CN107760731A - The extracting method of selenium element in a kind of selenium-rich crops - Google Patents

The extracting method of selenium element in a kind of selenium-rich crops Download PDF

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CN107760731A
CN107760731A CN201710932316.8A CN201710932316A CN107760731A CN 107760731 A CN107760731 A CN 107760731A CN 201710932316 A CN201710932316 A CN 201710932316A CN 107760731 A CN107760731 A CN 107760731A
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selenium
parts
selenium element
fermentation
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兰宇玲
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    • C12PFERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P9/00Preparation of organic compounds containing a metal or atom other than H, N, C, O, S or halogen

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Abstract

The invention discloses a kind of extracting method of selenium element in selenium-rich crops, used raw materials by weight portion ratio is:58 parts of selenium-rich crops, 8 10 parts of plant enzyme, 0.3 2 parts of probiotics, 1.5 2 parts of brown sugar, 35 parts of medical stone emulsion;By the selenium-rich crops ground into end, the probiotics of activation is added, and is stirred, carries out cold fermentation, fermentation temperature is 28 36 DEG C;Add 40 DEG C of medical stone emulsions;It is put into plant enzyme;Installation note oxygen pump, is continuously injected into oxygen, when there is white hair bacterium, note oxygen pump is removed, into anaerobic fermentation process;Continue fermentation 22 days under air-proof condition, zymotic fluid is obtained after filtering, by zymotic fluid censorship to detect the content of selenium element, selenium element content, which reaches 735 mg/kgs, can stop fermenting.The present invention starts with from material quality, according to the characteristic of raw material, takes effective technique, at utmost retains the selenium element of raw material.

