CN107793048A - A kind of high heat-insulation noise-reduction radiation-proof vacuum glass and its manufacture method - Google Patents

A kind of high heat-insulation noise-reduction radiation-proof vacuum glass and its manufacture method Download PDF

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CN107793048A
CN107793048A CN201711235011.8A CN201711235011A CN107793048A CN 107793048 A CN107793048 A CN 107793048A CN 201711235011 A CN201711235011 A CN 201711235011A CN 107793048 A CN107793048 A CN 107793048A
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parts
vacuum glass
nanometer
high heat
adiabatic gum
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闵会
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Tengzhou Yao Hai Glass Carving Co Ltd
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Tengzhou Yao Hai Glass Carving Co Ltd
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    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C27/00Joining pieces of glass to pieces of other inorganic material; Joining glass to glass other than by fusing
    • C03C27/06Joining glass to glass by processes other than fusing
    • C03C27/10Joining glass to glass by processes other than fusing with the aid of adhesive specially adapted for that purpose
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09JADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J11/00Features of adhesives not provided for in group C09J9/00, e.g. additives
    • C09J11/02Non-macromolecular additives
    • C09J11/04Non-macromolecular additives inorganic
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09JADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J11/00Features of adhesives not provided for in group C09J9/00, e.g. additives
    • C09J11/02Non-macromolecular additives
    • C09J11/06Non-macromolecular additives organic
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09JADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J4/00Adhesives based on organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond ; adhesives, based on monomers of macromolecular compounds of groups C09J183/00 - C09J183/16
    • C09J4/06Organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond in combination with a macromolecular compound other than an unsaturated polymer of groups C09J159/00 - C09J187/00

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Ceramic Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Materials Engineering (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Building Environments (AREA)
  • Adhesives Or Adhesive Processes (AREA)

Abstract

The invention discloses a kind of high heat-insulation noise-reduction radiation-proof vacuum glass and its manufacture method, the vacuum glass, is made by being bonded adiabatic gum on vacuum glass base material;The adiabatic gum includes according to the raw material of parts by weight:1 15 parts of 5 25 parts of bonding agent, 5 25 parts of vermiculite, calcium silicates and alumina silicate fibre, 0.2 20 parts of nanometer tungsten oxide, 0.2 20 parts of Nanometer-sized Antimony Doped Tin, 1 20 parts of nano titanium oxide, 1 20 parts of nano barium sulfate, 1 20 parts of ceramic powder, 0.1 5 parts of organic silicon defoamer, 2 20 parts of cyanoacrylate, 1 20 parts of lauryl alcohol fat, 0.5 15 parts of epoxidized soybean oil.Raw material is mixed, adds bonding agent, stir, spray, solidify after produce.Thermal conductivity factor of the present invention is low, good effect of heat insulation, and sound insulating and absorbing noise reduction is good, and radiation-proof effect is good, and adiabatic gum composition is arranged in pairs or groups in the present invention, and reasonable, production method is easy to operate, and constructing operation is convenient, difficult for drop-off, service life length.

Description

A kind of high heat-insulation noise-reduction radiation-proof vacuum glass and its manufacture method
Technical field
The present invention relates to glass technology field, specifically a kind of high heat-insulation noise-reduction radiation-proof vacuum glass and its manufacturer Method.
Background technology
Vacuum glass is to enclose two panels plate glass surrounding, and its gap is evacuated and seal vents, two Gap between sheet glass is 0.1-0.2mm, and the typically at least a piece of two panels of vacuum glass is low emissivity glass, thus will It is preferably minimized by the lost heat of the conduction, convection current and radiation mode of vacuum glass, the guarantor of its operation principle and glass vacuum-bottle Warm mechanism of heat insulation is identical.Vacuum glass is glass technology and material science, vacuum technique, physical measurement techniques, industrial automation And architecture science etc., the outstanding achievement that a variety of subjects, multiple technologies, kinds of processes cooperation coordinate.The thermal and insulating performance of vacuum glass It is much better than " hollow " glass being widely used at present.However, most vacuum glass heat-insulating effect and bad in the market, and If it is poorly sealed to have a strong impact on its heat insulation effect after long-time use, and function would be single.
