whole Body circuit is abnormal or does not work, then the voltage for inputting the detector is 0.
In addition, following additional technical feature is also had according to the rotational structure disclosed by the invention for more collimaters:
According to some embodiments of the present invention, the HVDC source module includes positive high voltage direct current source module and negative high voltage direct current Source module;
The positive high voltage DC source module status:
The HVDC source is exported predetermined positive high voltage and is conveyed to the high pressure by described control unit sets component and further Be conveyed to the positive high voltage direct current source module be used for export positive supply binding post predeterminated voltage to the detector;Meanwhile institute Control unit is stated by sentencing to the working state signal transmitted by the positive high voltage DC source from the feedback component It is disconnected, if normally, controlling the switch control assembly to start and being powered to the positive high voltage DC source, if abnormal or do not work, Then power off;
The negative high voltage DC source module status:
The HVDC source is exported predetermined negative high-pressure delivery and sets component and further to the high pressure by described control unit Be conveyed to the negative high voltage direct current source module be used for export negative supply binding post predeterminated voltage to the detector;Meanwhile institute Control unit is stated by sentencing to the working state signal transmitted by the negative high voltage DC source from the feedback component It is disconnected, if normally, controlling the switch control assembly to start and being powered to the negative high voltage DC source, if abnormal or do not work, Then power off.
According to one embodiment of present invention, the high pressure sets component to include high pressure and sets D/A conversion unit and high pressure Setting signal conditioning unit, the high pressure set D/A conversion unit to be coupled described control unit and will come from goal-selling voltage Value signal is changed and is transmitted to the high pressure setting signal conditioning unit, it is conditioned after magnitude of voltage be conveyed to the high straightening Stream source, which is exported, gives detector voltage binding post, and default high-voltage value is transported to institute by the high pressure setting signal conditioning unit State the setting pin in HVDC source;
According to one embodiment of present invention, it is described to switch control assembly including connection described control unit for controlling solid-state The on-off circuit of relay, and by the solid-state relay that the on-off circuit controls and control powering for the solid-state relay Part.
According to one embodiment of present invention, the feedback component includes being used to nurse one's health coming from the HVDC source signal Feedback signal conditioning unit and by the feedback signal carry out analog-to-digital conversion and be transmitted to described control unit and thus to electricity The feedback modulus converting unit that road working condition is judged.
According to some embodiments of the present invention, the protection circuit also include host computer and for described control unit with The communication unit to be communicated between the host computer.
Preferably, it is highest protection voltage that the host computer, which is provided with, and it is defeated that the highest protects the setting of voltage to allow The voltage entered onto detector is no more than this protection voltage, further ensure that the protection to detector.
The HVDC source being related in this case includes feedback pin (FB), sets pin(VREF), feeder ear(VIN), it is high Pressure side(HV), the feedback pin is connected with the feedback component, described to set pin to set component to be connected with the high pressure, institute State feeder ear to be connected with the switch control assembly, the high tension terminal of the high-pressure side and the detector is connected, if described HVDC source is positive high voltage DC source, then high-pressure side is positive high voltage end, is connected with the detector positive high voltage binding post, if institute It is negative high voltage DC source to state HVDC source, then high-pressure side is negative high-voltage end, is connected with the detector negative high voltage binding post.
It is any to refer to that " one embodiment ", " embodiment ", " illustrative examples " etc. mean to combine embodiment description Specific component, structure or feature are contained at least one embodiment of the present invention.This specification everywhere this is schematic Statement is not necessarily referring to identical embodiment.Specific component, structure or feature are described with reference to any embodiment moreover, working as When, advocated, component, structure or feature with reference to as being realized other embodiments all fall within those skilled in the art Within the scope of.
Although detailed retouch is carried out to the embodiment of the present invention with reference to multiple illustrative examples of the present invention State, it must be understood that those skilled in the art can be designed that various other improvement and embodiment, these improve and implemented Example will fall within spirit and scope.Specifically, in the scope of foregoing disclosure, accompanying drawing and claim Within, rational variations and modifications can be made in terms of the arrangement that parts and/or sub-combination are laid out, without departing from The spirit of the present invention.Except the variations and modifications in terms of parts and/or layout, its scope is by appended claims and its is equal Thing limits.

Claims (7)