Description

The extracting method of selenium element in a kind of selenium-rich crops
Technical field
The present invention relates to a kind of extracting method of selenium element, the extracting method of selenium element in especially a kind of selenium-rich crops.
Background technology
The production of selenium-rich crops is exactly certain particular time in crop growth, and the liquid of selenium element is rich in by foliage-spray Thrown under fertilizer or root and apply the fertilizer containing selenium element, by the absorption of crops, conversion process, be finally enriched in agricultural product.When Before, large area successfully produces for selenium-rich rice, wheat, watermelon, apple, garlic, shallot, turns into qualified selenium-rich product. The selenium element not still indispensable nutrient of human body, but also be the beneficial element of plant, after increasing selenium fertilizer, robust plant Growth, yield increase, quality improve.
Selenium is the essential trace elements of the human body, and China is a selenium deficiency big country.Selenium is also classified as human body by Chinese Soclety of Nutrition One of required 15 kinds of nutrients, it is a large amount of clinical experiments have proved that human body selenium deficiency can cause the function of some vitals both at home and abroad Imbalance, many serious diseases are caused to occur, more than 40, whole world country is in selenium deficiency area, several hundred million populations in 22, China province It is very high all in selenium deficiency or the incidence of disease such as low selenium area, these regional population tumour, hepatopathy, angiocardiopathies, low selenium or scarce Selenium crowd is not only able to the generation of pre- preventing tumor, hepatopathy etc. by appropriate selenium-supply, and can improve body immunity, safeguards The vitals normal function such as the heart, liver, lung, stomach, prevents the generation of senile Cardial or cerebral vascular diseases.
The technique of enriched selenium of crops, which is popularized, to come, and selenium-rich crops plant by large area, but how to make from selenium-rich Selenium element is extracted in thing and rarely has document report, prevents the popularization of technique of enriched selenium from preferably benefiting the people.
The content of the invention
To solve existing problem above, the invention discloses a kind of extracting method of selenium element in selenium-rich crops, its is specific What scheme was realized in:
(1) raw materials by weight portion ratio is used by:Selenium-rich crops 5-8 parts, plant enzyme 8-10 parts, probiotics 0.3- 2 parts, brown sugar 1.5-2 parts, medical stone emulsion 3-5 parts;By the selenium-rich crops ground into end, the probiotics of activation is added, and is stirred Mix uniformly, carry out cold fermentation, fermentation temperature is 28-36 DEG C;
(2) under conditions of being stirred continuously, medical stone emulsion is warming up to 40 DEG C, adds the mixture that step (1) obtains In;
(3) plant enzyme is put into, continues to stir;
(4) installation note oxygen pump, is continuously injected into oxygen, when there is white hair bacterium, removes note oxygen pump, into anaerobic fermentation mistake Journey;If not occurring white hair bacterium, continue to inject oxygen, until when there is white hair bacterium, into anaerobic fermentation process, remove note oxygen Pump;
(5) continue fermentation 22 days under air-proof condition, zymotic fluid is obtained after filtering, zymotic fluid censorship is first to detect selenium The content of element, selenium element content, which reaches 735 mg/kgs, can stop fermenting, if selenium element content is not up to 735 milligrams/thousand Gram then continue to ferment, until selenium element content reaches more than 735 mg/kgs.
Preferably, the selenium-rich crops are the one or both in the wheat of artificial selenium-rich, rice in planting process Mixture, selenium element content are containing more than 4.6-520 mg/kgs in the selenium-rich crops.
Preferably, the blade face selenium fertilizer of selenium-rich crops institute spray should pass through illumination in more than 15 days, and soak four with clear water Hour.
Preferably, the plant enzyme contains multidimensional sugar, collagen and pectin albumen, total acidity 20-27%, and sends out The ferment time is more than 3 years.
Preferably, the probiotics is activation.
Preferably, the brown sugar can also be the mixture of the one or both in glucose, sucrose.
Preferably, the medical stone emulsion is after filtering.
Beneficial effect:The present invention starts with from material quality, according to the characteristic of raw material, takes effective technique, at utmost Retain the selenium element of raw material, the absorptivity of selenium element can be brought up to 67%;Selenium-supply is for prevention cardiovascular and cerebrovascular disease, colon Scorching, diabetes have facilitation;Body immunity can be improved, safeguards the vitals normal function such as the heart, liver, lung, stomach, it is long Phase eats, good for health;For control cancer the incidence of disease and anticancer it is significant.
Embodiment
In conjunction with the embodiments, the present invention is described in further details.
Embodiment 1
The extracting method of selenium element in a kind of selenium-rich crops, what its concrete scheme was realized in:
(1) raw materials by weight portion ratio is used by:It is 5 parts of selenium-rich crops, 8 parts of plant enzyme, 0.3 part of probiotics, red Sugared 1.5 parts, 3 parts of medical stone emulsion;By the selenium-rich crops ground into end, the probiotics of activation is added, and is stirred, is carried out Cold fermentation, fermentation temperature are 28-36 DEG C;
(2) under conditions of being stirred continuously, the medical stone emulsion after filtering is warming up to 40 DEG C, step (1) is added and obtains Mixture in;