The content of the invention
It is an object of the invention to provide a kind of high heat-insulation noise-reduction radiation-proof vacuum glass and its manufacture method, with solution State the problem of being proposed in background technology.
To achieve the above object, the present invention provides following technical scheme:
A kind of high heat-insulation noise-reduction radiation-proof vacuum glass, it is made by being bonded adiabatic gum on vacuum glass base material;The adiabatic gum is pressed Include according to the raw material of parts by weight:It is bonding agent 5-25 parts, vermiculite 5-25 parts, calcium silicates and alumina silicate fibre 1-15 parts, nano oxidized Tungsten 0.2-20 parts, Nanometer-sized Antimony Doped Tin 0.2-20 parts, nano titanium oxide 1-20 parts, nano barium sulfate 1-20 parts, ceramic powder 1-20 parts, organic silicon defoamer 0.1-5 parts, cyanoacrylate 2-20 parts, lauryl alcohol fat 1-20 parts, epoxidized soybean oil 0.5-15 Part.
As the further scheme of the present invention:The mass ratio of calcium silicates and alumina silicate fibre is 0.2-8:1.
As the further scheme of the present invention:The adiabatic gum includes according to the raw material of parts by weight:Bonding agent 8-22 parts, leech Stone 8-22 parts, calcium silicates and alumina silicate fibre 1-12 parts, nanometer tungsten oxide 0.5-15 parts, Nanometer-sized Antimony Doped Tin 0.5-15 parts, Nano titanium oxide 2-18 parts, nano barium sulfate 2-18 parts, ceramic powder 2-18 parts, organic silicon defoamer 0.1-4 parts, cyanoacrylate Acid esters 4-18 parts, lauryl alcohol fat 2-18 parts, epoxidized soybean oil 0.8-12 parts.
As the further scheme of the present invention:The adiabatic gum includes according to the raw material of parts by weight:Bonding agent 10-20 parts, Vermiculite 10-20 parts, calcium silicates and alumina silicate fibre 2-10 parts, nanometer tungsten oxide 1-12 parts, Nanometer-sized Antimony Doped Tin 1-12 parts, receive Rice titanium dioxide 5-15 parts, nano barium sulfate 5-15 parts, ceramic powder 5-15 parts, organic silicon defoamer 0.1-3 parts, alpha-cyanoacrylate Ester 5-15 parts, lauryl alcohol fat 3-15 parts, epoxidized soybean oil 1-10 parts.
A kind of manufacture method of high heat-insulation noise-reduction radiation-proof vacuum glass, comprises the following steps:
1)Prepare raw material:Weigh bonding agent, vermiculite, calcium silicates and alumina silicate fibre, nanometer tungsten oxide respectively according to parts by weight, receive Rice antimony tin oxide, nano titanium oxide, nano barium sulfate, ceramic powder, organic silicon defoamer, cyanoacrylate, lauryl alcohol Fat, epoxidized soybean oil;
2)By vermiculite, calcium silicates and alumina silicate fibre, nanometer tungsten oxide, Nanometer-sized Antimony Doped Tin, nano titanium oxide, nano-sulfur Sour barium, ceramic powder, organic silicon defoamer, cyanoacrylate, lauryl alcohol fat, epoxidized soybean oil mix 30-120min, then Bonding agent is added, stirs and produces adiabatic gum;
3)Adiabatic gum is equably sprayed on one block of vacuum glass base material, take another block of vacuum glass base material to be placed on previous true The spray-coating surface of empty glass baseplate, vacuum glass is produced after solidification.
As the further scheme of the present invention:Step 3)In, 28-45 DEG C of spraying temperature, spray gun pressure 0.3-2MPa.
