CN107794108A - A kind of round wires concentric gallows empty conductor conduction anti-corrosion grease and preparation method thereof - Google Patents

A kind of round wires concentric gallows empty conductor conduction anti-corrosion grease and preparation method thereof Download PDF

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Publication number
CN107794108A
CN107794108A CN201711137152.6A CN201711137152A CN107794108A CN 107794108 A CN107794108 A CN 107794108A CN 201711137152 A CN201711137152 A CN 201711137152A CN 107794108 A CN107794108 A CN 107794108A
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parts
corrosion
base oil
round wires
kettle
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乔传威
郑金周
贾书伟
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Zhengzhou Optris Technology Co Ltd
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Zhengzhou Optris Technology Co Ltd
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    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
    • C10M169/04—Mixtures of base-materials and additives
    • C10M169/044—Mixtures of base-materials and additives the additives being a mixture of non-macromolecular and macromolecular compounds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/04—Elements
    • C10M2201/041—Carbon; Graphite; Carbon black
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/06—Metal compounds
    • C10M2201/062—Oxides; Hydroxides; Carbonates or bicarbonates
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/08—Inorganic acids or salts thereof
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    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/08—Inorganic acids or salts thereof
    • C10M2201/082—Inorganic acids or salts thereof containing nitrogen
    • C10M2201/083—Inorganic acids or salts thereof containing nitrogen nitrites
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    • C10M2203/00—Organic non-macromolecular hydrocarbon compounds and hydrocarbon fractions as ingredients in lubricant compositions
    • C10M2203/10—Petroleum or coal fractions, e.g. tars, solvents, bitumen
    • C10M2203/1006—Petroleum or coal fractions, e.g. tars, solvents, bitumen used as base material
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    • C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/02—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers
    • C10M2205/022—Ethene
    • C—CHEMISTRY; METALLURGY
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    • C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/02—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers
    • C10M2205/024—Propene
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    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/02—Hydroxy compounds
    • C10M2207/023—Hydroxy compounds having hydroxy groups bound to carbon atoms of six-membered aromatic rings
    • C10M2207/025—Hydroxy compounds having hydroxy groups bound to carbon atoms of six-membered aromatic rings with condensed rings
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    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/02—Hydroxy compounds
    • C10M2207/023—Hydroxy compounds having hydroxy groups bound to carbon atoms of six-membered aromatic rings
    • C10M2207/026—Hydroxy compounds having hydroxy groups bound to carbon atoms of six-membered aromatic rings with tertiary alkyl groups
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    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/10—Carboxylix acids; Neutral salts thereof
    • C10M2207/12—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms
    • C10M2207/125—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids
    • C10M2207/127—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids polycarboxylic
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    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
    • C10M2215/06—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to carbon atoms of six-membered aromatic rings
    • C10M2215/064—Di- and triaryl amines
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    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/086—Imides
    • C—CHEMISTRY; METALLURGY
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    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/22—Heterocyclic nitrogen compounds
    • C10M2215/223—Five-membered rings containing nitrogen and carbon only
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
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    • C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
    • C10M2219/04—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions containing sulfur-to-oxygen bonds, i.e. sulfones, sulfoxides
    • C10M2219/044—Sulfonic acids, Derivatives thereof, e.g. neutral salts
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
    • C10M2223/02—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
    • C10M2223/04—Phosphate esters
    • C10M2223/045—Metal containing thio derivatives
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
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    • C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
    • C10M2223/02—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
    • C10M2223/04—Phosphate esters
    • C10M2223/047—Thioderivatives not containing metallic elements
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/06—Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/12—Inhibition of corrosion, e.g. anti-rust agents or anti-corrosives
    • C—CHEMISTRY; METALLURGY
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    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/14—Electric or magnetic purposes
    • C10N2040/16—Dielectric; Insulating oil or insulators
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
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    • C10N2050/00—Form in which the lubricant is applied to the material being lubricated
    • C10N2050/10—Semi-solids; greasy

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Lubricants (AREA)