(3) plant enzyme that total acidity is 27% and fermentation time is more than 3 years is put into, continues to stir;
(4) installation note oxygen pump, is continuously injected into oxygen, when there is white hair bacterium, removes note oxygen pump, into anaerobic fermentation mistake Journey;If not occurring white hair bacterium, continue to inject oxygen, until when there is white hair bacterium, into anaerobic fermentation process, remove note oxygen Pump;
(5) continue fermentation 22 days under air-proof condition, zymotic fluid is obtained after filtering, zymotic fluid censorship is first to detect selenium The content of element, selenium element content, which reaches 735 mg/kgs, can stop fermenting, if selenium element content is not up to 735 milligrams/thousand Gram then continue to ferment, until selenium element content reaches more than 735 mg/kgs.
Embodiment 2
The extracting method of selenium element in a kind of selenium-rich crops, what its concrete scheme was realized in:
(1) raw materials by weight portion ratio is used by:It is 6 parts of selenium-rich crops, 8 parts of plant enzyme, 0.3 part of probiotics, red Sugared 1.5 parts, 4 parts of medical stone emulsion;By the selenium-rich crops ground into end, the probiotics of activation is added, and is stirred, is carried out Cold fermentation, fermentation temperature are 28-36 DEG C;
(2) under conditions of being stirred continuously, the medical stone emulsion after filtering is warming up to 40 DEG C, step (1) is added and obtains Mixture in;
(3) plant enzyme that total acidity is 27% and fermentation time is more than 3 years is put into, continues to stir;
(4) installation note oxygen pump, is continuously injected into oxygen, when there is white hair bacterium, removes note oxygen pump, into anaerobic fermentation mistake Journey;If not occurring white hair bacterium, continue to inject oxygen, until when there is white hair bacterium, into anaerobic fermentation process, remove note oxygen Pump;
(5) continue fermentation 22 days under air-proof condition, zymotic fluid is obtained after filtering, zymotic fluid censorship is first to detect selenium The content of element, selenium element content, which reaches 735 mg/kgs, can stop fermenting, if selenium element content is not up to 735 milligrams/thousand Gram then continue to ferment, until selenium element content reaches more than 735 mg/kgs.
Embodiment 3
The extracting method of selenium element in a kind of selenium-rich crops, what its concrete scheme was realized in:
(1) raw materials by weight portion ratio is used by:8 parts of selenium-rich crops, 8 parts of plant enzyme, 1.5 parts of probiotics, Portugal Grape sugar 2 parts, 4 parts of medical stone emulsion;By the selenium-rich crops ground into end, the probiotics of activation is added, and is stirred, is carried out Cold fermentation, fermentation temperature are 28-36 DEG C;
(2) under conditions of being stirred continuously, the medical stone emulsion after filtering is warming up to 40 DEG C, step (1) is added and obtains Mixture in;
(3) plant enzyme that total acidity is 27% and fermentation time is more than 3 years is put into, continues to stir;
(4) installation note oxygen pump, is continuously injected into oxygen, when there is white hair bacterium, removes note oxygen pump, into anaerobic fermentation mistake Journey;If not occurring white hair bacterium, continue to inject oxygen, until when there is white hair bacterium, into anaerobic fermentation process, remove note oxygen Pump;
(5) continue fermentation 22 days under air-proof condition, zymotic fluid is obtained after filtering, zymotic fluid censorship is first to detect selenium The content of element, selenium element content, which reaches 735 mg/kgs, can stop fermenting, if selenium element content is not up to 735 milligrams/thousand Gram then continue to ferment, until selenium element content reaches more than 735 mg/kgs.
Embodiment 4
The extracting method of selenium element in a kind of selenium-rich crops, what its concrete scheme was realized in:
(1) raw materials by weight portion ratio is used by:8 parts of selenium-rich crops, 8 parts of plant enzyme, 2 parts of probiotics, sucrose 3 Part, 4 parts of medical stone emulsion;By the selenium-rich crops ground into end, the probiotics of activation is added, and is stirred, carries out low temperature Fermentation, fermentation temperature are 28-36 DEG C;
(2) under conditions of being stirred continuously, the medical stone emulsion after filtering is warming up to 40 DEG C, step (1) is added and obtains Mixture in;
(3) it is put into total acidity to be 27% and ask the plant enzyme for more than 3 years when fermenting, continues to stir;
(4) installation note oxygen pump, is continuously injected into oxygen, when there is white hair bacterium, removes note oxygen pump, into anaerobic fermentation mistake Journey;If not occurring white hair bacterium, continue to inject oxygen, until when there is white hair bacterium, into anaerobic fermentation process, remove note oxygen Pump;
(5) continue fermentation 22 days under air-proof condition, zymotic fluid is obtained after filtering, zymotic fluid censorship is first to detect selenium The content of element, selenium element content, which reaches 735 mg/kgs, can stop fermenting, if selenium element content is not up to 735 milligrams/thousand Gram then continue to ferment, until selenium element content reaches more than 735 mg/kgs.
Above-mentioned embodiment is only intended to clearly illustrate example of the present invention, and not to embodiment Limit.For those of ordinary skill in the field, other multi-forms can also be made on the basis of the above description Change or variation, there is no necessity and possibility to exhaust all the enbodiments, and thus amplifies out apparent Change or change still in protection scope of the present invention.