As the further scheme of the present invention:Step 3)In, the temperature of solidification is 150-200 DEG C, the time being heating and curing For 8-30min.
Compared with prior art, the beneficial effects of the invention are as follows:
The present invention is using vacuum glass made from above-mentioned adiabatic gum, and thermal conductivity factor is low, good effect of heat insulation, sound insulating and absorbing noise reduction Working well, radiation-proof effect is good, and adiabatic gum composition is arranged in pairs or groups in the present invention, and reasonable, production method is easy to operate, and constructing operation is convenient, It is difficult for drop-off, service life length.
Embodiment
Below in conjunction with the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely described, Obviously, described embodiment is only part of the embodiment of the present invention, rather than whole embodiments.Based in the present invention Embodiment, the every other embodiment that those of ordinary skill in the art are obtained under the premise of creative work is not made, all Belong to the scope of protection of the invention.
Embodiment 1
In the embodiment of the present invention, a kind of high heat-insulation noise-reduction radiation-proof vacuum glass, by being bonded adiabatic gum system on vacuum glass base material Into;The adiabatic gum includes according to the raw material of parts by weight:1 part of 5 parts of bonding agent, 5 parts of vermiculite, calcium silicates and alumina silicate fibre, receive 0.2 part of tungsten oxide of rice, 0.2 part of Nanometer-sized Antimony Doped Tin, 1 part of nano titanium oxide, 1 part of nano barium sulfate, 1 part of ceramic powder, have 0.1 part of machine silicon defoaming agent, 2 parts of cyanoacrylate, 1 part of lauryl alcohol fat, 0.5 part of epoxidized soybean oil.Calcium silicates and aluminium silicate fiber The mass ratio of dimension is 0.2:1.
A kind of manufacture method of high heat-insulation noise-reduction radiation-proof vacuum glass, comprises the following steps:
1)Prepare raw material:Weigh bonding agent, vermiculite, calcium silicates and alumina silicate fibre, nanometer tungsten oxide respectively according to parts by weight, receive Rice antimony tin oxide, nano titanium oxide, nano barium sulfate, ceramic powder, organic silicon defoamer, cyanoacrylate, lauryl alcohol Fat, epoxidized soybean oil.
2)By vermiculite, calcium silicates and alumina silicate fibre, nanometer tungsten oxide, Nanometer-sized Antimony Doped Tin, nano titanium oxide, receive Nano-barium sulfate, ceramic powder, organic silicon defoamer, cyanoacrylate, lauryl alcohol fat, epoxidized soybean oil mix 30min, then Bonding agent is added, stirs and produces adiabatic gum.
3)Adiabatic gum is equably sprayed on one block of vacuum glass base material, 28 DEG C, spray gun pressure 0.3MPa of spraying temperature, Take another block of vacuum glass base material to be placed on the spray-coating surface of previous vacuum glass base material, vacuum glass is produced after solidification, solidification Temperature is 150 DEG C, and the time being heating and curing is 8min.
Embodiment 2
In the embodiment of the present invention, a kind of high heat-insulation noise-reduction radiation-proof vacuum glass, by being bonded adiabatic gum system on vacuum glass base material Into;The adiabatic gum includes according to the raw material of parts by weight:15 parts of 25 parts of bonding agent, 25 parts of vermiculite, calcium silicates and alumina silicate fibre, 20 parts of nanometer tungsten oxide, 20 parts of Nanometer-sized Antimony Doped Tin, 20 parts of nano titanium oxide, 20 parts of nano barium sulfate, 20 parts of ceramic powder, 5 parts of organic silicon defoamer, 20 parts of cyanoacrylate, 20 parts of lauryl alcohol fat, 15 parts of epoxidized soybean oil.Calcium silicates and aluminium silicate fiber The mass ratio of dimension is 8:1.