Abstract

The invention discloses a kind of round wires concentric gallows empty conductor conduction anti-corrosion grease, including：58 parts of carbon black；15 20 parts of acid imide thickening agent；16 22 parts of sodium hydroxide；10 11 parts of deionized water；57 parts of viscosity index improver；Nanometer particle-modified 68 parts of polyacrylic resin；45 parts of antirust agent；57 parts of graphite powder；0.5 5 parts of antioxidant；13 parts of anti-corrosion corrosion inhibitor；105 120 parts of base oil；A kind of its preparation method of round wires concentric gallows empty conductor conduction anti-corrosion grease, comprises the following steps：（1）The half of base oil is mixed in saponification kettle with acid imide thickening agent, heats, dissolve；（2）Prepare sodium hydrate aqueous solution；（3）Second half base oil is added, and is cooled, sodium hydrate aqueous solution is added, stirs and heat up, saponification, dehydration, be transferred to mediation kettle；（4）Additive is added in proportion, is crossed homogeneous, is deaerated, goes out kettle.The present invention can greatly improve the conductance of anti-corrosion grease, reduce waste heat and produce, solve the problems, such as that current aerial condutor anti-corrosion grease condensate oil is serious.

Description

A kind of round wires concentric gallows empty conductor conduction anti-corrosion grease and preparation method thereof
Technical field
The present invention relates to technical field of lubricating oil, and in particular to be a kind of round wires concentric gallows empty conductor conduction anti-corrosion grease And preparation method thereof.
Background technology
At present, round wires concentric gallows empty conductor anti-corrosion grease is formula and the side of soap base thickening agent thickening mineral base oil mostly What method was produced, the product prepared by this method, conductive capability is general, and resistivity is larger, in the process of conveying electric energy for a long time In, it is easy to because electric current is excessive and it is very high to rise to temperature, produce waste heat, in this case, according to current technology The anti-corrosion grease condensate oil problem of preparation is serious, and its result can cause protective effect of the anti-corrosion grease to wire drastically to decline, and then influences The whole service life of wire.The present invention has aiming at the fully optimized that such a key technology difficulty is carried out at present, raising Imitate protectiveness.
The content of the invention
It is conductive the invention provides a kind of round wires concentric gallows empty conductor in order to solve the problems of in the prior art Anti-corrosion grease and preparation method thereof.
To achieve the above object, the technical solution used in the present invention is：
A kind of round wires concentric gallows empty conductor conduction anti-corrosion grease, includes following material by weight：Carbon black 5-8 parts；Acyl Imines thickening agent 15-20 parts；Sodium hydroxide 16-22 parts；Deionized water 10-11 parts；Viscosity index improver 5-7 parts；Nanoparticle Sub- modified polypropene acid resin 6-8 parts；Antirust agent 4-5 parts；Graphite powder 5-7 parts；Antioxidant 0.5-5 parts；Anti-corrosion corrosion inhibitor 1-3 Part；Base oil 105-120 parts；The viscosity index improver is non-dispersive type ethylene propylene copolymer；The antirust agent is ten Dialkylene succinic acid（T746）, barium mahogany sulfonate（T701）Both mixtures；The antioxidant be diphenylamines, betanaphthol, 2, One kind or any two kinds of mixture in 6- BHTs；The anti-corrosion corrosion inhibitor is dithiophosphates, Asia Any two or three of mixture in the double octyl group basic zinc salts of sodium nitrate, sulphur phosphorus, molybdate, BTA.
Preferably, the base oil is 650SN, and the characteristic of base oil meets：100 DEG C of kinematic viscosity requirements are in 11- 13mm2/s。
A kind of preparation method of round wires concentric gallows empty conductor conduction anti-corrosion grease, comprises the following steps：
（1）The half of required base oil is squeezed into saponification kettle, and is proportionally added into acid imide thickening agent, is then mixed and heated to 130-140℃；