Claims (10)

1. the extracting method of selenium element in a kind of selenium-rich crops, it is characterised in that what its concrete scheme was realized in:
(1) raw materials by weight portion ratio is used by:Selenium-rich crops 5-8 parts, plant enzyme 8-10 parts, probiotics 0.3-2 parts, Brown sugar 1.5-2 parts, medical stone emulsion 3-5 parts;By the selenium-rich crops ground into end, the probiotics of activation is added, and is stirred equal It is even, cold fermentation is carried out, fermentation temperature is 28-36 DEG C;
(2) under conditions of being stirred continuously, medical stone emulsion is warming up to 40 DEG C, added in the mixture that step (1) obtains;
(3) plant enzyme is put into, continues to stir;
(4) installation note oxygen pump, is continuously injected into oxygen, when there is white hair bacterium, note oxygen pump is removed, into anaerobic fermentation process;If Do not occur white hair bacterium, then continue to inject oxygen, until when there is white hair bacterium, into anaerobic fermentation process, remove note oxygen pump;
(5) continue fermentation 22 days under air-proof condition, zymotic fluid is obtained after filtering, by zymotic fluid censorship to detect selenium element Content, selenium element content, which reaches 735 mg/kgs, can stop fermenting, if selenium element content is not up to 735 mg/kgs Continue to ferment, until selenium element content reaches more than 735 mg/kgs.
2. the extracting method of selenium element in a kind of selenium-rich crops according to claim 1, it is characterised in that the selenium-rich is made Thing is the wheat of artificial selenium-rich, the mixture of one or both in rice in planting process, and selenium element content is the richness Containing more than 4.6-520 mg/kgs in selenium crop.
3. the extracting method of selenium element in a kind of selenium-rich crops according to claim 1, it is characterised in that the selenium-rich is made The blade face selenium fertilizer of thing institute spray should pass through illumination in more than 15 days, and be soaked four hours with clear water.
4. the extracting method of selenium element in a kind of selenium-rich crops according to claim 1, it is characterised in that the plant ferment Element is more than 3 years containing multidimensional sugar, collagen and pectin albumen, total acidity 20-27%, and fermentation time.
5. the extracting method of selenium element in a kind of selenium-rich crops according to claim 1, it is characterised in that the probiotics It is activation.
6. the extracting method of selenium element in a kind of selenium-rich crops according to claim 1, it is characterised in that the brown sugar It can be the mixture of the one or both in glucose, sucrose.
7. the extracting method of selenium element in a kind of selenium-rich crops according to claim 1, it is characterised in that the medical stone Emulsion is after filtering.
8. the extracting method of selenium element in a kind of selenium-rich crops according to claim 1, it is characterised in that its concrete scheme It is realized in:
(1) raw materials by weight portion ratio is used by:5 parts of selenium-rich crops, 8 parts of plant enzyme, 0.3 part of probiotics, brown sugar 1.5 Part, 3 parts of medical stone emulsion;By the selenium-rich crops ground into end, the probiotics of activation is added, and is stirred, carries out low temperature Fermentation, fermentation temperature are 28-36 DEG C;
(2) under conditions of being stirred continuously, the medical stone emulsion after filtering is warming up to 40 DEG C, addition step (1) obtains mixed In compound;
(3) plant enzyme that total acidity is 27% and fermentation time is more than 3 years is put into, continues to stir;
(4) installation note oxygen pump, is continuously injected into oxygen, when there is white hair bacterium, note oxygen pump is removed, into anaerobic fermentation process;If Do not occur white hair bacterium, then continue to inject oxygen, until when there is white hair bacterium, into anaerobic fermentation process, remove note oxygen pump;
