CN107753988A - A kind of fragrant stacte product preparation method of Sliced with health maintenance effect - Google Patents
A kind of fragrant stacte product preparation method of Sliced with health maintenance effect Download PDFInfo
- Publication number
- CN107753988A CN107753988A CN201610696688.0A CN201610696688A CN107753988A CN 107753988 A CN107753988 A CN 107753988A CN 201610696688 A CN201610696688 A CN 201610696688A CN 107753988 A CN107753988 A CN 107753988A
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- Prior art keywords
- agalloch eaglewood
- sliced
- fragrant
- product preparation
- health maintenance
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/01—Deodorant compositions
- A61L9/013—Deodorant compositions containing animal or plant extracts, or vegetable material
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/83—Thymelaeaceae (Mezereum family), e.g. leatherwood or false ohelo
- A61K36/835—Aquilaria
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/0012—Galenical forms characterised by the site of application
- A61K9/0014—Skin, i.e. galenical aspects of topical compositions
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/0012—Galenical forms characterised by the site of application
- A61K9/007—Pulmonary tract; Aromatherapy
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/20—Pills, tablets, discs, rods
- A61K9/2004—Excipients; Inactive ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/015—Disinfection, sterilisation or deodorisation of air using gaseous or vaporous substances, e.g. ozone
- A61L9/02—Disinfection, sterilisation or deodorisation of air using gaseous or vaporous substances, e.g. ozone using substances evaporated in the air by heating or combustion
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/15—Preparation or pretreatment of starting material involving mechanical treatment, e.g. chopping up, cutting or grinding
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Epidemiology (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Medicinal Chemistry (AREA)
- Pharmacology & Pharmacy (AREA)
- Chemical & Material Sciences (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Botany (AREA)
- Alternative & Traditional Medicine (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Pulmonology (AREA)
- Medical Informatics (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Dermatology (AREA)
- Zoology (AREA)
- Fats And Perfumes (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The present invention relates to the stacte product preparation method that a kind of Sliced with health maintenance effect is fragrant, agalloch eaglewood chooses 200kg, is completed from being weighed in D level clean areas of the inner packing process in pharmaceutical technology, gets on the removal of impurity and non-medicinal effects in sorting table, cleaned 2 times, dried with circulating water；Agalloch eaglewood medicinal material after drying, which is placed in 70 DEG C of heated-air circulation oven, dries, and control temperature is no more than 70 DEG C, dries to moisture 5% or so；Operated by post SOP is pulverized and sieved, by agalloch eaglewood airslide disintegrating mill low-temperature grinding, load closed container；Pelletized with dry granulating machine stand-by.The present invention has the beneficial effect that：The standard being used as medicine with agalloch eaglewood carrys out chosen material, using cell wall breaking technology, agalloch eaglewood medicinal material is subjected to ultramicro grinding, utilize the distinctive lubricant component of agalloch eaglewood, using dry granulation process, be made by several process, the Sliced perfume (or spice) without any addition, natural environmental-protective, taste alcohol just, be advantageous to absorption of human body and possess unique effects.
Description
Technical field
Using pharmaceutical manufacturing technique productions and prepare the technologies of fragrant product the present invention relates to a kind of, more particularly to it is a kind of have support
The stacte product preparation method of the Sliced perfume of raw effect.
Background technology
Agalloch eaglewood is the antibacterial that seldom has in nature and the medicinal material for strengthening immunologic function, its fragrant odour, enter lung, kidney,
Spleen, stomach, warp, be gilt-edged medicinal material in qi-activating drug, can adjust the operation of gas in human body, dredge internal organ function, to lung, kidney, liver,
Stomach, intestines, heart etc. are all highly effective.
Agalloch eaglewood is also the rarity on China's history of Chinese materia medica, and ancient Chinese medicine doctor is on the books.《Compendium of Materia Medica》Calling it, " smell is pungent, micro-
Temperature is nontoxic.Have the effect of sending down abnormally ascending, receive kidney middle benefit gas, clear liver ", " control heat in the upper and cold in the lower, the circulation of vital energy in the wrong direction is panted, and large intestine void is closed, urine gas leaching, man
Sub- cold sperm ".《Japan hanako materia medica》It is " in tune, tonifying five zang organs, benefiting male body essence and invigorating sex functions, to warm up waist and knee, go perverse trend that it is medicinal, which then to record its,.Ending tendon transfer,
Vomit and diarrhoea, cold air, break disease addiction, control cold wind paralysis, joint is not appointed, and wet wind skin is itched, pain in the chest and abdomen, diarrhea due to disorder of qi ".
Now, agalloch eaglewood is still widely used in pharmacy, is listed in the water melon frost of national hospital of traditional Chinese hospital's acute disease indispensability Chinese patent drug
The main component of curing capsule of bringing down a fever just has agalloch eaglewood, exactly because also agalloch eaglewood is very rare in nature, there is high medicine again
With value.
