CN107793917A - A kind of water-based UV varnish of Diamond Search and preparation method and application - Google Patents
A kind of water-based UV varnish of Diamond Search and preparation method and application Download PDFInfo
- Publication number
- CN107793917A CN107793917A CN201711022016.2A CN201711022016A CN107793917A CN 107793917 A CN107793917 A CN 107793917A CN 201711022016 A CN201711022016 A CN 201711022016A CN 107793917 A CN107793917 A CN 107793917A
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- China
- Prior art keywords
- water
- varnish
- parts
- thickener
- defoamer
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
- C09D175/04—Polyurethanes
- C09D175/14—Polyurethanes having carbon-to-carbon unsaturated bonds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
Abstract
The present invention relates to a kind of water-based UV varnish of Diamond Search, it is characterised in that by weight, including following component：70~90 parts of polyurethane acroleic acid dispersion, 1.4~3.7 parts of coalescents, 1.5~2.5 parts of light trigger, 10~20 parts of water.The water-based UV varnish easy construction of Diamond Search of the present invention, operation is very simple, and coating equipment cleaning is very convenient, it is only necessary to common clear water.And finish paint has fabulous gloss, adhesive force and mechanical and physical performance, chemical resistance on furniture to be decorated, has fabulous decoration and protective effect to wood furniture.
Description
Technical field
The invention belongs to technical field of coatings, and in particular to a kind of water-based UV of Diamond Search (ultraviolet light) cured varnish and its system
Preparation Method and application.
Background technology
UV is coating material solidified in publicity, and it is mainly characterized in that without solvent, clean and effective, 100% film-forming, paint film
Energy is excellent, can effectively reduce organic volatile (VOC) discharge etc., therefore extremely wide application has been obtained in recent decades；But
It is actually traditional UV coating material solidified not entirely without noxious pollutant and Diamond Search.It is coating material solidified mainly due to traditional UV
Use the prepolymer of low molecule amount, viscosity is higher, it is necessary to add and adjusted containing a large amount of small molecule response type reactive diluents
System viscosity and rheological characteristic, improve the performance of cured film., can be right and these reactive diluents largely have toxicity and excitant
Environment and health cause necessarily to damage.
The content of the invention
Based on above-mentioned background technology, the present invention provides a kind of water-based UV varnish of Diamond Search.The water-based UV varnish using water as point
Dispersion media, its coalescents and auxiliary material are water-based synthesis or Over emulsfication, can be compatible with water.The water-based UV varnish is free of
Reactive diluent (monomer), only makees diluent with water, few to add or be not added with coalescents, therefore the structure of oligomer just determines painting
The final performance of film.
The water-based UV varnish, by weight, including following components：70~90 parts of polyurethane acroleic acid dispersion, into
1.4~3.7 parts of film auxiliary agent, 1.5~2.5 parts of light trigger, and/or, the water-based UV varnish, and 10~20 parts of water.
Wherein, the solid content of the polyurethane acroleic acid dispersant is 40%~42%, and viscosity is 10~200mpa.s；
The pH value of the polyurethane acroleic acid dispersion is 7.0~9.0.
The polyurethane acroleic acid dispersant can use conventional reagent, it is preferred that the polyurethane acroleic acid dispersant is
Watersoluble polyurethane acrylic acid dispersant.
Polyurethane acroleic acid dispersant of the present invention is preferably from ten thousand magnificent 4681 water-based ultraviolet (UV) curable polyurethane acroleic acids
Dispersion, ten thousand China 4617, DSM R-452 in it is one or two kinds of.
The watersoluble polyurethane acrylic acid dispersion overall performance is preferable, has preferable hardness, pliability, feel, anti-
Impact and tensile strength, and extraordinary physical property and chemical resistance etc. can be provided.
Present invention further propose that, the water-based system compatibility of the light trigger is good；The light trigger is preferred
Using one or two kinds of in TPO photoinitiator or 1173 light triggers.