A kind of manufacture method of high heat-insulation noise-reduction radiation-proof vacuum glass, comprises the following steps:
1)Prepare raw material:Weigh bonding agent, vermiculite, calcium silicates and alumina silicate fibre, nanometer tungsten oxide respectively according to parts by weight, receive Rice antimony tin oxide, nano titanium oxide, nano barium sulfate, ceramic powder, organic silicon defoamer, cyanoacrylate, lauryl alcohol Fat, epoxidized soybean oil.
2)By vermiculite, calcium silicates and alumina silicate fibre, nanometer tungsten oxide, Nanometer-sized Antimony Doped Tin, nano titanium oxide, receive Nano-barium sulfate, ceramic powder, organic silicon defoamer, cyanoacrylate, lauryl alcohol fat, epoxidized soybean oil mix 120min, Bonding agent is added, stirs and produces adiabatic gum.
3)Adiabatic gum is equably sprayed on one block of vacuum glass base material, 45 DEG C of spraying temperature, spray gun pressure 2MPa, taken Another block of vacuum glass base material is placed on the spray-coating surface of previous vacuum glass base material, and vacuum glass, the temperature of solidification are produced after solidification Spend for 200 DEG C, the time being heating and curing is 30min.
Embodiment 3
In the embodiment of the present invention, a kind of high heat-insulation noise-reduction radiation-proof vacuum glass, by being bonded adiabatic gum system on vacuum glass base material Into;The adiabatic gum includes according to the raw material of parts by weight:1 part of 8 parts of bonding agent, 8 parts of vermiculite, calcium silicates and alumina silicate fibre, receive 0.5 part of tungsten oxide of rice, 0.5 part of Nanometer-sized Antimony Doped Tin, 2 parts of nano titanium oxide, 2 parts of nano barium sulfate, 2 parts of ceramic powder, have 0.1 part of machine silicon defoaming agent, 4 parts of cyanoacrylate, 2 parts of lauryl alcohol fat, 0.8 part of epoxidized soybean oil.Calcium silicates and aluminium silicate fiber The mass ratio of dimension is 1:1.
A kind of manufacture method of high heat-insulation noise-reduction radiation-proof vacuum glass, comprises the following steps:
1)Prepare raw material:Weigh bonding agent, vermiculite, calcium silicates and alumina silicate fibre, nanometer tungsten oxide respectively according to parts by weight, receive Rice antimony tin oxide, nano titanium oxide, nano barium sulfate, ceramic powder, organic silicon defoamer, cyanoacrylate, lauryl alcohol Fat, epoxidized soybean oil.
2)By vermiculite, calcium silicates and alumina silicate fibre, nanometer tungsten oxide, Nanometer-sized Antimony Doped Tin, nano titanium oxide, receive Nano-barium sulfate, ceramic powder, organic silicon defoamer, cyanoacrylate, lauryl alcohol fat, epoxidized soybean oil mix 50min, then Bonding agent is added, stirs and produces adiabatic gum.
3)Adiabatic gum is equably sprayed on one block of vacuum glass base material, 30 DEG C, spray gun pressure 0.5MPa of spraying temperature, Take another block of vacuum glass base material to be placed on the spray-coating surface of previous vacuum glass base material, vacuum glass is produced after solidification, solidification Temperature is 170 DEG C, and the time being heating and curing is 10min.
Embodiment 4
In the embodiment of the present invention, a kind of high heat-insulation noise-reduction radiation-proof vacuum glass, by being bonded adiabatic gum system on vacuum glass base material Into;The adiabatic gum includes according to the raw material of parts by weight:12 parts of 22 parts of bonding agent, 22 parts of vermiculite, calcium silicates and alumina silicate fibre, 15 parts of nanometer tungsten oxide, 15 parts of Nanometer-sized Antimony Doped Tin, 18 parts of nano titanium oxide, 18 parts of nano barium sulfate, 18 parts of ceramic powder, 4 parts of organic silicon defoamer, 18 parts of cyanoacrylate, 18 parts of lauryl alcohol fat, 12 parts of epoxidized soybean oil.Calcium silicates and aluminium silicate fiber The mass ratio of dimension is 6:1.
