CN107715153A - Radix tetrastigme purple perilla schizonepeta mixed extract and aerial fog type air freshener - Google Patents
Radix tetrastigme purple perilla schizonepeta mixed extract and aerial fog type air freshener Download PDFInfo
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- CN107715153A CN107715153A CN201711008366.3A CN201711008366A CN107715153A CN 107715153 A CN107715153 A CN 107715153A CN 201711008366 A CN201711008366 A CN 201711008366A CN 107715153 A CN107715153 A CN 107715153A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/01—Deodorant compositions
- A61L9/013—Deodorant compositions containing animal or plant extracts, or vegetable material
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/14—Disinfection, sterilisation or deodorisation of air using sprayed or atomised substances including air-liquid contact processes
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L2209/00—Aspects relating to disinfection, sterilisation or deodorisation of air
- A61L2209/20—Method-related aspects
- A61L2209/21—Use of chemical compounds for treating air or the like
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Abstract
The present invention relates to radix tetrastigme purple perilla schizonepeta mixed extract made of one kind using radix tetrastigme, purple perilla and schizonepeta as raw material, the mixed extract can improve immune function of human body rich in materials such as polysaccharide, melanterite and amino acid with its manufactured air freshener products.Accordingly, the invention further relates to the method for preparing radix tetrastigme purple perilla schizonepeta mixed extract, the content of the material such as radix tetrastigme purple perilla schizonepeta mixed extract, polysaccharide, melanterite and amino acid prepared with this method is higher.By the use of radix tetrastigme purple perilla schizonepeta mixed extract of the invention as aerial fog type air freshener made of raw material components, can not only make with fresh air, moreover it is possible to improve immune function of human body, filled up gaps in market.Accordingly, present invention also offers a kind of method for the aerial fog type air freshener for preparing the present invention, this method technique is simple, safe operation is easy and favorable reproducibility, and reliable guarantee can be provided for the large-scale production of product.
Description
Technical field
The present invention relates to daily-use chemical industry technical field, more particularly to using made of radix tetrastigme, purple perilla and schizonepeta as raw material
Radix tetrastigme-purple perilla-schizonepeta mixed extract, and with the radix tetrastigme-purple perilla-aerial fog type air made of schizonepeta mixed extract
Freshener.
Background technology
In recent years, aerosol-type air freshener China develop it is very fast, but be also faced with simultaneously problems and
Pressure.Such as：1) effect sex chromosome mosaicism, air freshener is substantially come in covering environment by fragrant in the market
Peculiar smell, so as to reach purpose with fresh air, the air freshener for being now able to improve immune function of human body is not gone out also on the market
Product；2) cost pressure, air freshener is mostly using organic matters such as alcohol, refined White Mineral Oils as solvent, face for a long time
Face larger cost pressure；3) organic matter such as safety problem, alcohol, refined White Mineral Oil is the air freshener of solvent, easily hair
, potential safety hazard be present in the security incidents such as raw combustion explosion；4) environmental protection pressure, due to most of VOCs (VOC)
Photochemical reaction can occur, cause the destruction of atmospheric ozone layer, the probability for making one to suffer from diseases of respiratory system increases.
The content of the invention
An object of the present invention is, there is provided it is a kind of using radix tetrastigme made of radix tetrastigme, purple perilla and schizonepeta as raw material-
Purple perilla-schizonepeta mixed extract, the mixed extract are clear with its manufactured air rich in materials such as polysaccharide, melanterite and amino acid
New agent product can improve immune function of human body.Accordingly, radix tetrastigme-purple perilla-schizonepeta is prepared present invention also offers one kind to mix
The method for closing extract solution, the radix tetrastigme-purple perilla-thing such as schizonepeta mixed extract, polysaccharide, melanterite and amino acid prepared with this method
The content of matter is higher.
It is a further object of the invention to provide a kind of radix tetrastigme-purple perilla-schizonepeta mixed extract with the present invention to make
For aerial fog type air freshener made of raw material components, aerial fog type air freshener of the invention can not only make it is with fresh air,
Immune function of human body can also be improved, has filled up gaps in market.Accordingly, present invention also offers a kind of aerosol for preparing the present invention
The method of type air freshener, this method technique is simple, safe operation is easy and favorable reproducibility, can be the scale metaplasia of product
Production provides reliable ensure.
For radix tetrastigme-purple perilla-schizonepeta mixed extract, the technical scheme is that：It by it is following by weight
Raw material components be made：Fresh 5~7 parts of radix tetrastigme leaf, fresh 2~3 parts of schizonepeta, dry 1~2 part of purple perilla, 20~25 parts of purified water,
1~2 part of ethanol, 1~2 part of ether, 2~2.5 parts of glacial acetic acid, 1.5~2 parts of sodium bicarbonate.