Wherein, TPO photoinitiator is specially 2,4,6 one trimethylbenzoyl phosphinic acid ethyl esters or 1173 light triggers.
2,4,6 one trimethylbenzoyl phosphinic acid ethyl esters, there is very wide ultra-violet absorption spectrum, should in varnish and colored paint
With good, there is certain color inhibition effect.
1173 light triggers are specially 2- hydroxy-2-methyl -1- phenyl -1- acetone；It is low with smell, anti-yellowing property
Well, the characteristics of efficient.
Present invention further propose that, the coalescents are specially：0.4~1.2 part of defoamer, wetting agent 0.3~0.6
Part, 0.2~0.4 part of levelling agent, 0.2~1.5 part of thickener, 0~2 part of cosolvent.The addition of the coalescents can enter one
Step improves the filming performance and paint film self performance of paint film.
The defoamer is selected from organosiloxane class defoamer, the hydrophobic solid without organosilicon and brokenly bubble polymer
Mix one kind in species defoamer；Present invention preferably employs the BYK024 of German BYK companies, German Di Gao companies
TEGO810 type products.
The wetting agent is organosilicon moistening flatting agent；The wetting agent has a variety of work(such as reduction surface tension, wetting
Can, dynamic moisture ability of the system to various base materials can be improved, reduces surface tension strongly；Present invention preferably employs Bi Ke chemistry
BYK349 type products.
The levelling agent is polysiloxane-based levelling agent；The levelling agent can effectively reduce body surface tension force, promote stream
It is flat, while there is improvement transparency, slipping, anti-shrinkage cavity effect.Present invention preferably employs the high company's T EGO450 models of German enlightening
Product.
The one kind of the thickener in polyethers thickener, polyether-modified polyurethanes thickener；Polyethers of the present invention
Class thickener is preferably using the modest R299 type products of the RM-2050D type products or Shanghai moral of ROHM AND HAAS.The cosolvent
For TPNB.
The present invention especially with the addition of cosolvent and two kinds of defoamers, have its described water-based UV varnish preferably penetrating
Property and gloss.As the preferred scheme of the present invention, the water-based UV varnish, by weight, including following component：70~90 parts
Watersoluble polyurethane acrylic acid dispersion, 0.5~1.1 part of defoamer, 0.4~0.6 part of wetting agent, 0.2~0.4 part of levelling agent, 0.3
~1.5 parts of thickeners, 0~1.5 part of cosolvent, 1.5~2.5 parts of light trigger, 10~20 parts of water.
It is further proposed that preferred scheme, described water-based UV varnish, by weight, including following component：70~90 parts
Watersoluble polyurethane acrylic acid dispersion, 0.5~0.7 part of defoamer BYK024,0.3~0.5 part of defoamer TEGO810,0.3~
0.6 part of wetting agent, 0.2~0.4 part of levelling agent, 0.3~0.4 part of thickener, 0.8~1.2 part of cosolvent, light trigger 1.5~
2.5 parts, 14~17 parts of water.
Optimal case proposed by the present invention, described water-based UV varnish, by weight, including following component：80 parts of water
Property polyurethane acroleic acid dispersion, 0.5~0.6 part of defoamer BYK024,0.3~0.5 part of defoamer TEGO810,0.3~0.6
Part wetting agent, 0.2~0.4 part of levelling agent, 0.3~0.4 part of thickener, 0.8~1.2 part of cosolvent, light trigger 1.5~2.5
Part, 14~17 parts of water.
Second object of the present invention is, there is provided the preparation method of above-mentioned water-based UV varnish, take 50%~75% it is poly-
Urethane acrylic acid dispersion, disperse 10~20 minutes after coalescents component is sequentially added to it, add light trigger stirring
After uniformly, remaining polyurethane acroleic acid dispersant and water are added.