（2）Sodium hydroxide is mixed with deionized water in proportion, sodium hydrate aqueous solution is made；
（3）After waiting acid imide thickening agent to be all dissolved in base oil, second half remaining base oil is added, and is cooled to 95-100 DEG C, then by step（2）Sodium hydrate aqueous solution be slowly added to, stir and heat up, saponification, dehydration, temperature rise to 135-145 DEG C, it is transferred in mediation kettle and carries out circulation shear；
（4）Then be proportionally added into successively carbon black, viscosity index improver, nanometer particle-modified polyacrylic resin, antirust agent, Graphite powder, antioxidant, anti-corrosion corrosion inhibitor, cone penetration is adjusted, after qualified, cross homogeneous, degassing, you can go out kettle.
Beneficial effects of the present invention
The invention provides a kind of round wires concentric gallows empty conductor conduction anti-corrosion grease and preparation method thereof, can significantly improve anti- The conductance of rotten fat, electric conductivity is splendid, reduces waste heat and produces, it is serious to solve current aerial condutor anti-corrosion grease condensate oil, reaches To effective protection to aerial condutor, extend protective period limit.
Embodiment
Technical scheme will be clearly and completely described by specific embodiment below, it is clear that retouched The embodiment stated is only the part of the embodiment of the present invention, rather than whole embodiments.
Embodiment 1
A kind of round wires concentric gallows empty conductor conduction anti-corrosion grease, includes following material by weight：5 parts of carbon black；Acyl is sub- 15 parts of amine thickening agent；16 parts of sodium hydroxide；10 parts of deionized water；5 parts of viscosity index improver；Nanometer particle-modified polyacrylic acid 6 parts of resin；4 parts of antirust agent；5 parts of graphite powder；0.5 part of antioxidant；1 part of anti-corrosion corrosion inhibitor；105 parts of base oil；The viscosity Index improver is non-dispersive type ethylene propylene copolymer；The antirust agent is dodecenylsuccinic acid（T746）, mahogany acid Barium（T701）Both mixtures；The antioxidant is DBPC 2,6 ditertiary butyl p cresol；The anti-corrosion corrosion inhibitor is nitrous acid Sodium, molybdate, the mixture of BTA three.
Wherein, the base oil is 650SN, and the characteristic of base oil meets：100 DEG C of kinematic viscosity requirements are in 11mm2/s。
A kind of preparation method of round wires concentric gallows empty conductor conduction anti-corrosion grease, comprises the following steps：
（1）50 parts of base oil is squeezed into saponification kettle, and adds 15 parts of acid imide thickening agent, is then mixed and heated to 130 ℃；
（2）16 parts of sodium hydroxide and the mixing of 10 parts of deionized water is taken, sodium hydrate aqueous solution is made；
（3）After waiting acid imide thickening agent to be all dissolved in base oil, remaining 55 parts of base oil is added, and be cooled to 95 DEG C, then by step（2）Sodium hydrate aqueous solution be slowly added to, stir and heat up, saponification, dehydration, temperature rise to 135 DEG C, It is transferred in mediation kettle and carries out circulation shear；
（4）Then sequentially add 5 parts of carbon black, 5 parts of viscosity index improver, 6 parts of nanometer particle-modified polyacrylic acid tree Fat, 4 parts of antirust agent, 5 parts of graphite powder, 0.5 part of antioxidant, 1 part of anti-corrosion corrosion inhibitor, cone penetration is adjusted, after qualified, Cross homogeneous, degassing, you can go out kettle.
Embodiment 2
A kind of round wires concentric gallows empty conductor conduction anti-corrosion grease, includes following material by weight：7 parts of carbon black；Acyl is sub- 18 parts of amine thickening agent；19 parts of sodium hydroxide；10.5 parts of deionized water；6 parts of viscosity index improver；Nanometer particle-modified polypropylene 7 parts of acid resin；4.5 parts of antirust agent；6 parts of graphite powder；3 parts of antioxidant；2 parts of anti-corrosion corrosion inhibitor；113 parts of base oil；It is described viscous Degree index improver is non-dispersive type ethylene propylene copolymer；The antirust agent is dodecenylsuccinic acid（T746）, oil sulphur Sour barium（T701）Both mixtures；The antioxidant is the mixture of both diphenylamines, betanaphthol；The anti-corrosion corrosion inhibitor For dithiophosphates, natrium nitrosum, the double octyl group basic zinc salt threes of sulphur phosphorus mixture.