(5) continue fermentation 22 days under air-proof condition, zymotic fluid is obtained after filtering, by zymotic fluid censorship to detect selenium element Content, selenium element content, which reaches 735 mg/kgs, can stop fermenting, if selenium element content is not up to 735 mg/kgs Continue to ferment, until selenium element content reaches more than 735 mg/kgs.
9. the extracting method of selenium element in a kind of selenium-rich crops according to claim 1, it is characterised in that its concrete scheme It is realized in:
(1) raw materials by weight portion ratio is used by:6 parts of selenium-rich crops, 8 parts of plant enzyme, 0.3 part of probiotics, brown sugar 1.5 Part, 4 parts of medical stone emulsion;By the selenium-rich crops ground into end, the probiotics of activation is added, and is stirred, carries out low temperature Fermentation, fermentation temperature are 28-36 DEG C;
(2) under conditions of being stirred continuously, the medical stone emulsion after filtering is warming up to 40 DEG C, addition step (1) obtains mixed In compound;
(3) plant enzyme that total acidity is 27% and fermentation time is more than 3 years is put into, continues to stir;
(4) installation note oxygen pump, is continuously injected into oxygen, when there is white hair bacterium, note oxygen pump is removed, into anaerobic fermentation process;If Do not occur white hair bacterium, then continue to inject oxygen, until when there is white hair bacterium, into anaerobic fermentation process, remove note oxygen pump;
(5) continue fermentation 22 days under air-proof condition, zymotic fluid is obtained after filtering, by zymotic fluid censorship to detect selenium element Content, selenium element content, which reaches 735 mg/kgs, can stop fermenting, if selenium element content is not up to 735 mg/kgs Continue to ferment, until selenium element content reaches more than 735 mg/kgs.
10. the extracting method of selenium element in a kind of selenium-rich crops according to claim 1, it is characterised in that its specific side What case was realized in:
(1) raw materials by weight portion ratio is used by:8 parts of selenium-rich crops, 8 parts of plant enzyme, 1.5 parts of probiotics, glucose 2 Part, 4 parts of medical stone emulsion;By the selenium-rich crops ground into end, the probiotics of activation is added, and is stirred, carries out low temperature Fermentation, fermentation temperature are 28-36 DEG C;
(2) under conditions of being stirred continuously, the medical stone emulsion after filtering is warming up to 40 DEG C, addition step (1) obtains mixed In compound;
(3) plant enzyme that total acidity is 27% and fermentation time is more than 3 years is put into, continues to stir;
(4) installation note oxygen pump, is continuously injected into oxygen, when there is white hair bacterium, note oxygen pump is removed, into anaerobic fermentation process;If Do not occur white hair bacterium, then continue to inject oxygen, until when there is white hair bacterium, into anaerobic fermentation process, remove note oxygen pump;
(5) continue fermentation 22 days under air-proof condition, zymotic fluid is obtained after filtering, by zymotic fluid censorship to detect selenium element Content, selenium element content, which reaches 735 mg/kgs, can stop fermenting, if selenium element content is not up to 735 mg/kgs Continue to ferment, until selenium element content reaches more than 735 mg/kgs.
CN201710932316.8A 2017-09-22 2017-09-22 The extracting method of selenium element in a kind of selenium-rich crops Pending CN107760731A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109043512A (en) * 2018-07-14 2018-12-21 兰宇玲 A kind of selenium-rich bosom ginger ferment and preparation method thereof

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CN106472228A (en) * 2016-10-12 2017-03-08 湖北鑫尔绿色食品有限公司 The implantation methods of selenium-rich oil tea
CN106993809A (en) * 2017-03-23 2017-08-01 兰宇玲 A kind of selenium-rich method of blueberry ferment
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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109043512A (en) * 2018-07-14 2018-12-21 兰宇玲 A kind of selenium-rich bosom ginger ferment and preparation method thereof

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