Present invention further propose that, the preparation method is specifically, take 50%~75% polyurethane acroleic acid to disperse
Body, stirred with 300-400r/min speed, defoamer, wetting agent, levelling agent, the group of cosolvent in formula are sequentially added to it
Point, and 1 ‰~10 ‰ thickener adjustment viscosity, disperse 15~20 minutes under 1500r/min speed conditions；Adjust rotating speed
To 800~1000r/min, add after light trigger stirs, add remaining polyurethane acroleic acid dispersant, remaining
Thickener and water.
Or, the preparation method is specifically, take 50%~75% polyurethane acroleic acid dispersion, with 300-400r/min
Speed stirring, sequentially add defoamer, wetting agent, levelling agent, the component of cosolvent in formula to it, and thickener,
Disperse 15~20 minutes under 1500r/min speed conditions；Rotating speed is adjusted to 800~1000r/min, adds light trigger stirring
After uniformly, remaining polyurethane acroleic acid dispersant and water are added.
The addition manner of thickener can front and rear two parts add, can also disposably add；Do not require it is certain need with
Other auxiliary agents add in the lump.When thickener adds at twice, first time addition is less, and its addition is preferably 2 ‰~5 ‰.
Third object of the present invention is that above-mentioned water-based UV varnish applies in plate fitment, wooden furniture, cabinet or timber floor
The application loaded onto；
Application in the following way：After the water of addition 0~10% is diluted in the water-based UV varnish, painting is filled to base
On material, dried 30~60 minutes under 40 DEG C~45 DEG C of temperature conditionss, using ultraviolet source irradiation 5~10 seconds, film-forming
.
The application method and work progress of the above-mentioned water-based UV varnish of Diamond Search are relatively simple, flexible, and rate of drying is fast,
Efficiency high, physics and chemical property are excellent, at the same there are solvent-borne type UV performance characteristics but more green, environmentally friendly, Neng Gouchong
Divide and meet Furniture manufacturing manufacturer at a high speed, efficiently requiring.
It is green using water as decentralized medium present invention employs green watersoluble polyurethane acrylic acid dispersion,
Easy construction, UV (ultraviolet light) curing efficiency are high, Diamond Search discharge.Cured paint film causes hardness high, physical property and chemical-resistant
It is excellent, and there is excellent adhesive force on all kinds of base materials, it is highly suitable for floor, timber, plate fitment or solid wood furniture
Application.Meanwhile the product is green product, injury is not produced to workmen's body.
The water-based UV varnish easy construction of Diamond Search of the present invention, operation is very simple, and coating equipment cleaning is very
It is convenient, it is only necessary to common clear water.And finish paint has fabulous gloss, adhesive force and mechanical thing on furniture to be decorated
Rationality energy, chemical resistance, there is fabulous decoration and protective effect to wood furniture.
Embodiment
Following examples are used to illustrate the present invention, but are not limited to the scope of the present invention.
Reagent used in following examples, it can pass through commercially available acquisition.
Embodiment 1
The present embodiment is a kind of water-based UV varnish of Diamond Search, composed of the following components：
Embodiment 2
The present embodiment is a kind of water-based UV varnish of Diamond Search, composed of the following components：
Embodiment 3
The present embodiment is a kind of water-based UV varnish of Diamond Search, composed of the following components：
Embodiment 4
The present embodiment is the preparation method of the water-based UV varnish described in embodiment 1, is specially：
4kg watersoluble polyurethane acrylic acid dispersion 4617 is taken, is stirred with 300-400r/min speed, added successively to it
Enter defoamer BYK024, wetting agent BYK349, levelling agent TEGO450 component in formula, and 0.03kg thickener
2050D, disperse 15 minutes under 1500r/min speed conditions；Rotating speed is adjusted to 800~1000r/min, adds light trigger
After stirring, remaining watersoluble polyurethane acrylic acid dispersant 4617 and water are added, stirs, produces.
Embodiment 5
The present embodiment is the preparation method of the water-based UV varnish described in embodiment 2, identical with the preparation method of embodiment 1.