Wherein, the base oil is 650SN, and the characteristic of base oil meets：100 DEG C of kinematic viscosity requirements are in 12mm2/s。
A kind of preparation method of round wires concentric gallows empty conductor conduction anti-corrosion grease, comprises the following steps：
（1）57 parts of base oil is squeezed into saponification kettle, and adds 18 parts of acid imide thickening agents, is then mixed and heated to 135 DEG C；
（2）19 parts of sodium hydroxide and the mixing of 10.5 parts of deionized water is taken, sodium hydrate aqueous solution is made；
（3）After waiting acid imide thickening agent to be all dissolved in base oil, remaining 56 parts of base oil is added, and be cooled to 98 DEG C, then by step（2）Sodium hydrate aqueous solution be slowly added to, stir and heat up, saponification, dehydration, temperature rise to 138 DEG C, It is transferred in mediation kettle and carries out circulation shear；
（4）Then sequentially add 7 parts of carbon black, 6 parts of viscosity index improver, 7 parts of nanometer particle-modified polyacrylic acid tree Fat, 4.5 parts of antirust agent, 6 parts of graphite powder, 3 parts of antioxidant, 2 parts of anti-corrosion corrosion inhibitor, cone penetration is adjusted, after qualified, Cross homogeneous, degassing, you can go out kettle.
Embodiment 3
A kind of round wires concentric gallows empty conductor conduction anti-corrosion grease, includes following material by weight：8 parts of carbon black；Acyl is sub- 20 parts of amine thickening agent；22 parts of sodium hydroxide；11 parts of deionized water；7 parts of viscosity index improver；Nanometer particle-modified polyacrylic acid 8 parts of resin；5 parts of antirust agent；7 parts of graphite powder；5 parts of antioxidant；3 parts of anti-corrosion corrosion inhibitor；120 parts of base oil；The viscosity refers to Number modifier is non-dispersive type ethylene propylene copolymer；The antirust agent is dodecenylsuccinic acid（T746）, barium mahogany sulfonate （T701）Both mixtures；The antioxidant is diphenylamines；The anti-corrosion corrosion inhibitor is natrium nitrosum, the double octyl group alkali of sulphur phosphorus Property zinc salt, the mixture of BTA three.
Preferably, the base oil is 650SN, and the characteristic of base oil meets：100 DEG C of kinematic viscosity requirements are in 13mm2/s。
A kind of preparation method of round wires concentric gallows empty conductor conduction anti-corrosion grease, comprises the following steps：
（1）60 parts of base oil is squeezed into saponification kettle, and adds 20 parts of acid imide thickening agent, is then mixed and heated to 140 ℃；
（2）22 parts of sodium hydroxide and the mixing of 11 parts of deionized water is taken, sodium hydrate aqueous solution is made；
（3）After waiting acid imide thickening agent to be all dissolved in base oil, remaining 60 parts of base oil is added, and is cooled to 100 DEG C, then by step（2）Sodium hydrate aqueous solution be slowly added to, stir and heat up, saponification, dehydration, temperature rise to 145 DEG C, it is transferred in mediation kettle and carries out circulation shear；
（4）Then sequentially add 8 parts of carbon black, 7 parts of viscosity index improver, 8 parts of nanometer particle-modified polyacrylic acid tree Fat, 5 parts of antirust agent, 7 parts of graphite powder, 5 parts of antioxidant, 3 parts of anti-corrosion corrosion inhibitor, adjust cone penetration, after qualified, mistake Homogeneous, degassing, you can go out kettle.
Although the present invention disclosed as above with preferred embodiment, they be not for limiting the present invention, it is any to be familiar with This those skilled in the art, the various change made without departing from the spirit and scope of the invention or retouching, all should still belong to the present invention Patent covering scope within.