Compared with prior art, the present invention is made using radix tetrastigme, purple perilla and schizonepeta as raw material, and using specific formula
Radix tetrastigme-purple perilla-schizonepeta mixed extract, after measured, the mixed extract can strengthen rich in polysaccharide, melanterite and amino acid etc.
The material of immune function of human body, it can be used for making the air freshener products with immune function of human body can be improved；In addition,
When making aerial fog type air freshener with radix tetrastigme-purple perilla-schizonepeta mixed extract of the present invention, it can be replaced various having with water
Solvent, control cost is not only contributed to, but also there is the characteristics of safe and environment-friendly.
As prioritization scheme, foregoing radix tetrastigme-purple perilla-schizonepeta mixed extract is by following raw material group by weight
Divide and be made：Fresh 6 parts of radix tetrastigme leaf, fresh 2 parts of schizonepeta, dry 1 part of purple perilla, 23 parts of purified water, 2 parts of ethanol, 1 part of ether, ice second
2.5 parts of acid, 1.5 parts of sodium bicarbonate.Manufactured radix tetrastigme-purple perilla-schizonepeta mixed extract under the conditions of specific raw material proportioning herein
Smell is more pleasant.
The preparation method of foregoing radix tetrastigme-purple perilla-schizonepeta mixed extract, step are as follows：
A. fresh radix tetrastigme leaf, fresh schizonepeta, dry purple perilla are mixed, and smashed to pieces, A materials are made；
B. purified water, ethanol, ether, glacial acetic acid, sodium bicarbonate are added into A materials, is stirred, immersion 24~48 is small
When, B materials are made；
C. B materials are placed in the pressure cooker that operating pressure is 50KPa~70KPa and boiled, be incubated 2~4 hours, filter off
Slag, obtain C materials；
D. by C materials at a temperature of 4 DEG C~25 DEG C, it is 800~1000g to control centrifugal force, centrifuges 20~30 minutes, takes
Clear liquid, obtain D materials；
E. D materials are distilled, obtains radix tetrastigme-purple perilla-schizonepeta mixed extract.
After measured, in radix tetrastigme-purple perilla-schizonepeta mixed extract made from the method for the present invention, polysaccharide, melanterite and ammonia
The content of the materials such as base acid is higher.
For aerial fog type air freshener, aerial fog type air freshener of the invention includes pure and fresh liquid and propellant；It is described
Pure and fresh liquid includes the radix tetrastigme-purple perilla-schizonepeta mixed extract prepared as the method previously described.
Compared with prior art, the raw material components of aerial fog type air freshener of the invention include the present invention radix tetrastigme-
Purple perilla-schizonepeta mixed extract, immunologic function with fresh air, but also that human body can be improved can not only be made.
In foregoing aerial fog type air freshener, the pure and fresh liquid is made up of following raw material components by weight：Three
Ye Qing-purple perilla -2~5 parts of schizonepeta mixed extract, 3~4 parts of ethanol, 1~2 part of peppermint oil, 0.5~1 part of orange peel essential oil, purifying
15~25 parts of water, 1~2 part of sodium benzoate, 2~3 parts of ethyl hydroxy benzoate.It is stable according to pure and fresh fluidity shape made of said ratio, no
It is perishable, and there is special delicate fragrance, there is stimulating effect.For control cost, preferably, the pure and fresh liquid by pressing below
The raw material components of parts by weight meter are made：Radix tetrastigme-purple perilla -3.5 parts of schizonepeta mixed extract, 3.5 parts of ethanol, 1 part of peppermint oil, tangerine
0.5 part of peel essential oil, 20 parts of purified water, 1 part of sodium benzoate, 2 parts of ethyl hydroxy benzoate.
In foregoing aerial fog type air freshener, the propellant is the third butane；The quality of the propellant is described clear
The 24~28% of the quality of new liquid.For third butane as propellant, dosage is less with respect to dimethyl ether, and safer, to environment also more
Add close friend.
In foregoing aerial fog type air freshener, the quality of the propellant is the 24% of the quality of the pure and fresh liquid.Its
Advantage is, can not only ensure atomizing effect, and efficiently controlled cost.
The method for preparing the aerial fog type air freshener of the present invention, step are as follows：
I mixes each raw material components for preparing pure and fresh liquid, and stirs, and pure and fresh liquid is made；
II carries out the pure and fresh liquid obtained by step I canned under agitation, and fit on aerosol valve simultaneously seals, then
Fill propellant.