The preparation method is specially：4kg watersoluble polyurethane acrylic acid dispersion R-452 is taken, with 300-400r/min
Speed stirring, sequentially added to it formula in defoamer BYK024, defoamer TEGO810, wetting agent BYK349, levelling agent
TEGO450, cosolvent TPNB component, and 0.03kg thickener 2050D, 15 are disperseed under 1500r/min speed conditions
Minute；Rotating speed is adjusted to 800~1000r/min, adds after light trigger stirs, adds remaining aqueous polyurethane third
Olefin(e) acid dispersion R-452 and water, stir, and produce.
Embodiment 6
The present embodiment is the preparation method of the water-based UV varnish described in embodiment 3, identical with the preparation method of embodiment 1.
The preparation method is specially：6kg watersoluble polyurethane acrylic acid dispersion 4617, with 300-400r/min speed
Rate is stirred, and defoamer BYK024, defoamer TEGO810, wetting agent BYK349, levelling agent in formula are sequentially added to it
TEGO450, cosolvent TPNB component and 0.03kg thickener 2050D, 15 are disperseed under 1500r/min speed conditions
Minute；Rotating speed is adjusted to 800~1000r/min, adds after light trigger stirs, adds remaining aqueous polyurethane third
Olefin(e) acid dispersion R-452 and water, stir, and produce.
Test example
Subjects：The water-based UV varnish of Diamond Search described in embodiment 1,2,3
Contrast object：Solvent-borne type UV clear finish
Test method：
1st, the water of addition 0~10% is diluted to spray viscosity in the water-based UV varnish of embodiment 1~3, is applied
It is filled on base material, is dried 40~60 minutes under 40 DEG C~45 DEG C of temperature conditionss, using ultraviolet source irradiation 5~10 seconds, Gu
It is melted into film.
2nd, the spraying method of solvent-borne type UV clear finish：After UV clear finish is diluted to spray viscosity, painting is filled on base material, 40
DEG C temperature conditionss under, 3min levellings dry after, solidified using water-based UV varnish identical mode.
Detect the performance of 1~3 varnish of embodiment and solvent-borne type UV clear finish, Construction Comparison result such as following table：
Table 1：The Construction Comparison result of the finish paint of embodiment 1,2,3 and solvent-borne type UV finish paints
As can be known from the above table, the water-based UV varnish performances described in embodiment 1~3 have reached the performance of solvent-borne type UV products,
And it is less than solvent-borne type UV clear finish in VOC discharge, not even containing VOC.It is truly realized the Diamond Search of UV products.
Although above the present invention is made to retouch in detail with general explanation, embodiment and experiment
State, but on the basis of the present invention, it can be made some modifications or improvements, this is apparent to those skilled in the art
's.Therefore, these modifications or improvements without departing from theon the basis of the spirit of the present invention, are belonged to claimed
Scope.
Claims (10)
- A kind of 1. water-based UV varnish of Diamond Search, it is characterised in that by weight, including following component：Polyurethane acroleic acid disperses 70~90 parts of body, 1.4~3.7 parts of coalescents, 1.5~2.5 parts of light trigger, 10~20 parts of water.
- 2. water-based UV varnish according to claim 1, it is characterised in that the solid content of the polyurethane acroleic acid dispersant For 40%~42%, viscosity is 10~200mpa.s, and pH value is 7.0~9.0；Preferably, the polyurethane acroleic acid dispersant is watersoluble polyurethane acrylic acid dispersant.
- 3. water-based UV varnish according to claim 1 or 2, it is characterised in that the light trigger is selected from 2,4,6 one front threes It is one or two kinds of in base benzoyl phosphinic acid ethyl ester, 2- hydroxy-2-methyl -1- phenyl -1- acetone.
- 4. water-based UV varnish according to claims 1 to 3, it is characterised in that the coalescents are specially：Defoamer 0.4~1.2 part, 0.3~0.6 part of wetting agent, 0.2~0.4 part of levelling agent, 0.2~1.5 part of thickener, 0~2 part of cosolvent.