Agalloch eaglewood line spices are formulated by nanmu bark powder and agalloch eaglewood powder, and nanmu bark powder plays adhesive effect.Agalloch eaglewood line spices
Make relative complex.
Therefore, in general in the market only has agalloch eaglewood line spices, is substantially and beats powder, plus one as raw material using rudimentary agalloch eaglewood
A little industrial essence material, are equipped with a certain proportion of adhesive auxiliary material and are fabricated, not only environment is polluted, and human body is exhaled
Desorption system damages, and is no advantage completely, and Sliced perfume (or spice) in the market does not have temporarily.
Therefore, according to problem above, it is necessary to effectively be innovated to prior art.
The content of the invention
For disadvantages described above, the present invention provides a kind of the smoked of perfume of the Sliced with health maintenance effect for being beneficial to health
Fragrant product preparation method, pass through the production method and technical process of unique feature so that the stacte product have unique health maintenance effect
And environmental protection standard is complied fully with, to none evil of the benefit of human body hundred.
To achieve the above object, the present invention uses following technical scheme：
A kind of fragrant stacte product preparation method of Sliced with health maintenance effect, is comprised the steps of：
(1) if being intended to final obtained 400,000, agalloch eaglewood selection 200kg, from inner packing process is weighed in pharmaceutical technology
In D level clean areas in complete, first, get on the removal of impurity and non-medicinal effects in sorting table, cleaned 2 times, dried with circulating water；
(2) the agalloch eaglewood medicinal material after drying, which is placed in 70 DEG C of heated-air circulation oven, dries, and control temperature is no more than 70 DEG C,
Dry to moisture 5% or so；
(3) in the D levels area in pharmaceutical technology, operated by post SOP is pulverized and sieved, by agalloch eaglewood airslide disintegrating mill
Low-temperature grinding, 200 mesh sieves are crossed, will be fitted into after the material metage after sieving in clean closed container；
(4) agalloch eaglewood fine powder is accurately weighed by recipe quantity, is pelletized with dry granulating machine stand-by；
(5) by the flat punchings of technological requirement selection Φ 11mm, first-class punch die, loading is first regulated according to piece weight-normality lattice, then
Pressure and rotating speed are adjusted, the piece weight, thickness, outward appearance of extrusion is conformed to quality requirements；In tableting processes, claimed one every about 15 minutes
Secondary average piece weight, it is ensured that tablet weight variation checks slice, thin piece outward appearance at any time in ± 5% allowed band, and QA took out every about 30 minutes
Look into once；
(6) after tabletting terminates, contained with the clean turnover barrel for being cased with bag film, tighten sack, weigh, capping is sealed, outside
Labelling.
Determined using the hot dipping under ethanol soluble extractives determination method item, with ethanol as solvent, 10.0% must not be less than；Adopt
Determined in accordance with the law with sulfur dioxide residual quantity, install apparatus, according to must not provide 400mg/Kg.
The fragrant stacte product preparation method of Sliced of the present invention with health maintenance effect has the beneficial effect that：With agalloch eaglewood
The standard being used as medicine carrys out chosen material, using cell wall breaking technology, agalloch eaglewood medicinal material is carried out into ultramicro grinding, utilizes the distinctive oil of agalloch eaglewood
Fat composition, using dry granulation process, it is made by several process, the Sliced perfume (or spice) is without any addition, natural environmental-protective, taste alcohol
Just, be advantageous to absorption of human body and possess the unique effects of agalloch eaglewood medicinal material.
Brief description of the drawings
The present invention is described in further detail below according to accompanying drawing.
Fig. 1 is the technological process of the stacte product preparation method that the Sliced with health maintenance effect is fragrant described in the embodiment of the present invention
Schematic diagram.
Embodiment
As shown in figure 1, the stacte product preparation method of the perfume of the Sliced with health maintenance effect described in the embodiment of the present invention, is
It is easy to the understanding this programme become apparent from, links is stated in detail by the way of chapter merogenesis is divided below：
1st, summarize：Character is light brown disk, specification 0.5g × 20 piece/bottle, shading, closed preservation.
Inventory 2. (400,000) agalloch eaglewood 200kg
3. Sliced agent producing process
In 3.1 this product production processes, from " weighing " to " inner packing " process is completed in D level clean areas, is strictly held
Capable S.O.P. of clearing out a gathering place is cleared out a gathering place.
Agalloch eaglewood raw material used in 3.2 this products, to pass through the tightened sampling inspection of QC departments, ensure that raw material reaches《Middle traditional Chinese medicines
Allusion quotation》2015 editions agalloch eaglewood quality of medicinal material standards, each link in production process are all carried out strict monitor check by QA departments, and
Make a record.