Preparation method technique of the invention is simple, safe operation is easy and favorable reproducibility, can be the scale metaplasia of product
Production provides reliable ensure.
Embodiment
With reference to embodiment, the present invention is further illustrated, but is not intended as the foundation limited the present invention.
In the present invention, the methanol content in ethanol used meets the national standard of medical ethanol or edible ethanol.
In the present invention, orange peel essential oil and peppermint oil can be using the products of the natural medicinal oil Co., Ltd of Jiangxi deodar.
In the present invention, fresh schizonepeta used includes stem, leaf and flower spike, and dry purple perilla used includes stem and leaf.
Embodiment 1
Radix tetrastigme-purple perilla-schizonepeta mixed extract made from the present embodiment, by following raw material components system by weight
Into：Fresh 6 parts of radix tetrastigme leaf, fresh 2 parts of schizonepeta, dry 1 part of purple perilla, 23 parts of purified water, 2 parts of ethanol, 1 part of ether, glacial acetic acid 2.5
Part, 1.5 parts of sodium bicarbonate.
Radix tetrastigme-purple perilla-schizonepeta mixed extract is made according to following steps：
A. fresh radix tetrastigme leaf, fresh schizonepeta, dry purple perilla are mixed, and smashed to pieces, A materials are made；
B. purified water, ethanol, ether, glacial acetic acid, sodium bicarbonate are added into A materials, is stirred, is soaked 36 hours, system
Obtain B materials；
C. B materials are placed in the pressure cooker that operating pressure is 60KPa and boiled, be incubated 3 hours, filter and remove residue, obtain C things
Material；
D. by C materials at a temperature of 15 DEG C, it is 900g to control centrifugal force, centrifuges 25 minutes, takes supernatant, obtain D materials；
E. D materials are distilled, obtains radix tetrastigme-purple perilla-schizonepeta mixed extract.
With radix tetrastigme-purple perilla-aerial fog type air freshener made of schizonepeta mixed extract, including pure and fresh liquid and projectile
Agent.Wherein, pure and fresh liquid is made up of following raw material components by weight：Radix tetrastigme-purple perilla -3.5 parts of schizonepeta mixed extract,
3.5 parts of ethanol, 1 part of peppermint oil, 0.5 part of orange peel essential oil, 20 parts of purified water, 1 part of sodium benzoate, 2 parts of ethyl hydroxy benzoate.Propellant is
Third butane, propane content is 30wt% in the third butane.The quality of propellant is the 24% of the quality of pure and fresh liquid.
The method for preparing the aerial fog type air freshener of the present embodiment, step are as follows：
I mixes each raw material components for preparing pure and fresh liquid, and stirs, and pure and fresh liquid is made；
II carries out the pure and fresh liquid obtained by step I canned under agitation, and fit on aerosol valve simultaneously seals, then
Fill propellant.
Embodiment 2
As different from Example 1, radix tetrastigme-purple perilla-schizonepeta mixed extract made from the present embodiment is by below by weight
The raw material components of amount part meter are made：Fresh 7 parts of radix tetrastigme leaf, fresh 3 parts of schizonepeta, dry 2 parts of purple perilla, 25 parts of purified water, ethanol 2
Part, 2 parts of ether, 2.5 parts of glacial acetic acid, 2 parts of sodium bicarbonate.
Embodiment 3
As different from Example 1, radix tetrastigme-purple perilla-schizonepeta mixed extract made from the present embodiment is by below by weight
The raw material components of amount part meter are made：Fresh 6 parts of radix tetrastigme leaf, fresh 2.5 parts of schizonepeta, dry 1.5 parts of purple perilla, 22 parts of purified water, second
1.5 parts of alcohol, 1.5 parts of ether, 23 parts of glacial acetic acid, 1.8 parts of sodium bicarbonate.
Embodiment 4
As different from Example 1, radix tetrastigme-purple perilla-schizonepeta mixed extract made from the present embodiment is by below by weight
The raw material components of amount part meter are made：Fresh 5 parts of radix tetrastigme leaf, fresh 2 parts of schizonepeta, dry 1 part of purple perilla, 20 parts of purified water, ethanol 1
Part, 1 part of ether, 2 parts of glacial acetic acid, 1.5 parts of sodium bicarbonate.