A kind of manufacture method of high heat-insulation noise-reduction radiation-proof vacuum glass, comprises the following steps:
1)Prepare raw material:Weigh bonding agent, vermiculite, calcium silicates and alumina silicate fibre, nanometer tungsten oxide respectively according to parts by weight, receive Rice antimony tin oxide, nano titanium oxide, nano barium sulfate, ceramic powder, organic silicon defoamer, cyanoacrylate, lauryl alcohol Fat, epoxidized soybean oil.
2)By vermiculite, calcium silicates and alumina silicate fibre, nanometer tungsten oxide, Nanometer-sized Antimony Doped Tin, nano titanium oxide, receive Nano-barium sulfate, ceramic powder, organic silicon defoamer, cyanoacrylate, lauryl alcohol fat, epoxidized soybean oil mix 100min, Bonding agent is added, stirs and produces adiabatic gum.
3)Adiabatic gum is equably sprayed on one block of vacuum glass base material, 42 DEG C, spray gun pressure 1.5MPa of spraying temperature, Take another block of vacuum glass base material to be placed on the spray-coating surface of previous vacuum glass base material, vacuum glass is produced after solidification, solidification Temperature is 190 DEG C, and the time being heating and curing is 25min.
Embodiment 5
In the embodiment of the present invention, a kind of high heat-insulation noise-reduction radiation-proof vacuum glass, by being bonded adiabatic gum system on vacuum glass base material Into;The adiabatic gum includes according to the raw material of parts by weight:2 parts of 10 parts of bonding agent, 10 parts of vermiculite, calcium silicates and alumina silicate fibre, It is 1 part of nanometer tungsten oxide, 1 part of Nanometer-sized Antimony Doped Tin, 5 parts of nano titanium oxide, 5 parts of nano barium sulfate, 5 parts of ceramic powder, organic 0.1 part of silicon defoaming agent, 5 parts of cyanoacrylate, 3 parts of lauryl alcohol fat, 1 part of epoxidized soybean oil.Calcium silicates and alumina silicate fibre Mass ratio is 2:1.
A kind of manufacture method of high heat-insulation noise-reduction radiation-proof vacuum glass, comprises the following steps:
1)Prepare raw material:Weigh bonding agent, vermiculite, calcium silicates and alumina silicate fibre, nanometer tungsten oxide respectively according to parts by weight, receive Rice antimony tin oxide, nano titanium oxide, nano barium sulfate, ceramic powder, organic silicon defoamer, cyanoacrylate, lauryl alcohol Fat, epoxidized soybean oil.
2)By vermiculite, calcium silicates and alumina silicate fibre, nanometer tungsten oxide, Nanometer-sized Antimony Doped Tin, nano titanium oxide, receive Nano-barium sulfate, ceramic powder, organic silicon defoamer, cyanoacrylate, lauryl alcohol fat, epoxidized soybean oil mix 70min, then Bonding agent is added, stirs and produces adiabatic gum.
3)Adiabatic gum is equably sprayed on one block of vacuum glass base material, 42 DEG C, spray gun pressure 0.8MPa of spraying temperature, Take another block of vacuum glass base material to be placed on the spray-coating surface of previous vacuum glass base material, vacuum glass is produced after solidification, solidification Temperature is 160 DEG C, and the time being heating and curing is 8-30min.