Claims (3)

  1. A kind of 1. round wires concentric gallows empty conductor conduction anti-corrosion grease, it is characterised in that：Include following material by weight： Carbon black 5-8 parts；Acid imide thickening agent 15-20 parts；Sodium hydroxide 16-22 parts；Deionized water 10-11 parts；Viscosity index improver 5-7 parts；Nanometer particle-modified polyacrylic resin 6-8 parts；Antirust agent 4-5 parts；Graphite powder 5-7 parts；Antioxidant 0.5-5 parts；It is anti- Corrosion inhibitor 1-3 parts；Base oil 105-120 parts；The viscosity index improver is non-dispersive type ethylene propylene copolymer；Institute It is dodecenylsuccinic acid to state antirust agent（T746）, barium mahogany sulfonate（T701）Both mixtures；The antioxidant is hexichol One kind or any two kinds of mixture in amine, betanaphthol, DBPC 2,6 ditertiary butyl p cresol；The anti-corrosion corrosion inhibitor is two sulphur For any two or three of mixing in phosphate, natrium nitrosum, the double octyl group basic zinc salts of sulphur phosphorus, molybdate, BTA Thing.
  2. A kind of 2. round wires concentric gallows empty conductor conduction anti-corrosion grease according to claim 1, it is characterised in that：The basis Oil is 650SN, and the characteristic of base oil meets：100 DEG C of kinematic viscosity requirements are in 11-13mm2s。
  3. A kind of 3. preparation method of round wires concentric gallows empty conductor conduction anti-corrosion grease, it is characterised in that：Comprise the following steps：
    The half of required base oil is squeezed into saponification kettle, and is proportionally added into acid imide thickening agent, is then mixed and heated to 130-140℃；
    Sodium hydroxide is mixed with deionized water in proportion, sodium hydrate aqueous solution is made；
    After waiting acid imide thickening agent to be all dissolved in base oil, second half remaining base oil is added, and be cooled to 95- 100 DEG C, then by step（2）Sodium hydrate aqueous solution be slowly added to, stir and heat up, saponification, dehydration, temperature rise to 135- 145 DEG C, it is transferred in mediation kettle and carries out circulation shear；
    Then carbon black, viscosity index improver, nanometer particle-modified polyacrylic resin, antirust agent, stone are proportionally added into successively Ink powder, antioxidant, anti-corrosion corrosion inhibitor, cone penetration is adjusted, after qualified, cross homogeneous, degassing, you can go out kettle.
CN201711137152.6A 2017-11-16 2017-11-16 A kind of round wires concentric gallows empty conductor conduction anti-corrosion grease and preparation method thereof Pending CN107794108A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110527581A (en) * 2019-09-23 2019-12-03 上海鸿辉光通科技股份有限公司 A kind of aerial condutor high-temperature anticorrosion rouge and preparation method thereof

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104804809A (en) * 2015-04-28 2015-07-29 天津市金海利油脂有限公司 Lubricating grease for protecting aluminum-conductor steel-reinforced cables and preparation method of lubricating grease
CN105273799A (en) * 2015-12-02 2016-01-27 国家电网公司 Electric force compounded grease and preparation method thereof
CN107057812A (en) * 2017-04-22 2017-08-18 郑州市欧普士科技有限公司 A kind of steel strand wires special anti-corrosion fat and preparation method thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104804809A (en) * 2015-04-28 2015-07-29 天津市金海利油脂有限公司 Lubricating grease for protecting aluminum-conductor steel-reinforced cables and preparation method of lubricating grease
CN105273799A (en) * 2015-12-02 2016-01-27 国家电网公司 Electric force compounded grease and preparation method thereof
CN107057812A (en) * 2017-04-22 2017-08-18 郑州市欧普士科技有限公司 A kind of steel strand wires special anti-corrosion fat and preparation method thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110527581A (en) * 2019-09-23 2019-12-03 上海鸿辉光通科技股份有限公司 A kind of aerial condutor high-temperature anticorrosion rouge and preparation method thereof
CN110527581B (en) * 2019-09-23 2021-09-14 上海鸿辉光通科技股份有限公司 High-temperature anti-corrosion grease for overhead conductor and preparation method thereof

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