Table 1 have recorded radix tetrastigme-purple perilla-schizonepeta mixing obtained by embodiment 1, embodiment 2, embodiment 3 and embodiment 4
In extract solution, the content detection result (mg/g) of polysaccharide, melanterite and amino acid, according to testing result, three obtained by embodiment 1
In Ye Qing-purple perilla-schizonepeta mixed extract, the content of polysaccharide, melanterite and amino acid is higher；In addition, compare other 3 groups of implementations
Example, radix tetrastigme-purple perilla-schizonepeta mixed extract obtained by embodiment 1 have more pleasant smell.Therefore, three leaves are made
During green grass or young crops-purple perilla-schizonepeta mixed extract, the raw material components proportioning in preferred embodiment 1.
Table 1
Embodiment 5
As different from Example 1, in the present embodiment, radix tetrastigme-purple perilla-schizonepeta mixed extract is made according to the following steps
：
A. fresh radix tetrastigme leaf, fresh schizonepeta, dry purple perilla are mixed, and smashed to pieces, A materials are made；
B. purified water, ethanol, ether, glacial acetic acid, sodium bicarbonate are added into A materials, is stirred, is soaked 48 hours, system
Obtain B materials；
C. B materials are placed in the pressure cooker that operating pressure is 70KPa and boiled, be incubated 4 hours, filter and remove residue, obtain C things
Material；
D. by C materials at a temperature of 25 DEG C, it is 1000g to control centrifugal force, centrifuges 30 minutes, takes supernatant, obtain D things
Material；
E. D materials are distilled, obtains radix tetrastigme-purple perilla-schizonepeta mixed extract.
Embodiment 6
As different from Example 1, in the present embodiment, radix tetrastigme-purple perilla-schizonepeta mixed extract is made according to the following steps
：
A. fresh radix tetrastigme leaf, fresh schizonepeta, dry purple perilla are mixed, and smashed to pieces, A materials are made；
B. purified water, ethanol, ether, glacial acetic acid, sodium bicarbonate are added into A materials, is stirred, is soaked 24 hours, system
Obtain B materials；
C. B materials are placed in the pressure cooker that operating pressure is 50KPa and boiled, be incubated 2~4 hours, filter and remove residue, obtain
C materials；
D. by C materials at a temperature of 4 DEG C, it is 800g to control centrifugal force, centrifuges 20 minutes, takes supernatant, obtain D materials；
E. D materials are distilled, obtains radix tetrastigme-purple perilla-schizonepeta mixed extract.
In radix tetrastigme-purple perilla-schizonepeta mixed extract obtained by the expression of table 2 embodiment 1, embodiment 5 and embodiment 6,
The content of polysaccharide, melanterite and amino acid.As shown in Table 2, radix tetrastigme-purple obtained by embodiment 1, embodiment 5 and embodiment 6
In Soviet Union-schizonepeta mixed extract, the content of polysaccharide, melanterite and amino acid is higher, and difference very little, substantially may not be used in industry
With the presence for considering difference.
Table 2
Embodiment 7
As different from Example 1, in the present embodiment, pure and fresh liquid is made up of following raw material components by weight：Three
Ye Qing-purple perilla -5 parts of schizonepeta mixed extract, 4 parts of ethanol, 2 parts of peppermint oil, 1 part of orange peel essential oil, 25 parts of purified water, sodium benzoate
2 parts, 3 parts of ethyl hydroxy benzoate.
Embodiment 8
As different from Example 1, in the present embodiment, pure and fresh liquid is made up of following raw material components by weight：Three
Ye Qing-purple perilla -3.5 parts of schizonepeta mixed extract, 3.5 parts of ethanol, 1.5 parts of peppermint oil, 0.7 part of orange peel essential oil, 20 parts of purified water,
1.5 parts of sodium benzoate, 2.5 parts of ethyl hydroxy benzoate.
Embodiment 9
As different from Example 1, in the present embodiment, pure and fresh liquid is made up of following raw material components by weight：Three
Ye Qing-purple perilla -2 parts of schizonepeta mixed extract, 3 parts of ethanol, 1 part of peppermint oil, 0.5 part of orange peel essential oil, 15 parts of purified water, benzoic acid
1 part of sodium, 2 parts of ethyl hydroxy benzoate.
Through experiment, pure and fresh fluidity shape is stable made of embodiment 1, embodiment 7, embodiment 8 and embodiment 9, is unlikely to deteriorate,
And there is special delicate fragrance, there is stimulating effect.From the point of view of material cost, the pure and fresh liquid in preferred embodiment 1 is former
Material proportioning.
Embodiment 10
As different from Example 1, in the present embodiment, the quality of propellant is the 28% of the quality of pure and fresh liquid.