Embodiment 6
In the embodiment of the present invention, a kind of high heat-insulation noise-reduction radiation-proof vacuum glass, by being bonded adiabatic gum system on vacuum glass base material Into;The adiabatic gum includes according to the raw material of parts by weight:10 parts of 20 parts of bonding agent, 20 parts of vermiculite, calcium silicates and alumina silicate fibre, 12 parts of nanometer tungsten oxide, 12 parts of Nanometer-sized Antimony Doped Tin, 15 parts of nano titanium oxide, 15 parts of nano barium sulfate, 15 parts of ceramic powder, 3 parts of organic silicon defoamer, 15 parts of cyanoacrylate, 15 parts of lauryl alcohol fat, 10 parts of epoxidized soybean oil.Calcium silicates and aluminium silicate fiber The mass ratio of dimension is 5:1.
A kind of manufacture method of high heat-insulation noise-reduction radiation-proof vacuum glass, comprises the following steps:
1)Prepare raw material:Weigh bonding agent, vermiculite, calcium silicates and alumina silicate fibre, nanometer tungsten oxide respectively according to parts by weight, receive Rice antimony tin oxide, nano titanium oxide, nano barium sulfate, ceramic powder, organic silicon defoamer, cyanoacrylate, lauryl alcohol Fat, epoxidized soybean oil.
2)By vermiculite, calcium silicates and alumina silicate fibre, nanometer tungsten oxide, Nanometer-sized Antimony Doped Tin, nano titanium oxide, receive Nano-barium sulfate, ceramic powder, organic silicon defoamer, cyanoacrylate, lauryl alcohol fat, epoxidized soybean oil mix 80min, then Bonding agent is added, stirs and produces adiabatic gum.
3)Adiabatic gum is equably sprayed on one block of vacuum glass base material, 40 DEG C, spray gun pressure 1.5MPa of spraying temperature, Take another block of vacuum glass base material to be placed on the spray-coating surface of previous vacuum glass base material, vacuum glass is produced after solidification, solidification Temperature is 170 DEG C, and the time being heating and curing is 15min.
It is obvious to a person skilled in the art that the invention is not restricted to the details of above-mentioned one exemplary embodiment, Er Qie In the case of without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter From the point of view of which point, embodiment all should be regarded as exemplary, and be nonrestrictive, the scope of the present invention is by appended power Profit requires rather than described above limits, it is intended that all in the implication and scope of the equivalency of claim by falling Change is included in the present invention.
Moreover, it will be appreciated that although the present specification is described in terms of embodiments, not each embodiment is only wrapped Containing an independent technical scheme, this narrating mode of specification is only that those skilled in the art should for clarity Using specification as an entirety, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art It is appreciated that other embodiment.

Claims (7)

1. a kind of high heat-insulation noise-reduction radiation-proof vacuum glass, it is made by being bonded adiabatic gum on vacuum glass base material;Characterized in that, The adiabatic gum includes according to the raw material of parts by weight:Bonding agent 5-25 parts, vermiculite 5-25 parts, calcium silicates and alumina silicate fibre 1-15 Part, nanometer tungsten oxide 0.2-20 parts, Nanometer-sized Antimony Doped Tin 0.2-20 parts, nano titanium oxide 1-20 parts, nano barium sulfate 1- 20 parts, ceramic powder 1-20 parts, organic silicon defoamer 0.1-5 parts, cyanoacrylate 2-20 parts, lauryl alcohol fat 1-20 parts, epoxy Soybean oil 0.5-15 parts.
2. high heat-insulation noise-reduction radiation-proof vacuum glass according to claim 1, it is characterised in that calcium silicates and aluminium silicate fiber The mass ratio of dimension is 0.2-8:1.
3. high heat-insulation noise-reduction radiation-proof vacuum glass according to claim 1, it is characterised in that the adiabatic gum is according to weight The raw material of amount part includes:Bonding agent 8-22 parts, vermiculite 8-22 parts, calcium silicates and alumina silicate fibre 1-12 parts, nanometer tungsten oxide 0.5-15 parts, Nanometer-sized Antimony Doped Tin 0.5-15 parts, nano titanium oxide 2-18 parts, nano barium sulfate 2-18 parts, ceramic powder 2- 18 parts, organic silicon defoamer 0.1-4 parts, cyanoacrylate 4-18 parts, lauryl alcohol fat 2-18 parts, epoxidized soybean oil 0.8-12 Part.