1. a kind of mass spectrometer detector high tension protection circuit, it is characterised in that including control unit, HVDC source module, use Component is set in the high pressure for controlling the HVDC source output predetermined high pressure and being connected with described control unit, given for controlling The switch control assembly of the HVDC source module power supply, and the HVDC source module communications status is fed back into institute The feedback component of control unit is stated, the HVDC source module communications status is fed back to the control list by the feedback component Member is transferred to described control unit, carries out judging whether integrated circuit whether state is normal by described control unit, and and then controls Make the switch control assembly to be powered to the HVDC source module, while the high pressure sets component by described in control HVDC source output predetermined high pressure value is delivered to the HVDC source, if described control unit is judging the integrated circuit just Often, then the voltage for inputting the detector is normal value, if described control unit judges that the integrated circuit is abnormal or not work Make, then the voltage for inputting the detector is 0.
2. mass spectrometer detector high tension protection circuit according to claim 1, it is characterised in that HVDC source mould Block includes positive high voltage direct current source module and negative high voltage direct current source module;
The positive high voltage DC source module status:
The HVDC source is exported predetermined positive high voltage and is conveyed to the high pressure by described control unit sets component and further Be conveyed to the positive high voltage direct current source module be used for export positive supply binding post predeterminated voltage to the detector;Meanwhile institute Control unit is stated by sentencing to the working state signal transmitted by the positive high voltage DC source from the feedback component It is disconnected, if normally, controlling the switch control assembly to start and being powered to the positive high voltage DC source, if abnormal or do not work, Then power off;
The negative high voltage DC source module status:
The HVDC source is exported predetermined negative high-pressure delivery and sets component and further to the high pressure by described control unit Be conveyed to the negative high voltage direct current source module be used for export negative supply binding post predeterminated voltage to the detector;Meanwhile institute Control unit is stated by sentencing to the working state signal transmitted by the negative high voltage DC source from the feedback component It is disconnected, if normally, controlling the switch control assembly to start and being powered to the negative high voltage DC source, if abnormal or do not work, Then power off.
3. according to the described mass spectrometer detector high tension protection circuit of any one of claim 1 or 2, it is characterised in that described High pressure sets component to include high pressure and sets D/A conversion unit and high pressure setting signal conditioning unit, and the high pressure sets digital-to-analogue to turn Unit is changed to be coupled described control unit and will be changed from goal-selling voltage value signal and be transmitted to the high pressure setting letter Number conditioning unit, it is conditioned after magnitude of voltage be conveyed to the HVDC source and exported and give detector voltage binding post.
4. according to the described mass spectrometer detector high tension protection circuit of any one of claim 1 or 2, it is characterised in that described Switch control assembly includes being coupled the on-off circuit for being used to control solid-state relay of described control unit, and by the switch electricity The solid-state relay of road control and the power supply part of the control solid-state relay.
5. according to the described mass spectrometer detector high tension protection circuit of any one of claim 1 or 2, it is characterised in that described Feedback component includes being used for nursing one's health feedback signal conditioning unit from the HVDC source signal and by the feedback signal Feedback modulus conversion that is carrying out analog-to-digital conversion and be transmitted to described control unit and thus being judged circuitry operating conditions is single Member.
6. mass spectrometer detector high tension protection circuit according to claim 1, it is characterised in that the protection circuit is also wrapped Include host computer and the communication unit for being communicated between described control unit and the host computer.
7. mass spectrometer detector high tension protection circuit according to claim 6, it is characterised in that the host computer is provided with It is highest protection voltage.
CN201711112487.2A 2017-11-13 2017-11-13 A kind of mass spectrometer detector high tension protection circuit Pending CN107809102A (en)

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CN201711112487.2A CN107809102A (en) 2017-11-13 2017-11-13 A kind of mass spectrometer detector high tension protection circuit

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116316406A (en) * 2022-09-08 2023-06-23 瑞莱谱(杭州)医疗科技有限公司 Mass spectrometer detection protection circuit

Citations (5)

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Publication number Priority date Publication date Assignee Title
JPH05258714A (en) * 1992-03-16 1993-10-08 Hitachi Ltd Plasma mass analyzing device
CN103199714A (en) * 2013-04-17 2013-07-10 普瑞麦迪(北京)实验室技术有限公司 Power source device of electrophoresis system
US20130319862A1 (en) * 2012-06-04 2013-12-05 Beckman Coulter, Inc. Leakage current sense circuit for error detection in an improved capillary electrophoresis-electrospray ionization- mass spectrometry system
WO2016162658A1 (en) * 2015-04-09 2016-10-13 Kratos Analytical Limited Time of flight mass spectrometer
CN207801455U (en) * 2017-11-13 2018-08-31 江苏天瑞仪器股份有限公司 A kind of mass spectrometer detector high tension protection circuit

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH05258714A (en) * 1992-03-16 1993-10-08 Hitachi Ltd Plasma mass analyzing device
US20130319862A1 (en) * 2012-06-04 2013-12-05 Beckman Coulter, Inc. Leakage current sense circuit for error detection in an improved capillary electrophoresis-electrospray ionization- mass spectrometry system
CN103199714A (en) * 2013-04-17 2013-07-10 普瑞麦迪(北京)实验室技术有限公司 Power source device of electrophoresis system
WO2016162658A1 (en) * 2015-04-09 2016-10-13 Kratos Analytical Limited Time of flight mass spectrometer
CN207801455U (en) * 2017-11-13 2018-08-31 江苏天瑞仪器股份有限公司 A kind of mass spectrometer detector high tension protection circuit

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116316406A (en) * 2022-09-08 2023-06-23 瑞莱谱(杭州)医疗科技有限公司 Mass spectrometer detection protection circuit
CN116316406B (en) * 2022-09-08 2023-11-07 瑞莱谱(杭州)医疗科技有限公司 Mass spectrometer detection protection circuit

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