3.3 production processes and control
3.3.1 neck material：Neck material personnel get required material by production ordering and production inventory.When leading material, Ying Xianhe
Whether the material name of an article, lot number, quantity, specification are consistent with instruction, and check whether material inspection report is consistent.
3.3.2 weigh
Check the raw material name of an article, lot number, quantity, specification, the agalloch eaglewood of precise recipe quantity.Weighing apparatus should be first checked when weighing
Whether there is periodic check card, and adjust null balance rear ponderable quantity, answer during weighing 1 people to weigh 1 people verification.Should be timely after weighing
Record is filled in, and by weighing people, review people's signature.
3.3.3 selection cleaning
3.3.3.1 the agalloch eaglewood medicinal material received is picked out into impurity and non-medicinal effects on sorting table first.
3.3.3.2 cleaned 2 times, dried with circulating water.
3.3.4 dry
Agalloch eaglewood medicinal material after drying, which is placed in 70 DEG C of heated-air circulation oven, dries, and control temperature is no more than 70 DEG C, does
It is dry to moisture 5% or so.
3.3.3 pulverize and sieve
In D levels area, operated by post SOP is pulverized and sieved, by agalloch eaglewood airslide disintegrating mill low-temperature grinding, cross 200
Mesh sieve, it will be fitted into after the material metage after sieving in clean closed container.
3.3.5 granulation
Agalloch eaglewood fine powder is accurately weighed by recipe quantity, is pelletized with dry granulating machine stand-by.
3.3.6 tabletting
3.3.6.1 by the flat punchings of technological requirement selection Φ 11mm, first-class punch die.
3.3.6.2 loading is first regulated according to piece weight-normality lattice (0.5g/ pieces), then adjusts pressure and rotating speed, make extrusion
Piece weight, thickness, outward appearance etc. conform to quality requirements.
3.3.6.3 in tableting processes, the piece weight that is once averaged was claimed every about 15 minutes, it is ensured that tablet weight variation allows ± 5%
In the range of, and slice, thin piece outward appearance is checked at any time, QA was spot-check once every about 30 minutes.
3.3.6.4 after tabletting terminates, slice, thin piece is contained with the clean turnover barrel for being cased with bag film, tightens sack.Weigh, be capped
Seal, outer labelling, indicate the name of an article, specification, lot number, batch, machining state and weight, hand over intermediate station, fill in intermediate products friendship
Order and list please be examine, detect gainer.
4. raw material, intermediate products, final product quality standard and the method for inspection：
4.1 material quality standards and the method for inspection：
4.1.1 moisture
Press《Aquametry standard practice instructions》First method seasoning determines, and must not cross 13.0%.
4.1.2 sulfur dioxide residual quantity
According to《Sulfur dioxide residual quantity determination method standard practice instructions》Determine in accordance with the law, install apparatus in accordance with the law, according to rule
Surely 400mg/Kg must not be crossed.
4.1.3 extract
According to《Extract mensuration standard practice instructions》In ethanol soluble extractives determination method item under hot dipping measure, use
Ethanol as solvent, 10.0% must not be less than.
4.1.4 assay
According to《High performance liquid chromatography》Measure, is calculated by dry product, and tetrol containing agalloch eaglewood must not be less than 0.10%.
4.2 intermediate products quality standards and the method for inspection：
4.2.1 granule content：Calculated by dry product, tetrol containing agalloch eaglewood must not be less than 0.1%；
4.2.2 piece perfume (or spice) weight differential 0.5g ± 5%；
4.3 finished product inner controlling standard of enterprise and the method for inspection
4.3.1 extract
According to《Extract mensuration standard practice instructions》In ethanol soluble extractives determination method item under hot dipping measure, use
Ethanol as solvent, 10.0% must not be less than.
4.3.2 assay
According to《High performance liquid chromatography》Measure, is calculated by dry product, and tetrol containing agalloch eaglewood must not be less than 0.1%.
The cold soap of agalloch eaglewood ancient prescription described in the above embodiment of the present invention, application method are：
This Sliced perfume (or spice) is typically disposed in incense burner, by electrical heating, volatilizes the active ingredient in piece perfume (or spice) in agalloch eaglewood
Come, penetrated into by respiratory system and superficial skin in body, there is bactericidal antiphlogistic, warming middle energizer to arrest vomiting, promoting flow of qi and blood circulation effect, and
Distribute surrounding environment active ingredient can also sterile air, and give out the exclusive fragrance of agalloch eaglewood, it is not only environmentally friendly, also have work(concurrently
Can curative effect.
Above example is one kind of the present invention more preferably embodiment, and those skilled in the art are in the technical program
In the range of the usual variations and alternatives that carry out should include it is within the scope of the present invention.