4. high heat-insulation noise-reduction radiation-proof vacuum glass according to claim 1, it is characterised in that the adiabatic gum is according to weight The raw material of amount part includes:Bonding agent 10-20 parts, vermiculite 10-20 parts, calcium silicates and alumina silicate fibre 2-10 parts, nanometer tungsten oxide 1-12 parts, Nanometer-sized Antimony Doped Tin 1-12 parts, nano titanium oxide 5-15 parts, nano barium sulfate 5-15 parts, ceramic powder 5-15 parts, Organic silicon defoamer 0.1-3 parts, cyanoacrylate 5-15 parts, lauryl alcohol fat 3-15 parts, epoxidized soybean oil 1-10 parts.
5. a kind of manufacture method of high heat-insulation noise-reduction radiation-proof vacuum glass as described in claim 1-4 is any, its feature exist In comprising the following steps:
1)Prepare raw material:Weigh bonding agent, vermiculite, calcium silicates and alumina silicate fibre, nanometer tungsten oxide respectively according to parts by weight, receive Rice antimony tin oxide, nano titanium oxide, nano barium sulfate, ceramic powder, organic silicon defoamer, cyanoacrylate, lauryl alcohol Fat, epoxidized soybean oil;
2)By vermiculite, calcium silicates and alumina silicate fibre, nanometer tungsten oxide, Nanometer-sized Antimony Doped Tin, nano titanium oxide, nano-sulfur Sour barium, ceramic powder, organic silicon defoamer, cyanoacrylate, lauryl alcohol fat, epoxidized soybean oil mix 30-120min, then Bonding agent is added, stirs and produces adiabatic gum;
3)Adiabatic gum is equably sprayed on one block of vacuum glass base material, take another block of vacuum glass base material to be placed on previous true The spray-coating surface of empty glass baseplate, vacuum glass is produced after solidification.
6. the manufacture method of high heat-insulation noise-reduction radiation-proof vacuum glass according to claim 5, it is characterised in that step 3) In, 28-45 DEG C of spraying temperature, spray gun pressure 0.3-2MPa.
7. the manufacture method of high heat-insulation noise-reduction radiation-proof vacuum glass according to claim 5, it is characterised in that step 3) In, the temperature of solidification is 150-200 DEG C, and the time being heating and curing is 8-30min.
CN201711235011.8A 2017-11-30 2017-11-30 A kind of high heat-insulation noise-reduction radiation-proof vacuum glass and its manufacture method Pending CN107793048A (en)

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CN101428976A (en) * 2008-12-09 2009-05-13 中南大学 Glass nano- energy-saving paint and method for producing the same
CN101550307A (en) * 2009-05-14 2009-10-07 复旦大学 Transparent heat insulation coating material, preparation method and application thereof
CN105481269A (en) * 2014-09-15 2016-04-13 池州市英派科技有限公司 Manufacturing method of laminated glass
CN105563958A (en) * 2015-12-28 2016-05-11 太仓耀华玻璃有限公司 High-heat-insulation noise-reducing anti-radiation vacuum glass and manufacture method thereof
CN107188433A (en) * 2017-05-27 2017-09-22 句容耀皮节能玻璃科技发展有限公司 A kind of anti-moisture absorption heat-insulating laminated glass and preparation method thereof
CN107090198A (en) * 2017-06-22 2017-08-25 合肥钢骨玻璃制品有限公司 A kind of composite fireproof glass fire-resistant fluid and preparation method thereof
CN107325651A (en) * 2017-07-15 2017-11-07 合肥皖水信息科技有限公司 A kind of fire-proof glass curtain wall
CN107267011A (en) * 2017-08-01 2017-10-20 合肥择浚电气设备有限公司 A kind of coating with heat insulating reflecting function and preparation method thereof

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Application publication date: 20180313