- 5. water-based UV varnish according to claim 4, it is characterised in that the defoamer defoams selected from organosiloxane class One kind in the mixing species defoamer of agent, the hydrophobic solid without organosilicon and brokenly bubble polymer；And/or the wetting agent is organosilicon moistening flatting agent；And/or the levelling agent is polysiloxane-based levelling agent；And/or the one kind of the thickener in polyethers thickener, polyether-modified polyurethanes thickener；And/or the cosolvent is TPNB.
- 6. water-based UV varnish according to claim 1, it is characterised in that by weight, including following component：70~90 Part watersoluble polyurethane acrylic acid dispersion, 0.5~1.1 part of defoamer, 0.4~0.6 part of wetting agent, 0.2~0.4 part of levelling agent, 0.3~1.5 part of thickener, 0~1.5 part of cosolvent, 1.5~2.5 parts of light trigger, 10~20 parts of water.
- 7. water-based UV varnish according to claim 1, it is characterised in that by weight, including following component：70~90 Part watersoluble polyurethane acrylic acid dispersion, 0.5~0.7 part of defoamer BYK024,0.3~0.5 part of defoamer TEGO810,0.3~ 0.6 part of wetting agent, 0.2~0.4 part of levelling agent, 0.3~0.4 part of thickener, 0.8~1.2 part of cosolvent, light trigger 1.5~ 2.5 parts, 14~17 parts of water.
- 8. the preparation method of any water-based UV varnish of claim 1~7, it is characterised in that take 50%~75% poly- ammonia Ester acrylic acid dispersion, disperse 10~20 minutes after coalescents component is sequentially added to it, it is equal to add light trigger stirring After even, remaining polyurethane acroleic acid dispersant and water are added.
- 9. preparation method according to claim 8, it is characterised in that take 50%~75% polyurethane acroleic acid to disperse Body, stirred with 300-400r/min speed, defoamer, wetting agent, levelling agent, the group of cosolvent in formula are sequentially added to it Point, and 1 ‰~10 ‰ thickener adjustment viscosity, disperse 15~20 minutes under 1500r/min speed conditions；Adjust rotating speed To 800~1000r/min, add after light trigger stirs, add remaining polyurethane acroleic acid dispersant, remaining Thickener and water；Or, 50%~75% polyurethane acroleic acid dispersion is taken, stirred with 300-400r/min speed, sequentially added to it The component of defoamer, wetting agent, levelling agent, cosolvent in formula, and thickener, disperse under 1500r/min speed conditions 15~20 minutes；Rotating speed is adjusted to 800~1000r/min, adds after light trigger stirs, adds remaining polyurethane Acrylic acid dispersant and water.
- 10. the water-based UV varnish prepared by any described water-based UV varnish of claim 1~7 or claim 8 or 9 is board-like Furniture, wooden furniture, cabinet or timber floor apply the application loaded onto；Preferably, application in the following way：After the water of addition 0~10% is diluted in the water-based UV varnish, application To base material, dried 30~60 minutes under 40 DEG C~45 DEG C of temperature conditionss, using ultraviolet source irradiation 5~10 seconds, solidification Film forming.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711022016.2A CN107793917A (en) | 2017-10-27 | 2017-10-27 | A kind of water-based UV varnish of Diamond Search and preparation method and application |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711022016.2A CN107793917A (en) | 2017-10-27 | 2017-10-27 | A kind of water-based UV varnish of Diamond Search and preparation method and application |
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| CN110240858A (en) * | 2019-07-18 | 2019-09-17 | 广东美涂士建材股份有限公司 | A kind of height energetic interaction curable water-borne UV woodenware lacquer and preparation method thereof and construction technology |
| CN115322677A (en) * | 2022-09-21 | 2022-11-11 | 河北英利奥体育用品有限公司 | Coating material and coating method for sports floor |
| CN115746694A (en) * | 2022-11-24 | 2023-03-07 | 中华制漆(新丰）有限公司 | Water-based UV wood lacquer and preparation method thereof |
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