Embodiment 11
As different from Example 1, in the present embodiment, the quality of propellant is the 26% of the quality of pure and fresh liquid.
Research shows that the propellant in embodiment 1, embodiment 10 and embodiment 11 can realize preferable spray effect.
But from the point of view of manufacturing cost, propellant cost is minimum in embodiment 1.Table 3 represents embodiment 1, embodiment 10 and implemented
The atomizing effect of aerosol products made from example 11.
Table 3
The above-mentioned general description of invention to being related in the application and the description to its embodiment should not be understood
For be to the inventive technique scheme form limitation.Those skilled in the art can not disobey according to disclosure herein
On the premise of the involved invention inscape of the back of the body, to above-mentioned general description or/and embodiment (including embodiment)
In public technology feature increased, reduced or combined, form other technical sides for belonging within the application protection domain
Case.
Claims (9)
1. radix tetrastigme-purple perilla-schizonepeta mixed extract, it is characterised in that it is made up of following raw material components by weight：
Fresh 5~7 parts of radix tetrastigme leaf, fresh 2~3 parts of schizonepeta, dry 1~2 part of purple perilla, 20~25 parts of purified water, 1~2 part of ethanol, ether
1~2 part, 2~2.5 parts of glacial acetic acid, 1.5~2 parts of sodium bicarbonate.
2. radix tetrastigme-purple perilla-schizonepeta mixed extract according to claim 1, it is characterised in that it by it is following by weight
The raw material components of part meter are made：Fresh 6 parts of radix tetrastigme leaf, fresh 2 parts of schizonepeta, dry 1 part of purple perilla, 23 parts of purified water, 2 parts of ethanol,
1 part of ether, 2.5 parts of glacial acetic acid, 1.5 parts of sodium bicarbonate.
3. the preparation method of radix tetrastigme-purple perilla-schizonepeta mixed extract described in claim 1 or 2, it is characterised in that step
It is rapid as follows：
A. fresh radix tetrastigme leaf, fresh schizonepeta, dry purple perilla are mixed, and smashed to pieces, A materials are made；
B. purified water, ethanol, ether, glacial acetic acid, sodium bicarbonate are added into A materials, is stirred, is soaked 24~48 hours, system
Obtain B materials；
C. B materials are placed in the pressure cooker that operating pressure is 50KPa~70KPa and boiled, be incubated 2~4 hours, filter and remove residue,
Obtain C materials；
D. by C materials at a temperature of 4 DEG C~25 DEG C, it is 800~1000g to control centrifugal force, centrifuges 20~30 minutes, takes supernatant
Liquid, obtain D materials；
E. D materials are distilled, obtains radix tetrastigme-purple perilla-schizonepeta mixed extract.
A kind of 4. aerial fog type air freshener, it is characterised in that：Including pure and fresh liquid and propellant；The pure and fresh liquid is included according to power
Profit requires radix tetrastigme-purple perilla-schizonepeta mixed extract prepared by the method described in 3.
5. aerial fog type air freshener according to claim 4, it is characterised in that the pure and fresh liquid by it is following by weight
The raw material components of meter are made：Radix tetrastigme-purple perilla -2~5 parts of schizonepeta mixed extract, 3~4 parts of ethanol, 1~2 part of peppermint oil, tangerine
0.5~1 part of peel essential oil, 15~25 parts of purified water, 1~2 part of sodium benzoate, 2~3 parts of ethyl hydroxy benzoate.
6. aerial fog type air freshener according to claim 5, it is characterised in that the pure and fresh liquid by it is following by weight
The raw material components of meter are made：Radix tetrastigme-purple perilla -3.5 parts of schizonepeta mixed extract, 3.5 parts of ethanol, 1 part of peppermint oil, orange peel essential oil
0.5 part, 20 parts of purified water, 1 part of sodium benzoate, 2 parts of ethyl hydroxy benzoate.
7. according to the aerial fog type air freshener described in claim 4,5 or 6, it is characterised in that：The propellant is the third butane；
The quality of the propellant is the 24~28% of the quality of the pure and fresh liquid.
8. aerial fog type air freshener according to claim 7, it is characterised in that：The quality of the propellant is described clear
The 24% of the quality of new liquid.
9. prepare the method for the aerial fog type air freshener described in claim 4 to 8 any claim, it is characterised in that step
It is rapid as follows：
I mixes each raw material components for preparing pure and fresh liquid, and stirs, and pure and fresh liquid is made；
II carries out the pure and fresh liquid obtained by step I canned under agitation, and fit on aerosol valve simultaneously seals, and then fills
Propellant.
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