Claims (3)
1. the fragrant stacte product preparation method of a kind of Sliced with health maintenance effect, it is characterised in that comprise the steps of：
(1) if be intended to it is final be made 400,000, agalloch eaglewood chooses 200kg, from being weighed to D of the inner packing process in pharmaceutical technology
Completed in level clean area, first, get on the removal of impurity and non-medicinal effects in sorting table, cleaned 2 times, dried with circulating water；
(2) the agalloch eaglewood medicinal material after drying, which is placed in 70 DEG C of heated-air circulation oven, dries, and control temperature is no more than 70 DEG C, dries
To moisture 5% or so；
(3) in the D levels area in pharmaceutical technology, operated by post SOP is pulverized and sieved, by agalloch eaglewood airslide disintegrating mill low temperature
Crush, cross 200 mesh sieves, will be fitted into after the material metage after sieving in clean closed container；
(4) agalloch eaglewood fine powder is accurately weighed by recipe quantity, is pelletized with dry granulating machine stand-by；
(5) by the flat punchings of technological requirement selection Φ 11mm, first-class punch die, loading is first regulated according to piece weight-normality lattice, is then adjusted
Pressure and rotating speed, the piece weight, thickness, outward appearance of extrusion is set to conform to quality requirements；In tableting processes, claimed once to put down every about 15 minutes
Equal piece weight, it is ensured that tablet weight variation checks slice, thin piece outward appearance at any time in ± 5% allowed band, and QA spot-check one every about 30 minutes
It is secondary；
(6) after tabletting terminates, contained with the clean turnover barrel for being cased with bag film, tighten sack, weigh, capping is sealed, outer labeling
Label.
2. the fragrant stacte product preparation method of the Sliced according to claim 1 with health maintenance effect, it is characterised in that：Adopt
Determined with the hot dipping under ethanol soluble extractives determination method item, with ethanol as solvent, 10.0% must not be less than.
3. the fragrant stacte product preparation method of the Sliced according to claim 1 with health maintenance effect, it is characterised in that：Adopt
Determined in accordance with the law with sulfur dioxide residual quantity, install apparatus, according to must not provide 400mg/Kg.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610696688.0A CN107753988A (en) | 2016-08-22 | 2016-08-22 | A kind of fragrant stacte product preparation method of Sliced with health maintenance effect |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610696688.0A CN107753988A (en) | 2016-08-22 | 2016-08-22 | A kind of fragrant stacte product preparation method of Sliced with health maintenance effect |
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| Publication Number | Publication Date |
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| CN107753988A true CN107753988A (en) | 2018-03-06 |
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|---|---|---|---|
| CN201610696688.0A Pending CN107753988A (en) | 2016-08-22 | 2016-08-22 | A kind of fragrant stacte product preparation method of Sliced with health maintenance effect |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109453269A (en) * | 2019-01-11 | 2019-03-12 | 安徽金国源中药股份有限公司 | A kind of agalloch eaglewood end and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2000256158A (en) * | 1999-03-11 | 2000-09-19 | Shiyoueidou:Kk | Incense composition and its production |
| CN103054939A (en) * | 2013-02-03 | 2013-04-24 | 葛强 | Preparation technology of liquorice ultrafine powder granular decoction pieces |
| CN104043141A (en) * | 2014-05-29 | 2014-09-17 | 上海佳客博实业有限公司 | Perfumed slice and preparation method thereof |
-
2016
- 2016-08-22 CN CN201610696688.0A patent/CN107753988A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2000256158A (en) * | 1999-03-11 | 2000-09-19 | Shiyoueidou:Kk | Incense composition and its production |
| CN103054939A (en) * | 2013-02-03 | 2013-04-24 | 葛强 | Preparation technology of liquorice ultrafine powder granular decoction pieces |
| CN104043141A (en) * | 2014-05-29 | 2014-09-17 | 上海佳客博实业有限公司 | Perfumed slice and preparation method thereof |
Non-Patent Citations (4)
| Title |
|---|
| 国家药典委员会: "《中华人民共和国药典（2015年版）四部》", 30 June 2015, 中国医药科技出版社 * |
| 易军: "《药剂学复习指南》", 31 January 2014, 天津出版传媒集团天津科技翻译出版有限公司 * |
| 李钦，陈建伟: "《生药学》", 30 March 2016, 中国医药科技出版社 * |
| 谢秀琼，周淑芳，韩丽: "《现代中药制剂新技术》", 30 June 2004, 化学工业出版社现代生物技术与医药科技出版中心 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109453269A (en) * | 2019-01-11 | 2019-03-12 | 安徽金国源中药股份有限公司 | A kind of agalloch eaglewood end and preparation method thereof |
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